#------------------------------------------------------------------------------ #$Date: 2021-04-17 07:18:18 +0300 (Sat, 17 Apr 2021) $ #$Revision: 264273 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/26/7242667.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7242667 loop_ _publ_author_name 'Ali, Arif' 'Banerjee, Somesh' 'Kamaal, Saima' 'Usman, Mohammad' 'Das, Neeladrisingha' 'Afzal, Mohd' 'Alarifi, Abdullah' 'Sepay, Nayim' 'Roy, Partha' 'Ahmad, Musheer' _publ_section_title ; Ligand substituent effect on the cytotoxicity activity of two new copper(ii) complexes bearing 8-hydroxyquinoline derivatives: validated by MTT assay and apoptosis in MCF-7 cancer cell line (human breast cancer) ; _journal_issue 24 _journal_name_full 'RSC Advances' _journal_page_first 14362 _journal_page_last 14373 _journal_paper_doi 10.1039/D1RA00172H _journal_volume 11 _journal_year 2021 _chemical_formula_moiety 'C43 H32 Cu N3 O7, 2(H2 O), N O3' _chemical_formula_sum 'C43 H36 Cu N4 O12' _chemical_formula_weight 864.33 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _atom_sites_solution_primary iterative _audit_block_doi 10.5517/ccdc.csd.cc26hc8c _audit_creation_date 2020-10-24 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2020-10-24 deposited with the CCDC. 2021-03-30 downloaded from the CCDC. ; _cell_angle_alpha 66.799(2) _cell_angle_beta 71.044(2) _cell_angle_gamma 65.341(2) _cell_formula_units_Z 2 _cell_length_a 11.6573(7) _cell_length_b 12.7849(8) _cell_length_c 15.4024(9) _cell_measurement_reflns_used 9896 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.26 _cell_measurement_theta_min 2.66 _cell_volume 1881.8(2) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.9976 _diffrn_measured_fraction_theta_max 0.9976 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0310 _diffrn_reflns_av_unetI/netI 0.0326 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 31042 _diffrn_reflns_theta_full 24.9995 _diffrn_reflns_theta_max 25.00 _diffrn_reflns_theta_min 2.20 _exptl_absorpt_coefficient_mu 0.655 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6952 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1165 before and 0.0468 after correction. The Ratio of minimum to maximum transmission is 0.9323. The \l/2 correction factor is Not present. ; _exptl_crystal_colour blue _exptl_crystal_colour_primary blue _exptl_crystal_density_diffrn 1.5253 _exptl_crystal_description block _exptl_crystal_F_000 895.1575 _exptl_crystal_size_max 0.39 _exptl_crystal_size_mid 0.31 _exptl_crystal_size_min 0.19 _refine_diff_density_max 0.6469 _refine_diff_density_min -0.6896 _refine_diff_density_rms 0.0702 _refine_ls_d_res_high 