# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_7209321 _shelx_title ' [Cd(NCO)2(C5N4H4)]' _shelx_refln_list_code 4 _shelx_F_calc_maximum 175.22 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7546 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 3.5617 _cell_length_b 11.4103 _cell_length_c 12.0524 _cell_angle_alpha 71.286 _cell_angle_beta 83.404 _cell_angle_gamma 87.609 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2397.20 2509.92 15.89 o 2 0 0 2695.91 2722.20 17.66 o 3 0 0 788.94 824.95 17.73 o 4 0 0 0.39 2.92 0.88 o -4 1 0 6.49 7.20 1.13 o -3 1 0 808.77 815.37 13.74 o -2 1 0 3390.09 3505.10 39.97 o -1 1 0 752.59 811.09 10.38 o 0 1 0 9228.95 8105.81 169.86 o 1 1 0 52.11 76.71 1.63 o 2 1 0 4419.67 4607.02 35.10 o 3 1 0 1358.35 1409.20 44.01 o 4 1 0 15.53 20.90 1.74 o -4 2 0 8.92 11.57 1.29 o -3 2 0 1353.41 1332.69 16.38 o -2 2 0 1765.67 1835.05 20.99 o -1 2 0 4278.88 4300.57 34.86 o 0 2 0 2075.35 2072.98 12.91 o 1 2 0 0.73 10.36 0.67 o 2 2 0 2567.13 2732.06 23.95 o 3 2 0 1566.35 1601.98 24.36 o 4 2 0 3.23 5.03 1.18 o -4 3 0 0.71 -1.21 2.67 o -3 3 0 1560.48 1585.10 37.94 o -2 3 0 973.41 938.19 12.77 o -1 3 0 626.94 614.46 12.77 o 0 3 0 5928.13 5795.35 67.35 o 1 3 0 563.89 618.76 6.71 o 2 3 0 86.25 81.92 3.73 o 3 3 0 441.19 463.19 26.57 o 4 3 0 5.37 4.45 0.89 o -4 4 0 21.24 25.87 2.03 o -3 4 0 1139.34 1102.66 36.37 o -2 4 0 412.35 367.33 8.81 o -1 4 0 871.54 869.69 12.43 o 0 4 0 2795.47 2598.77 42.92 o 1 4 0 589.03 591.50 6.24 o 2 4 0 773.96 756.06 10.79 o 3 4 0 1027.47 1034.60 43.15 o 4 4 0 11.66 12.10 1.97 o -4 5 0 1.31 0.77 2.60 o -3 5 0 736.70 721.88 12.70 o -2 5 0 686.76 680.42 20.57 o -1 5 0 600.50 585.11 6.38 o 0 5 0 1477.61 1334.79 11.15 o 1 5 0 949.66 956.03 9.09 o 2 5 0 621.38 607.68 9.82 o 3 5 0 957.96 1009.44 84.87 o 4 5 0 12.91 16.50 2.64 o -4 6 0 22.77 22.44 2.39 o -3 6 0 377.06 379.59 13.37 o -2 6 0 367.93 351.42 9.50 o -1 6 0 93.45 86.74 3.62 o 0 6 0 2833.86 2825.01 20.14 o 1 6 0 147.86 144.57 3.66 o 2 6 0 743.90 698.56 13.68 o 3 6 0 745.66 768.06 17.51 o 4 6 0 0.18 3.03 2.11 o -4 7 0 4.39 4.54 1.79 o -3 7 0 1292.08 1267.16 41.28 o -2 7 0 1221.86 1220.87 16.51 o -1 7 0 83.68 72.58 2.97 o 0 7 0 2240.23 2364.08 24.13 o 1 7 0 707.20 686.32 14.96 o 2 7 0 400.66 396.65 33.36 o 3 7 0 464.49 457.52 