#------------------------------------------------------------------------------ #$Date: 2019-05-18 04:07:54 +0300 (Sat, 18 May 2019) $ #$Revision: 215286 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/12/34/7123483.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7123483 loop_ _publ_author_name 'Zhang, Gao-Peng' 'Huang, Shuai' 'Jiang, Yang-Jie' 'Liu, Xiu-Yan' 'Ding, Chang-Hua' 'Wei, Yin' 'Hou, Xue-Long' _publ_section_title ; Pd-catalyzed enantioselective cyclopropanation of nitriles with mono substituted allyl carbonates enabled by the bulky N-heterocyclic carbene ligand ; _journal_name_full 'Chemical Communications' _journal_paper_doi 10.1039/C9CC01960J _journal_year 2019 _chemical_absolute_configuration ad _chemical_formula_sum 'C19 H22 Br N O2 S' _chemical_formula_weight 408.34 _chemical_name_systematic ; ? ; _space_group_crystal_system triclinic _space_group_IT_number 1 _space_group_name_Hall 'P 1' _space_group_name_H-M_alt 'P 1' _symmetry_space_group_name_Hall 'P 1' _symmetry_space_group_name_H-M 'P 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2013 _audit_update_record ; 2018-07-20 deposited with the CCDC. 2019-05-09 downloaded from the CCDC. ; _cell_angle_alpha 85.185(3) _cell_angle_beta 81.590(3) _cell_angle_gamma 82.894(3) _cell_formula_units_Z 2 _cell_length_a 9.4750(9) _cell_length_b 9.6439(9) _cell_length_c 10.8290(10) _cell_measurement_reflns_used 9948 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 52.256 _cell_measurement_theta_min 4.374 _cell_volume 969.16(16) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0496 _diffrn_reflns_av_unetI/netI 0.0406 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 37202 _diffrn_reflns_point_group_measured_fraction_full 0.978 _diffrn_reflns_point_group_measured_fraction_max 0.977 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.000 _diffrn_reflns_theta_min 2.696 _exptl_absorpt_coefficient_mu 2.239 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.4595 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.399 _exptl_crystal_description prismatic _exptl_crystal_F_000 420 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.170 _exptl_crystal_size_min 0.130 _refine_diff_density_max 0.372 _refine_diff_density_min -0.431 _refine_diff_density_rms 0.037 _refine_ls_abs_structure_details ; Flack x determined using 2498 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.045(5) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 446 _refine_ls_number_reflns 7458 _refine_ls_number_restraints 5 _refine_ls_restrained_S_all 1.050 _refine_ls_R_factor_all 0.0529 _refine_ls_R_factor_gt 0.0383 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0444P)^2^+0.2222P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0947 _refine_ls_wR_factor_ref 0.1027 _reflns_Friedel_coverage 0.963 _reflns_Friedel_fraction_full 0.960 _reflns_Friedel_fraction_max 0.959 _reflns_number_gt 5921 _reflns_number_total 7458 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c9cc01960j2.cif _cod_data_source_block mo_d8v18407_0m _cod_database_code 7123483 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.663 _shelx_estimated_absorpt_t_max 0.760 _shelxl_version_number 2013-4 _shelx_res_file ; TITL mo_d8v18407_0m_a.res in P1 CELL 0.71073 9.475 9.6439 10.829 85.185 81.59 82.894 ZERR 2 0.0009 0.0009 0.001 0.003 0.003 0.003 LATT -1 SFAC C H N O S Br UNIT 38 44 2 4 2 2 OMIT 0 0 1 OMIT 0 0 -1 OMIT -1 0 0 OMIT -3.00 52.00 L.S. 8 ACTA BOND $H FMAP 2 PLAN 20 size 0.20 0.17 0.13 wpdb -1 dfix 0.82 0.02 n1 h1a n2 h2a mpla c25 > c30 mpla c22 c23 c24 mpla c33 > c38 mpla c14 > c19 mpla c6 > c11 mpla c3 c4 c5 htab conf HTAB N2 O2 HTAB N1 O3 WGHT 0.044400 0.222200 EXTI 0.007344 FVAR 0.95136 MOLE 2 BR1 6 0.898432 0.407726 1.395075 11.00000 0.13403 0.12952 = 0.10587 -0.00191 -0.06911 -0.02124 MOLE 1 BR2 6 0.373087 0.665907 0.228760 11.00000 0.13400 0.12368 = 0.10061 -0.03815 -0.06819 0.01028 MOLE 2 S1 5 0.729114 0.333097 0.854889 11.00000 0.03877 0.04325 = 0.06453 -0.00122 0.00067 -0.00284 MOLE 1 S2 5 0.535981 0.771147 0.763360 11.00000 0.04220 0.04164 = 0.05448 -0.00361 -0.00794 -0.00345 MOLE 2 N1 3 0.556792 0.354918 0.866546 11.00000 0.03805 0.04870 = 0.06380 0.00093 -0.00632 -0.01132 MOLE 1 N2 3 0.709174 0.758545 0.745725 11.00000 0.04422 0.04773 = 0.05069 0.00150 -0.00869 -0.00534 MOLE 2 O1 4 0.776744 0.192996 0.822712 11.00000 0.06202 0.04526 = 0.08456 -0.00907 0.00003 0.00197 O2 4 0.779213 0.448238 0.774412 11.00000 0.05027 0.05422 = 0.07433 0.00945 0.00469 -0.00419 MOLE 1 O3 4 0.493585 0.659731 0.851842 11.00000 0.04678 0.05084 = 0.06131 0.00675 0.00090 -0.00949 O4 4 0.482371 0.911815 0.790035 11.00000 0.06346 0.04404 = 0.06786 -0.01221 -0.00748 0.00161 MOLE 2 C1 1 0.474418 0.250287 0.942385 11.00000 0.05441 0.04963 = 0.05649 0.00318 -0.01056 -0.01409 AFIX 23 H1C 2 0.496098 0.244855 1.027587 11.00000 -1.20000 H1D 2 0.504227 0.159165 0.909457 11.00000 -1.20000 AFIX 0 C2 1 0.310347 0.285621 0.943427 11.00000 0.04291 0.06226 = 0.05200 -0.00933 0.00329 -0.01157 C3 1 0.279009 0.317133 0.807609 11.00000 0.04016 0.05706 = 0.06918 -0.00630 -0.00584 -0.00385 AFIX 13 H3 2 0.316224 0.402479 0.767065 11.00000 -1.20000 AFIX 0 C4 1 0.142892 0.289708 0.766777 11.00000 0.04220 0.10012 = 0.08451 -0.01510 -0.01276 0.00333 AFIX 23 H4A 2 0.074838 0.243664 0.827302 11.00000 -1.20000 H4B 2 0.100112 0.358230 0.708275 11.00000 -1.20000 AFIX 0 MOLE 1 C5 1 0.280691 0.206558 0.720812 11.00000 0.05055 0.05512 = 0.06278 -0.00457 -0.00899 -0.00585 AFIX 13 H5 2 0.292266 0.111188 0.759902 11.00000 -1.20000 AFIX 0 MOLE 2 C6 1 0.353529 0.220752 0.588621 11.00000 0.06046 0.05106 = 0.04790 -0.00329 -0.00941 -0.00174 C7 1 0.276758 0.242628 0.489200 11.00000 0.09181 0.08986 = 0.06734 0.00646 -0.03006 -0.01864 AFIX 43 H7 2 0.176931 0.255373 0.502642 11.00000 -1.20000 AFIX 0 C8 1 0.350450 0.245503 0.367629 11.00000 0.16623 0.10182 = 0.05700 0.00034 -0.03917 -0.02597 AFIX 43 H8 2 0.298469 0.264484 0.300482 11.00000 -1.20000 AFIX 0 C9 1 0.496326 0.221284 0.344650 11.00000 0.14625 0.07254 = 0.06664 -0.01038 0.00868 -0.02165 AFIX 43 H9 2 0.543610 0.219365 0.263156 11.00000 -1.20000 AFIX 0 C10 1 0.570869 0.200025 0.443825 11.00000 0.09767 0.06793 = 0.06516 -0.00954 0.01530 -0.01563 AFIX 43 H10 2 0.670520 0.183496 0.429716 11.00000 -1.20000 AFIX 0 C11 1 0.501867 0.202438 0.565016 11.00000 0.05533 0.05721 = 0.05981 -0.00011 0.00215 -0.00344 AFIX 43 H11 2 0.555413 0.191682 0.631331 11.00000 -1.20000 AFIX 0 C12 1 0.255454 0.415234 1.013212 11.00000 0.07670 0.07797 = 0.06794 -0.01831 0.00983 -0.01042 AFIX 137 H12A 2 0.152792 0.431215 1.018319 11.00000 -1.50000 H12B 2 0.296927 0.494506 0.969566 11.00000 -1.50000 H12C 2 0.281795 0.402262 1.096051 11.00000 -1.50000 AFIX 0 C13 1 0.244890 0.159339 1.011538 11.00000 0.06222 0.08129 = 0.06887 -0.00449 0.00404 -0.02449 AFIX 137 H13A 2 0.272347 0.144766 1.093945 11.00000 -1.50000 H13B 2 0.278856 0.077817 0.965937 11.00000 -1.50000 H13C 2 0.142158 0.175740 1.017714 11.00000 -1.50000 AFIX 0 C14 1 0.775786 0.349146 1.005288 11.00000 0.03109 0.03928 = 0.07372 0.00291 -0.00523 -0.00487 C15 1 0.836339 0.236646 1.072792 11.00000 0.04421 0.04784 = 0.08023 0.00402 -0.00201 -0.00104 AFIX 43 H15 2 0.853057 0.148809 1.040542 11.00000 -1.20000 AFIX 0 C16 1 0.872617 0.254526 1.189667 11.00000 0.05723 0.06699 = 0.07834 0.01373 -0.02147 0.00514 AFIX 43 H16 2 0.913347 0.178633 1.236317 11.00000 -1.20000 AFIX 0 C17 1 0.848265 0.383565 1.235505 11.00000 0.06681 0.07546 = 0.07436 0.00718 -0.03068 -0.01614 C18 1 0.783737 0.497100 1.170816 11.00000 0.08350 0.05352 = 0.09440 -0.00666 -0.02844 -0.00926 AFIX 43 H18 2 0.764408 0.583811 1.205089 11.00000 -1.20000 AFIX 0 C19 1 0.748461 0.480388 1.055253 11.00000 0.08321 0.04855 = 0.07971 0.00275 -0.03279 -0.00716 AFIX 43 H19 2 0.706221 0.556505 1.009864 11.00000 -1.20000 AFIX 0 MOLE 1 C20 1 0.781025 0.863156 0.661848 11.00000 0.05186 0.06259 = 0.05533 0.00673 -0.01327 -0.01859 AFIX 23 H20A 2 0.742597 0.955862 0.687541 11.00000 -1.20000 H20B 2 0.760204 0.856513 0.577602 11.00000 -1.20000 AFIX 0 C21 1 0.943001 0.845169 0.660874 11.00000 0.04589 0.05459 = 0.04405 -0.00587 -0.00171 -0.00874 C22 1 0.976145 0.871488 0.788780 11.00000 0.04118 0.05306 = 0.04804 -0.00389 -0.00609 -0.00895 AFIX 13 H22 2 0.941990 0.966780 0.813043 11.00000 -1.20000 AFIX 0 MOLE 2 C23 1 1.116042 0.812906 0.836980 11.00000 0.04272 0.11853 = 0.07337 -0.00603 -0.01350 -0.01409 AFIX 23 H23A 2 1.181811 0.747887 0.786560 11.00000 -1.20000 H23B 2 1.161493 0.873906 0.881958 11.00000 -1.20000 AFIX 0 MOLE 1 C24 1 0.975039 0.764839 0.898551 11.00000 0.04438 0.05575 = 0.05217 -0.00169 -0.01053 -0.00534 AFIX 13 H24 2 0.959581 0.670498 0.880223 11.00000 -1.20000 AFIX 0 C25 1 0.911362 0.806485 1.023840 11.00000 0.06369 0.05453 = 0.05050 -0.00582 -0.01254 -0.00799 C26 1 0.991416 0.792820 1.123442 11.00000 0.09505 0.10406 = 0.06482 -0.01109 -0.03513 -0.00518 AFIX 43 H26 2 1.088217 0.758741 1.109949 11.00000 -1.20000 AFIX 0 C27 1 0.930396 0.828521 1.240425 11.00000 0.15218 0.12713 = 0.06186 -0.01240 -0.04808 -0.01515 AFIX 43 H27 2 0.986421 0.820398 1.304934 11.00000 -1.20000 AFIX 0 C28 1 0.789287 0.875538 1.263116 11.00000 0.18457 0.09431 = 0.03953 -0.01638 -0.00475 -0.02396 AFIX 43 H28 2 0.748512 0.895913 1.343928 11.00000 -1.20000 AFIX 0 C29 1 0.704403 0.893855 1.167771 11.00000 0.10743 0.06326 = 0.06724 -0.00844 0.01343 -0.01109 AFIX 43 H29 2 0.607765 0.928176 1.182783 11.00000 -1.20000 AFIX 0 C30 1 0.769108 0.858948 1.048272 11.00000 0.08553 0.05906 = 0.04870 -0.00740 -0.00699 -0.01147 AFIX 43 H30 2 0.714034 0.871641 0.982974 11.00000 -1.20000 AFIX 0 C31 1 1.010052 0.702843 0.613609 11.00000 0.07348 0.07050 = 0.06667 -0.01973 0.01231 -0.01405 AFIX 137 H31A 2 1.112387 0.702191 0.595620 11.00000 -1.50000 H31B 2 0.972341 0.687417 0.538933 11.00000 -1.50000 H31C 2 0.987359 0.629918 0.676715 11.00000 -1.50000 AFIX 0 C32 1 0.999758 0.964114 0.569838 11.00000 0.06141 0.08003 = 0.06625 0.00937 -0.00032 -0.02598 AFIX 137 H32A 2 0.947345 1.052073 0.592524 11.00000 -1.50000 H32B 2 0.987348 0.947745 0.486063 11.00000 -1.50000 H32C 2 1.099866 0.966471 0.574333 11.00000 -1.50000 AFIX 0 C33 1 0.486247 0.740352 0.617491 11.00000 0.03712 0.04387 = 0.05456 -0.00086 -0.00796 -0.00960 C34 1 0.426066 0.850143 0.545265 11.00000 0.05534 0.04341 = 0.06903 -0.00636 -0.01544 0.00291 AFIX 43 H34 2 0.408253 0.939476 0.574475 11.00000 -1.20000 AFIX 0 C35 1 0.392413 0.827221 0.429827 11.00000 0.06160 0.06327 = 0.07081 0.00329 -0.01933 0.00312 AFIX 43 H35 2 0.351993 0.900949 0.380619 11.00000 -1.20000 AFIX 0 C36 1 0.418635 0.695989 0.388084 11.00000 0.05330 0.07142 = 0.07680 -0.02000 -0.02111 -0.00376 C37 1 0.475696 0.584819 0.460446 11.00000 0.10800 0.05315 = 0.08681 -0.01822 -0.04405 -0.00128 AFIX 43 H37 2 0.489941 0.495074 0.432124 11.00000 -1.20000 AFIX 0 C38 1 0.511417 0.607818 0.575032 11.00000 0.08152 0.03909 = 0.08166 -0.00712 -0.03015 0.00593 AFIX 43 H38 2 0.552487 0.533970 0.623708 11.00000 -1.20000 AFIX 0 H2A 2 0.739617 0.680031 