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Information card for entry 7121308
Preview
| Coordinates | 7121308.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H50 Ni P2 S |
|---|---|
| Calculated formula | C30 H50 Ni P2 S |
| Title of publication | Synthesis, crystal structure and reactivity of η<sup>2</sup>-thiophyne Ni complexes. |
| Authors of publication | Terada, Misaki; Nishii, Yuji; Miura, Masahiro |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2018 |
| Journal volume | 54 |
| Journal issue | 23 |
| Pages of publication | 2918 - 2921 |
| a | 9.911 ± 0.0016 Å |
| b | 16.711 ± 0.003 Å |
| c | 18.048 ± 0.002 Å |
| α | 90 ± 0.011° |
| β | 92.402 ± 0.01° |
| γ | 90 ± 0.008° |
| Cell volume | 2986.5 ± 0.8 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1856 |
| Residual factor for significantly intense reflections | 0.095 |
| Weighted residual factors for significantly intense reflections | 0.1638 |
| Weighted residual factors for all reflections included in the refinement | 0.2047 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 228452 (current) | 2019-11-17 | cif/ Updating files of 7121308, 7121309, 7121310, 7121311, 7121312, 7121313, 7121314 Original log message: Adding full bibliography for 7121308--7121314.cif. |
7121308.cif |
| 206631 | 2018-02-24 | cif/ Adding structures of 7121308, 7121309, 7121310, 7121311, 7121312, 7121313, 7121314 via cif-deposit CGI script. |
7121308.cif |
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Users of the data should acknowledge the original authors of the
structural data.