33.71 o 4 7 0 1.55 0.07 1.48 o -3 8 0 683.97 671.24 25.17 o -2 8 0 809.25 778.67 13.15 o -1 8 0 526.68 489.45 8.99 o 0 8 0 1796.69 1835.46 16.16 o 1 8 0 263.15 265.87 9.53 o 2 8 0 602.13 571.50 27.10 o 3 8 0 286.01 273.73 22.60 o -3 9 0 226.36 214.62 8.32 o -2 9 0 258.94 239.06 6.97 o -1 9 0 403.46 368.99 8.00 o 0 9 0 3359.08 3480.63 30.72 o 1 9 0 39.39 42.79 3.10 o 2 9 0 636.87 630.97 33.54 o 3 9 0 301.10 288.76 20.52 o -3 10 0 208.85 217.06 8.42 o -2 10 0 393.01 376.27 12.93 o -1 10 0 7.76 7.22 1.28 o 0 10 0 804.75 830.32 12.77 o 1 10 0 26.93 29.80 4.73 o 2 10 0 317.19 315.30 20.72 o 3 10 0 267.48 279.66 13.30 o -2 11 0 208.89 197.35 8.21 o -1 11 0 148.59 156.59 7.90 o 0 11 0 283.27 291.14 9.47 o 1 11 0 168.25 164.26 9.07 o 2 11 0 161.87 146.41 18.34 o -2 12 0 131.36 129.05 8.51 o -1 12 0 34.30 45.40 4.33 o 0 12 0 433.57 454.02 12.65 o 1 12 0 136.89 137.60 6.33 o 2 12 0 108.85 105.64 5.57 o -1 13 0 19.42 25.08 1.98 o 0 13 0 398.24 444.62 19.10 o 1 13 0 54.89 51.77 2.90 o 0 14 0 173.22 172.00 10.45 o -1 -13 1 287.56 282.92 9.88 o 0 -13 1 72.24 77.28 6.37 o 1 -13 1 57.02 57.12 4.57 o -2 -12 1 4.70 6.19 1.69 o -1 -12 1 282.31 268.39 17.02 o 0 -12 1 240.83 243.86 12.98 o 1 -12 1 86.50 90.35 11.78 o -2 -11 1 17.58 17.91 2.29 o -1 -11 1 280.73 266.68 9.38 o 0 -11 1 70.44 70.89 4.54 o 1 -11 1 122.46 138.11 6.30 o 2 -11 1 297.49 323.52 15.51 o -2 -10 1 0.39 3.47 0.80 o -1 -10 1 1392.71 1368.32 58.90 o 0 -10 1 524.85 535.94 9.99 o 1 -10 1 14.81 21.83 1.49 o 2 -10 1 546.31 543.62 28.63 o 3 -10 1 81.41 92.36 5.94 o -3 -9 1 285.74 261.66 19.82 o -2 -9 1 14.24 11.77 2.11 o -1 -9 1 698.42 689.46 16.44 o 0 -9 1 1329.36 1369.36 16.64 o 1 -9 1 72.65 69.83 3.17 o 2 -9 1 1189.35 1179.92 27.54 o 3 -9 1 15.35 14.03 1.52 o -3 -8 1 158.57 166.57 7.79 o -2 -8 1 76.99 75.25 4.55 o -1 -8 1 404.43 384.83 10.24 o 0 -8 1 552.58 522.64 7.66 o 1 -8 1 792.30 792.62 12.16 o 2 -8 1 2556.15 2455.43 45.60 o 3 -8 1 136.93 127.55 6.30 o -3 -7 1 296.85 293.08 10.56 o -2 -7 1 2.88 3.01 0.77 o -1 -7 1 1479.79 1468.37 17.52 o 0 -7 1 532.66 525.12 7.22 o 1 -7 1 89.63 89.72 3.41 o 2 -7 1 600.43 611.05 11.09 o 3 -7 1 20.74 26.15 1.65 o -4 -6 1 180.77 177.73 10.13 o -3 -6 1 411.62 401.39 14.67 o -2 -6 1 0.08 2.25 0.85 o -1 -6 1 1342.02 1291.92 26.79 o 0 -6 1 1063.19 