0.728196 11.00000 0.05658 H1A 2 0.524799 0.439815 0.865800 11.00000 0.04763 HKLF 4 REM mo_d8v18407_0m_a.res in P1 REM R1 = 0.0383 for 5921 Fo > 4sig(Fo) and 0.0529 for all 7458 data REM 446 parameters refined using 5 restraints END WGHT 0.0362 0.2759 REM Instructions for potential hydrogen bonds HTAB N2 O2 HTAB N1 O3 REM Highest difference peak 0.372, deepest hole -0.431, 1-sigma level 0.037 Q1 1 0.9484 0.3302 1.3543 11.00000 0.05 0.37 Q2 1 0.3875 0.6995 0.1609 11.00000 0.05 0.35 Q3 1 0.3253 0.7653 0.2624 11.00000 0.05 0.35 Q4 1 0.8833 0.3970 1.4577 11.00000 0.05 0.32 Q5 1 0.2845 0.6604 0.2761 11.00000 0.05 0.28 Q6 1 0.8541 0.4488 1.3832 11.00000 0.05 0.25 Q7 1 0.5065 0.7561 0.6964 11.00000 0.05 0.25 Q8 1 0.9810 0.4464 1.3606 11.00000 0.05 0.25 Q9 1 0.7613 0.3441 0.9286 11.00000 0.05 0.24 Q10 1 0.2862 0.2192 0.8213 11.00000 0.05 0.23 Q11 1 0.4152 0.6514 0.2414 11.00000 0.05 0.20 Q12 1 0.2874 0.3230 0.7163 11.00000 0.05 0.19 Q13 1 0.7593 0.2874 1.0558 11.00000 0.05 0.17 Q14 1 0.4968 0.6194 0.7939 11.00000 0.05 0.16 Q15 1 0.8038 0.3937 0.9995 11.00000 0.05 0.16 Q16 1 0.2701 0.4895 0.9564 11.00000 0.05 0.15 Q17 1 0.9205 0.4213 1.2650 11.00000 0.05 0.14 Q18 1 0.9707 0.7823 0.8115 11.00000 0.05 0.14 Q19 1 0.3623 0.3026 0.5785 11.00000 0.05 0.14 Q20 1 0.6494 0.3390 0.8648 11.00000 0.05 0.13 ; _shelx_res_checksum 17815 _shelx_hkl_file ; -1 0 0 638.54 40.00 -1 0 0 622.24 39.70 -3 0 0 422.26 28.80 -3 0 0 429.96 29.30 -3 0 0 454.95 28.90 -3 0 0 451.55 28.80 -3 0 0 419.16 28.50 -3 0 0 439.26 28.60 -3 0 0 466.65 29.10 3 0 0 455.15 29.30 3 0 0 445.66 29.00 3 0 0 466.45 29.00 3 0 0 438.26 28.80 3 0 0 451.45 29.10 -4 0 0 1027.90 66.99 -4 0 0 1011.80 66.49 -4 0 0 1051.09 67.49 -4 0 0 1009.00 66.39 -4 0 0 971.90 66.19 -4 0 0 1061.69 66.79 -4 0 0 965.80 66.59 4 0 0 1064.99 66.59 4 0 0 1031.20 66.79 4 0 0 1129.79 66.99 4 0 0 1142.69 67.19 4 0 0 1070.59 67.29 -5 0 0 1455.55 96.19 -5 0 0 1514.35 95.09 -5 0 0 1421.06 94.79 -5 0 0 1582.64 95.69 -5 0 0 1562.64 95.99 -5 0 0 1408.66 95.29 -5 0 0 1550.64 96.49 5 0 0 1431.56 95.49 5 0 0 1448.16 95.19 5 0 0 1553.94 95.99 5 0 0 1551.74 95.79 5 0 0 1518.75 96.69 5 0 0 1475.25 96.09 -6 0 0 50.89 6.80 -6 0 0 70.39 8.40 -6 0 0 50.49 5.70 -6 0 0 63.19 7.70 -6 0 0 64.89 7.60 -6 0 0 66.29 6.30 -6 0 0 87.99 10.30 -6 0 0 53.09 6.50 6 0 0 75.49 8.50 6 0 0 78.49 6.90 6 0 0 91.59 8.00 6 0 0 78.99 7.30 6 0 0 78.89 8.50 6 0 0 77.19 8.00 -7 0 0 2.40 3.00 -7 0 0 -2.30 3.30 -7 0 0 1.80 4.00 -7 0 0 6.10 2.40 -7 0 0 4.50 3.80 -7 0 0 6.20 4.50 -7 0 0 1.70 2.50 -7 0 0 4.20 3.10 7 0 0 6.00 4.50 7 0 0 5.80 5.10 7 0 0 5.50 4.10 7 0 0 5.90 3.70 7 0 0 8.40 3.90 7 0 0 5.80 3.00 -8 0 0 189.58 15.60 -8 0 0 157.18 15.30 -8 0 0 171.78 13.90 -8 0 0 167.08 12.60 -8 0 0 181.18 14.60 -8 0 0 176.38 16.10 -8 0 0 171.68 13.30 -8 0 0 161.88 14.10 8 0 0 162.38 14.70 8 0 0 180.38 14.60 8 0 0 175.18 15.60 8 0 0 165.08 13.60 8 0 0 185.98 18.00 8 0 0 188.58 16.10 -9 0 0 4.60 5.50 -9 0 0 9.40 4.30 -9 0 0 5.30 5.20 -9 0 0 5.00 4.20 -9 0 0 5.50 3.00 -9 0 0 5.60 5.70 9 0 0 4.80 6.20 9 0 0 3.40 5.70 9 0 0 4.00 5.40 9 0 0 5.50 4.40 -10 0 0 -2.20 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394.46 26.60 1 4 0 394.26 26.20 1 4 0 406.76 25.90 1 4 0 407.36 26.30 1 4 0 400.36 25.50 1 4 0 411.46 25.50 -2 -4 0 589.04 38.00 -2 -4 0 579.74 36.70 -2 -4 0 523.85 38.40 -2 -4 0 563.94 36.60 -2 -4 0 565.64 37.90 -2 -4 0 604.24 37.20 -2 -4 0 552.94 37.00 -2 -4 0 602.74 36.70 2 4 0 579.34 37.00 2 4 0 574.34 37.10 2 4 0 577.64 36.90 2 4 0 563.24 37.00 2 4 0 569.14 37.50 -3 -4 0 8.30 2.20 -3 -4 0 11.00 2.80 -3 -4 0 8.40 1.50 -3 -4 0 9.30 3.20 -3 -4 0 10.90 2.40 -3 -4 0 11.10 2.40 -3 -4 0 9.20 2.70 -3 -4 0 10.50 1.40 -3 -4 0 7.20 2.80 3 4 0 6.00 2.30 3 4 0 4.30 2.20 3 4 0 11.20 2.40 3 4 0 5.70 3.30 -4 -4 0 472.65 28.60 -4 -4 0 442.36 28.30 -4 -4 0 437.36 29.10 -4 -4 0 401.26 28.60 -4 -4 0 421.76 28.30 -4 -4 0 414.86 27.70 -4 -4 0 419.66 28.20 4 4 0 404.36 27.80 4 4 0 392.56 28.20 4 4 0 433.66 28.70 4 4 0 421.26 28.50 4 4 0 392.46 27.90 -5 -4 0 76.29 8.10 -5 -4 0 84.19 7.50 -5 -4 0 75.69 7.70 -5 -4 0 82.79 7.50 -5 -4 0 79.49 7.80 -5 -4 0 71.59 7.50 -5 -4 0 73.29 7.60 5 4 0 70.59 7.80 5 4 0 60.49 6.60 5 4 0 67.29 7.70 5 4 0 57.09 6.70 -6 -4 0 201.68 13.30 -6 -4 0 212.58 15.80 -6 -4 0 198.98 15.50 -6 -4 0 211.98 15.70 -6 -4 0 202.68 15.00 -6 -4 0 187.28 15.40 -6 -4 0 191.18 16.00 -6 -4 0 194.58 17.50 6 4 0 188.88 13.10 6 4 0 198.78 15.00 6 4 0 195.88 15.50 6 4 0 194.98 15.70 6 4 0 196.68 16.20 -7 -4 0 57.19 7.40 -7 -4 0 38.50 6.60 -7 -4 0 52.89 5.00 -7 -4 0 46.60 7.60 -7 -4 0 53.09 7.80 -7 -4 0 58.89 8.30 -7 -4 0 46.20 7.30 -7 -4 0 46.00 6.20 7 4 0 48.10 6.50 7 4 0 49.30 7.70 7 4 0 49.99 4.80 7 4 0 51.29 6.50 7 4 0 63.39 8.20 7 4 0 61.89 7.70 -8 -4 0 13.80 4.10 -8 -4 0 16.00 4.90 -8 -4 0 18.20 5.10 -8 -4 0 23.20 5.70 -8 -4 0 19.60 3.40 -8 -4 0 13.00 5.20 8 4 0 16.50 4.30 8 4 0 17.00 2.90 8 4 0 24.10 5.70 8 4 0 14.10 5.80 -9 -4 0 29.90 6.90 -9 -4 0 33.10 7.20 -9 -4 0 29.40 5.20 -9 -4 0 35.30 4.60 -9 -4 0 27.80 7.70 9 4 0 26.20 7.20 9 4 0 35.00 7.30 9 4 0 30.30 4.00 9 4 0 38.80 9.10 9 4 0 34.60 5.80 -10 -4 0 39.70 9.40 -10 -4 0 32.00 8.60 -10 -4 0 22.50 4.30 -10 -4 0 21.80 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57.89 7.50 5 -5 0 59.19 8.10 5 -5 0 59.09 7.10 -5 5 0 33.90 6.80 -5 5 0 46.10 6.30 -5 5 0 39.10 6.40 -5 5 0 37.30 6.50 -5 5 0 37.70 6.30 4 -5 0 412.96 27.60 4 -5 0 353.06 26.70 4 -5 0 371.26 28.10 4 -5 0 419.76 28.50 4 -5 0 407.46 27.20 4 -5 0 399.96 28.00 4 -5 0 396.86 27.40 -4 5 0 433.06 27.30 -4 5 0 388.16 27.50 -4 5 0 420.16 28.80 -4 5 0 388.76 27.40 -4 5 0 429.96 27.90 3 -5 0 657.13 44.10 3 -5 0 573.74 42.60 3 -5 0 693.23 43.20 3 -5 0 645.34 43.90 3 -5 0 650.53 42.30 3 -5 0 710.53 44.30 3 -5 0 641.14 42.30 3 -5 0 654.53 43.30 -3 5 0 696.63 43.10 -3 5 0 689.03 44.50 -3 5 0 652.43 43.50 -3 5 0 701.53 43.40 -3 5 0 649.24 43.20 2 -5 0 225.88 14.80 2 -5 0 192.48 15.90 2 -5 0 217.08 16.00 2 -5 0 229.28 15.10 2 -5 0 209.78 14.90 2 -5 0 208.68 16.20 2 -5 0 214.28 15.50 2 -5 0 213.18 14.90 2 -5 0 194.18 14.40 -2 5 0 220.58 15.00 -2 5 0 223.88 15.70 -2 5 0 227.98 15.10 -2 5 0 228.28 15.00 -2 5 0 226.68 16.30 1 -5 0 517.25 33.60 1 -5 0 529.45 34.30 1 -5 0 547.25 34.70 1 -5 0 499.35 34.00 1 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70.59 3 5 0 1167.58 71.59 3 5 0 1132.99 70.89 3 5 0 1147.09 70.99 3 5 0 1154.18 71.09 3 5 0 1157.78 70.99 -4 -5 0 221.68 15.10 -4 -5 0 201.98 16.40 -4 -5 0 200.38 14.90 -4 -5 0 245.88 15.90 -4 -5 0 217.08 15.10 -4 -5 0 198.58 15.60 -4 -5 0 213.68 16.10 4 5 0 204.58 15.90 4 5 0 207.48 15.60 4 5 0 222.08 15.20 4 5 0 196.58 15.20 4 5 0 200.98 15.00 -5 -5 0 158.48 13.90 -5 -5 0 167.08 12.70 -5 -5 0 148.69 13.10 -5 -5 0 147.89 13.30 -5 -5 0 172.98 12.80 -5 -5 0 171.48 13.30 -5 -5 0 156.78 12.20 5 5 0 157.38 12.90 5 5 0 165.58 13.30 5 5 0 174.58 13.00 5 5 0 168.38 13.50 5 5 0 154.78 12.40 -6 -5 0 89.69 9.10 -6 -5 0 98.89 9.00 -6 -5 0 79.49 8.40 -6 -5 0 78.79 8.70 -6 -5 0 104.29 10.40 -6 -5 0 98.79 8.80 6 5 0 75.79 9.30 6 5 0 68.79 7.60 6 5 0 70.69 7.90 6 5 0 66.29 9.10 -7 -5 0 171.58 14.70 -7 -5 0 180.38 15.60 -7 -5 0 177.28 14.70 -7 -5 0 161.48 14.60 -7 -5 0 161.28 13.70 -7 -5 0 180.98 14.60 7 5 0 163.18 13.10 7 5 0 161.28 13.80 7 5 0 174.78 15.60 7 5 0 160.78 14.40 7 5 0 178.58 15.00 -8 -5 0 24.10 6.90 -8 -5 0 29.00 6.80 -8 -5 0 25.30 6.70 -8 -5 0 24.50 5.30 8 5 0 26.20 7.00 8 5 0 32.10 6.60 8 5 0 31.50 5.10 8 5 0 32.00 7.30 -9 -5 0 -0.80 4.20 -9 -5 0 3.90 3.90 -9 -5 0 -0.10 4.80 -9 -5 0 -3.90 5.50 9 5 0 2.30 5.70 9 5 0 2.20 3.70 9 5 0 2.00 5.00 9 5 0 -5.60 3.80 -10 -5 0 9.90 4.40 -10 -5 0 6.10 7.20 -10 -5 0 9.70 6.10 -10 -5 0 7.10 6.10 10 5 0 9.50 4.40 10 5 0 5.40 5.90 10 5 0 5.40 5.40 10 5 0 10.80 6.70 -11 -5 0 27.20 7.90 -11 -5 0 19.10 7.60 -11 -5 0 23.40 8.70 11 5 0 30.70 9.30 11 5 0 18.50 7.50 11 5 0 23.30 5.70 11 5 0 20.80 7.60 9 -6 0 8.90 7.10 9 -6 0 9.20 7.40 9 -6 0 4.50 5.60 -9 6 0 1.20 5.80 -9 6 0 -6.20 5.60 -9 6 0 -6.50 4.70 -9 6 0 3.20 6.00 8 -6 0 -1.40 6.20 8 -6 0 -0.70 4.70 8 -6 0 1.00 6.10 -8 6 0 0.50 3.40 -8 6 0 6.90 5.50 -8 6 0 1.40 5.30 -8 6 0 4.90 5.40 7 -6 0 8.60 5.10 7 -6 0 2.40 4.00 7 -6 0 0.00 5.30 7 -6 0 7.70 6.40 -7 6 0 7.10 5.10 -7 6 0 11.90 5.90 -7 6 0 7.80 5.20 -7 6 0 2.70 4.00 6 -6 0 117.69 11.40 6 -6 0 107.99 10.60 6 -6 0 123.49 12.20 6 -6 0 128.39 13.20 -6 6 0 111.69 11.80 -6 6 0 96.19 10.80 -6 6 0 116.69 11.10 -6 6 0 118.79 13.00 -6 6 0 106.79 11.80 5 -6 0 315.97 23.20 5 -6 0 357.76 24.90 5 -6 0 315.47 22.80 5 -6 0 307.77 26.00 5 -6 0 315.77 23.20 -5 6 0 319.07 24.70 -5 6 0 306.57 23.10 -5 6 0 353.36 23.10 -5 6 0 339.57 23.80 -5 6 0 289.57 23.30 4 -6 0 0.40 2.90 4 -6 0 3.20 2.80 4 -6 0 4.10 4.10 4 -6 0 3.20 2.50 4 -6 0 5.50 4.00 4 -6 0 1.70 3.80 4 -6 0 6.40 4.10 -4 6 0 7.30 3.90 -4 6 0 -1.70 3.60 -4 6 0 3.10 3.20 -4 6 0 -0.30 2.60 -4 6 0 0.70 3.20 3 -6 0 533.95 34.60 3 -6 0 490.35 33.50 3 -6 0 548.35 34.20 3 -6 0 434.06 33.40 3 -6 0 531.55 35.60 3 -6 0 477.85 35.20 3 -6 0 505.25 35.20 3 -6 0 504.45 34.50 3 -6 0 499.65 33.40 -3 6 0 539.75 34.90 -3 6 0 548.95 34.40 -3 6 0 519.05 34.10 -3 6 0 532.75 34.80 -3 6 0 557.64 35.90 2 -6 0 378.96 25.90 2 -6 0 362.86 25.30 2 -6 0 362.26 26.40 2 -6 0 376.66 26.60 2 -6 0 373.16 25.40 2 -6 0 394.66 26.80 -2 6 0 399.56 26.90 -2 6 0 363.86 25.30 -2 6 0 376.16 25.00 -2 6 0 402.26 25.30 -2 6 0 371.26 26.00 1 -6 0 87.99 9.00 1 -6 0 81.09 7.70 1 -6 0 86.09 8.40 1 -6 0 98.29 7.20 1 -6 0 93.79 8.10 1 -6 0 79.59 8.50 1 -6 0 89.39 8.00 1 -6 0 75.49 8.00 -1 6 0 76.09 6.30 -1 6 0 72.39 6.90 -1 6 0 72.69 6.30 -1 6 0 75.59 8.10 0 -6 0 73.49 7.40 0 -6 0 60.89 6.10 0 -6 0 66.39 6.10 0 -6 0 65.89 7.00 0 -6 0 77.09 7.40 0 -6 0 62.89 7.00 0 -6 0 73.89 7.40 0 -6 0 72.69 7.20 0 6 0 70.29 7.80 0 6 0 68.19 5.40 0 6 0 71.29 7.40 0 6 0 68.89 5.30 -1 -6 0 37.60 5.30 -1 -6 0 38.30 5.40 -1 -6 0 34.00 5.00 -1 -6 0 34.50 5.50 -1 -6 0 37.30 5.40 -1 -6 0 30.60 4.20 -1 -6 0 38.10 5.20 -1 -6 0 30.90 4.40 -2 -6 0 48.70 5.60 -2 -6 0 45.40 6.70 -2 -6 0 50.69 5.40 -2 -6 0 53.79 6.60 -2 -6 0 46.80 6.50 -2 -6 0 53.79 5.40 -2 -6 0 48.10 6.10 -2 -6 0 46.10 6.10 2 6 0 54.69 6.20 2 6 0 53.49 5.00 2 6 0 52.39 4.70 2 6 0 54.09 6.60 -3 -6 0 377.26 25.50 -3 -6 0 374.86 24.70 -3 -6 0 347.17 25.20 -3 -6 0 362.76 24.30 -3 -6 0 368.96 24.40 -3 -6 0 366.06 26.30 -3 -6 0 356.66 24.90 -3 -6 0 351.56 26.60 -3 -6 0 359.86 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123.79 11.90 -5 7 0 129.99 14.40 -5 7 0 144.69 12.20 -5 7 0 120.29 12.40 -5 7 0 125.89 14.20 4 -7 0 558.44 39.10 4 -7 0 579.24 38.30 4 -7 0 595.54 40.70 4 -7 0 574.44 38.80 -4 7 0 549.65 38.60 -4 7 0 579.54 39.70 -4 7 0 577.74 39.20 -4 7 0 618.44 41.00 -4 7 0 600.74 38.80 3 -7 0 48.80 6.00 3 -7 0 36.50 6.50 3 -7 0 45.40 4.60 3 -7 0 42.10 6.50 3 -7 0 43.40 7.50 3 -7 0 48.00 5.60 3 -7 0 44.70 6.90 3 -7 0 49.20 5.60 -3 7 0 44.40 5.50 -3 7 0 35.60 6.60 -3 7 0 34.70 5.30 -3 7 0 31.50 5.30 -3 7 0 41.30 9.80 2 -7 0 181.48 13.30 2 -7 0 165.08 14.40 2 -7 0 167.68 14.50 2 -7 0 175.58 13.90 2 -7 0 188.88 14.30 2 -7 0 169.98 13.20 2 -7 0 