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Information card for entry 7123492
Preview
Coordinates | 7123492.cif |
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Original paper (by DOI) | HTML |
Formula | C20 H25 N O4 S |
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Calculated formula | C20 H25 N O4 S |
Title of publication | TMSOTf Mediated ‘5/6-endo-dig’ Reductive Hydroamination for the Stereoselective Synthesis of Pyrrolidine and Piperidine derivatives |
Authors of publication | Gharpure, Santosh J.; Vishwakarma, Dharmendra S.; Patel, Raj Kumar |
Journal of publication | Chemical Communications |
Year of publication | 2019 |
a | 9.714 ± 0.0005 Å |
b | 11.6951 ± 0.0005 Å |
c | 16.9879 ± 0.0008 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1929.93 ± 0.16 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0581 |
Residual factor for significantly intense reflections | 0.0438 |
Weighted residual factors for significantly intense reflections | 0.0907 |
Weighted residual factors for all reflections included in the refinement | 0.1013 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
215288 (current) | 2019-05-18 | cif/ Adding structures of 7123486, 7123487, 7123488, 7123489, 7123490, 7123491, 7123492 via cif-deposit CGI script. |
7123492.cif |
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Users of the data should acknowledge the original authors of the
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