Crystallography Open Database

Information card for entry 7151769

Preview

Coordinates	7151769.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H48 Cl O4 P
Calculated formula	C42 H48 Cl O4 P
Title of publication	A facile approach to highly functional trisubstituted furans via intramolecular Wittig reactions.
Authors of publication	Chen, Ko-Wei; Syu, Siang-en; Jang, Yeong-Jiunn; Lin, Wenwei
Journal of publication	Organic & biomolecular chemistry
Year of publication	2011
Journal volume	9
Journal issue	7
Pages of publication	2098 - 2106
a	13.9348 ± 0.0003 Å
b	12.1131 ± 0.0002 Å
c	23.212 ± 0.0005 Å
α	90°
β	92.073 ± 0.001°
γ	90°
Cell volume	3915.47 ± 0.14 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1092
Residual factor for significantly intense reflections	0.0711
Weighted residual factors for significantly intense reflections	0.2109
Weighted residual factors for all reflections included in the refinement	0.2455
Goodness-of-fit parameter for all reflections included in the refinement	1.1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180303 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/17.	7151769.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7151769.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7151769.cif
21260	2011-06-22	../uploads/cif-deposit/cod/cif Adding structures of 7151769, 7151770, 7151771 via cif-deposit CGI script.	7151769.cif