1053.94 12.71 o 1 -6 1 332.61 300.51 4.91 o 2 -6 1 900.26 865.91 15.91 o 3 -6 1 23.76 27.71 1.79 o 4 -6 1 215.95 190.01 10.17 o -4 -5 1 196.44 172.17 11.50 o -3 -5 1 698.81 700.16 12.63 o -2 -5 1 4.99 8.75 0.93 o -1 -5 1 1922.45 1961.48 27.40 o 0 -5 1 2549.43 2506.53 17.94 o 1 -5 1 363.48 334.80 4.87 o 2 -5 1 1954.70 1964.36 37.53 o 3 -5 1 251.78 240.55 13.89 o -3 -4 1 428.44 417.88 9.25 o -2 -4 1 4.40 11.11 3.27 o -1 -4 1 4461.45 4612.87 48.68 o 0 -4 1 1308.29 1231.29 13.98 o 1 -4 1 811.60 837.12 7.95 o 2 -4 1 2091.28 2052.64 87.53 o 3 -4 1 119.61 110.08 4.19 o 4 -4 1 226.35 231.45 8.64 o -4 -3 1 199.93 206.52 6.91 o -3 -3 1 1417.01 1399.61 23.94 o -2 -3 1 79.71 92.19 3.38 o -1 -3 1 5021.45 5278.67 31.57 o 0 -3 1 4712.27 4598.66 27.16 o 1 -3 1 1475.02 1572.02 11.65 o 2 -3 1 2864.63 2799.23 33.65 o 3 -3 1 99.66 106.61 4.09 o 4 -3 1 264.19 268.25 9.56 o -4 -2 1 299.90 302.74 18.64 o -3 -2 1 2896.55 2941.35 28.80 o -2 -2 1 347.74 359.58 11.33 o -1 -2 1 3589.29 3623.02 69.43 o 0 -2 1 2714.10 2841.41 26.53 o 1 -2 1 2024.85 2158.43 22.27 o 2 -2 1 2162.05 2209.85 14.93 o 3 -2 1 96.55 96.12 3.24 o 4 -2 1 410.01 443.05 10.36 o -4 -1 1 200.10 208.38 14.22 o -3 -1 1 1339.54 1341.89 14.93 o -2 -1 1 349.87 365.39 6.76 o -1 -1 1 30701.36 29292.88 476.35 o 0 -1 1 6068.97 5905.75 83.59 o 1 -1 1 1826.33 1845.96 11.23 o 2 -1 1 3450.35 3740.12 22.41 o 3 -1 1 307.78 309.79 10.02 o 4 -1 1 362.40 369.02 9.44 o -4 0 1 323.51 323.89 9.13 o -3 0 1 1212.05 1236.19 31.00 o -2 0 1 36.50 40.34 1.70 o -1 0 1 5544.86 5567.22 63.97 o 0 0 1 3347.69 3001.28 20.95 o 1 0 1 1867.92 1804.74 12.23 o 2 0 1 5478.11 5645.83 46.54 o 3 0 1 19.94 20.70 1.76 o 4 0 1 435.50 434.57 18.97 o -4 1 1 444.00 433.60 10.84 o -3 1 1 690.08 730.10 34.65 o -2 1 1 310.45 298.20 4.26 o -1 1 1 5.83 4.31 0.42 o 0 1 1 998.84 1056.81 11.88 o 1 1 1 3672.92 3936.83 23.48 o 2 1 1 6154.35 6419.93 72.83 o 3 1 1 57.86 64.14 3.70 o 4 1 1 507.20 520.60 14.91 o -4 2 1 520.90 535.96 18.45 o -3 2 1 710.98 713.75 14.91 o -2 2 1 0.60 1.78 0.52 o -1 2 1 4341.61 4302.42 126.18 o 0 2 1 4267.04 4479.75 32.54 o 1 2 1 35.73 43.49 1.22 o 2 2 1 880.33 877.14 14.73 o 3 2 1 215.39 199.87 5.61 o 4 2 1 314.02 317.26 8.68 o -4 3 1 272.39 281.31 10.31 o -3 3 1 607.69 578.42 24.52 o -2 3 1 4.63 6.40 1.58 o -1 3 1 5195.83 