181.68 13.10 2 -7 0 195.68 15.30 -2 7 0 167.98 12.60 -2 7 0 178.68 14.80 -2 7 0 148.69 12.30 1 -7 0 144.69 11.50 1 -7 0 136.99 10.10 1 -7 0 134.79 11.40 1 -7 0 140.09 11.70 1 -7 0 148.39 12.50 1 -7 0 123.79 11.20 1 -7 0 120.19 9.90 1 -7 0 130.79 10.90 1 -7 0 135.49 11.10 -1 7 0 111.79 11.30 -1 7 0 106.59 9.30 0 -7 0 133.19 11.10 0 -7 0 126.99 9.90 0 -7 0 123.39 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0 215.28 18.60 -4 -7 0 214.58 16.60 -4 -7 0 226.88 15.80 4 7 0 220.08 16.80 4 7 0 243.78 18.20 4 7 0 237.28 16.70 4 7 0 244.28 17.00 4 7 0 229.88 16.70 -5 -7 0 171.98 13.60 -5 -7 0 152.88 11.60 -5 -7 0 151.98 12.20 -5 -7 0 166.88 14.80 -5 -7 0 161.88 13.30 -5 -7 0 155.78 12.50 5 7 0 135.09 12.20 5 7 0 134.19 14.70 5 7 0 135.49 13.50 5 7 0 129.99 12.10 5 7 0 150.78 12.80 -6 -7 0 58.59 8.60 -6 -7 0 66.09 7.60 -6 -7 0 64.29 10.50 -6 -7 0 62.39 7.80 6 7 0 53.99 7.40 6 7 0 55.59 8.50 6 7 0 56.49 8.70 6 7 0 69.09 7.80 6 7 0 55.59 7.60 -7 -7 0 14.20 4.90 -7 -7 0 12.90 6.30 -7 -7 0 19.00 6.40 -7 -7 0 14.90 5.00 7 7 0 14.80 4.60 7 7 0 10.90 5.00 7 7 0 18.20 5.20 7 7 0 14.90 6.30 -8 -7 0 2.90 4.50 -8 -7 0 2.70 5.30 -8 -7 0 2.00 4.30 -8 -7 0 -0.40 5.50 8 7 0 3.20 4.20 8 7 0 -3.40 3.60 8 7 0 -2.20 4.10 8 7 0 -1.80 5.60 -9 -7 0 8.30 4.60 -9 -7 0 8.00 5.60 -9 -7 0 17.60 7.40 -9 -7 0 7.30 6.60 9 7 0 19.90 6.70 9 7 0 24.40 5.60 9 7 0 26.70 8.00 9 7 0 14.60 4.70 -10 -7 0 10.80 4.60 -10 -7 0 11.10 7.10 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2 -8 0 38.20 5.60 2 -8 0 44.40 7.80 2 -8 0 36.70 10.80 2 -8 0 43.80 6.90 2 -8 0 34.90 6.40 2 -8 0 42.20 6.40 2 -8 0 27.60 4.70 2 -8 0 38.80 5.70 -2 8 0 25.30 4.20 -2 8 0 28.00 6.30 -2 8 0 24.30 4.80 -2 8 0 23.80 4.10 1 -8 0 31.20 6.00 1 -8 0 33.90 6.30 1 -8 0 29.60 5.80 1 -8 0 24.10 5.90 1 -8 0 26.10 5.40 1 -8 0 31.30 4.80 1 -8 0 28.70 5.30 1 -8 0 34.30 4.80 1 -8 0 32.10 7.00 -1 8 0 28.80 4.00 -1 8 0 34.80 4.20 -1 8 0 31.10 6.10 0 -8 0 2.00 3.60 0 -8 0 4.80 3.10 0 -8 0 1.20 3.40 0 -8 0 3.10 3.90 0 -8 0 5.50 3.30 0 -8 0 -3.60 3.70 0 -8 0 2.30 4.00 0 -8 0 7.80 4.50 0 8 0 3.30 4.10 0 8 0 -1.30 3.30 0 8 0 2.50 2.00 0 8 0 1.70 1.90 -1 -8 0 76.99 9.40 -1 -8 0 91.79 10.40 -1 -8 0 74.99 8.50 -1 -8 0 73.39 9.50 -1 -8 0 79.49 9.30 -1 -8 0 89.79 9.70 -1 -8 0 83.59 9.30 -1 -8 0 77.19 7.80 -1 -8 0 88.39 8.20 1 8 0 82.19 6.50 1 8 0 80.59 9.30 1 8 0 82.19 8.70 1 8 0 79.99 6.60 -2 -8 0 66.09 9.20 -2 -8 0 74.79 9.40 -2 -8 0 75.89 7.80 -2 -8 0 66.59 8.60 -2 -8 0 66.49 7.80 -2 -8 0 73.59 8.00 -2 -8 0 61.89 8.60 -2 -8 0 75.29 9.70 -2 -8 0 71.09 8.10 2 8 0 81.59 9.00 2 8 0 95.99 6.80 2 8 0 81.09 6.80 -3 -8 0 46.00 7.50 -3 -8 0 50.49 5.70 -3 -8 0 49.80 8.00 -3 -8 0 45.50 6.50 -3 -8 0 41.60 7.40 -3 -8 0 47.80 7.10 -3 -8 0 41.70 6.40 -3 -8 0 58.19 7.40 3 8 0 44.30 5.70 3 8 0 45.20 7.60 3 8 0 48.40 6.70 3 8 0 41.70 6.60 -4 -8 0 22.70 3.60 -4 -8 0 22.60 4.80 -4 -8 0 20.50 3.30 -4 -8 0 18.70 6.10 -4 -8 0 31.30 5.70 4 8 0 17.40 4.80 4 8 0 29.60 6.60 4 8 0 27.50 4.60 4 8 0 28.60 5.10 4 8 0 18.90 4.50 -5 -8 0 36.20 5.90 -5 -8 0 29.70 7.20 -5 -8 0 32.20 4.50 -5 -8 0 43.10 7.10 5 8 0 32.00 5.70 5 8 0 31.70 5.60 5 8 0 36.00 7.50 5 8 0 31.20 5.50 5 8 0 23.70 5.30 -6 -8 0 15.00 4.60 -6 -8 0 23.50 6.90 -6 -8 0 16.30 6.60 -6 -8 0 14.80 4.20 6 8 0 10.50 5.80 6 8 0 16.90 4.60 6 8 0 10.80 4.60 6 8 0 10.10 4.60 -7 -8 0 18.70 5.00 -7 -8 0 10.10 5.30 -7 -8 0 12.20 6.10 -7 -8 0 22.30 7.10 7 8 0 21.20 7.10 7 8 0 23.40 6.50 7 8 0 12.10 4.90 7 8 0 21.20 5.10 -8 -8 0 12.90 5.20 -8 -8 0 12.10 5.20 -8 -8 0 6.70 6.50 -8 -8 0 6.60 6.30 8 8 0 2.20 4.40 8 8 0 15.50 7.20 8 8 0 17.60 5.60 8 8 0 6.50 5.10 -9 -8 0 8.20 5.90 -9 -8 0 -3.70 4.60 -9 -8 0 4.80 6.30 -9 -8 0 -1.90 6.70 9 8 0 5.60 4.30 9 8 0 3.70 5.00 9 8 0 4.00 5.40 -10 -8 0 3.90 7.10 -10 -8 0 7.10 8.00 10 8 0 -1.70 4.60 10 8 0 -7.50 4.70 10 8 0 8.50 7.60 7 -9 0 -1.30 7.20 7 -9 0 7.50 7.40 -7 9 0 6.60 5.00 -7 9 0 7.20 5.70 -7 9 0 -2.70 6.30 -7 9 0 -2.20 4.90 6 -9 0 17.90 10.20 6 -9 0 4.70 6.70 -6 9 0 13.90 6.30 -6 9 0 8.10 4.80 -6 9 0 15.90 7.30 -6 9 0 12.80 5.90 5 -9 0 29.90 8.90 5 -9 0 23.30 7.30 5 -9 0 30.40 7.50 -5 9 0 28.20 7.90 -5 9 0 25.40 5.60 -5 9 0 30.90 6.30 -5 9 0 34.00 6.30 4 -9 0 29.60 7.20 4 -9 0 27.30 5.50 4 -9 0 41.50 8.80 -4 9 0 35.60 8.00 -4 9 0 36.00 6.10 -4 9 0 25.50 5.80 -4 9 0 27.80 5.10 3 -9 0 18.90 6.90 3 -9 0 31.00 5.20 3 -9 0 24.90 5.00 3 -9 0 23.30 4.80 3 -9 0 23.40 6.50 -3 9 0 18.80 5.00 -3 9 0 25.10 4.80 -3 9 0 28.90 4.80 -3 9 0 17.50 6.30 2 -9 0 3.80 3.90 2 -9 0 0.80 5.30 2 -9 0 1.00 5.20 2 -9 0 4.60 3.70 2 -9 0 2.00 3.60 2 -9 0 0.70 3.70 -2 9 0 1.10 2.90 -2 9 0 5.50 3.10 1 -9 0 47.60 5.90 1 -9 0 41.20 7.20 1 -9 0 42.60 5.90 1 -9 0 42.70 8.30 1 -9 0 51.49 8.30 1 -9 0 37.80 6.50 1 -9 0 42.90 6.90 -1 9 0 34.90 4.80 -1 9 0 39.90 7.20 -1 9 0 35.10 4.90 0 -9 0 128.49 13.60 0 -9 0 114.09 13.10 0 -9 0 116.89 12.10 0 -9 0 116.89 10.30 0 -9 0 122.59 10.40 0 -9 0 114.19 12.00 0 9 0 129.29 12.00 0 9 0 114.29 8.80 -1 -9 0 82.29 10.00 -1 -9 0 79.39 8.30 -1 -9 0 76.39 8.90 -1 -9 0 68.39 9.50 -1 -9 0 82.69 9.10 -1 -9 0 63.79 10.10 -1 -9 0 62.69 8.90 -1 -9 0 71.09 8.00 1 9 0 81.39 9.80 1 9 0 73.49 6.30 -2 -9 0 17.80 4.50 -2 -9 0 3.70 4.80 -2 -9 0 16.90 4.60 -2 -9 0 17.30 5.90 -2 -9 0 17.60 4.40 -2 -9 0 18.00 6.80 -2 -9 0 14.20 4.60 2 9 0 11.00 2.80 2 9 0 6.50 4.60 -3 -9 0 2.70 3.10 -3 -9 0 8.30 3.60 -3 -9 0 8.10 4.60 -3 -9 0 0.40 5.10 -3 -9 0 8.50 4.50 -3 -9 0 3.60 5.00 -3 -9 0 1.90 4.30 3 9 0 6.90 3.00 3 9 0 5.50 3.00 3 9 0 13.30 5.00 -4 -9 0 32.90 6.20 -4 -9 0 48.90 5.90 -4 -9 0 46.10 7.00 -4 -9 0 42.10 6.80 -4 -9 0 41.20 5.20 -4 -9 0 34.50 7.90 4 9 0 32.80 5.40 4 9 0 53.19 8.60 4 9 0 45.00 5.90 4 9 0 29.60 6.30 -5 -9 0 42.30 8.90 -5 -9 0 46.70 7.90 -5 -9 0 39.10 6.40 5 9 0 38.60 6.80 5 9 0 38.90 8.00 5 9 0 36.40 6.60 5 9 0 42.60 6.60 -6 -9 0 9.90 6.70 -6 -9 0 7.90 4.80 -6 -9 0 12.70 6.10 6 9 0 15.20 5.20 6 9 0 11.00 6.60 6 9 0 13.40 5.00 6 9 0 11.50 4.80 -7 -9 0 3.30 3.70 -7 -9 0 5.00 5.90 -7 -9 0 8.40 4.60 -7 -9 0 5.10 6.50 7 9 0 4.60 4.70 7 9 0 -9.90 5.40 7 9 0 -0.50 4.50 7 9 0 5.10 4.60 -8 -9 0 8.50 7.00 -8 -9 0 -0.70 6.80 -8 -9 0 8.80 4.60 -8 -9 0 2.70 4.90 8 9 0 -1.20 4.30 8 9 0 -2.10 11.30 8 9 0 1.60 4.80 8 9 0 1.10 5.60 -9 -9 0 17.20 7.90 9 9 0 9.80 6.20 9 9 0 1.20 6.80 9 9 0 9.60 6.30 9 9 0 6.30 6.10 6 -10 0 -0.30 8.00 6 -10 0 1.10 7.20 -6 10 0 4.90 6.50 -6 10 0 -3.50 4.60 -6 10 0 -1.90 5.90 -6 10 0 6.80 4.90 5 -10 0 20.10 5.40 5 -10 0 5.70 7.60 5 -10 0 10.10 7.20 -5 10 0 13.60 5.90 -5 10 0 16.50 5.10 -5 10 0 15.00 5.50 4 -10 0 15.50 7.10 4 -10 0 13.90 6.80 4 -10 0 13.40 3.90 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8.70 7.90 -3 -8 3 21.50 4.70 -3 -8 3 16.50 6.00 -3 -8 3 15.00 4.90 -3 -8 3 15.20 4.40 -3 -8 3 13.40 5.50 -3 -8 3 25.80 4.40 2 8 -3 16.30 5.70 -2 -8 3 24.90 5.30 -2 -8 3 18.80 5.60 -2 -8 3 12.80 4.00 -2 -8 3 11.50 5.30 -2 -8 3 13.80 4.80 -2 -8 3 10.70 6.10 -2 -8 3 25.60 5.20 -2 -8 3 18.20 5.00 -2 -8 3 20.70 5.70 -1 -8 3 36.20 6.60 -1 -8 3 52.79 6.80 -1 -8 3 33.90 5.60 -1 -8 3 48.60 7.30 -1 -8 3 36.90 7.80 -1 -8 3 36.50 6.40 -1 -8 3 37.20 6.80 -1 -8 3 32.20 6.60 -1 -8 3 37.80 6.50 0 -8 3 71.69 8.70 0 -8 3 55.99 8.00 0 -8 3 72.29 9.40 0 -8 3 69.89 9.10 0 -8 3 63.49 8.30 0 -8 3 70.59 8.40 0 -8 3 51.19 8.50 0 -8 3 64.39 7.90 0 -8 3 66.29 9.10 0 -8 3 69.59 9.20 1 -8 3 51.99 6.70 1 -8 3 44.30 6.90 1 -8 3 50.49 7.50 1 -8 3 46.50 7.50 1 -8 3 47.30 7.30 1 -8 3 44.10 7.60 1 -8 3 50.99 6.90 1 -8 3 46.80 7.20 1 -8 3 57.89 7.40 1 -8 3 39.90 7.20 -2 8 -3 31.10 6.80 2 -8 3 46.10 6.10 2 -8 3 50.89 7.60 2 -8 3 37.40 6.60 2 -8 3 50.09 8.10 2 -8 3 40.10 6.80 2 -8 3 39.20 6.70 2 -8 3 51.79 8.10 2 -8 3 44.30 6.30 -3 8 -3 35.40 7.00 -3 8 -3 34.30 4.60 -3 8 -3 42.40 5.00 3 -8 3 22.50 5.30 3 -8 3 31.40 5.10 3 -8 3 31.80 6.20 3 -8 3 38.10 7.60 3 -8 3 27.50 6.20 3 -8 3 35.80 7.10 3 -8 3 31.20 5.70 -4 8 -3 6.30 5.70 -4 8 -3 7.80 5.60 -4 8 -3 16.80 4.00 -4 8 -3 8.70 3.70 4 -8 3 9.40 4.40 4 -8 3 5.50 4.00 4 -8 3 13.90 5.30 4 -8 3 17.80 7.00 4 -8 3 10.30 5.80 4 -8 3 17.00 3.90 4 -8 3 11.90 6.00 -5 8 -3 12.70 4.50 -5 8 -3 6.80 5.90 -5 8 -3 4.50 5.50 -5 8 -3 13.90 4.40 5 -8 3 13.50 6.50 5 -8 3 10.70 5.50 5 -8 3 9.10 4.70 -6 8 -3 28.50 6.20 -6 8 -3 29.30 8.20 -6 8 -3 27.00 7.10 -6 8 -3 19.50 5.70 6 -8 3 42.30 8.40 6 -8 3 29.80 7.80 -7 8 -3 3.20 5.70 -7 8 -3 2.30 4.50 7 -8 3 1.90 5.90 -8 8 -3 -5.00 6.40 -8 8 -3 -8.80 4.60 -8 8 -3 -6.00 4.70 8 -8 3 2.20 6.40 8 -8 3 0.40 6.50 9 7 -3 7.40 7.00 9 7 -3 2.50 4.70 -9 -7 3 1.80 6.90 -9 -7 3 4.60 7.60 -9 -7 3 5.90 3.80 8 7 -3 16.10 5.30 8 7 -3 6.90 5.00 8 7 -3 1.30 6.80 8 7 -3 0.50 4.60 -8 -7 3 -2.30 4.70 -8 -7 3 9.50 7.40 -8 -7 3 10.20 5.10 -8 -7 3 2.20 6.50 7 7 -3 13.30 5.90 7 7 -3 11.70 4.60 7 7 -3 14.80 7.50 -7 -7 3 20.40 7.50 -7 -7 3 9.30 7.30 -7 -7 3 11.30 4.80 6 7 -3 20.50 4.80 6 7 -3 18.80 5.80 6 7 -3 26.20 7.70 -6 -7 3 23.20 6.40 -6 -7 3 25.40 4.90 -6 -7 3 20.70 6.90 -6 -7 3 21.10 7.40 -6 -7 3 9.30 4.20 5 7 -3 14.50 6.10 5 7 -3 27.90 5.60 5 7 -3 20.20 4.30 -5 -7 3 17.90 4.60 -5 -7 3 19.90 3.90 -5 -7 3 18.00 9.10 -5 -7 3 27.10 7.90 -5 -7 3 25.10 4.60 -5 -7 3 25.50 4.20 4 7 -3 6.90 3.70 4 7 -3 12.50 5.60 4 7 -3 14.90 4.20 -4 -7 3 17.30 4.40 -4 -7 3 19.40 5.50 -4 -7 3 18.10 6.70 -4 -7 3 23.20 5.60 -4 -7 3 23.30 6.20 -4 -7 3 17.70 3.60 -4 -7 3 20.60 3.70 3 7 -3 10.30 3.20 3 7 -3 6.40 4.80 -3 -7 3 15.60 4.40 -3 -7 3 12.80 4.50 -3 -7 3 6.30 4.60 -3 -7 3 15.70 4.10 -3 -7 3 15.70 3.70 -3 -7 3 10.60 5.90 -3 -7 3 11.40 3.40 -3 -7 3 14.00 5.00 2 7 -3 57.09 5.30 2 7 -3 54.89 5.70 2 7 -3 50.19 7.60 -2 -7 3 79.69 8.50 -2 -7 3 73.89 7.10 -2 -7 3 65.19 7.40 -2 -7 3 71.89 8.40 -2 -7 3 77.29 7.70 -2 -7 3 69.39 8.60 -2 -7 3 69.69 8.00 -2 -7 3 84.99 10.60 -2 -7 3 60.79 7.30 1 7 -3 189.58 15.10 -1 -7 3 184.38 14.30 -1 -7 3 190.18 15.20 -1 -7 3 174.58 14.80 -1 -7 3 180.18 15.00 -1 -7 3 189.08 16.40 -1 -7 3 181.28 14.80 -1 -7 3 201.58 14.90 -1 -7 3 196.28 14.50 -1 -7 3 173.18 14.80 -1 -7 3 182.88 14.20 0 -7 3 237.08 16.80 0 -7 3 222.38 18.40 0 -7 3 224.68 17.20 0 -7 3 238.48 17.30 0 -7 3 244.98 17.50 0 -7 3 229.28 17.20 0 -7 3 221.08 17.60 0 -7 3 220.78 17.90 0 -7 3 211.38 17.30 0 -7 3 235.98 17.30 -1 7 -3 -0.40 4.10 1 -7 3 5.30 4.00 1 -7 3 8.00 3.60 1 -7 3 8.00 4.10 1 -7 3 3.70 4.00 1 -7 3 7.00 4.30 1 -7 3 8.40 4.00 1 -7 3 5.80 3.50 1 -7 3 7.70 3.60 1 -7 3 10.40 4.30 1 -7 3 4.50 3.80 -2 7 -3 26.60 5.80 -2 7 -3 29.20 3.60 -2 7 -3 27.50 3.60 2 -7 3 31.40 6.20 2 -7 3 23.60 5.70 2 -7 3 28.50 5.80 2 -7 3 27.70 5.70 2 -7 3 38.10 5.30 2 -7 3 31.00 5.60 2 -7 3 28.30 5.40 2 -7 3 19.90 7.00 2 -7 3 35.60 5.00 -3 7 -3 39.40 7.00 3 -7 3 34.00 7.20 3 -7 3 49.99 8.10 3 -7 3 54.49 6.30 3 -7 3 52.59 7.50 3 -7 3 51.19 6.30 3 -7 3 53.99 8.30 3 -7 3 46.00 6.60 3 -7 3 51.99 8.00 -4 7 -3 114.79 12.20 -4 7 -3 103.29 11.40 -4 7 -3 115.99 11.30 -4 7 -3 100.49 9.50 4 -7 3 108.89 10.40 4 -7 3 101.79 9.10 4 -7 3 114.39 10.40 4 -7 3 118.59 10.90 4 -7 3 110.19 8.80 -5 7 -3 50.09 6.90 -5 7 -3 39.80 8.20 -5 7 -3 42.60 6.70 -5 7 -3 57.89 8.00 -5 7 -3 44.60 6.60 5 -7 3 51.39 7.20 5 -7 3 50.89 5.00 5 -7 3 61.19 8.20 5 -7 3 45.30 8.00 -6 7 -3 0.70 4.10 -6 7 -3 1.20 