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Information card for entry 7232259
Preview
| Coordinates | 7232259.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H24 N2 Ni O4 S2 |
|---|---|
| Calculated formula | C22 H24 N2 Ni O4 S2 |
| Title of publication | Synthesis and characterisation of κ2-N,O-oxazoline-enolate complexes of nickel(ii): explorations in coordination chemistry and metal-mediated polymerisation |
| Authors of publication | Adjei, Jeanette A.; Lough, Alan J.; Gossage, Robert A. |
| Journal of publication | RSC Advances |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 7 |
| Pages of publication | 3956 |
| a | 9.8995 ± 0.0005 Å |
| b | 14.7668 ± 0.0008 Å |
| c | 16.2988 ± 0.0009 Å |
| α | 90° |
| β | 104.652 ± 0.002° |
| γ | 90° |
| Cell volume | 2305.1 ± 0.2 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0392 |
| Residual factor for significantly intense reflections | 0.0264 |
| Weighted residual factors for significantly intense reflections | 0.0607 |
| Weighted residual factors for all reflections included in the refinement | 0.0667 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 213384 (current) | 2019-01-30 | cif/ Adding structures of 7232254, 7232255, 7232256, 7232257, 7232258, 7232259 via cif-deposit CGI script. |
7232259.cif |
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Users of the data should acknowledge the original authors of the
structural data.