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Information card for entry 7157145
Preview
| Coordinates | 7157145.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H24 N2 O5 S |
|---|---|
| Calculated formula | C27 H24 N2 O5 S |
| Title of publication | Primary amine catalyzed diastereo- and enantioselective Michael reaction of thiazolones and α,β-unsaturated ketones. |
| Authors of publication | Lu, Min; Li, Hong; Zou, Chuncheng; Li, Jianchang; Liu, Chengyu; Sun, Maolin; Ma, Yueyue; Cheng, Ruihua; Ye, Jinxing |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2019 |
| Journal volume | 17 |
| Journal issue | 42 |
| Pages of publication | 9305 - 9312 |
| a | 8.5917 ± 0.0013 Å |
| b | 13.421 ± 0.002 Å |
| c | 21.279 ± 0.003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2453.7 ± 0.6 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0522 |
| Residual factor for significantly intense reflections | 0.0433 |
| Weighted residual factors for significantly intense reflections | 0.1057 |
| Weighted residual factors for all reflections included in the refinement | 0.1114 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 225108 (current) | 2019-11-08 | cif/ Updating files of 7157145 Original log message: Adding full bibliography for 7157145.cif. |
7157145.cif |
| 219309 | 2019-10-12 | cif/ Adding structures of 7157145 via cif-deposit CGI script. |
7157145.cif |
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Users of the data should acknowledge the original authors of the
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