4.90 -6 7 -3 3.50 4.10 -6 7 -3 -2.90 5.00 -6 7 -3 -5.60 3.70 6 -7 3 1.10 2.70 6 -7 3 1.90 4.80 6 -7 3 2.00 5.60 -7 7 -3 12.00 5.60 -7 7 -3 19.20 7.20 -7 7 -3 3.30 4.80 -7 7 -3 8.20 5.90 7 -7 3 3.90 5.40 7 -7 3 19.70 7.40 7 -7 3 10.10 4.10 -8 7 -3 2.40 5.90 -8 7 -3 -0.90 5.70 -8 7 -3 8.30 5.40 8 -7 3 10.60 6.40 8 -7 3 -0.60 4.00 -9 7 -3 -0.40 5.50 -9 7 -3 5.20 5.80 -9 7 -3 6.80 5.90 -9 7 -3 -1.40 6.10 9 -7 3 3.90 7.80 9 -7 3 -6.30 5.90 10 6 -3 8.50 5.70 10 6 -3 12.10 11.80 10 6 -3 1.90 8.20 10 6 -3 14.70 5.90 -10 -6 3 7.20 6.90 -10 -6 3 8.00 8.50 -10 -6 3 0.10 3.70 9 6 -3 4.40 7.20 9 6 -3 7.60 6.70 9 6 -3 11.20 4.70 9 6 -3 14.10 5.30 -9 -6 3 2.50 6.40 -9 -6 3 8.10 7.20 -9 -6 3 8.10 6.30 -9 -6 3 2.80 3.90 8 6 -3 21.30 7.60 8 6 -3 19.50 5.10 8 6 -3 33.30 7.80 -8 -6 3 21.20 7.50 -8 -6 3 18.50 7.60 -8 -6 3 22.00 6.50 -8 -6 3 24.30 4.80 7 6 -3 2.50 5.80 7 6 -3 -2.30 4.10 7 6 -3 -2.10 3.90 7 6 -3 -5.60 3.00 -7 -6 3 -1.90 3.80 -7 -6 3 -1.60 3.50 -7 -6 3 1.70 5.80 -7 -6 3 6.10 5.90 6 6 -3 59.99 6.70 6 6 -3 41.40 7.30 6 6 -3 49.00 6.80 -6 -6 3 52.19 9.60 -6 -6 3 45.40 6.80 -6 -6 3 40.30 7.50 5 6 -3 65.89 7.90 5 6 -3 75.09 8.00 5 6 -3 67.19 7.20 5 6 -3 94.69 10.80 5 6 -3 61.69 8.20 -5 -6 3 62.09 6.10 -5 -6 3 59.49 9.80 -5 -6 3 64.39 8.30 -5 -6 3 55.59 8.20 -5 -6 3 71.19 9.40 4 6 -3 16.10 4.40 4 6 -3 18.10 4.40 4 6 -3 20.90 3.90 4 6 -3 22.00 6.00 4 6 -3 23.50 5.00 -4 -6 3 32.30 5.70 -4 -6 3 52.79 8.50 -4 -6 3 28.70 5.50 -4 -6 3 32.00 6.40 -4 -6 3 25.50 5.20 -4 -6 3 30.10 3.70 -4 -6 3 27.00 3.40 -4 -6 3 25.70 3.80 3 6 -3 145.19 13.70 3 6 -3 159.38 12.40 3 6 -3 142.39 14.00 -3 -6 3 172.08 14.50 -3 -6 3 170.18 12.00 -3 -6 3 161.98 12.90 -3 -6 3 187.68 16.00 -3 -6 3 159.38 12.80 -3 -6 3 172.48 13.60 -3 -6 3 165.98 11.90 -3 -6 3 165.38 12.00 -3 -6 3 142.59 12.70 2 6 -3 48.30 6.80 2 6 -3 49.00 7.20 2 6 -3 48.50 5.10 2 6 -3 45.40 4.60 -2 -6 3 56.69 6.90 -2 -6 3 52.09 5.90 -2 -6 3 58.09 6.60 -2 -6 3 54.19 6.90 -2 -6 3 65.29 9.20 -2 -6 3 51.89 6.90 -2 -6 3 49.80 6.60 -2 -6 3 54.79 6.00 1 6 -3 193.68 16.00 1 6 -3 198.18 15.40 -1 -6 3 209.58 14.90 -1 -6 3 209.68 14.90 -1 -6 3 194.98 15.30 -1 -6 3 206.88 15.40 -1 -6 3 208.98 15.70 -1 -6 3 194.28 15.50 -1 -6 3 209.48 15.20 0 6 -3 550.94 39.00 0 -6 3 545.75 38.70 0 -6 3 574.44 38.80 0 -6 3 608.04 38.60 0 -6 3 570.34 39.20 0 -6 3 584.04 38.50 0 -6 3 578.74 38.60 0 -6 3 597.34 38.20 0 -6 3 620.84 38.50 0 -6 3 573.84 38.50 -1 6 -3 59.09 7.30 -1 6 -3 61.29 7.70 1 -6 3 66.49 7.70 1 -6 3 62.29 8.10 1 -6 3 76.89 8.20 1 -6 3 66.59 7.60 1 -6 3 73.89 6.90 1 -6 3 75.09 7.30 1 -6 3 72.39 8.90 1 -6 3 70.69 7.20 1 -6 3 83.99 8.00 -2 6 -3 38.50 5.00 -2 6 -3 38.20 4.70 -2 6 -3 46.70 6.70 2 -6 3 68.49 6.40 2 -6 3 74.79 7.70 2 -6 3 60.39 6.20 2 -6 3 69.69 6.70 2 -6 3 53.99 6.80 2 -6 3 77.99 8.90 2 -6 3 58.99 7.60 2 -6 3 51.49 7.30 2 -6 3 63.89 8.20 -3 6 -3 24.30 5.60 -3 6 -3 24.30 4.20 -3 6 -3 29.50 5.40 -3 6 -3 22.50 3.80 3 -6 3 30.60 5.50 3 -6 3 36.70 4.90 3 -6 3 25.60 5.80 3 -6 3 27.90 4.00 3 -6 3 33.20 5.10 3 -6 3 35.60 4.80 3 -6 3 32.10 6.40 3 -6 3 39.40 6.70 3 -6 3 28.10 5.60 -4 6 -3 3.10 2.80 -4 6 -3 2.50 3.10 -4 6 -3 0.30 4.00 -4 6 -3 5.30 4.30 4 -6 3 3.70 3.80 4 -6 3 4.80 2.10 4 -6 3 4.60 4.40 4 -6 3 9.80 2.60 4 -6 3 4.40 3.70 4 -6 3 9.40 4.90 4 -6 3 6.00 2.70 4 -6 3 4.90 2.10 4 -6 3 7.30 4.40 -5 6 -3 115.49 10.20 -5 6 -3 131.99 11.60 -5 6 -3 113.49 10.90 5 -6 3 124.39 10.90 5 -6 3 130.39 14.40 5 -6 3 104.09 11.10 5 -6 3 111.89 9.60 -6 6 -3 84.09 8.90 -6 6 -3 79.99 10.70 -6 6 -3 94.59 10.20 -6 6 -3 81.29 9.70 -6 6 -3 91.19 9.70 6 -6 3 70.89 8.30 6 -6 3 87.79 11.20 6 -6 3 66.49 8.50 -7 6 -3 10.70 5.60 -7 6 -3 10.30 5.20 -7 6 -3 13.60 6.20 -7 6 -3 9.50 5.10 -7 6 -3 10.40 5.00 7 -6 3 24.80 6.10 7 -6 3 16.30 4.90 7 -6 3 10.50 5.70 -8 6 -3 7.10 5.80 -8 6 -3 2.30 5.20 -8 6 -3 -1.50 4.30 -8 6 -3 -1.70 4.50 8 -6 3 7.40 6.40 -9 6 -3 -2.80 5.60 -9 6 -3 5.30 6.10 -9 6 -3 4.80 5.40 9 -6 3 6.80 6.40 9 -6 3 4.40 7.50 9 -6 3 -2.20 5.90 10 5 -3 11.90 9.10 10 5 -3 7.00 5.00 10 5 -3 15.00 7.30 10 5 -3 13.70 5.60 -10 -5 3 0.70 7.10 -10 -5 3 15.70 10.00 -10 -5 3 16.90 4.90 -10 -5 3 11.60 7.30 9 5 -3 4.90 4.60 9 5 -3 4.60 7.30 9 5 -3 1.00 5.50 9 5 -3 10.60 5.00 -9 -5 3 5.40 5.80 -9 -5 3 6.70 7.40 -9 -5 3 5.80 6.30 -9 -5 3 6.00 4.10 8 5 -3 62.89 7.80 8 5 -3 73.09 10.70 8 5 -3 63.49 10.20 8 5 -3 75.39 9.40 -8 -5 3 77.99 11.70 -8 -5 3 78.29 11.30 -8 -5 3 58.09 9.30 -8 -5 3 67.99 8.30 7 5 -3 34.60 7.80 7 5 -3 23.00 6.00 7 5 -3 19.00 4.60 -7 -5 3 27.60 4.90 -7 -5 3 20.70 9.70 -7 -5 3 23.20 5.90 -7 -5 3 28.10 7.30 6 5 -3 0.10 2.90 6 5 -3 0.70 4.50 6 5 -3 1.60 6.10 6 5 -3 7.00 4.30 6 5 -3 4.60 3.40 -6 -5 3 6.10 3.60 -6 -5 3 5.20 5.20 -6 -5 3 0.80 3.50 -6 -5 3 3.30 3.70 -6 -5 3 0.20 4.70 -6 -5 3 3.90 5.40 5 5 -3 19.30 4.20 5 5 -3 8.70 4.60 5 5 -3 18.00 4.00 5 5 -3 16.70 4.60 5 5 -3 14.00 3.80 5 5 -3 16.70 5.40 -5 -5 3 42.10 8.20 -5 -5 3 30.00 4.10 -5 -5 3 29.40 4.40 -5 -5 3 27.20 5.30 -5 -5 3 25.90 6.10 -5 -5 3 28.80 5.30 4 5 -3 21.70 5.40 4 5 -3 28.70 4.50 4 5 -3 18.00 5.00 4 5 -3 23.50 4.40 4 5 -3 26.20 4.80 4 5 -3 16.60 3.50 -4 -5 3 25.50 3.50 -4 -5 3 33.20 6.00 -4 -5 3 28.60 5.00 -4 -5 3 33.50 5.50 -4 -5 3 28.80 4.40 -4 -5 3 31.80 4.10 3 5 -3 19.50 3.70 3 5 -3 22.80 4.90 3 5 -3 18.10 3.90 3 5 -3 20.20 4.60 3 5 -3 13.50 3.80 -3 -5 3 27.90 3.20 -3 -5 3 23.60 3.30 -3 -5 3 21.60 4.30 -3 -5 3 20.50 4.50 -3 -5 3 29.60 5.10 -3 -5 3 20.10 3.30 -3 -5 3 23.00 2.90 2 5 -3 298.17 23.10 2 5 -3 310.17 22.50 2 5 -3 322.37 21.20 2 5 -3 317.87 21.70 2 5 -3 300.97 22.30 -2 -5 3 352.66 21.70 -2 -5 3 328.47 22.50 -2 -5 3 345.97 22.70 -2 -5 3 316.07 21.80 -2 -5 3 304.47 22.50 -2 -5 3 337.67 22.10 -2 -5 3 331.37 21.50 1 5 -3 551.34 36.50 1 5 -3 550.64 35.10 1 5 -3 592.44 35.40 1 5 -3 519.25 37.00 -1 -5 3 530.25 36.50 -1 -5 3 544.65 36.40 -1 -5 3 548.05 35.90 -1 -5 3 530.15 36.60 -1 -5 3 562.34 36.10 -1 -5 3 548.75 36.10 -1 -5 3 558.34 35.90 -1 -5 3 550.54 36.50 0 5 -3 123.39 10.40 0 -5 3 110.39 9.70 0 -5 3 113.69 10.20 0 -5 3 130.39 9.80 0 -5 3 118.99 10.00 0 -5 3 121.69 9.60 0 -5 3 126.69 9.80 0 -5 3 116.49 10.00 0 -5 3 124.39 9.80 -1 5 -3 273.77 18.10 -1 5 -3 294.17 19.60 -1 5 -3 243.68 19.30 -1 5 -3 283.67 18.00 1 -5 3 276.27 18.70 1 -5 3 283.87 19.00 1 -5 3 272.57 19.50 1 -5 3 277.97 18.90 1 -5 3 276.37 20.00 1 -5 3 279.67 19.80 1 -5 3 258.17 19.30 1 -5 3 284.17 19.40 -2 5 -3 25.30 4.10 -2 5 -3 21.40 3.10 -2 5 -3 21.70 3.60 -2 5 -3 23.00 3.10 2 -5 3 11.70 3.80 2 -5 3 16.40 3.20 2 -5 3 10.60 3.70 2 -5 3 20.60 4.40 2 -5 3 11.10 3.20 2 -5 3 10.40 3.60 2 -5 3 17.00 3.20 2 -5 3 13.60 4.00 -3 5 -3 48.80 6.80 -3 5 -3 57.49 7.90 -3 5 -3 49.40 5.50 -3 5 -3 46.10 5.60 -3 5 -3 52.59 6.60 -3 5 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17.10 7.90 -10 -3 3 8.40 5.30 -10 -3 3 13.00 8.20 -10 -3 3 1.50 5.70 9 3 -3 69.09 12.60 9 3 -3 96.79 13.30 9 3 -3 75.19 8.10 9 3 -3 60.79 11.30 -9 -3 3 63.29 11.20 -9 -3 3 80.89 9.80 -9 -3 3 74.89 11.60 -9 -3 3 73.19 16.00 8 3 -3 146.59 16.00 8 3 -3 137.79 15.40 8 3 -3 152.08 13.70 8 3 -3 142.09 11.80 -8 -3 3 154.48 15.50 -8 -3 3 142.49 12.80 -8 -3 3 158.88 13.40 -8 -3 3 162.88 15.70 -8 -3 3 138.99 14.90 7 3 -3 21.30 6.20 7 3 -3 29.10 4.50 7 3 -3 21.90 5.10 7 3 -3 31.70 7.70 7 3 -3 29.30 5.80 -7 -3 3 15.60 5.00 -7 -3 3 39.10 8.00 -7 -3 3 21.40 6.10 -7 -3 3 23.10 6.20 -7 -3 3 35.70 7.00 -7 -3 3 26.30 5.20 -7 -3 3 32.60 6.10 6 3 -3 39.00 6.40 6 3 -3 29.90 5.40 6 3 -3 45.10 5.50 6 3 -3 46.40 5.90 6 3 -3 37.20 7.10 6 3 -3 43.80 7.60 -6 -3 3 35.90 5.60 -6 -3 3 29.80 6.70 -6 -3 3 31.90 5.40 -6 -3 3 32.50 6.10 -6 -3 3 36.80 5.50 -6 -3 3 30.40 6.60 5 3 -3 28.40 4.30 5 3 -3 30.40 5.50 5 3 -3 31.00 6.00 5 3 -3 16.40 4.50 5 3 -3 23.70 4.10 5 3 -3 25.10 4.00 -5 -3 3 15.90 4.70 -5 -3 3 22.10 4.20 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55.79 5.70 -3 -2 3 53.69 5.40 -3 -2 3 55.39 5.00 2 2 -3 3894.01 251.47 2 2 -3 3764.52 251.27 2 2 -3 3894.31 251.77 2 2 -3 4302.27 251.67 2 2 -3 4167.08 251.37 -2 -2 3 4004.00 251.77 -2 -2 3 3970.20 251.07 -2 -2 3 3607.84 250.97 -2 -2 3 4189.38 251.07 -2 -2 3 3969.50 251.37 -2 -2 3 4143.39 251.57 1 2 -3 176.68 12.60 1 2 -3 201.88 12.90 1 2 -3 191.28 13.50 1 2 -3 175.78 13.10 1 2 -3 198.08 12.80 -1 -2 3 191.28 12.70 -1 -2 3 179.48 12.90 -1 -2 3 192.78 12.80 -1 -2 3 173.88 12.50 -1 -2 3 194.78 13.10 -1 -2 3 177.68 12.90 0 2 -3 900.21 58.09 0 2 -3 809.22 58.49 0 2 -3 837.92 58.09 0 2 -3 834.72 57.89 0 2 -3 903.71 58.49 0 2 -3 834.42 58.09 0 2 -3 838.52 58.59 0 -2 3 942.71 58.59 0 -2 3 958.80 57.89 0 -2 3 961.60 58.19 0 -2 3 1017.70 58.19 0 -2 3 1015.40 58.09 0 -2 3 985.10 58.49 0 -2 3 976.70 58.39 -1 2 -3 147.59 10.70 -1 2 -3 136.29 10.30 -1 2 -3 151.98 10.40 -1 2 -3 141.29 10.10 -1 2 -3 149.99 10.00 -1 2 -3 141.49 10.40 1 -2 3 143.59 9.50 1 -2 3 144.89 10.00 1 -2 3 134.79 10.30 1 -2 3 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3 -9 4 7.50 4.60 3 -9 4 6.20 5.70 3 -9 4 11.30 4.50 3 -9 4 12.60 6.00 3 -9 4 2.50 4.60 -4 9 -4 19.30 7.20 -4 9 -4 30.50 4.60 -4 9 -4 13.80 4.20 4 -9 4 17.30 4.60 4 -9 4 16.30 6.90 4 -9 4 23.50 6.30 4 -9 4 21.80 4.90 4 -9 4 17.50 7.00 4 -9 4 37.60 6.10 -5 9 -4 7.50 6.50 -5 9 -4 2.00 4.10 -5 9 -4 6.50 3.90 5 -9 4 16.00 7.10 5 -9 4 15.60 6.10 5 -9 4 17.00 7.30 -6 9 -4 7.70 4.70 -6 9 -4 6.90 6.80 -6 9 -4 2.40 4.70 6 -9 4 2.90 6.50 6 -9 4 13.00 7.70 6 -9 4 10.30 6.00 8 8 -4 -1.40 5.50 8 8 -4 5.20 5.10 -8 -8 4 -5.30 3.90 -8 -8 4 3.00 8.00 -8 -8 4 -1.20 7.60 -8 -8 4 5.50 5.30 7 8 -4 9.00 7.50 7 8 -4 11.30 4.80 7 8 -4 2.00 5.10 -7 -8 4 -1.00 4.30 -7 -8 4 7.60 7.70 -7 -8 4 -0.90 3.90 -7 -8 4 2.90 7.60 6 8 -4 21.00 5.00 6 8 -4 13.80 5.60 6 8 -4 23.70 8.10 -6 -8 4 17.10 7.70 -6 -8 4 8.10 4.70 -6 -8 4 12.30 8.20 -6 -8 4 10.30 3.50 -6 -8 4 8.20 4.40 5 8 -4 5.10 6.50 5 8 -4 11.70 4.70 5 8 -4 11.70 3.90 -5 -8 4 14.00 7.10 -5 -8 4 7.90 4.40 -5 -8 4 28.10 9.20 -5 -8 4 11.30 4.10 4 8 -4 23.20 11.30 4 8 -4 19.20 3.80 4 8 -4 21.10 4.90 -4 -8 4 11.80 4.70 -4 -8 4 25.60 8.10 -4 -8 4 4.00 5.70 -4 -8 4 14.10 4.60 -4 -8 4 17.90 3.80 -4 -8 4 13.80 4.00 3 8 -4 24.50 3.60 3 8 -4 16.20 6.40 3 8 -4 20.00 4.10 -3 -8 4 23.80 7.80 -3 -8 4 23.80 4.70 -3 -8 4 17.20 4.30 -3 -8 4 16.00 5.20 -3 -8 4 21.30 5.70 -3 -8 4 24.70 6.70 -3 -8 4 20.30 4.50 2 8 -4 5.00 5.00 -2 -8 4 3.80 3.60 -2 -8 4 10.10 4.50 -2 -8 4 7.60 5.80 -2 -8 4 5.50 3.70 -2 -8 4 7.70 4.20 -2 -8 4 7.70 4.00 -1 -8 4 11.00 4.80 -1 -8 4 19.60 5.40 -1 -8 4 14.50 5.40 -1 -8 4 15.00 4.70 -1 -8 4 17.60 6.70 -1 -8 4 7.70 4.70 -1 -8 4 12.80 6.50 -1 -8 4 14.70 4.60 -1 -8 4 9.60 4.10 -1 -8 4 9.90 5.20 0 -8 4 65.89 9.00 0 -8 4 80.89 9.10 0 -8 4 64.59 9.00 0 -8 4 75.69 9.00 0 -8 4 72.79 8.20 0 -8 4 69.29 9.00 0 -8 4 73.99 10.40 0 -8 4 76.79 10.00 0 -8 4 77.79 9.40 0 -8 4 76.49 9.30 1 -8 4 41.40 6.80 1 -8 4 42.80 7.70 1 -8 4 37.00 7.10 1 -8 4 37.50 6.70 1 -8 4 46.00 7.10 1 -8 4 46.10 6.10 1 -8 4 47.70 7.70 1 -8 4 36.60 6.70 1 -8 4 46.10 6.50 -2 8 -4 63.29 8.80 2 -8 4 66.89 7.90 2 -8 4 53.29 8.20 2 -8 4 71.49 9.40 2 -8 4 63.69 7.50 2 -8 4 53.89 9.40 2 -8 4 61.69 8.70 2 -8 4 43.70 12.10 2 -8 4 58.59 7.70 -3 8 -4 -2.80 6.10 -3 8 -4 0.00 2.70 -3 