0.8409 _refine_ls_d_res_low 9.2774 _refine_ls_goodness_of_fit_ref 1.0623 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 68 _refine_ls_number_parameters 549 _refine_ls_number_reflns 6608 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0623 _refine_ls_R_factor_all 0.0406 _refine_ls_R_factor_gt 0.0368 _refine_ls_shift/su_max 0.0002 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0496P)^2^+2.2989P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0985 _refine_ls_wR_factor_ref 0.1024 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 13 _reflns_limit_h_min -12 _reflns_limit_k_max 15 _reflns_limit_k_min -13 _reflns_limit_l_max 18 _reflns_limit_l_min 0 _reflns_number_gt 6083 _reflns_number_total 6608 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 29deca_0m_a.res in P-1 REM Old TITL 29deca_0m in P-1 REM SHELXT solution in P-1 REM R1 0.097, Rweak 0.007, Alpha 0.048, Orientation as input REM Formula found by SHELXT: C44 N5 O10 Br CELL 0.71073 11.6573 12.7849 15.4024 66.799 71.044 65.341 ZERR 2 0.0007 0.0008 0.0009 0.002 0.002 0.002 LATT 1 SFAC C H Cu N O UNIT 86 72 2 8 24 L.S. 10 PLAN 20 SIZE 0.39 0.31 0.19 TEMP -173(2) BOND $H LIST 6 FMAP 2 Htab ACTA OMIT -3 50 OMIT 1 0 1 WGHT 0.049575 2.298901 FVAR 0.528883 REM REM REM Cu1 3 0.42571 0.35286 0.27207 11.00000 0.01690 0.00991 0.01061 = -0.00173 -0.00236 -0.00352 O1 5 0.69862 0.68892 -0.02543 11.00000 0.03544 0.02895 0.02336 = -0.00061 -0.00256 -0.01962 O2 5 0.60748 0.54446 0.02650 11.00000 0.04487 0.03656 0.03053 = -0.00977 -0.00489 -0.01458 AFIX 147 H2 2 0.62464 0.55189 -0.03254 11.00000 -1.50000 AFIX 0 O3 5 0.65466 0.33817 0.21864 11.00000 0.01749 0.01473 0.02078 = -0.00575 -0.00263 -0.00665 O4 5 0.38274 0.48202 0.15651 11.00000 0.02116 0.01243 0.01305 = -0.00343 -0.00164 -0.00364 O5 5 0.23260 0.31174 0.32408 11.00000 0.01969 0.02252 0.01620 = -0.00399 -0.00901 -0.00441 O6 5 -0.03181 0.62265 0.04195 11.00000 0.07721 0.04542 0.03997 = -0.00945 -0.02073 -0.01471 AFIX 147 H6 2 -0.01886 0.59712 -0.00416 11.00000 -1.50000 AFIX 0 O7 5 -0.00030 0.42566 0.12772 11.00000 0.02720 0.02560 0.02393 = -0.00877 -0.00834 -0.00630 N1 4 0.51764 0.22637 0.19987 11.00000 0.01726 0.01179 0.01071 = 0.00088 -0.00334 -0.00482 N2 4 0.33867 0.48516 0.33516 11.00000 0.01908 0.01528 0.01384 = -0.00369 -0.00182 -0.00645 N3 4 0.44117 0.22791 0.40094 11.00000 0.01471 0.01136 0.01422 = -0.00360 -0.00326 -0.00388 C1 1 0.64094 0.62461 0.04018 11.00000 0.01984 0.01637 0.02174 = -0.00202 -0.00520 -0.00583 C2 1 0.60357 0.63285 0.14109 11.00000 0.02055 0.01966 0.02423 = -0.00601 -0.00224 -0.01106 C3 1 0.53294 0.74614 0.15417 11.00000 0.02838 0.01799 0.03118 = -0.00564 -0.00478 -0.01067 AFIX 43 H3 2 0.51029 0.81456 0.10022 11.00000 -1.20000 AFIX 0 C4 1 0.49556 0.75969 0.24514 11.00000 0.02944 0.02687 0.04189 = -0.01910 -0.00013 -0.01266 AFIX 43 H4 2 0.44592 0.83686 0.25374 11.00000 -1.20000 AFIX 0 C5 1 0.53066 0.66060 0.32352 11.00000 0.03572 0.04043 0.02859 = -0.01927 0.00098 -0.02148 AFIX 43 H5 2 0.50508 0.66965 0.38606 11.00000 -1.20000 AFIX 0 C6 1 0.60296 0.54834 0.31087 11.00000 0.03338 0.02919 0.02265 = -0.00612 -0.00762 -0.01720 AFIX 43 H6a 2 0.62761 0.48097 0.36498 11.00000 -1.20000 AFIX 0 C7 1 0.64031 0.53239 0.21998 11.00000 0.02280 0.02051 0.02283 = -0.00554 -0.00488 -0.01279 C8 1 0.72873 0.41182 0.20865 11.00000 0.02282 0.01801 0.02469 = -0.00329 -0.00781 -0.01034 AFIX 23 H8a 2 0.78320 0.37023 0.25813 11.00000 -1.20000 H8b 2 0.78585 0.42275 0.14452 11.00000 -1.20000 AFIX 0 C9 1 0.72410 0.23943 0.18611 11.00000 0.02056 0.01283 0.01265 = 0.00026 -0.00361 -0.00519 C10 1 0.85548 0.19596 0.16365 11.00000 0.01998 0.01943 0.02006 = -0.00149 -0.00602 -0.00693 AFIX 43 H10 2 0.90489 0.23336 0.17194 11.00000 -1.20000 AFIX 0 C11 1 0.91765 0.09548 0.12813 11.00000 0.01521 0.02047 0.02564 = -0.00400 -0.00336 -0.00011 AFIX 43 H11 2 1.00895 0.06537 0.11345 11.00000 -1.20000 AFIX 0 C12 1 0.84921 0.04090 0.11451 11.00000 0.02104 0.01689 0.02150 = -0.00585 -0.00200 -0.00124 AFIX 43 H12 2 0.89278 -0.02661 0.09054 11.00000 -1.20000 AFIX 0 C13 1 0.71328 0.08481 0.13608 11.00000 0.02166 0.01382 0.01375 = -0.00163 -0.00248 -0.00379 C14 1 0.63726 0.03628 0.11810 11.00000 0.02617 0.01298 0.01848 = -0.00579 -0.00308 -0.00389 AFIX 43 H14 2 0.67683 -0.02834 0.09076 11.00000 -1.20000 AFIX 0 C15 1 0.50638 0.08332 0.14046 11.00000 0.02481 0.01610 0.01752 = -0.00392 -0.00400 -0.00839 AFIX 43 H15 2 0.45383 0.05304 0.12754 11.00000 -1.20000 AFIX 0 C16 1 0.45040 0.17697 0.18277 11.00000 0.01963 0.01421 0.01451 = -0.00078 -0.00359 -0.00551 AFIX 43 H16 2 0.35930 0.20663 0.20013 11.00000 -1.20000 AFIX 0 C17 1 0.64958 0.18335 0.17457 11.00000 0.01608 0.01237 0.01133 = -0.00021 -0.00237 -0.00329 C18 1 0.31534 0.58851 0.17303 11.00000 0.01832 0.01332 0.01814 = -0.00446 -0.00168 -0.00423 C19 1 0.26935 0.69485 0.10382 11.00000 0.03032 0.01688 0.01652 = -0.00308 -0.00503 -0.00365 AFIX 43 H19 2 0.28393 0.69524 0.03933 11.00000 -1.20000 AFIX 0 C20 1 0.20059 0.80342 0.12810 11.00000 0.03471 0.01398 0.02637 = -0.00141 -0.00922 0.00059 AFIX 43 H20 2 0.17023 0.87577 0.07899 11.00000 -1.20000 AFIX 0 C21 1 0.17616 0.80811 0.21982 11.00000 0.02969 0.01412 0.02866 = -0.00815 -0.00524 -0.00010 AFIX 43 H21 2 0.12976 0.88259 0.23385 11.00000 -1.20000 AFIX 0 C22 1 0.22067 0.70102 0.29344 11.00000 0.01907 0.01791 