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Information card for entry 7124303
Preview
| Coordinates | 7124303.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H28 N2 Si |
|---|---|
| Calculated formula | C28 H28 N2 Si |
| Title of publication | Lewis Acid-Catalyzed Synthesis of Silafluorene Derivatives from Biphenyls and Dihydrosilanes via Double Sila-Friedel-Crafts Reaction |
| Authors of publication | Dong, Yafang; Takata, Yuta; Yoshigoe, Yusuke; Sekine, Kohei; Kuninobu, Yoichiro |
| Journal of publication | Chemical Communications |
| Year of publication | 2019 |
| a | 9.4768 ± 0.0004 Å |
| b | 10.9099 ± 0.0004 Å |
| c | 13.1313 ± 0.0005 Å |
| α | 113.798 ± 0.003° |
| β | 91.992 ± 0.004° |
| γ | 112.004 ± 0.004° |
| Cell volume | 1123.73 ± 0.09 Å3 |
| Cell temperature | 123 K |
| Ambient diffraction temperature | 123 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0467 |
| Residual factor for significantly intense reflections | 0.0402 |
| Weighted residual factors for significantly intense reflections | 0.106 |
| Weighted residual factors for all reflections included in the refinement | 0.11 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.085 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 219314 (current) | 2019-10-13 | cif/ Adding structures of 7124303 via cif-deposit CGI script. |
7124303.cif |
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Users of the data should acknowledge the original authors of the
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