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Information card for entry 7117448
Preview
| Coordinates | 7117448.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H49 N O Si2 |
|---|---|
| Calculated formula | C30 H49 N O Si2 |
| Title of publication | Ni(ii)-catalyzed dehydrative alkynylation of unactivated (hetero)aryl C-H bonds using oxygen: a user-friendly approach. |
| Authors of publication | Liu, Yan-Hua; Liu, Yue-Jin; Yan, Sheng-Yi; Shi, Bing-Feng |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2015 |
| Journal volume | 51 |
| Journal issue | 58 |
| Pages of publication | 11650 - 11653 |
| a | 12.502 ± 0.0008 Å |
| b | 15.8137 ± 0.0009 Å |
| c | 17.4136 ± 0.001 Å |
| α | 74.497 ± 0.002° |
| β | 75.487 ± 0.001° |
| γ | 76.75 ± 0.002° |
| Cell volume | 3162.7 ± 0.3 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.2309 |
| Residual factor for significantly intense reflections | 0.1479 |
| Weighted residual factors for significantly intense reflections | 0.3813 |
| Weighted residual factors for all reflections included in the refinement | 0.441 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.191 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 141481 (current) | 2015-07-09 | cif/ Adding structures of 7117448 via cif-deposit CGI script. |
7117448.cif |
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