Crystallography Open Database

Information card for entry 7156976

Preview

Coordinates	7156976.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H20 Cl2 O6
Calculated formula	C23 H20 Cl2 O6
Title of publication	A facile copper(i)-catalyzed homo-coupling of indanone derivatives using diaziridinone under mild conditions.
Authors of publication	Han, Wenyong; Yang, Yihui; Zhu, Yingguang; Shi, Yian
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	17
Journal issue	29
Pages of publication	6998 - 7001
a	12.9425 ± 0.0009 Å
b	15.6165 ± 0.0011 Å
c	10.6618 ± 0.0007 Å
α	90°
β	101.551 ± 0.003°
γ	90°
Cell volume	2111.3 ± 0.3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0493
Residual factor for significantly intense reflections	0.0387
Weighted residual factors for significantly intense reflections	0.0956
Weighted residual factors for all reflections included in the refinement	0.1028
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
225021 (current)	2019-11-08	cif/ Updating files of 7156976, 7156977 Original log message: Adding full bibliography for 7156976--7156977.cif.	7156976.cif
217050	2019-07-16	cif/ Adding structures of 7156976, 7156977 via cif-deposit CGI script.	7156976.cif