8 -4 -0.60 2.50 3 -8 4 4.50 3.80 3 -8 4 0.00 3.60 3 -8 4 1.40 4.00 3 -8 4 -5.40 4.40 3 -8 4 -1.90 4.40 3 -8 4 4.70 5.20 -4 8 -4 20.70 4.20 -4 8 -4 19.00 6.50 -4 8 -4 23.10 4.70 4 -8 4 21.70 4.80 4 -8 4 16.30 6.10 4 -8 4 20.50 6.70 4 -8 4 14.80 4.70 4 -8 4 14.70 4.00 4 -8 4 22.50 5.70 -5 8 -4 30.70 5.60 -5 8 -4 29.60 7.50 -5 8 -4 32.80 6.00 5 -8 4 34.20 6.00 5 -8 4 38.70 8.50 5 -8 4 27.20 6.20 5 -8 4 20.90 7.00 -6 8 -4 9.60 4.90 -6 8 -4 9.60 5.00 -6 8 -4 12.70 6.60 6 -8 4 2.10 6.20 6 -8 4 6.40 4.60 6 -8 4 12.10 7.30 6 -8 4 12.40 5.60 -7 8 -4 10.90 5.50 -7 8 -4 3.00 5.90 -7 8 -4 -2.60 4.40 7 -8 4 -0.20 6.90 7 -8 4 2.50 6.40 7 -8 4 4.30 5.90 9 7 -4 3.70 7.90 9 7 -4 8.30 6.70 9 7 -4 3.80 5.10 9 7 -4 -2.50 6.60 -9 -7 4 4.50 6.90 -9 -7 4 -0.70 7.90 -9 -7 4 11.70 4.40 8 7 -4 11.10 7.90 8 7 -4 17.10 6.50 8 7 -4 9.80 5.10 8 7 -4 8.30 6.40 -8 -7 4 11.10 8.00 -8 -7 4 15.20 8.30 -8 -7 4 9.50 5.70 -8 -7 4 14.40 5.00 7 7 -4 8.10 4.60 7 7 -4 1.70 4.90 7 7 -4 3.60 5.60 7 7 -4 0.00 6.50 -7 -7 4 -0.50 5.50 -7 -7 4 1.30 4.20 -7 -7 4 14.40 7.80 -7 -7 4 8.60 4.70 6 7 -4 15.00 4.60 6 7 -4 15.20 5.60 6 7 -4 12.90 7.20 6 7 -4 13.40 5.90 -6 -7 4 13.20 6.70 -6 -7 4 24.30 8.90 -6 -7 4 13.80 4.40 -6 -7 4 13.40 4.50 5 7 -4 26.30 6.40 5 7 -4 24.00 5.80 5 7 -4 25.20 4.70 -5 -7 4 21.60 4.80 -5 -7 4 39.10 9.40 -5 -7 4 28.70 7.30 -5 -7 4 25.20 4.30 4 7 -4 11.20 4.00 4 7 -4 6.20 5.70 4 7 -4 5.80 3.00 -4 -7 4 10.20 7.40 -4 -7 4 5.50 4.80 -4 -7 4 6.50 3.90 -4 -7 4 2.40 3.10 3 7 -4 4.90 3.20 3 7 -4 5.90 2.60 3 7 -4 -6.00 4.20 3 7 -4 2.70 4.60 -3 -7 4 2.80 4.70 -3 -7 4 6.60 3.10 -3 -7 4 6.90 3.30 -3 -7 4 8.60 4.40 -3 -7 4 9.20 3.70 -3 -7 4 6.70 4.00 -3 -7 4 12.70 7.40 2 7 -4 36.80 4.30 2 7 -4 34.90 6.90 2 7 -4 34.60 4.80 2 7 -4 45.10 7.00 -2 -7 4 33.00 6.00 -2 -7 4 28.10 4.90 -2 -7 4 34.00 5.40 -2 -7 4 38.50 6.70 -2 -7 4 38.10 6.30 -2 -7 4 41.00 9.20 -2 -7 4 33.90 5.50 -2 -7 4 34.50 5.90 -2 -7 4 38.90 5.20 1 7 -4 16.50 5.10 1 7 -4 10.50 5.10 -1 -7 4 27.10 4.80 -1 -7 4 24.30 5.90 -1 -7 4 36.70 5.20 -1 -7 4 24.60 5.60 -1 -7 4 21.40 5.30 -1 -7 4 24.70 5.40 -1 -7 4 28.50 4.80 -1 -7 4 27.70 5.30 0 7 -4 70.29 9.60 0 -7 4 88.19 9.50 0 -7 4 72.49 9.90 0 -7 4 91.09 8.50 0 -7 4 99.09 9.50 0 -7 4 94.19 9.90 0 -7 4 96.59 9.30 0 -7 4 96.99 9.40 0 -7 4 99.79 10.00 0 -7 4 92.19 9.30 -1 7 -4 32.10 5.80 -1 7 -4 49.70 6.80 1 -7 4 30.90 5.70 1 -7 4 26.10 5.00 1 -7 4 22.90 5.90 1 -7 4 34.70 7.40 1 -7 4 17.80 4.90 1 -7 4 23.00 5.90 1 -7 4 33.90 5.00 1 -7 4 25.80 5.90 1 -7 4 29.00 5.70 1 -7 4 23.80 5.10 -2 7 -4 69.19 6.60 -2 7 -4 74.09 6.20 -2 7 -4 77.99 9.60 2 -7 4 74.69 9.90 2 -7 4 59.29 9.00 2 -7 4 70.79 9.00 2 -7 4 81.89 8.50 2 -7 4 76.09 9.90 2 -7 4 77.09 7.80 2 -7 4 77.09 7.90 2 -7 4 78.99 9.30 2 -7 4 77.79 9.20 -3 7 -4 182.18 13.10 -3 7 -4 185.38 13.50 -3 7 -4 223.38 15.90 3 -7 4 171.88 15.10 3 -7 4 163.38 14.50 3 -7 4 163.18 16.60 3 -7 4 172.28 15.20 3 -7 4 182.48 13.90 3 -7 4 166.88 13.40 3 -7 4 168.18 15.80 3 -7 4 168.88 13.50 -4 7 -4 41.50 5.70 -4 7 -4 42.30 6.20 -4 7 -4 34.30 7.00 4 -7 4 45.30 6.30 4 -7 4 43.80 5.30 4 -7 4 51.69 6.30 4 -7 4 58.89 8.10 4 -7 4 45.70 6.00 4 -7 4 49.70 8.70 4 -7 4 40.70 7.70 -5 7 -4 10.30 5.60 -5 7 -4 11.30 4.40 -5 7 -4 11.80 4.40 5 -7 4 17.40 4.50 5 -7 4 17.10 6.70 5 -7 4 15.60 5.10 5 -7 4 7.30 5.50 -6 7 -4 6.10 4.40 -6 7 -4 -0.50 4.10 -6 7 -4 2.50 4.10 -6 7 -4 1.30 5.30 6 -7 4 4.50 4.60 6 -7 4 2.50 2.80 6 -7 4 -0.80 6.20 6 -7 4 6.00 5.80 -7 7 -4 4.60 5.70 -7 7 -4 7.60 5.00 -7 7 -4 21.70 5.00 -7 7 -4 7.50 5.50 7 -7 4 16.40 6.70 7 -7 4 19.70 4.30 7 -7 4 17.60 8.00 7 -7 4 9.80 5.50 -8 7 -4 23.10 7.10 -8 7 -4 23.40 6.70 -8 7 -4 28.40 7.40 8 -7 4 11.90 7.60 8 -7 4 23.30 6.80 8 -7 4 37.80 9.80 8 -7 4 11.10 4.80 10 6 -4 19.40 9.30 -10 -6 4 12.60 8.20 9 6 -4 6.70 5.70 9 6 -4 5.20 4.70 9 6 -4 12.20 8.60 9 6 -4 4.70 5.80 -9 -6 4 -9.40 4.60 -9 -6 4 17.90 13.60 -9 -6 4 -4.40 3.90 -9 -6 4 8.10 7.80 8 6 -4 12.50 5.90 8 6 -4 0.60 5.00 8 6 -4 6.60 5.60 8 6 -4 22.50 8.30 -8 -6 4 -3.30 6.40 -8 -6 4 6.70 4.60 -8 -6 4 9.00 5.70 -8 -6 4 9.00 6.50 7 6 -4 3.70 6.40 7 6 -4 8.00 5.50 7 6 -4 4.40 4.70 -7 -6 4 3.30 4.20 -7 -6 4 -4.20 5.80 -7 -6 4 12.60 7.80 -7 -6 4 0.80 4.80 6 6 -4 40.70 7.80 6 6 -4 39.40 6.80 6 6 -4 31.80 5.70 6 6 -4 39.80 8.60 -6 -6 4 50.09 6.50 -6 -6 4 43.80 7.00 -6 -6 4 52.89 10.20 -6 -6 4 40.60 8.30 5 6 -4 81.79 12.10 5 6 -4 84.69 9.10 5 6 -4 104.39 12.00 5 6 -4 102.99 18.40 5 6 -4 93.69 10.40 -5 -6 4 121.09 9.60 -5 -6 4 134.99 17.70 -5 -6 4 118.99 11.10 -5 -6 4 85.19 9.20 4 6 -4 143.99 14.70 4 6 -4 169.78 14.80 4 6 -4 162.58 12.10 4 6 -4 170.68 13.00 4 6 -4 150.58 13.10 4 6 -4 158.08 13.50 -4 -6 4 167.58 14.50 -4 -6 4 162.48 12.10 -4 -6 4 144.19 11.20 -4 -6 4 149.29 13.30 -4 -6 4 142.59 11.70 3 6 -4 2.60 2.40 3 6 -4 8.60 4.90 3 6 -4 9.20 4.80 3 6 -4 8.80 4.60 3 6 -4 7.50 3.20 -3 -6 4 16.80 4.60 -3 -6 4 12.10 3.40 -3 -6 4 7.30 4.40 -3 -6 4 18.50 4.70 -3 -6 4 15.70 5.00 2 6 -4 179.08 15.10 2 6 -4 168.38 12.00 2 6 -4 182.08 12.80 2 6 -4 169.28 14.10 -2 -6 4 165.98 12.70 -2 -6 4 168.38 12.90 -2 -6 4 153.88 13.90 -2 -6 4 161.38 13.70 -2 -6 4 170.08 14.30 -2 -6 4 177.38 14.20 -2 -6 4 183.58 12.60 -2 -6 4 168.48 13.20 1 6 -4 50.09 6.60 1 6 -4 39.00 4.90 1 6 -4 44.00 4.80 1 6 -4 42.70 6.90 -1 -6 4 58.39 6.40 -1 -6 4 48.80 6.50 -1 -6 4 51.59 6.80 -1 -6 4 54.79 6.70 -1 -6 4 46.40 6.20 -1 -6 4 50.39 6.80 -1 -6 4 45.40 6.70 -1 -6 4 57.39 6.00 0 -6 4 191.58 13.30 0 -6 4 166.38 13.80 0 -6 4 181.08 13.90 0 -6 4 195.58 13.80 0 -6 4 169.58 14.60 0 -6 4 172.68 14.40 0 -6 4 173.28 13.80 0 -6 4 174.38 14.20 0 -6 4 177.68 14.00 -1 6 -4 232.78 18.90 -1 6 -4 277.47 19.30 -1 6 -4 256.67 17.30 -1 6 -4 276.67 17.00 1 -6 4 234.38 18.70 1 -6 4 252.97 18.30 1 -6 4 245.08 19.20 1 -6 4 226.28 19.40 1 -6 4 259.37 19.40 1 -6 4 281.67 18.90 1 -6 4 265.27 17.90 -2 6 -4 206.98 16.70 -2 6 -4 237.78 17.20 -2 6 -4 235.38 15.30 2 -6 4 230.88 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103.49 10.40 7 -6 4 94.39 12.60 7 -6 4 74.89 9.50 -8 6 -4 4.90 5.10 -8 6 -4 -1.50 5.40 -8 6 -4 -0.80 5.00 -8 6 -4 -5.10 5.50 -8 6 -4 -2.70 4.40 8 -6 4 -0.20 4.00 8 -6 4 -2.50 5.10 8 -6 4 2.30 6.30 8 -6 4 0.80 7.00 -9 6 -4 16.50 7.00 -9 6 -4 24.40 8.30 -9 6 -4 14.90 7.30 -9 6 -4 13.30 6.10 9 -6 4 18.30 8.20 9 -6 4 7.70 8.30 9 -6 4 20.70 7.00 10 5 -4 11.50 6.50 10 5 -4 2.20 7.30 10 5 -4 6.00 8.00 10 5 -4 4.00 6.50 -10 -5 4 -0.10 6.60 -10 -5 4 12.60 5.20 -10 -5 4 -3.50 7.50 9 5 -4 18.90 5.70 9 5 -4 18.70 5.90 9 5 -4 11.50 8.10 9 5 -4 7.30 6.10 -9 -5 4 7.40 7.60 -9 -5 4 11.60 7.30 -9 -5 4 19.00 7.30 -9 -5 4 7.60 4.90 8 5 -4 10.10 6.20 8 5 -4 17.50 8.10 8 5 -4 15.40 5.20 8 5 -4 25.90 5.90 -8 -5 4 23.60 8.10 -8 -5 4 14.30 7.50 -8 -5 4 13.10 5.90 -8 -5 4 13.60 5.10 7 5 -4 24.80 6.70 7 5 -4 32.40 5.90 7 5 -4 31.50 8.30 -7 -5 4 33.40 6.90 -7 -5 4 34.80 9.20 -7 -5 4 27.50 8.10 -7 -5 4 43.90 6.60 6 5 -4 23.20 7.10 6 5 -4 25.30 5.60 6 5 -4 33.00 9.70 6 5 -4 28.10 5.30 -6 -5 4 28.60 5.40 -6 -5 4 30.90 7.40 -6 -5 4 26.90 5.70 5 5 -4 19.50 5.90 5 5 -4 10.50 4.30 5 5 -4 20.60 4.20 5 5 -4 13.70 5.40 5 5 -4 11.70 4.50 5 5 -4 26.60 4.60 -5 -5 4 16.70 4.50 -5 -5 4 15.80 4.10 -5 -5 4 9.60 5.00 -5 -5 4 9.30 2.70 -5 -5 4 18.30 5.40 -5 -5 4 11.10 4.60 4 5 -4 168.28 13.80 4 5 -4 186.38 14.70 4 5 -4 172.88 15.10 4 5 -4 171.78 14.00 4 5 -4 167.58 12.80 4 5 -4 170.28 13.00 -4 -5 4 181.38 12.90 -4 -5 4 163.08 13.50 -4 -5 4 172.88 14.70 -4 -5 4 163.28 13.20 -4 -5 4 166.78 14.00 -4 -5 4 152.78 12.10 3 5 -4 169.18 13.40 3 5 -4 150.98 12.70 3 5 -4 149.88 12.30 3 5 -4 161.68 13.90 3 5 -4 154.28 11.40 -3 -5 4 148.09 12.10 -3 -5 4 163.28 11.70 -3 -5 4 160.48 13.20 -3 -5 4 157.58 12.80 -3 -5 4 148.99 11.50 -3 -5 4 142.99 11.00 -3 -5 4 156.38 12.60 2 5 -4 43.90 5.70 2 5 -4 28.50 5.40 2 5 -4 39.20 4.60 2 5 -4 33.50 3.90 2 5 -4 41.50 5.70 -2 -5 4 21.20 3.00 -2 -5 4 16.60 4.20 -2 -5 4 31.40 3.80 -2 -5 4 22.80 3.00 -2 -5 4 23.80 3.40 -2 -5 4 24.30 3.90 -2 -5 4 31.40 5.00 -2 -5 4 35.20 5.50 -2 -5 4 22.00 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62.99 10.10 -8 5 -4 82.29 10.60 -8 5 -4 61.99 10.00 -8 5 -4 58.39 9.10 -8 5 -4 70.19 8.80 8 -5 4 73.29 11.10 8 -5 4 66.89 8.80 8 -5 4 69.99 9.50 -9 5 -4 12.10 5.50 -9 5 -4 -2.80 5.50 -9 5 -4 5.40 5.60 -9 5 -4 1.20 5.60 9 -5 4 -2.00 4.20 9 -5 4 -3.50 6.90 9 -5 4 -7.50 6.70 9 -5 4 7.90 5.80 -10 5 -4 10.20 7.10 -10 5 -4 6.80 6.90 -10 5 -4 1.00 7.40 -10 5 -4 4.90 7.00 10 -5 4 18.70 9.10 10 -5 4 13.80 7.10 10 -5 4 10.10 8.30 10 4 -4 25.50 9.40 10 4 -4 21.30 5.80 10 4 -4 22.50 10.40 10 4 -4 24.50 7.00 -10 -4 4 23.60 10.20 -10 -4 4 32.00 9.00 -10 -4 4 27.30 9.10 -10 -4 4 28.30 6.70 9 4 -4 -3.40 6.80 9 4 -4 -3.40 4.70 9 4 -4 4.60 5.20 -9 -4 4 3.20 6.90 -9 -4 4 -3.20 5.70 -9 -4 4 2.70 5.20 -9 -4 4 2.80 4.90 8 4 -4 22.00 6.10 8 4 -4 39.30 9.20 8 4 -4 46.90 9.50 8 4 -4 30.60 5.80 -8 -4 4 31.80 8.40 -8 -4 4 41.40 9.30 -8 -4 4 27.30 6.10 -8 -4 4 43.50 9.50 7 4 -4 27.40 7.40 7 4 -4 32.90 6.00 7 4 -4 21.70 6.80 7 4 -4 23.20 5.40 7 4 -4 38.40 8.60 -7 -4 4 23.00 5.60 -7 -4 4 31.00 6.90 -7 -4 4 34.90 8.10 -7 -4 4 28.40 9.20 6 4 -4 232.08 19.80 6 4 -4 227.18 17.80 6 4 -4 264.27 18.40 6 4 -4 264.47 20.20 6 4 -4 231.18 19.80 -6 -4 4 266.07 18.50 -6 -4 4 255.07 19.60 -6 -4 4 237.58 18.40 -6 -4 4 235.98 19.70 -6 -4 4 220.28 18.20 -6 -4 4 222.68 17.60 5 4 -4 444.66 31.30 5 4 -4 435.06 29.70 5 4 -4 459.45 31.20 5 4 -4 414.36 31.30 5 4 -4 426.16 29.90 5 4 -4 435.26 29.50 -5 -4 4 425.86 30.20 -5 -4 4 462.85 31.40 -5 -4 4 469.25 31.10 -5 -4 4 397.26 29.20 -5 -4 4 415.16 29.90 -5 -4 4 465.65 29.90 4 4 -4 11.80 4.60 4 4 -4 5.40 2.80 4 4 -4 5.70 3.30 4 4 -4 9.60 3.60 4 4 -4 4.30 3.80 4 4 -4 4.20 3.50 -4 -4 4 2.30 3.60 -4 -4 4 9.70 3.50 -4 -4 4 6.60 3.60 -4 -4 4 5.20 3.10 -4 -4 4 4.10 4.00 -4 -4 4 7.50 2.50 3 4 -4 433.16 30.00 3 4 -4 456.65 30.10 3 4 -4 431.96 31.00 3 4 -4 443.46 30.20 3 4 -4 410.06 29.00 3 4 -4 456.95 29.50 -3 -4 4 408.66 29.40 -3 -4 4 462.15 29.80 -3 -4 4 436.46 29.90 -3 -4 4 463.35 30.40 -3 -4 4 476.35 29.30 -3 -4 4 414.56 28.90 2 4 -4 604.24 38.50 2 4 -4 582.54 38.70 2 4 -4 554.64 39.50 2 4 -4 531.55 38.70 2 4 -4 580.24 37.80 -2 -4 4 578.84 37.80 -2 -4 4 581.54 38.10 -2 -4 4 604.44 38.20 -2 -4 4 602.74 38.80 -2 -4 4 619.54 38.10 -2 -4 4 568.74 38.70 -2 -4 4 595.84 38.70 -1 -4 4 174.38 12.70 -1 -4 4 175.58 11.70 -1 -4 4 165.98 12.00 -1 -4 4 154.98 11.50 -1 -4 4 174.58 12.40 -1 -4 4 178.88 11.80 -1 -4 4 174.88 12.00 -1 -4 4 148.59 12.60 -1 -4 4 165.88 12.80 0 4 -4 49.40 4.80 0 4 -4 54.29 6.20 0 4 -4 48.00 5.90 0 4 -4 42.90 4.30 0 4 -4 43.60 5.90 0 4 -4 46.10 4.10 0 -4 4 35.60 5.10 0 -4 4 34.00 4.90 0 -4 4 32.30 4.50 0 -4 4 35.30 5.00 0 -4 4 37.60 5.00 0 -4 4 38.80 4.60 0 -4 4 38.70 4.30 -1 4 -4 190.78 12.30 -1 4 -4 158.18 12.10 -1 4 -4 166.38 11.20 -1 4 -4 153.88 12.00 -1 4 -4 167.48 10.80 1 -4 4 153.18 10.70 1 -4 4 134.59 10.30 1 -4 4 141.39 11.80 1 -4 4 140.99 10.30 1 -4 4 164.28 11.60 1 -4 4 155.88 11.80 1 -4 4 154.98 10.90 1 -4 4 146.49 11.40 1 -4 4 138.79 12.30 -2 4 -4 31.50 4.30 -2 4 -4 32.80 4.10 -2 4 -4 32.10 4.30 -2 4 -4 29.40 3.50 -2 4 -4 30.80 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35.00 