Crystallography Open Database

Information card for entry 7211822

Preview

Coordinates	7211822.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H29 N3 O72 Pr3 W12
Calculated formula	C21 H29 N3 O72 Pr3 W12
Title of publication	High-dimensional frameworks dependent on coordination mode of ligand controlled by acidity of reaction solution. Syntheses, structures, magnetic and fluorescence properties of eight new compounds
Authors of publication	Hu, Mi-Xia; Chen, Ya-Guang; Zhang, Chun-Jing; Kong, Qing-Jiao
Journal of publication	CrystEngComm
Year of publication	2010
Journal volume	12
Journal issue	5
Pages of publication	1454
a	23.44 ± 0.005 Å
b	20.489 ± 0.005 Å
c	29.486 ± 0.005 Å
α	90 ± 0.005°
β	90 ± 0.005°
γ	90 ± 0.005°
Cell volume	14161 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.1019
Residual factor for significantly intense reflections	0.0506
Weighted residual factors for significantly intense reflections	0.0945
Weighted residual factors for all reflections included in the refinement	0.1122
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180449 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/18.	7211822.cif
92410	2014-01-12	cif/ Adding structures of 7211819, 7211820, 7211821, 7211822, 7211823, 7211824, 7211825, 7211826 via cif-deposit CGI script.	7211822.cif