Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7122455
Preview
Coordinates | 7122455.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23.9 H24 I N3 O3 |
---|---|
Calculated formula | C23.9 H24 I N3 O3 |
Title of publication | Catalytic enantioselective ene-type reactions of vinylogous hydrazone: construction of α-methylene-γ-butyrolactone derivatives. |
Authors of publication | Zhang, Hang; Yao, Qian; Cao, Weidi; Ge, Shulin; Xu, Jinxiu; Liu, Xiaohua; Feng, Xiaoming |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2018 |
Journal volume | 54 |
Journal issue | 88 |
Pages of publication | 12511 - 12514 |
a | 12.05 ± 0.006 Å |
b | 12.052 ± 0.007 Å |
c | 16.964 ± 0.016 Å |
α | 90.01 ± 0.03° |
β | 90.05 ± 0.02° |
γ | 90.012 ± 0.011° |
Cell volume | 2464 ± 3 Å3 |
Cell temperature | 300 ± 2 K |
Ambient diffraction temperature | 300 ± 2 K |
Number of distinct elements | 5 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0899 |
Residual factor for significantly intense reflections | 0.0674 |
Weighted residual factors for significantly intense reflections | 0.1918 |
Weighted residual factors for all reflections included in the refinement | 0.2115 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
228198 (current) | 2019-11-17 | cif/ Updating files of 7122454, 7122455, 7122456, 7122457 Original log message: Adding full bibliography for 7122454--7122457.cif. |
7122455.cif |
211463 | 2018-10-14 | cif/ Adding structures of 7122454, 7122455, 7122456, 7122457 via cif-deposit CGI script. |
7122455.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.