10.00 9 3 -5 27.00 6.80 -9 -3 5 28.00 9.10 -9 -3 5 26.10 8.10 -9 -3 5 25.50 8.40 -9 -3 5 33.10 9.50 8 3 -5 21.10 6.90 8 3 -5 15.70 5.50 8 3 -5 17.70 8.80 8 3 -5 23.10 5.20 8 3 -5 19.00 7.90 -8 -3 5 19.70 7.70 -8 -3 5 20.00 6.10 -8 -3 5 24.40 7.90 7 3 -5 8.20 5.50 7 3 -5 12.50 6.00 7 3 -5 10.00 7.40 7 3 -5 10.20 4.50 -7 -3 5 15.70 6.00 -7 -3 5 9.20 5.00 -7 -3 5 10.30 5.70 6 3 -5 198.48 18.00 6 3 -5 219.78 15.90 6 3 -5 207.38 18.00 6 3 -5 188.58 17.50 6 3 -5 190.68 15.60 -6 -3 5 228.98 17.00 -6 -3 5 195.88 17.30 -6 -3 5 198.18 15.50 -6 -3 5 207.68 17.90 -6 -3 5 169.48 15.10 -6 -3 5 203.98 15.80 5 3 -5 121.09 10.90 5 3 -5 93.49 9.70 5 3 -5 117.89 12.10 5 3 -5 119.79 12.30 5 3 -5 138.69 12.80 5 3 -5 102.79 10.00 -5 -3 5 137.29 11.50 -5 -3 5 127.19 12.00 -5 -3 5 113.39 10.50 -5 -3 5 106.79 9.70 -5 -3 5 109.59 11.70 -5 -3 5 127.89 10.40 4 3 -5 210.58 15.70 4 3 -5 179.88 16.50 4 3 -5 208.48 16.50 4 3 -5 195.98 14.50 4 3 -5 193.38 16.30 -4 -3 5 227.98 16.50 -4 -3 5 212.38 15.40 -4 -3 5 205.18 15.80 -4 -3 5 167.38 14.40 -4 -3 5 200.98 14.60 -4 -3 5 185.68 15.10 3 3 -5 366.26 27.00 3 3 -5 363.46 25.20 3 3 -5 402.06 26.20 3 3 -5 363.46 26.10 3 3 -5 361.76 25.20 3 3 -5 381.06 26.50 -3 -3 5 390.56 26.20 -3 -3 5 380.06 25.60 -3 -3 5 435.06 25.70 -3 -3 5 350.46 25.10 -3 -3 5 315.97 24.90 -3 -3 5 362.36 26.20 -3 -3 5 394.76 25.70 2 3 -5 342.67 24.70 2 3 -5 347.07 23.70 2 3 -5 344.87 24.10 2 3 -5 368.76 24.50 2 3 -5 331.77 25.20 -2 -3 5 362.86 24.10 -2 -3 5 357.46 24.40 -2 -3 5 347.17 23.70 -2 -3 5 356.16 24.20 -2 -3 5 369.56 23.80 -2 -3 5 338.37 24.20 -2 -3 5 345.67 23.50 1 3 -5 1594.24 101.99 1 3 -5 1673.63 100.99 1 3 -5 1615.24 101.69 1 3 -5 1595.34 100.59 1 3 -5 1646.34 100.79 -1 -3 5 1630.34 100.69 -1 -3 5 1515.95 101.09 -1 -3 5 1614.84 100.99 -1 -3 5 1462.85 100.19 -1 -3 5 1565.64 100.79 -1 -3 5 1511.65 100.69 0 3 -5 5.20 3.20 0 3 -5 7.50 2.60 0 3 -5 5.40 2.40 0 3 -5 6.60 2.40 0 3 -5 7.50 3.60 0 3 -5 2.10 2.00 0 3 -5 11.20 3.50 0 -3 5 6.60 2.70 0 -3 5 4.80 2.10 0 -3 5 5.90 2.50 0 -3 5 11.20 3.20 0 -3 5 5.70 2.10 0 -3 5 5.40 2.40 0 -3 5 9.80 2.50 -1 3 -5 160.38 11.80 -1 3 -5 124.79 12.00 -1 3 -5 141.59 12.30 -1 3 -5 146.59 11.60 -1 3 -5 147.49 11.40 -1 3 -5 151.98 10.90 1 -3 5 137.39 11.00 1 -3 5 145.19 11.30 1 -3 5 149.29 11.40 1 -3 5 157.18 11.40 1 -3 5 163.78 10.90 1 -3 5 159.68 10.20 1 -3 5 151.48 10.10 1 -3 5 150.58 11.90 -2 3 -5 57.79 6.50 -2 3 -5 54.49 6.90 -2 3 -5 66.19 6.90 -2 3 -5 75.59 7.50 -2 3 -5 69.09 6.10 2 -3 5 70.69 6.80 2 -3 5 62.39 7.20 2 -3 5 71.69 5.80 2 -3 5 73.39 4.70 2 -3 5 57.69 6.40 2 -3 5 56.29 5.90 2 -3 5 66.79 7.00 2 -3 5 59.89 7.30 -3 3 -5 446.26 28.40 -3 3 -5 404.46 29.10 -3 3 -5 444.36 28.60 -3 3 -5 436.76 28.60 -3 3 -5 395.56 28.80 3 -3 5 382.76 28.30 3 -3 5 434.46 28.20 3 -3 5 424.46 28.80 3 -3 5 421.46 26.80 3 -3 5 431.96 27.90 3 -3 5 414.46 26.80 3 -3 5 405.26 29.10 3 -3 5 411.16 29.40 3 -3 5 446.26 28.90 -4 3 -5 148.69 13.10 -4 3 -5 166.08 10.60 -4 3 -5 148.79 12.90 -4 3 -5 175.88 12.40 -4 3 -5 175.88 12.50 -4 3 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1.30 4.90 -9 3 -5 0.50 5.20 9 -3 5 4.30 4.60 9 -3 5 8.60 5.70 9 -3 5 4.10 5.30 9 -3 5 5.80 7.00 -10 3 -5 23.90 8.10 -10 3 -5 21.80 7.30 -10 3 -5 14.40 6.70 10 -3 5 35.40 10.10 10 -3 5 16.20 7.00 10 -3 5 30.00 7.40 10 -3 5 19.10 6.10 -11 3 -5 5.40 6.80 -11 3 -5 15.60 7.80 11 -3 5 20.20 9.40 11 -3 5 6.70 5.80 11 -3 5 14.70 7.00 10 2 -5 7.30 5.60 10 2 -5 16.00 10.30 10 2 -5 2.90 6.80 -10 -2 5 5.60 7.10 -10 -2 5 10.40 7.00 -10 -2 5 -8.60 7.40 -10 -2 5 9.40 6.20 9 2 -5 4.30 6.40 9 2 -5 7.60 5.20 9 2 -5 0.30 5.20 9 2 -5 3.40 8.40 -9 -2 5 7.50 7.90 -9 -2 5 -8.70 5.40 -9 -2 5 4.30 5.70 -9 -2 5 0.60 7.20 8 2 -5 4.40 8.80 8 2 -5 4.00 3.70 8 2 -5 5.20 4.40 8 2 -5 1.70 7.50 8 2 -5 -0.30 5.40 -8 -2 5 2.90 6.00 -8 -2 5 1.20 5.40 -8 -2 5 3.90 5.00 7 2 -5 9.60 7.10 7 2 -5 1.50 3.20 7 2 -5 3.60 3.80 7 2 -5 3.90 5.10 7 2 -5 2.30 5.00 -7 -2 5 -1.40 5.60 -7 -2 5 1.20 4.70 -7 -2 5 2.40 3.90 -7 -2 5 -2.00 4.20 -7 -2 5 6.10 4.00 6 2 -5 98.69 11.40 6 2 -5 100.59 12.30 6 2 -5 84.69 9.30 6 2 -5 85.99 11.50 6 2 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7.20 5.10 -6 6 -8 10.30 6.70 6 -6 8 11.40 7.30 6 -6 8 6.60 4.80 6 -6 8 6.50 5.70 -7 6 -8 1.60 4.60 -7 6 -8 0.70 5.70 -7 6 -8 -0.10 6.50 -7 6 -8 -0.80 3.80 7 -6 8 -1.50 5.80 7 -6 8 5.60 6.40 7 5 -8 1.60 7.40 7 5 -8 -1.00 8.10 7 5 -8 -7.50 2.70 -7 -5 8 2.20 6.20 -7 -5 8 3.90 6.90 -7 -5 8 4.60 7.30 6 5 -8 5.70 4.60 6 5 -8 -1.20 7.10 6 5 -8 4.10 7.30 6 5 -8 5.60 6.40 -6 -5 8 3.30 6.50 -6 -5 8 -0.50 5.70 -6 -5 8 -0.80 5.50 5 5 -8 11.00 8.00 5 5 -8 7.70 6.00 5 5 -8 3.90 4.30 5 5 -8 12.70 7.50 -5 -5 8 10.30 6.90 -5 -5 8 11.90 6.10 -5 -5 8 17.30 6.00 4 5 -8 18.00 8.00 4 5 -8 9.70 6.00 4 5 -8 9.60 4.80 4 5 -8 19.70 7.10 -4 -5 8 15.10 6.50 -4 -5 8 9.90 5.00 -4 -5 8 13.90 4.60 -4 -5 8 12.50 6.00 3 5 -8 -3.30 4.20 3 5 -8 2.60 4.00 3 5 -8 -1.40 5.90 3 5 -8 3.90 5.50 -3 -5 8 6.60 4.40 -3 -5 8 4.70 4.50 -3 -5 8 3.60 5.40 -3 -5 8 2.90 3.70 2 5 -8 24.60 5.90 2 5 -8 27.70 5.60 2 5 -8 26.00 6.40 2 5 -8 31.00 8.60 -2 -5 8 34.60 6.90 -2 -5 8 21.00 5.30 -2 -5 8 34.30 5.90 -2 -5 8 29.20 4.70 1 5 -8 22.80 5.50 1 5 -8 22.60 5.40 1 5 -8 15.30 7.30 -1 -5 8 31.40 6.40 -1 -5 8 26.90 5.10 -1 -5 8 17.50 5.90 -1 -5 8 27.90 4.20 0 5 -8 54.19 7.80 0 5 -8 75.59 10.80 0 5 -8 48.90 6.60 0 5 -8 60.19 8.40 0 -5 8 51.89 6.80 0 -5 8 67.69 8.40 0 -5 8 61.29 7.40 0 -5 8 55.09 5.70 0 -5 8 47.70 6.90 -1 5 -8 271.47 19.80 -1 5 -8 250.57 19.80 -1 5 -8 253.47 20.10 -1 5 -8 248.98 18.50 -1 5 -8 249.97 21.70 1 -5 8 224.58 17.90 1 -5 8 238.78 19.00 1 -5 8 259.17 19.00 1 -5 8 277.97 16.90 1 -5 8 251.07 16.50 1 -5 8 244.58 18.80 1 -5 8 247.88 19.00 -2 5 -8 18.40 5.60 -2 5 -8 8.90 4.80 -2 5 -8 18.80 4.50 -2 5 -8 17.60 6.70 -2 5 -8 6.20 5.70 2 -5 8 10.70 5.10 2 -5 8 18.00 4.00 2 -5 8 15.50 5.00 2 -5 8 19.50 5.20 -3 5 -8 11.70 6.60 -3 5 -8 32.60 5.30 -3 5 -8 24.70 6.30 -3 5 -8 21.20 7.20 -3 5 -8 24.20 6.10 3 -5 8 40.90 5.60 3 -5 8 44.40 6.50 3 -5 8 38.80 7.00 3 -5 8 24.40 5.70 -4 5 -8 19.10 5.90 -4 5 -8 25.20 6.40 -4 5 -8 19.60 4.90 -4 5 -8 20.80 6.40 4 -5 8 24.50 5.80 4 -5 8 20.90 4.20 -5 5 -8 6.30 5.70 -5 5 -8 12.10 5.70 -5 5 -8 9.10 4.70 -5 5 -8 7.70 5.60 5 -5 8 18.20 4.10 5 -5 8 15.30 6.80 5 -5 8 13.10 5.30 5 -5 8 9.60 5.30 -6 5 -8 148.59 13.80 -6 5 -8 156.28 13.50 -6 5 -8 127.89 14.70 -6 5 -8 139.99 13.50 6 -5 8 144.09 15.40 6 -5 8 122.29 12.70 6 -5 8 130.29 11.80 6 -5 8 143.99 14.30 -7 5 -8 23.20 6.60 -7 5 -8 11.00 6.40 -7 5 -8 22.50 5.40 -7 5 -8 19.70 6.80 7 -5 8 22.70 5.00 7 -5 8 28.10 8.30 7 -5 8 24.60 6.80 7 -5 8 24.00 5.10 -8 5 -8 13.40 6.60 -8 5 -8 5.20 6.00 -8 5 -8 4.10 6.40 8 -5 8 1.80 5.90 8 -5 8 11.00 8.00 8 4 -8 11.60 10.80 8 4 -8 0.40 7.30 8 4 -8 10.10 9.50 -8 -4 8 6.80 6.60 -8 -4 8 -0.70 7.60 7 4 -8 8.60 4.90 7 4 -8 10.80 8.30 7 4 -8 0.00 6.60 7 4 -8 7.30 8.20 -7 -4 8 5.70 7.50 -7 -4 8 16.60 7.20 -7 -4 8 7.60 6.50 6 4 -8 9.70 7.50 6 4 -8 4.50 6.70 6 4 -8 14.50 5.10 6 4 -8 12.00 7.00 -6 -4 8 11.10 6.50 -6 -4 8 1.90 5.70 -6 -4 8 8.70 6.10 5 4 -8 9.90 6.80 5 4 -8 7.60 7.20 5 4 -8 7.60 5.90 -5 -4 8 8.80 6.50 -5 -4 8 8.10 5.70 -5 -4 8 -0.50 5.00 4 4 -8 7.60 4.30 4 4 -8 10.70 6.40 4 4 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3 -10 5.30 6.80 0 3 -10 9.70 3.20 0 3 -10 4.10 4.90 0 -3 10 8.50 4.30 0 -3 10 14.00 3.50 0 -3 10 6.90 4.40 0 -3 10 10.20 4.80 0 -3 10 9.20 2.60 -1 3 -10 19.20 5.60 -1 3 -10 20.50 6.60 -1 3 -10 13.10 7.90 -1 3 -10 14.50 5.80 1 -3 10 35.10 5.00 1 -3 10 21.70 5.20 1 -3 10 28.50 5.70 1 -3 10 30.40 5.90 -2 3 -10 2.80 5.30 -2 3 -10 14.00 7.90 -2 3 -10 13.10 7.10 -2 3 -10 18.60 5.50 -2 3 -10 11.40 4.90 2 -3 10 19.00 4.50 2 -3 10 20.90 5.10 2 -3 10 14.80 4.60 -3 3 -10 26.90 7.20 -3 3 -10 26.20 6.70 -3 3 -10 26.00 8.50 -3 3 -10 28.00 6.00 -3 3 -10 28.50 7.50 3 -3 10 27.40 5.60 3 -3 10 25.70 5.70 3 -3 10 34.10 5.70 -4 3 -10 28.30 6.30 -4 3 -10 31.50 10.60 -4 3 -10 17.60 6.60 4 -3 10 22.40 4.90 4 -3 10 20.40 5.50 4 -3 10 18.80 5.50 -5 3 -10 42.90 7.50 -5 3 -10 53.89 8.20 5 -3 10 43.40 6.40 5 -3 10 27.60 6.50 5 -3 10 41.50 7.40 -6 3 -10 10.00 5.40 -6 3 -10 7.40 7.80 -6 3 -10 1.20 4.90 -6 3 -10 7.50 6.20 6 -3 10 1.10 4.70 6 -3 10 4.10 4.30 6 -3 10 3.90 5.80 -7 3 -10 17.30 7.50 -7 3 -10 11.50 6.30 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-13 7.40 9.80 -1 3 -13 -4.40 7.20 1 -3 13 1.90 5.40 1 -3 13 3.20 4.00 1 -3 13 -1.90 4.80 -2 3 -13 38.00 10.90 -2 3 -13 17.70 7.20 2 -3 13 23.70 6.40 2 -3 13 18.20 6.40 2 -3 13 19.90 5.40 -3 3 -13 12.20 7.70 -3 3 -13 8.90 6.50 -3 3 -13 22.40 10.60 3 -3 13 7.80 5.20 3 -3 13 11.60 5.60 3 -3 13 3.60 4.60 2 2 -13 4.00 6.10 2 2 -13 -0.20 9.00 2 2 -13 2.30 7.50 -2 -2 13 -2.60 5.30 -2 -2 13 3.30 6.40 1 2 -13 8.90 9.50 1 2 -13 1.10 6.50 1 2 -13 -8.90 12.60 -1 -2 13 4.20 5.30 -1 -2 13 6.30 6.10 0 2 -13 0.80 6.20 0 2 -13 9.10 9.30 0 2 -13 9.60 9.20 0 2 -13 3.70 5.70 0 -2 13 -3.00 3.40 0 -2 13 3.20 5.50 0 -2 13 -2.20 4.60 -1 2 -13 3.50 9.20 -1 2 -13 11.30 7.10 -1 2 -13 16.70 6.80 -1 2 -13 11.80 9.10 1 -2 13 -0.60 6.10 1 -2 13 9.50 5.80 1 -2 13 15.50 5.80 1 -2 13 8.40 4.40 -2 2 -13 2.10 6.40 -2 2 -13 -1.60 9.00 2 -2 13 -0.30 4.20 2 -2 13 6.40 4.80 2 -2 13 2.70 5.50 -3 2 -13 -0.20 5.90 -3 2 -13 5.30 9.60 -3 2 -13 -1.40 6.20 3 -2 13 2.30 4.60 3 -2 13 3.60 5.20 -4 2 -13 4.10 6.20 -4 2 -13 -1.90 6.50 -4 2 -13 -8.10 8.10 4 -2 13 -0.40 4.70 4 -2 13 0.40 4.80 2 1 -13 3.50 7.20 2 1 -13 4.50 6.60 2 1 -13 -2.30 8.90 -2 -1 13 -4.90 4.90 -2 -1 13 6.90 6.50 1 1 -13 4.80 6.50 1 1 -13 1.00 8.80 1 1 -13 19.40 11.60 1 1 -13 13.80 6.10 -1 -1 13 12.60 6.70 -1 -1 13 17.30 6.70 -1 -1 13 14.80 5.60 0 1 -13 3.70 7.00 0 1 -13 0.00 6.10 0 1 -13 12.60 9.00 0 1 -13 2.30 4.00 0 1 -13 6.80 8.30 0 -1 13 6.50 5.70 0 -1 13 -2.70 5.60 0 -1 13 0.10 3.70 0 -1 13 -4.50 4.20 -1 1 -13 27.50 8.10 -1 1 -13 53.49 11.10 -1 1 -13 47.50 8.30 1 -1 13 22.70 6.90 1 -1 13 33.90 5.90 1 -1 13 32.40 6.40 1 -1 13 21.20 8.50 -2 1 -13 27.70 7.80 -2 1 -13 31.80 11.60 -2 1 -13 27.30 14.10 2 -1 13 35.70 6.40 2 -1 13 30.90 6.00 2 -1 13 31.90 6.90 -3 1 -13 -13.30 6.80 -3 1 -13 -1.40 8.00 -3 1 -13 5.00 5.60 -3 1 -13 -9.50 5.20 3 -1 13 2.00 4.50 3 -1 13 2.30 4.70 -4 1 -13 -11.70 9.00 -4 1 -13 -5.90 5.40 -4 1 -13 2.00 7.70 -4 1 -13 9.10 6.40 4 -1 13 7.70 5.80 4 -1 13 -0.40 6.30 4 -1 13 -0.70 4.70 -5 1 -13 4.90 7.80 -5 1 -13 5.30 6.50 -5 1 -13 4.00 8.30 5 -1 13 7.30 5.30 5 -1 13 7.20 5.30 2 0 -13 -9.30 8.50 2 0 -13 -1.00 8.40 2 0 -13 -2.60 6.70 2 0 -13 1.30 6.90 -2 0 13 -3.90 5.80 -2 0 13 -7.00 6.00 -2 0 13 -1.80 4.70 1 0 -13 3.30 9.00 1 0 -13 -4.00 7.90 1 0 -13 16.70 6.70 1 0 -13 -4.00 5.60 1 0 -13 1.80 6.30 -1 0 13 -1.60 3.60 -1 0 13 7.00 4.90 -1 0 13 -3.30 5.40 -1 0 13 1.20 4.10 -1 0 13 1.30 6.20 0 0 -13 1.50 6.40 0 0 -13 8.30 7.60 0 0 -13 23.40 10.20 0 0 -13 10.70 9.00 0 0 -13 7.00 6.60 0 0 13 16.30 6.80 0 0 13 13.80 4.10 0 0 13 13.10 5.40 0 0 13 11.40 4.50 -1 0 -13 0.30 5.90 -1 0 -13 7.90 12.80 -1 0 -13 3.10 7.60 1 0 13 4.20 4.40 1 0 13 1.10 5.30 1 0 13 3.30 4.30 1 0 13 -0.50 6.00 -2 0 -13 4.80 7.90 -2 0 -13 7.70 6.10 -2 0 -13 -5.70 8.40 2 0 13 10.90 4.80 2 0 13 0.20 5.30 2 0 13 4.30 4.30 2 0 13 13.30 5.90 -3 0 -13 1.80 5.50 -3 0 -13 -13.40 9.20 -3 0 -13 0.90 7.40 -3 0 -13 -2.50 5.50 3 0 13 -2.60 4.50 3 0 13 1.60 4.70 3 0 13 -5.20 4.30 -4 0 -13 4.30 5.50 -4 0 -13 9.30 7.50 -4 0 -13 4.20 6.20 -4 0 -13 3.00 7.40 4 0 13 5.70 5.10 4 0 13 8.60 5.00 4 0 13 4.30 4.70 -5 0 -13 23.70 6.80 -5 0 -13 20.10 7.20 -5 0 -13 14.70 12.40 -5 0 -13 25.30 10.40 5 0 13 25.70 7.10 5 0 13 21.80 6.40 5 0 13 25.00 6.40 6 0 13 4.40 5.80 2 -1 -13 4.00 8.00 2 -1 -13 6.10 5.90 2 -1 -13 5.50 8.20 2 -1 -13 4.30 8.20 2 -1 -13 0.60 6.70 -2 1 13 12.20 8.10 -2 1 13 5.60 4.00 -2 1 13 1.40 7.10 -2 1 13 8.30 5.60 1 -1 -13 20.00 9.10 1 -1 -13 9.80 6.50 1 -1 -13 -2.60 6.20 1 -1 -13 4.50 7.50 1 -1 -13 0.60 6.90 -1 1 13 -0.10 4.90 -1 1 13 2.90 5.60 -1 1 13 6.80 5.00 -1 1 13 5.80 6.70 -1 1 13 0.90 4.10 0 -1 -13 45.10 11.50 0 -1 -13 39.60 7.40 0 -1 -13 20.10 7.90 0 -1 -13 20.40 10.90 0 -1 -13 28.70 8.80 0 1 13 24.80 5.80 0 1 13 14.40 5.30 0 1 13 29.20 7.40 0 1 13 21.90 5.20 -1 -1 -13 45.30 6.30 -1 -1 -13 46.30 11.30 -1 -1 -13 56.99 16.30 -1 -1 -13 43.80 9.30 1 1 13 32.40 8.10 1 1 13 32.40 6.60 1 1 13 36.70 6.20 1 1 13 28.50 7.60 -2 -1 -13 -13.00 9.40 -2 -1 -13 8.60 6.60 -2 -1 -13 -2.00 7.80 2 1 13 1.60 5.50 2 1 13 -0.40 3.80 2 1 13 -0.50 4.50 2 1 13 -1.70 4.90 -3 -1 -13 -2.90 4.90 -3 -1 -13 5.80 5.90 -3 -1 -13 -4.30 6.60 -3 -1 -13 -22.60 7.90 3 1 13 -2.40 4.60 3 1 13 1.00 5.10 3 1 13 -3.90 4.80 -4 -1 -13 7.40 6.30 -4 -1 -13 19.10 8.10 -4 -1 -13 2.50 7.30 -4 -1 -13 -2.60 5.40 4 1 13 8.50 5.40 4 1 13 6.50 5.40 4 1 13 -2.40 4.90 -5 -1 -13 0.80 9.20 -5 -1 -13 -3.30 5.10 -5 -1 -13 4.20 6.00 5 1 13 -3.10 4.90 5 1 13 -0.30 4.50 5 1 13 -2.20 4.80 -6 -1 -13 9.20 7.90 -6 -1 -13 17.20 8.50 -6 -1 -13 18.30 6.70 6 1 13 11.80 5.70 6 1 13 14.50 6.30 6 1 13 13.00 6.30 2 -2 -13 -0.70 8.30 2 -2 -13 2.20 7.60 2 -2 -13 2.40 6.70 2 -2 -13 6.70 9.00 2 -2 -13 -1.50 7.50 -2 2 13 5.50 5.80 -2 2 13 11.70 5.70 -2 2 13 8.10 7.50 -2 2 13 5.20 4.40 1 -2 -13 -1.30 8.30 1 -2 -13 1.40 6.90 1 -2 -13 7.20 6.80 1 -2 -13 12.80 8.70 -1 2 13 4.80 7.00 -1 2 13 3.00 4.10 -1 2 13 6.80 5.20 -1 2 13 0.70 4.90 0 -2 -13 2.10 7.10 0 -2 -13 9.10 12.20 0 -2 -13 6.40 6.20 0 -2 -13 8.20 8.30 0 2 13 2.90 7.50 0 2 13 3.40 5.10 0 2 13 3.90 4.80 -1 -2 -13 0.60 5.80 -1 -2 -13 2.10 5.50 -1 -2 -13 7.40 10.60 -1 -2 -13 5.40 5.30 1 2 13 1.20 5.30 1 2 13 4.50 5.00 1 2 13 11.20 5.00 1 2 13 6.20 6.20 -2 -2 -13 2.60 5.40 -2 -2 -13 7.10 5.00 -2 -2 -13 -14.50 9.40 -2 -2 -13 0.40 5.60 2 2 13 -1.50 5.50 2 2 13 -1.90 3.50 2 2 13 4.20 4.80 2 2 13 1.30 4.80 -3 -2 -13 1.80 3.80 -3 -2 -13 6.60 4.20 -3 -2 -13 5.00 6.50 -3 -2 -13 1.60 5.10 -3 -2 -13 9.60 9.70 3 2 13 0.20 5.40 3 2 13 -3.00 4.50 3 2 13 4.70 5.50 -4 -2 -13 15.50 6.10 -4 -2 -13 13.90 12.70 -4 -2 -13 5.40 5.40 4 2 13 9.50 6.00 4 2 13 14.70 5.90 4 2 13 9.20 4.10 -5 -2 -13 53.69 9.40 -5 -2 -13 28.10 8.10 -5 -2 -13 30.30 6.90 -5 -2 -13 55.89 13.90 5 2 13 31.00 7.20 5 2 13 27.40 6.60 5 2 13 35.40 7.10 -6 -2 -13 16.00 17.80 -6 -2 -13 9.70 5.70 -6 -2 -13 3.20 7.10 -6 -2 -13 11.30 7.10 6 2 13 -0.10 5.40 6 2 13 11.10 5.90 6 2 13 13.10 6.50 2 -3 -13 4.60 7.20 2 -3 -13 3.30 8.40 2 -3 -13 1.70 7.60 -2 3 13 9.50 6.60 -2 3 13 2.70 5.00 -2 3 13 -4.20 4.20 -2 3 13 -9.80 6.60 1 -3 -13 12.90 7.20 1 -3 -13 10.60 7.90 1 -3 -13 8.10 8.30 -1 3 13 3.50 4.80 -1 3 13 13.40 9.40 -1 3 13 6.50 7.20 -1 3 13 7.50 4.80 0 -3 -13 22.40 8.70 0 -3 -13 27.60 8.60 0 -3 -13 17.30 9.70 0 -3 -13 33.90 7.40 0 3 13 44.00 8.10 0 3 13 38.00 7.00 0 3 13 27.40 7.40 0 3 13 36.60 6.00 0 3 13 38.10 7.20 -1 -3 -13 11.40 9.90 -1 -3 -13 2.60 7.40 -1 -3 -13 8.60 9.60 -1 -3 -13 7.30 5.30 -1 -3 -13 5.60 11.50 1 3 13 2.40 6.20 1 3 13 2.10 4.90 1 3 13 7.20 5.10 1 3 13 4.20 6.30 1 3 13 5.60 4.10 -2 -3 -13 3.60 7.70 -2 -3 -13 -4.60 5.30 -2 -3 -13 -3.60 4.20 -2 -3 -13 2.40 10.40 -2 -3 -13 23.00 10.80 2 3 13 -4.70 4.90 2 3 13 -4.00 4.90 2 3 13 4.90 6.40 2 3 13 2.10 3.80 -3 -3 -13 13.50 7.40 -3 -3 -13 12.80 5.90 -3 -3 -13 14.30 4.40 -3 -3 -13 26.10 15.40 -3 -3 -13 12.00 8.30 -3 -3 -13 12.40 5.50 3 3 13 13.00 6.30 3 3 13 9.70 5.90 3 3 13 7.10 6.30 -4 -3 -13 4.50 6.10 -4 -3 -13 2.50 5.10 -4 -3 -13 9.50 15.10 -4 -3 -13 1.20 4.60 -4 -3 -13 -1.10 5.30 -4 -3 -13 -4.80 6.60 4 3 13 -1.70 5.30 4 3 13 -5.80 3.00 4 3 13 3.30 5.60 -5 -3 -13 24.50 7.60 -5 -3 -13 41.10 7.20 -5 -3 -13 33.40 4.60 -5 -3 -13 51.99 9.50 5 3 13 47.90 8.20 5 3 13 38.50 10.50 -6 -3 -13 -8.20 6.40 6 3 13 -3.90 5.60 1 -4 -13 18.00 6.90 1 -4 -13 5.70 8.10 1 -4 -13 -8.90 7.10 -1 4 13 4.40 5.20 -1 4 13 10.50 8.10 -1 4 13 -7.90 4.80 -1 4 13 -0.60 4.20 0 -4 -13 16.20 8.10 0 -4 -13 0.90 5.80 0 -4 -13 7.30 6.10 0 4 13 9.80 6.00 0 4 13 17.20 9.10 0 4 13 15.50 6.30 0 4 13 7.70 5.50 0 4 13 3.70 4.20 -1 -4 -13 -1.30 4.90 -1 -4 -13 0.20 7.60 -1 -4 -13 -0.90 6.80 1 4 13 -0.10 6.80 1 4 13 1.50 3.70 1 4 13 3.00 5.60 1 4 13 0.50 5.60 1 4 13 -6.10 6.00 -2 -4 -13 1.20 5.10 -2 -4 -13 -3.50 6.50 -2 -4 -13 7.30 6.90 -2 -4 -13 7.50 6.80 2 4 13 -1.10 6.60 2 4 13 8.10 6.00 2 4 13 8.30 6.40 2 4 13 -3.50 5.60 2 4 13 6.10 3.50 -3 -4 -13 11.50 7.70 -3 -4 -13 28.30 8.30 -3 -4 -13 29.20 5.60 3 4 13 30.90 8.20 3 4 13 21.30 7.70 3 4 13 21.90 7.00 3 4 13 29.40 4.80 3 4 13 38.50 8.30 -4 -4 -13 20.60 4.90 -4 -4 -13 20.80 7.30 -4 -4 -13 7.50 6.50 -4 -4 -13 27.80 8.30 4 4 13 26.50 7.40 4 4 13 17.90 7.30 -5 -4 -13 4.50 4.20 -5 -4 -13 15.10 7.50 -5 -4 -13 1.40 6.10 -5 -4 -13 4.60 4.80 5 4 13 6.50 6.30 5 4 13 2.10 6.10 5 4 13 8.80 4.70 0 -5 -13 8.40 6.10 0 -5 -13 3.60 7.80 0 -5 -13 7.70 6.60 0 5 13 -0.30 4.10 0 5 13 3.80 6.10 0 5 13 2.10 5.30 0 5 13 6.70 7.70 -1 -5 -13 3.60 6.00 -1 -5 -13 -2.50 6.20 -1 -5 -13 2.70 7.00 1 5 13 -2.90 3.40 1 5 13 2.50 8.60 1 5 13 3.30 5.30 1 5 13 6.50 5.90 -2 -5 -13 2.70 5.50 -2 -5 -13 4.10 6.30 -2 -5 -13 5.90 7.70 2 5 13 2.90 3.30 2 5 13 -5.40 5.40 2 5 13 -4.70 6.60 2 5 13 -9.60 5.00 -3 -5 -13 -0.70 5.80 -3 -5 -13 4.80 6.90 -3 -5 -13 -8.60 5.00 3 5 13 -1.00 5.20 3 5 13 -9.10 6.10 3 5 13 1.40 6.50 3 5 13 3.50 3.40 -4 -5 -13 15.50 8.00 -4 -5 -13 15.40 8.10 -4 -5 -13 17.10 4.90 -4 -5 -13 24.60 5.70 4 5 13 14.90 6.70 4 5 13 12.90 7.10 4 5 13 4.20 7.00 -1 -1 -14 8.50 9.00 1 1 14 4.60 4.80 -2 -1 -14 17.40 8.80 -2 -1 -14 3.80 7.50 2 1 14 3.10 4.70 2 1 14 5.00 5.10 2 1 14 3.90 6.30 2 1 14 1.00 5.00 -2 -2 -14 -2.80 8.30 2 2 14 8.80 6.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 99991 loop_ _space_group_symop_operation_xyz 'x, y, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Br1 Br 0.89843(10) 0.40773(9) 1.39508(8) 0.1177(4) Uani 1 1 d . . Br2 Br 0.37309(9) 0.66591(9) 0.22876(8) 0.1145(4) Uani 1 1 d . . S1 S 0.72911(14) 0.33310(13) 0.85489(13) 0.0499(4) Uani 1 1 d . . S2 S 0.53598(13) 0.77115(12) 0.76336(12) 0.0461(3) Uani 1 1 d . . N1 N 0.5568(5) 0.3549(5) 0.8665(5) 0.0500(11) Uani 1 1 d D . N2 N 0.7092(5) 0.7585(5) 0.7457(4) 0.0476(11) Uani 1 1 d D . O1 O 0.7767(5) 0.1930(4) 0.8227(4) 0.0654(11) Uani 1 1 d . . O2 O 0.7792(4) 0.4482(4) 0.7744(4) 0.0619(11) Uani 1 1 d . . O3 O 0.4936(4) 0.6597(4) 0.8518(4) 0.0541(10) Uani 1 1 d . . O4 O 0.4824(4) 0.9118(4) 0.7900(4) 0.0588(10) Uani 1 1 d . . C1 C 0.4744(6) 0.2503(6) 0.9424(6) 0.0529(13) Uani 1 1 d . . H1C H 0.4961 0.2449 1.0276 0.063 Uiso 1 1 calc R U H1D H 0.5042 0.1592 0.9095 0.063 Uiso 1 1 calc R U C2 C 0.3103(6) 0.2856(6) 0.9434(5) 0.0526(13) Uani 1 1 d . . C3 C 0.2790(5) 0.3171(6) 0.8076(5) 0.0557(12) Uani 1 1 d . . H3 H 0.3162 0.4025 0.7671 0.067 Uiso 1 1 calc R U C4 C 0.1429(7) 0.2897(8) 0.7668(8) 0.0757(19) Uani 1 1 d . . H4A H 0.0748 0.2437 0.8273 0.091 Uiso 1 1 calc R U H4B H 0.1001 0.3582 0.7083 0.091 Uiso 1 1 calc R U C5 C 0.2807(5) 0.2066(5) 0.7208(5) 0.0560(12) Uani 1 1 d . . H5 H 0.2923 0.1112 0.7599 0.067 Uiso 1 1 calc R U C6 C 0.3535(6) 0.2208(5) 0.5886(5) 0.0533(12) Uani 1 1 d . . C7 C 0.2768(9) 0.2426(7) 0.4892(7) 0.081(2) Uani 1 1 d . . H7 H 0.1769 0.2554 0.5026 0.097 Uiso 1 1 calc R U C8 C 0.3504(14) 0.2455(10) 0.3676(8) 0.105(3) Uani 1 1 d . . H8 H 0.2985 0.2645 0.3005 0.126 Uiso 1 1 calc R U C9 C 0.4963(14) 0.2213(8) 0.3446(8) 0.096(3) Uani 1 1 d . . H9 H 0.5436 0.2194 0.2632 0.116 Uiso 1 1 calc R U C10 C 0.5709(10) 0.2000(7) 0.4438(7) 0.079(2) Uani 1 1 d . . H10 H 0.6705 0.1835 0.4297 0.095 Uiso 1 1 calc R U C11 C 0.5019(7) 0.2024(6) 0.5650(6) 0.0589(15) Uani 1 1 d . . H11 H 0.5554 0.1917 0.6313 0.071 Uiso 1 1 calc R U C12 C 0.2555(9) 0.4152(7) 1.0132(7) 0.0753(19) Uani 1 1 d . . H12A H 0.1528 0.4312 1.0183 0.113 Uiso 1 1 calc R U H12B H 0.2969 0.4945 0.9696 0.113 Uiso 1 1 calc R U H12C H 0.2818 0.4023 1.0961 0.113 Uiso 1 1 calc R U C13 C 0.2449(7) 0.1593(7) 1.0115(6) 0.0707(18) Uani 1 1 d . . H13A H 0.2723 0.1448 1.0939 0.106 Uiso 1 1 calc R U H13B H 0.2789 0.0778 0.9659 0.106 Uiso 1 1 calc R U H13C H 0.1422 0.1757 1.0177 0.106 Uiso 1 1 calc R U C14 C 0.7758(6) 0.3491(5) 1.0053(6) 0.0485(13) Uani 1 1 d . . C15 C 0.8363(6) 0.2366(6) 1.0728(6) 0.0589(16) Uani 1 1 d . . H15 H 0.8531 0.1488 1.0405 0.071 Uiso 1 1 calc R U C16 C 0.8726(7) 0.2545(7) 1.1897(7) 0.0684(18) Uani 1 1 d . . H16 H 0.9133 0.1786 1.2363 0.082 Uiso 1 1 calc R U C17 C 0.8483(8) 0.3836(7) 1.2355(7) 0.0701(18) Uani 1 1 d . . C18 C 0.7837(8) 0.4971(7) 1.1708(8) 0.075(2) Uani 1 1 d . . H18 H 0.7644 0.5838 1.2051 0.090 Uiso 1 1 calc R U C19 C 0.7485(8) 0.4804(6) 1.0553(7) 0.0687(18) Uani 1 1 d . . H19 H 0.7062 0.5565 1.0099 0.082 Uiso 1 1 calc R U C20 C 0.7810(6) 0.8632(6) 0.6618(6) 0.0556(14) Uani 1 1 d . . H20A H 0.7426 0.9559 0.6875 0.067 Uiso 1 1 calc R U H20B H 0.7602 0.8565 0.5776 0.067 Uiso 1 1 calc R U C21 C 0.9430(6) 0.8452(6) 0.6609(5) 0.0482(13) Uani 1 1 d . . C22 C 0.9761(5) 0.8715(5) 0.7888(4) 0.0471(10) Uani 1 1 d . . H22 H 0.9420 0.9668 0.8130 0.057 Uiso 1 1 calc R U C23 C 1.1160(8) 0.8129(9) 0.8370(7) 0.077(2) Uani 1 1 d . . H23A H 1.1818 0.7479 0.7866 0.093 Uiso 1 1 calc R U H23B H 1.1615 0.8739 0.8820 0.093 Uiso 1 1 calc R U C24 C 0.9750(5) 0.7648(5) 0.8986(5) 0.0505(11) Uani 1 1 d . . H24 H 0.9596 0.6705 0.8802 0.061 Uiso 1 1 calc R U C25 C 0.9114(6) 0.8065(5) 1.0238(5) 0.0555(13) Uani 1 1 d . . C26 C 0.9914(9) 0.7928(8) 1.1234(7) 0.086(2) Uani 1 1 d . . H26 H 1.0882 0.7587 1.1099 0.103 Uiso 1 1 calc R U C27 C 0.9304(14) 0.8285(11) 1.2404(8) 0.110(3) Uani 1 1 d . . H27 H 0.9864 0.8204 1.3049 0.132 Uiso 1 1 calc R U C28 C 0.7893(15) 0.8755(9) 1.2631(7) 0.106(3) Uani 1 1 d . . H28 H 0.7485 0.8959 1.3439 0.127 Uiso 1 1 calc R U C29 C 0.7044(10) 0.8939(7) 1.1678(7) 0.082(2) Uani 1 1 d . . H29 H 0.6078 0.9282 1.1828 0.098 Uiso 1 1 calc R U C30 C 0.7691(8) 0.8589(6) 1.0483(6) 0.0642(16) Uani 1 1 d . . H30 H 0.7140 0.8716 0.9830 0.077 Uiso 1 1 calc R U C31 C 1.0101(8) 0.7028(7) 0.6136(7) 0.0711(18) Uani 1 1 d . . H31A H 1.1124 0.7022 0.5956 0.107 Uiso 1 1 calc R U H31B H 0.9723 0.6874 0.5389 0.107 Uiso 1 1 calc R U H31C H 0.9874 0.6299 0.6767 0.107 Uiso 1 1 calc R U C32 C 0.9998(8) 0.9641(7) 0.5698(6) 0.0694(18) Uani 1 1 d . . H32A H 0.9473 1.0521 0.5925 0.104 Uiso 1 1 calc R U H32B H 0.9873 0.9477 0.4861 0.104 Uiso 1 1 calc R U H32C H 1.0999 0.9665 0.5743 0.104 Uiso 1 1 calc R U C33 C 0.4862(6) 0.7404(5) 0.6175(5) 0.0447(13) Uani 1 1 d . . C34 C 0.4261(7) 0.8501(6) 0.5453(6) 0.0558(15) Uani 1 1 d . . H34 H 0.4083 0.9395 0.5745 0.067 Uiso 1 1 calc R U C35 C 0.3924(7) 0.8272(7) 0.4298(7) 0.0655(17) Uani 1 1 d . . H35 H 0.3520 0.9009 0.3806 0.079 Uiso 1 1 calc R U C36 C 0.4186(7) 0.6960(7) 0.3881(7) 0.0654(17) Uani 1 1 d . . C37 C 0.4757(9) 0.5848(7) 0.4604(8) 0.079(2) Uani 1 1 d . . H37 H 0.4899 0.4951 0.4321 0.095 Uiso 1 1 calc R U C38 C 0.5114(8) 0.6078(6) 0.5750(7) 0.0664(18) Uani 1 1 d . . H38 H 0.5525 0.5340 0.6237 0.080 Uiso 1 1 calc R U H2A H 0.740(6) 0.680(4) 0.728(5) 0.057(18) Uiso 1 1 d D . H1A H 0.525(5) 0.440(3) 0.866(5) 0.048(15) Uiso 1 1 d D . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.1340(9) 0.1295(8) 0.1059(7) -0.0019(5) -0.0691(6) -0.0212(6) Br2 0.1340(8) 0.1237(7) 0.1006(6) -0.0382(5) -0.0682(6) 0.0103(6) S1 0.0388(8) 0.0433(7) 0.0645(9) -0.0012(6) 0.0007(6) -0.0028(5) S2 0.0422(8) 0.0416(6) 0.0545(8) -0.0036(6) -0.0079(6) -0.0035(5) N1 0.038(3) 0.049(3) 0.064(3) 0.001(2) -0.006(2) -0.011(2) N2 0.044(3) 0.048(3) 0.051(3) 0.002(2) -0.009(2) -0.005(2) O1 0.062(3) 0.045(2) 0.085(3) -0.0091(19) 0.000(2) 0.0020(18) O2 0.050(3) 0.054(2) 0.074(3) 0.0095(18) 0.005(2) -0.0042(18) O3 0.047(2) 0.051(2) 0.061(2) 0.0067(17) 0.0009(18) -0.0095(16) O4 0.063(3) 0.044(2) 0.068(2) -0.0122(17) -0.007(2) 0.0016(17) C1 0.054(3) 0.050(3) 0.056(3) 0.003(2) -0.011(3) -0.014(2) C2 0.043(3) 0.062(3) 0.052(3) -0.009(2) 0.003(2) -0.012(2) C3 0.040(3) 0.057(3) 0.069(3) -0.006(2) -0.006(2) -0.004(2) C4 0.042(4) 0.100(5) 0.085(5) -0.015(4) -0.013(3) 0.003(3) C5 0.051(3) 0.055(3) 0.063(3) -0.005(2) -0.009(2) -0.006(2) C6 0.060(3) 0.051(3) 0.048(3) -0.003(2) -0.009(2) -0.002(2) C7 0.092(5) 0.090(5) 0.067(4) 0.006(3) -0.030(4) -0.019(4) C8 0.166(11) 0.102(6) 0.057(5) 0.000(4) -0.039(6) -0.026(6) C9 0.146(9) 0.073(5) 0.067(5) -0.010(4) 0.009(5) -0.022(5) C10 0.098(6) 0.068(4) 0.065(5) -0.010(3) 0.015(4) -0.016(4) C11 0.055(4) 0.057(3) 0.060(4) 0.000(3) 0.002(3) -0.003(2) C12 0.077(5) 0.078(4) 0.068(4) -0.018(3) 0.010(4) -0.010(3) C13 0.062(4) 0.081(4) 0.069(4) -0.004(3) 0.004(3) -0.024(3) C14 0.031(3) 0.039(3) 0.074(4) 0.003(2) -0.005(3) -0.005(2) C15 0.044(3) 0.048(3) 0.080(5) 0.004(3) -0.002(3) -0.001(2) C16 0.057(4) 0.067(4) 0.078(5) 0.014(3) -0.021(4) 0.005(3) C17 0.067(5) 0.075(4) 0.074(5) 0.007(3) -0.031(4) -0.016(3) C18 0.084(5) 0.054(3) 0.094(5) -0.007(3) -0.028(4) -0.009(3) C19 0.083(5) 0.049(3) 0.080(4) 0.003(3) -0.033(4) -0.007(3) C20 0.052(4) 0.063(3) 0.055(3) 0.007(3) -0.013(3) -0.019(3) C21 0.046(3) 0.055(3) 0.044(3) -0.006(2) -0.002(2) -0.009(2) C22 0.041(2) 0.053(3) 0.048(3) -0.004(2) -0.0061(19) -0.009(2) C23 0.043(4) 0.119(6) 0.073(4) -0.006(4) -0.014(3) -0.014(3) C24 0.044(3) 0.056(3) 0.052(3) -0.002(2) -0.011(2) -0.005(2) C25 0.064(3) 0.055(3) 0.050(3) -0.006(2) -0.013(2) -0.008(3) C26 0.095(5) 0.104(5) 0.065(4) -0.011(4) -0.035(4) -0.005(4) C27 0.152(10) 0.127(7) 0.062(5) -0.012(5) -0.048(6) -0.015(7) C28 0.185(12) 0.094(6) 0.040(4) -0.016(4) -0.005(5) -0.024(6) C29 0.107(7) 0.063(4) 0.067(5) -0.008(3) 0.013(4) -0.011(4) C30 0.086(5) 0.059(3) 0.049(3) -0.007(2) -0.007(3) -0.011(3) C31 0.073(4) 0.071(4) 0.067(4) -0.020(3) 0.012(3) -0.014(3) C32 0.061(4) 0.080(4) 0.066(4) 0.009(3) 0.000(3) -0.026(3) C33 0.037(3) 0.044(3) 0.055(3) -0.001(2) -0.008(2) -0.010(2) C34 0.055(4) 0.043(3) 0.069(4) -0.006(3) -0.015(3) 0.003(2) C35 0.062(4) 0.063(4) 0.071(4) 0.003(3) -0.019(3) 0.003(3) C36 0.053(4) 0.071(4) 0.077(4) -0.020(3) -0.021(3) -0.004(3) C37 0.108(6) 0.053(3) 0.087(5) -0.018(3) -0.044(4) -0.001(3) C38 0.082(5) 0.039(3) 0.082(5) -0.007(3) -0.030(4) 0.006(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 S1 O2 119.7(3) O1 S1 N1 108.0(3) O2 S1 N1 106.3(2) O1 S1 C14 107.2(3) O2 S1 C14 107.6(3) N1 S1 C14 107.4(3) O4 S2 O3 118.7(3) O4 S2 N2 108.0(3) O3 S2 N2 107.0(2) O4 S2 C33 107.7(3) O3 S2 C33 107.9(3) N2 S2 C33 107.0(3) C1 N1 S1 118.8(4) C1 N1 H1A 120(4) S1 N1 H1A 112(4) C20 N2 S2 118.3(4) C20 N2 H2A 112(4) S2 N2 H2A 108(4) N1 C1 C2 112.5(5) N1 C1 H1C 109.1 C2 C1 H1C 109.1 N1 C1 H1D 109.1 C2 C1 H1D 109.1 H1C C1 H1D 107.8 C12 C2 C13 109.9(5) C12 C2 C3 107.4(5) C13 C2 C3 114.7(5) C12 C2 C1 110.8(5) C13 C2 C1 105.2(5) C3 C2 C1 108.8(4) C5 C3 C4 60.4(4) C5 C3 C2 123.0(5) C4 C3 C2 122.6(5) C5 C3 H3 113.6 C4 C3 H3 113.6 C2 C3 H3 113.6 C5 C4 C3 59.6(4) C5 C4 H4A 117.8 C3 C4 H4A 117.8 C5 C4 H4B 117.8 C3 C4 H4B 117.8 H4A C4 H4B 114.9 C3 C5 C4 60.0(4) C3 C5 C6 121.0(5) C4 C5 C6 123.3(5) C3 C5 H5 114.0 C4 C5 H5 114.0 C6 C5 H5 114.0 C7 C6 C11 118.8(6) C7 C6 C5 121.6(6) C11 C6 C5 119.4(5) C6 C7 C8 119.2(8) C6 C7 H7 120.4 C8 C7 H7 120.4 C9 C8 C7 121.9(9) C9 C8 H8 119.1 C7 C8 H8 119.1 C8 C9 C10 118.3(8) C8 C9 H9 120.9 C10 C9 H9 120.9 C9 C10 C11 121.4(9) C9 C10 H10 119.3 C11 C10 H10 119.3 C6 C11 C10 120.4(7) C6 C11 H11 119.8 C10 C11 H11 119.8 C2 C12 H12A 109.5 C2 C12 H12B 109.5 H12A C12 H12B 109.5 C2 C12 H12C 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 C2 C13 H13A 109.5 C2 C13 H13B 109.5 H13A C13 H13B 109.5 C2 C13 H13C 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 C15 C14 C19 119.9(6) C15 C14 S1 121.6(5) C19 C14 S1 118.4(4) C14 C15 C16 119.6(6) C14 C15 H15 120.2 C16 C15 H15 120.2 C17 C16 C15 119.6(6) C17 C16 H16 120.2 C15 C16 H16 120.2 C16 C17 C18 121.7(7) C16 C17 Br1 119.5(5) C18 C17 Br1 118.8(6) C17 C18 C19 119.0(6) C17 C18 H18 120.5 C19 C18 H18 120.5 C18 C19 C14 120.1(6) C18 C19 H19 119.9 C14 C19 H19 119.9 N2 C20 C21 112.8(4) N2 C20 H20A 109.0 C21 C20 H20A 109.0 N2 C20 H20B 109.0 C21 C20 H20B 109.0 H20A C20 H20B 107.8 C22 C21 C20 109.1(4) C22 C21 C31 114.3(5) C20 C21 C31 111.0(5) C22 C21 C32 106.6(5) C20 C21 C32 105.7(5) C31 C21 C32 109.6(5) C21 C22 C24 124.8(4) C21 C22 C23 123.0(5) C24 C22 C23 59.9(4) C21 C22 H22 113.0 C24 C22 H22 113.0 C23 C22 H22 113.0 C24 C23 C22 59.5(4) C24 C23 H23A 117.8 C22 C23 H23A 117.8 C24 C23 H23B 117.8 C22 C23 H23B 117.8 H23A C23 H23B 115.0 C25 C24 C23 120.8(5) C25 C24 C22 119.8(4) C23 C24 C22 60.6(4) C25 C24 H24 115.0 C23 C24 H24 115.0 C22 C24 H24 115.0 C30 C25 C26 117.1(6) C30 C25 C24 121.2(5) C26 C25 C24 121.7(6) C27 C26 C25 121.3(8) C27 C26 H26 119.3 C25 C26 H26 119.3 C28 C27 C26 120.5(9) C28 C27 H27 119.7 C26 C27 H27 119.7 C27 C28 C29 121.0(8) C27 C28 H28 119.5 C29 C28 H28 119.5 C28 C29 C30 117.7(9) C28 C29 H29 121.2 C30 C29 H29 121.2 C25 C30 C29 122.3(7) C25 C30 H30 118.8 C29 C30 H30 118.8 C21 C31 H31A 109.5 C21 C31 H31B 109.5 H31A C31 H31B 109.5 C21 C31 H31C 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 C21 C32 H32A 109.5 C21 C32 H32B 109.5 H32A C32 H32B 109.5 C21 C32 H32C 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 C34 C33 C38 120.2(6) C34 C33 S2 119.8(4) C38 C33 S2 120.0(4) C33 C34 C35 119.8(5) C33 C34 H34 120.1 C35 C34 H34 120.1 C36 C35 C34 119.6(6) C36 C35 H35 120.2 C34 C35 H35 120.2 C35 C36 C37 121.2(6) C35 C36 Br2 119.3(5) C37 C36 Br2 119.6(5) C38 C37 C36 119.3(6) C38 C37 H37 120.3 C36 C37 H37 120.3 C37 C38 C33 119.8(6) C37 C38 H38 120.1 C33 C38 H38 120.1 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Br1 C17 1.898(7) Br2 C36 1.892(7) S1 O1 1.426(4) S1 O2 1.437(4) S1 N1 1.608(5) S1 C14 1.773(7) S2 O4 1.426(4) S2 O3 1.434(4) S2 N2 1.615(5) S2 C33 1.771(6) N1 C1 1.473(7) N1 H1A 0.84(3) N2 C20 1.463(7) N2 H2A 0.80(3) C1 C2 1.548(8) C1 H1C 0.9700 C1 H1D 0.9700 C2 C12 1.512(8) C2 C13 1.521(8) C2 C3 1.541(8) C3 C5 1.477(7) C3 C4 1.483(9) C3 H3 0.9800 C4 C5 1.488(9) C4 H4A 0.9700 C4 H4B 0.9700 C5 C6 1.499(7) C5 H5 0.9800 C6 C7 1.373(9) C6 C11 1.383(9) C7 C8 1.397(12) C7 H7 0.9300 C8 C9 1.362(14) C8 H8 0.9300 C9 C10 1.358(13) C9 H9 0.9300 C10 C11 1.379(9) C10 H10 0.9300 C11 H11 0.9300 C12 H12A 0.9600 C12 H12B 0.9600 C12 H12C 0.9600 C13 H13A 0.9600 C13 H13B 0.9600 C13 H13C 0.9600 C14 C15 1.370(8) C14 C19 1.398(8) C15 C16 1.389(10) C15 H15 0.9300 C16 C17 1.359(10) C16 H16 0.9300 C17 C18 1.376(10) C18 C19 1.369(10) C18 H18 0.9300 C19 H19 0.9300 C20 C21 1.522(8) C20 H20A 0.9700 C20 H20B 0.9700 C21 C22 1.512(7) C21 C31 1.535(8) C21 C32 1.544(8) C22 C24 1.505(7) C22 C23 1.522(8) C22 H22 0.9800 C23 C24 1.512(9) C23 H23A 0.9700 C23 H23B 0.9700 C24 C25 1.469(7) C24 H24 0.9800 C25 C30 1.376(9) C25 C26 1.395(9) C26 C27 1.367(12) C26 H26 0.9300 C27 C28 1.351(14) C27 H27 0.9300 C28 C29 1.386(14) C28 H28 0.9300 C29 C30 1.398(9) C29 H29 0.9300 C30 H30 0.9300 C31 H31A 0.9600 C31 H31B 0.9600 C31 H31C 0.9600 C32 H32A 0.9600 C32 H32B 0.9600 C32 H32C 0.9600 C33 C34 1.378(8) C33 C38 1.376(8) C34 C35 1.376(9) C34 H34 0.9300 C35 C36 1.361(9) C35 H35 0.9300 C36 C37 1.377(10) C37 C38 1.375(10) C37 H37 0.9300 C38 H38 0.9300 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N2 H2A O2 0.80(3) 2.25(4) 2.984(6) 153(6) N1 H1A O3 0.84(3) 2.10(3) 2.922(6) 167(5) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O1 S1 N1 C1 49.2(5) O2 S1 N1 C1 178.9(4) C14 S1 N1 C1 -66.1(5) O4 S2 N2 C20 -49.6(5) O3 S2 N2 C20 -178.4(4) C33 S2 N2 C20 66.2(5) S1 N1 C1 C2 -179.6(4) N1 C1 C2 C12 -68.0(7) N1 C1 C2 C13 173.2(5) N1 C1 C2 C3 49.9(6) C12 C2 C3 C5 -163.0(5) C13 C2 C3 C5 -40.5(7) C1 C2 C3 C5 77.0(6) C12 C2 C3 C4 -89.6(7) C13 C2 C3 C4 33.0(8) C1 C2 C3 C4 150.4(5) C2 C3 C4 C5 -112.3(6) C2 C3 C5 C4 111.7(6) C4 C3 C5 C6 113.2(6) C2 C3 C5 C6 -135.1(5) C3 C4 C5 C6 -109.4(6) C3 C5 C6 C7 -109.8(6) C4 C5 C6 C7 -37.4(8) C3 C5 C6 C11 74.5(7) C4 C5 C6 C11 146.9(6) C11 C6 C7 C8 0.1(9) C5 C6 C7 C8 -175.7(6) C6 C7 C8 C9 2.8(12) C7 C8 C9 C10 -2.9(13) C8 C9 C10 C11 0.1(12) C7 C6 C11 C10 -2.9(9) C5 C6 C11 C10 173.0(5) C9 C10 C11 C6 2.8(10) O1 S1 C14 C15 -4.4(6) O2 S1 C14 C15 -134.4(5) N1 S1 C14 C15 111.5(5) O1 S1 C14 C19 176.1(5) O2 S1 C14 C19 46.1(5) N1 S1 C14 C19 -68.1(5) C19 C14 C15 C16 -1.2(9) S1 C14 C15 C16 179.3(5) C14 C15 C16 C17 -0.3(10) C15 C16 C17 C18 2.2(11) C15 C16 C17 Br1 -179.8(5) C16 C17 C18 C19 -2.6(12) Br1 C17 C18 C19 179.5(6) C17 C18 C19 C14 1.0(11) C15 C14 C19 C18 0.8(10) S1 C14 C19 C18 -179.6(6) S2 N2 C20 C21 175.9(4) N2 C20 C21 C22 -65.0(6) N2 C20 C21 C31 61.9(6) N2 C20 C21 C32 -179.3(5) C20 C21 C22 C24 82.8(6) C31 C21 C22 C24 -42.2(7) C32 C21 C22 C24 -163.6(5) C20 C21 C22 C23 156.7(5) C31 C21 C22 C23 31.7(8) C32 C21 C22 C23 -89.6(7) C21 C22 C23 C24 -114.3(5) C22 C23 C24 C25 -109.1(5) C21 C22 C24 C25 -137.9(5) C23 C22 C24 C25 110.8(6) C21 C22 C24 C23 111.3(6) C23 C24 C25 C30 131.9(6) C22 C24 C25 C30 60.3(7) C23 C24 C25 C26 -49.1(8) C22 C24 C25 C26 -120.6(6) C30 C25 C26 C27 0.8(11) C24 C25 C26 C27 -178.3(7) C25 C26 C27 C28 1.4(14) C26 C27 C28 C29 -2.5(15) C27 C28 C29 C30 1.5(13) C26 C25 C30 C29 -1.8(9) C24 C25 C30 C29 177.3(5) C28 C29 C30 C25 0.8(10) O4 S2 C33 C34 8.6(6) O3 S2 C33 C34 137.9(5) N2 S2 C33 C34 -107.3(5) O4 S2 C33 C38 -173.2(5) O3 S2 C33 C38 -43.9(6) N2 S2 C33 C38 70.9(6) C38 C33 C34 C35 -0.6(9) S2 C33 C34 C35 177.5(5) C33 C34 C35 C36 0.1(10) C34 C35 C36 C37 1.3(11) C34 C35 C36 Br2 -179.6(5) C35 C36 C37 C38 -2.3(12) Br2 C36 C37 C38 178.6(6) C36 C37 C38 C33 1.8(12) C34 C33 C38 C37 -0.3(10) S2 C33 C38 C37 -178.5(6)