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Information card for entry 7156264
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Coordinates | 7156264.cif |
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Original paper (by DOI) | HTML |
Formula | C15 H15 Cl N4 |
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Calculated formula | C15 H15 Cl N4 |
Title of publication | Copper-catalyzed ambient-temperature decarboxylative annulation of isatins with amidine hydrochlorides: a facile access to 2-(1,3,5-triazin-2-yl)aniline derivatives. |
Authors of publication | Jia, Feng-Cheng; Xu, Cheng; Wang, Yu-Wei; Chen, Zhi-Peng; Chen, Yun-Feng; Wu, An-Xin |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2018 |
Journal volume | 16 |
Journal issue | 23 |
Pages of publication | 4223 - 4226 |
a | 10.585 ± 0.002 Å |
b | 8.8309 ± 0.0018 Å |
c | 15.039 ± 0.003 Å |
α | 90° |
β | 96.741 ± 0.003° |
γ | 90° |
Cell volume | 1396.1 ± 0.5 Å3 |
Cell temperature | 273 ± 2 K |
Ambient diffraction temperature | 273 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0784 |
Residual factor for significantly intense reflections | 0.0582 |
Weighted residual factors for significantly intense reflections | 0.1829 |
Weighted residual factors for all reflections included in the refinement | 0.2028 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.005 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
230830 (current) | 2019-11-17 | cif/ Updating files of 7156264 Original log message: Adding full bibliography for 7156264.cif. |
7156264.cif |
207818 | 2018-05-16 | cif/ Adding structures of 7156264 via cif-deposit CGI script. |
7156264.cif |
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Users of the data should acknowledge the original authors of the
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