5059.48 56.93 o 0 3 1 1129.20 1151.33 8.39 o 1 3 1 602.41 541.68 5.51 o 2 3 1 1721.42 1690.91 23.39 o 3 3 1 239.12 228.86 6.21 o 4 3 1 213.27 214.31 6.76 o -4 4 1 189.43 200.99 8.13 o -3 4 1 954.97 938.98 14.48 o -2 4 1 51.53 49.06 2.49 o -1 4 1 2967.74 2961.74 50.62 o 0 4 1 3086.29 2930.51 18.66 o 1 4 1 494.21 476.98 6.41 o 2 4 1 2552.08 2594.10 20.96 o 3 4 1 253.73 245.41 10.19 o 4 4 1 150.64 165.24 10.94 o -4 5 1 105.15 108.27 5.41 o -3 5 1 859.00 828.82 21.99 o -2 5 1 1.55 3.16 0.77 o -1 5 1 2544.28 2593.57 23.69 o 0 5 1 519.17 452.03 5.32 o 1 5 1 1008.41 1015.53 9.20 o 2 5 1 1630.10 1697.30 22.22 o 3 5 1 163.03 174.50 7.28 o 4 5 1 204.88 224.31 11.11 o -4 6 1 356.73 368.82 14.46 o -3 6 1 1128.17 1071.50 23.07 o -2 6 1 2.65 4.50 1.68 o -1 6 1 3564.72 3645.99 24.33 o 0 6 1 1730.85 1692.84 13.47 o 1 6 1 254.16 247.25 4.13 o 2 6 1 1345.36 1366.64 32.06 o 3 6 1 97.47 99.52 5.41 o 4 6 1 196.18 196.86 8.37 o -4 7 1 288.84 303.69 14.42 o -3 7 1 1023.32 994.31 32.78 o -2 7 1 17.35 17.60 2.33 o -1 7 1 1895.17 1911.95 19.53 o 0 7 1 1547.51 1661.13 14.14 o 1 7 1 179.09 162.97 10.95 o 2 7 1 1176.53 1137.85 44.23 o 3 7 1 72.14 78.19 6.40 o 4 7 1 208.95 220.64 12.28 o -3 8 1 320.10 302.58 8.33 o -2 8 1 71.22 70.52 3.28 o -1 8 1 2419.43 2377.13 23.40 o 0 8 1 685.68 717.64 10.39 o 1 8 1 647.39 668.41 14.74 o 2 8 1 1514.30 1540.33 111.01 o 3 8 1 161.61 156.78 17.09 o -3 9 1 287.79 286.55 8.17 o -2 9 1 30.42 31.36 3.84 o -1 9 1 861.07 828.27 13.18 o 0 9 1 833.82 830.46 12.19 o 1 9 1 210.50 226.32 7.94 o 2 9 1 1202.26 1266.83 119.38 o 3 9 1 6.09 10.61 5.70 o -3 10 1 183.31 188.79 12.56 o -2 10 1 0.61 3.78 2.05 o -1 10 1 243.57 237.96 8.56 o 0 10 1 944.78 951.34 13.74 o 1 10 1 120.54 125.34 5.90 o 2 10 1 994.25 1003.94 94.37 o 3 10 1 0.11 0.98 0.99 o -3 11 1 183.41 194.26 9.18 o -2 11 1 2.50 3.59 0.91 o -1 11 1 536.22 529.81 13.94 o 0 11 1 495.55 529.39 13.36 o 1 11 1 181.53 170.82 19.08 o 2 11 1 420.17 399.77 22.49 o -2 12 1 1.62 1.36 2.83 o -1 12 1 728.87 711.10 16.94 o 0 12 1 168.26 157.13 10.53 o 1 12 1 151.00 159.27 6.98 o 2 12 1 163.14 151.05 11.34 o -2 13 1 1.28 -1.65 1.79 o -1 13 1 344.73 376.84 13.00 o 0 13 1 95.10 106.22 5.49 o 1 13 1 52.09 65.70 3.65 o -1 14 1 150.76 175.80 10.20 o 0 14 1 38.72 47.10 4.08 o -1 -13 2 181.74 199.17 9.81 