Crystallography Open Database

Information card for entry 7121810

Preview

Coordinates	7121810.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H80 B2 N12 O4 Si2 W2
Calculated formula	C53 H80 B2 N12 O4 Si2 W2
Title of publication	Bis(alkylidynyl)arsines.
Authors of publication	Frogley, Benjamin J.; Hill, Anthony F.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	55
Pages of publication	7649 - 7652
a	11.0937 ± 0.0003 Å
b	13.1532 ± 0.0003 Å
c	22.7516 ± 0.0004 Å
α	91.059 ± 0.002°
β	98.161 ± 0.002°
γ	108.441 ± 0.002°
Cell volume	3110.38 ± 0.13 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0381
Residual factor for significantly intense reflections	0.0287
Weighted residual factors for significantly intense reflections	0.0575
Weighted residual factors for all reflections included in the refinement	0.0618
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
228060 (current)	2019-11-17	cif/ Updating files of 7121808, 7121809, 7121810 Original log message: Adding full bibliography for 7121808--7121810.cif.	7121810.cif
208151	2018-06-06	cif/ Adding structures of 7121808, 7121809, 7121810 via cif-deposit CGI script.	7121810.cif