Crystallography Open Database

Information card for entry 7156265

Preview

Coordinates	7156265.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H26 Br2 Cl0 N4 O2 Pd
Calculated formula	C30 H26 Br2 N4 O2 Pd
Title of publication	Synthesis of topologically constrained naphthalimide appended palladium(ii)-N-heterocyclic carbene complexes - insights into additive controlled product selectivity.
Authors of publication	Panyam, Pradeep Kumar Reddy; Sreedharan, Ramdas; Gandhi, Thirumanavelan
Journal of publication	Organic & biomolecular chemistry
Year of publication	2018
Journal volume	16
Journal issue	23
Pages of publication	4357 - 4364
a	40.319 ± 0.005 Å
b	8.136 ± 0.005 Å
c	8.974 ± 0.005 Å
α	90 ± 0.005°
β	90 ± 0.005°
γ	90 ± 0.005°
Cell volume	2944 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.0342
Weighted residual factors for significantly intense reflections	0.0708
Weighted residual factors for all reflections included in the refinement	0.0738
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
230831 (current)	2019-11-17	cif/ Updating files of 7156265 Original log message: Adding full bibliography for 7156265.cif.	7156265.cif
207941	2018-05-23	cif/ Adding structures of 7156265 via cif-deposit CGI script.	7156265.cif