o 1 -13 2 246.39 270.02 12.91 o -1 -12 2 171.85 170.84 14.77 o 0 -12 2 0.11 0.25 1.44 o 1 -12 2 340.94 356.73 15.72 o -2 -11 2 218.95 218.54 8.84 o -1 -11 2 486.30 491.91 28.47 o 0 -11 2 7.28 7.42 1.69 o 1 -11 2 622.90 650.25 21.60 o 2 -11 2 227.10 232.23 8.45 o -2 -10 2 262.31 238.76 18.04 o -1 -10 2 1208.45 1187.85 28.46 o 0 -10 2 22.11 21.40 1.45 o 1 -10 2 867.02 899.43 14.43 o 2 -10 2 76.25 83.45 4.41 o -3 -9 2 7.09 7.99 1.97 o -2 -9 2 121.95 118.07 5.94 o -1 -9 2 482.06 457.44 11.94 o 0 -9 2 317.63 316.66 12.87 o 1 -9 2 1827.23 1849.14 35.34 o 2 -9 2 371.39 358.69 11.00 o 3 -9 2 102.42 103.34 5.19 o -3 -8 2 41.04 37.70 2.93 o -2 -8 2 584.87 544.35 18.91 o -1 -8 2 398.03 366.81 8.06 o 0 -8 2 16.32 18.52 1.58 o 1 -8 2 307.23 311.50 7.25 o 2 -8 2 493.24 486.89 14.05 o 3 -8 2 116.43 116.72 5.79 o -3 -7 2 62.46 69.39 6.65 o -2 -7 2 679.34 649.48 14.84 o -1 -7 2 539.32 512.37 11.44 o 0 -7 2 1.09 5.51 0.77 o 1 -7 2 419.03 442.92 15.08 o 2 -7 2 157.82 155.19 5.14 o 3 -7 2 154.92 158.36 14.60 o -3 -6 2 24.50 24.74 2.86 o -2 -6 2 644.89 633.43 11.02 o -1 -6 2 1986.52 1990.00 27.87 o 0 -6 2 0.10 2.54 0.46 o 1 -6 2 2675.42 2598.81 19.88 o 2 -6 2 799.24 806.04 12.56 o 3 -6 2 30.44 31.87 2.51 o 4 -6 2 204.55 218.92 11.36 o -3 -5 2 75.35 69.74 3.66 o -2 -5 2 774.69 753.83 11.82 o -1 -5 2 2036.19 2021.13 18.45 o 0 -5 2 20.84 28.25 1.27 o 1 -5 2 2657.35 2694.08 19.62 o 2 -5 2 909.45 884.62 13.23 o 3 -5 2 283.41 277.61 7.34 o 4 -5 2 311.50 318.04 10.58 o -4 -4 2 366.61 350.75 14.88 o -3 -4 2 171.35 168.62 5.58 o -2 -4 2 1313.82 1354.54 16.38 o -1 -4 2 3377.30 3416.42 22.64 o 0 -4 2 128.81 122.66 2.67 o 1 -4 2 5158.35 5301.65 32.61 o 2 -4 2 683.42 685.93 10.43 o 3 -4 2 357.66 346.97 9.73 o -4 -3 2 848.69 811.54 20.52 o -3 -3 2 538.99 514.16 10.35 o -2 -3 2 723.75 694.85 15.64 o -1 -3 2 5013.77 5165.41 37.55 o 0 -3 2 4.22 4.82 0.89 o 1 -3 2 4585.44 4821.82 31.24 o 2 -3 2 325.68 303.44 7.45 o 3 -3 2 478.74 457.69 9.32 o 4 -3 2 426.25 405.48 17.80 o -4 -2 2 418.39 458.83 31.41 o -3 -2 2 37.64 36.75 2.21 o -2 -2 2 3812.54 3865.55 31.89 o -1 -2 2 6128.26 6440.24 44.49 o 0 -2 2 730.97 721.01 6.30 o 1 -2 2 5934.24 6377.32 38.03 o 2 -2 2 1614.44 1705.66 12.61 o 3 -2 2 315.87 320.92 7.63 o 4 -2 2 408.75 434.00 18.57 o -4 -1 2 356.70 371.04 13.99 o -3 -1 2 53.86 58.69 3.16 o -2 -1 2 2550.27 2573.27 23.17 o -1 -1 2 5909.89 5723.98 110.29 o 0 -1 2 231.00 185.12 3.09 o 1 -1 2 7071.72 7397.45 37.24 o 2 -1 2 781.51 796.96 7.65 o 3 -1 2 148.84 143.33 4.69 o 4 -1 2 547.24 587.83 21.10 o -4 0 2 370.44 402.97 16.74 o -3 0 2 56.60 52.69 2.96 o -2 0 2 202.69 187.71 3.27 o -1 0 2 936.92 851.30 7.12 o 0 0 2 1486.21 1562.46 10.90 o 1 0 2 6971.60 6882.14 38.89 o 2 0 2 708.29 721.12 7.19 o 3 0 2 399.01 402.61 11.46 o 4 0 2 1110.26 1177.58 22.87 o -4 1 2 568.66 567.28 19.14 o -3 1 2 57.28 59.43 3.17 o -2 1 2 2048.99 2049.96 19.93 o -1 1 2 2029.32 2107.22 40.88 o 0 1 2 335.13 278.42 3.72 o 1 1 2 152.66 129.01 2.31 o 2 1 2 3737.46 3873.11 36.72 o 3 1 2 231.89 241.99 4.61 o 4 1 2 904.35 957.58 16.52 o -4 2 2 604.49 603.95 13.28 o -3 2 2 87.51 93.37 4.16 o -2 2 2 2735.19 2734.94 53.49 o -1 2 2 865.51 836.96 15.54 o 0 2 2 78.94 105.38 1.73 o 1 2 2 961.20 933.84 21.41 o 2 2 2 2229.17 2264.81 17.29 o 3 2 2 225.13 210.09 5.68 o 4 2 2 700.62 743.70 32.18 o -4 3 2 548.27 569.18 12.87 o -3 3 2 6.09 9.43 1.47 o -2 3 2 1601.68 1688.29 40.01 o -1 3 2 3848.15 3683.60 45.17 o 0 3 2 186.55 217.04 2.77 o 1 3 2 7471.94 7381.68 46.36 o 2 3 2 857.10 872.28 15.47 o 3 3 2 256.04 240.50 6.24 o 4 3 2 509.17 534.93 14.87 o -4 4 2 487.66 496.45 14.49 o -3 4 2 114.81 100.45 3.96 o -2 4 2 484.37 460.34 8.33 o -1 4 2 2496.31 2456.03 49.61 o 0 4 2 162.12 192.84 2.79 o 1 4 2 4887.10 4761.48 28.91 o 2 4 2 1146.18 1147.77 13.60 o 3 4 2 312.74 325.94 7.53 o 4 4 2 325.06 333.44 15.97 o -4 5 2 438.58 483.46 14.22 o -3 5 2 179.89 160.18 5.38 o -2 5 2 1240.25 1210.18 42.29 o -1 5 2 3665.88 3711.19 29.36 o 0 5 2 44.11 50.06 1.42 o 1 5 2 3261.51 3500.69 63.98 o 2 5 2 881.63 834.57 21.31 o 3 5 2 283.58 290.57 9.65 o 4 5 2 380.52 403.92 21.74 o -4 6 2 465.62 525.17 21.24 o -3 6 2 175.42 158.88 5.94 o -2 6 2 1092.94 1102.86 52.13 o -1 6 2 4247.62 4561.08 35.65 o 0 6 2 163.07 197.39 3.45 o 1 6 2 3148.56 3214.87 26.63 o 2 6 2 356.87 356.38 8.72 o 3 6 2 299.12 306.54 11.87 o 4 6 2 418.33 450.14 13.82 o -3 7 2 61.39 57.84 4.90 o -2 7 2 898.66 884.55 15.36 o -1 7 2 1997.90 1915.36 74.61 o 0 7 2 288.42 305.65 4.79 o 1 7 2 3710.70 3930.39 52.74 o 2 7 2 965.38 975.61 37.02 o 3 7 2 195.85 205.45 14.98 o 4 7 2 272.79 299.19 22.74 o -3 8 2 117.76 