0.02344 = -0.00802 -0.00130 -0.00595 C23 1 0.19949 0.69376 0.39083 11.00000 0.02183 0.02201 0.02628 = -0.01449 0.00030 -0.00681 AFIX 43 H23 2 0.15364 0.76442 0.41059 11.00000 -1.20000 AFIX 0 C24 1 0.24479 0.58537 0.45655 11.00000 0.02615 0.02848 0.01896 = -0.01184 -0.00171 -0.00957 AFIX 43 H24 2 0.22879 0.57975 0.52250 11.00000 -1.20000 AFIX 0 C25 1 0.31533 0.48193 0.42618 11.00000 0.02369 0.01966 0.01709 = -0.00482 -0.00431 -0.00742 AFIX 43 H25 2 0.34743 0.40702 0.47251 11.00000 -1.20000 AFIX 0 C26 1 0.29096 0.59254 0.26876 11.00000 0.01621 0.01314 0.01712 = -0.00421 -0.00121 -0.00524 C27 1 0.54180 0.19287 0.44057 11.00000 0.01648 0.01688 0.01935 = -0.00806 -0.00482 -0.00252 AFIX 43 H27 2 0.61276 0.21936 0.40292 11.00000 -1.20000 AFIX 0 C28 1 0.54801 0.11831 0.53576 11.00000 0.02242 0.02019 0.02270 = -0.01141 -0.01280 0.00456 AFIX 43 H28 2 0.62051 0.09700 0.56242 11.00000 -1.20000 AFIX 0 C29 1 0.44826 0.07716 0.58910 11.00000 0.03014 0.01422 0.01263 = -0.00357 -0.00639 0.00233 AFIX 43 H29 2 0.45142 0.02626 0.65344 11.00000 -1.20000 AFIX 0 C30 1 0.33997 0.10950 0.54958 11.00000 0.02400 0.01123 0.01404 = -0.00436 -0.00089 -0.00179 C31 1 0.23459 0.06684 0.59930 11.00000 0.03197 0.01509 0.01749 = -0.00404 0.00532 -0.00696 AFIX 43 H31 2 0.23507 0.01224 0.66263 11.00000 -1.20000 AFIX 0 C32 1 0.13290 0.10358 0.55693 11.00000 0.02321 0.02108 0.03128 = -0.01399 0.00944 -0.01136 AFIX 43 H32 2 0.06432 0.07223 0.59043 11.00000 -1.20000 AFIX 0 C33 1 0.12727 0.18739 0.46413 11.00000 0.01901 0.02453 0.02627 = -0.01563 0.00014 -0.00756 AFIX 43 H33 2 0.05380 0.21450 0.43680 11.00000 -1.20000 AFIX 0 C34 1 0.22737 0.22947 0.41368 11.00000 0.01823 0.01473 0.01727 = -0.00867 -0.00302 -0.00352 C35 1 0.33845 0.18904 0.45434 11.00000 0.01762 0.01052 0.01353 = -0.00566 -0.00228 -0.00238 C36 1 0.13224 0.35932 0.26891 11.00000 0.01931 0.02530 0.02014 = -0.00707 -0.00933 -0.00278 AFIX 23 H36a 2 0.17172 0.37031 0.19989 11.00000 -1.20000 H36b 2 0.08693 0.30044 0.28972 11.00000 -1.20000 AFIX 0 C37 1 0.03658 0.47810 0.28154 11.00000 0.01617 0.02183 0.02188 = -0.00473 -0.00173 -0.00889 C38 1 0.02080 0.51272 0.36132 11.00000 0.02580 0.02881 0.01894 = -0.00829 -0.00209 -0.01091 AFIX 43 H38 2 0.07153 0.45999 0.40898 11.00000 -1.20000 AFIX 0 C39 1 -0.06689 0.62186 0.37236 11.00000 0.03371 0.03186 0.02679 = -0.01267 -0.00075 -0.01183 AFIX 43 H39 2 -0.07554 0.64323 0.42722 11.00000 -1.20000 AFIX 0 C40 1 -0.14216 0.70030 0.30442 11.00000 0.03765 0.02738 0.03855 = -0.01854 -0.00476 -0.00154 AFIX 43 H40 2 -0.20379 0.77458 0.31288 11.00000 -1.20000 AFIX 0 C41 1 -0.12661 0.66923 0.22397 11.00000 0.03490 0.02596 0.03287 = -0.01042 -0.01288 