Crystallography Open Database

Information card for entry 7222328

Preview

Coordinates	7222328.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H36 N6 O6 Zn
Calculated formula	C38 H36 N6 O6 Zn
Title of publication	Formation of Zn(ii) and Pb(ii) coordination polymers of tetrakis(4-pyridyl)cyclobutane controlled by benzene and toluene
Authors of publication	Dai, Ming; Gu, Tian-Yi; Zhao, Xin; Li, Hong-Xi; Lang, Jian-Ping
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	43
Pages of publication	8345
a	9.4863 ± 0.0009 Å
b	9.8132 ± 0.0009 Å
c	11.1496 ± 0.0011 Å
α	68.615 ± 0.009°
β	89.254 ± 0.008°
γ	63.457 ± 0.01°
Cell volume	850.48 ± 0.18 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0617
Residual factor for significantly intense reflections	0.0516
Weighted residual factors for significantly intense reflections	0.1267
Weighted residual factors for all reflections included in the refinement	0.1334
Goodness-of-fit parameter for all reflections included in the refinement	0.921
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
171054 (current)	2015-12-09	cif/ Updating files of 7222327, 7222328, 7222329, 7222330, 7222331 Original log message: Adding full bibliography for 7222327--7222331.cif.	7222328.cif
158830	2015-09-29	cif/ Adding structures of 7222327, 7222328, 7222329, 7222330, 7222331 via cif-deposit CGI script.	7222328.cif