120.82 4.83 o -2 8 2 594.70 572.51 14.67 o -1 8 2 1899.78 1891.61 20.05 o 0 8 2 81.72 79.97 4.24 o 1 8 2 2031.61 2155.60 67.06 o 2 8 2 389.62 382.12 17.16 o 3 8 2 197.19 196.35 12.79 o -3 9 2 70.93 62.15 3.25 o -2 9 2 295.94 291.26 7.72 o -1 9 2 1353.31 1323.75 32.53 o 0 9 2 0.03 2.24 0.50 o 1 9 2 1472.22 1440.13 30.69 o 2 9 2 108.87 105.42 5.58 o 3 9 2 177.63 182.92 12.21 o -3 10 2 31.62 37.22 3.21 o -2 10 2 432.49 439.12 9.93 o -1 10 2 509.65 502.53 13.02 o 0 10 2 52.33 60.41 2.85 o 1 10 2 681.23 704.45 21.68 o 2 10 2 419.92 421.31 44.62 o 3 10 2 69.54 80.26 6.45 o -3 11 2 12.10 8.58 2.08 o -2 11 2 565.40 536.88 20.86 o -1 11 2 259.19 249.45 9.15 o 0 11 2 50.44 60.12 3.89 o 1 11 2 230.10 247.94 7.01 o 2 11 2 243.71 236.23 22.60 o -2 12 2 265.52 257.60 10.00 o -1 12 2 281.66 275.97 9.98 o 0 12 2 0.90 3.10 0.95 o 1 12 2 322.10 331.29 32.22 o 2 12 2 40.20 43.11 3.99 o -2 13 2 63.78 60.01 4.36 o -1 13 2 190.02 199.53 8.37 o 0 13 2 7.58 9.41 1.50 o 1 13 2 406.06 424.59 44.39 o 2 13 2 103.99 116.04 8.23 o -1 14 2 282.60 289.23 14.88 o 0 14 2 1.82 3.88 2.23 o -1 -12 3 19.98 25.46 1.92 o 1 -12 3 324.84 308.75 14.28 o -2 -11 3 458.33 454.05 19.31 o -1 -11 3 104.26 104.49 5.23 o 1 -11 3 280.65 301.68 13.96 o 2 -11 3 0.14 0.76 1.15 o -2 -10 3 166.94 164.42 7.33 o -1 -10 3 1.55 2.73 1.60 o 0 -10 3 657.94 648.65 14.21 o 1 -10 3 490.78 514.89 13.08 o 2 -10 3 20.78 31.81 7.21 o -2 -9 3 194.44 188.99 7.96 o -1 -9 3 16.32 26.02 2.39 o 0 -9 3 255.06 269.05 6.08 o 1 -9 3 1097.64 1156.73 20.31 o 2 -9 3 38.22 36.33 2.54 o 3 -9 3 342.46 346.45 20.38 o -3 -8 3 77.39 81.40 4.66 o -2 -8 3 415.58 400.24 11.92 o -1 -8 3 187.39 173.52 6.70 o 0 -8 3 271.66 286.46 12.40 o 1 -8 3 266.41 272.89 6.84 o 2 -8 3 65.83 63.64 3.78 o 3 -8 3 320.38 329.67 11.15 o -3 -7 3 70.51 69.05 4.29 o -2 -7 3 1291.14 1257.94 17.57 o -1 -7 3 147.18 127.11 9.46 o 0 -7 3 2428.96 2327.70 58.22 o 1 -7 3 559.34 590.16 10.07 o 2 -7 3 0.05 4.87 1.18 o 3 -7 3 235.23 229.89 8.73 o -3 -6 3 59.96 52.40 3.63 o -2 -6 3 1685.11 1619.60 20.00 o -1 -6 3 55.89 50.42 2.53 o 0 -6 3 1812.38 1864.10 18.47 o 1 -6 3 1488.87 1504.72 14.08 o 2 -6 3 74.73 71.81 7.02 o 3 -6 3 363.19 343.92 11.01 o -3 -5 3 181.39 174.08 5.87 o -2 -5 3 1481.78 1460.79 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