0.00037 AFIX 43 H41 2 -0.17740 0.72289 0.17651 11.00000 -1.20000 AFIX 0 C42 1 -0.03733 0.56020 0.21186 11.00000 0.02106 0.02353 0.02442 = -0.00677 -0.00315 -0.00771 C43 1 -0.02149 0.53061 0.12310 11.00000 0.02105 0.02305 0.02192 = -0.00557 -0.00880 -0.00369 AFIX 6 O8 5 0.15175 -0.19926 0.59717 11.00000 0.03071 0.02659 0.03404 = -0.00356 -0.01153 -0.00536 H8c 2 0.14753 -0.14884 0.54130 11.00000 -1.50000 H8d 2 0.08868 -0.16383 0.63408 11.00000 -1.50000 AFIX 0 AFIX 6 O9 5 0.78362 0.87657 -0.05918 11.00000 0.04051 0.03697 0.03701 = -0.00949 -0.00817 -0.01879 H9a 2 0.85015 0.85686 -0.03702 11.00000 -1.50000 H9b 2 0.80465 0.88635 -0.11939 11.00000 -1.50000 AFIX 0 O10 5 0.13089 -0.03341 0.40767 11.00000 0.05983 0.03617 0.02109 = -0.00225 -0.00427 -0.03083 O11 5 0.27764 0.02117 0.29292 11.00000 0.02223 0.04913 0.04403 = -0.01825 0.00213 -0.01254 O12 5 0.08176 0.09367 0.27327 11.00000 0.03517 0.04087 0.04278 = -0.00975 -0.02373 0.00203 N4 4 0.16492 0.02648 0.32435 11.00000 0.02004 0.01640 0.02219 = -0.00617 -0.00525 -0.00599 HKLF 4 END Q1 1 0.527778 0.525 0.066667 11 0.05 0.65 Q2 1 0.75 0.825 -0.044444 11 0.05 0.62 Q3 1 -0.027778 0.7 0.044444 11 0.05 0.57 Q4 1 -0.055556 0.675 0.177778 11 0.05 0.51 Q5 1 0.055556 0.35 0.333333 11 0.05 0.49 Q6 1 0.083333 0.45 0.155556 11 0.05 0.45 Q7 1 0.055556 0.575 0.066667 11 0.05 0.42 Q8 1 -0.111111 0.625 0.422222 11 0.05 0.37 Q9 1 0.25 0.05 0.244444 11 0.05 0.36 Q10 1 -0.027778 0.575 0.266667 11 0.05 0.35 Q11 1 -0.083333 0.575 0.355556 11 0.05 0.31 Q12 1 0.055556 0.45 0.244444 11 0.05 0.3 Q13 1 0.305556 0.6 0.222222 11 0.05 0.3 Q14 1 0.138889 0.15 0.511111 11 0.05 0.29 Q15 1 0.333333 0.15 0.511111 11 0.05 0.29 Q16 1 0.277778 0.65 0.266667 11 0.05 0.28 Q17 1 0.222222 -0.075 0.4 11 0.05 0.28 Q18 1 0.694444 0.1 0.177778 11 0.05 0.28 Q19 1 0.388889 0.225 0.422222 11 0.05 0.27 Q20 1 0.277778 0.225 0.444444 11 0.05 0.27 REM The information below was added by Olex2. REM REM R1 = 0.0368 for 6083 Fo > 4sig(Fo) and 0.0406 for all 6608 data REM 549 parameters refined using 0 restraints REM Highest difference peak 0.6469, deepest hole -0.6896 REM Mean Shift 0.0073, Max Shift 0.8567. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0406 REM R1_gt = 0.0368 REM wR_ref = 0.1024 REM GOOF = 1.0623 REM Shift_max = 0.8567 REM Shift_mean = 0.0073 REM Reflections_all = 6608 REM Reflections_gt = 6083 REM Parameters = 549 REM Hole = -0.6896 REM Peak = 0.6469 REM Flack = n/a ; _cod_data_source_file d1ra00172h2.cif _cod_data_source_block complex2 _cod_database_code 7242667 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All O(H) groups, All O(H,H) groups 2.a Free rotating group: O8(H8c,H8d), O9(H9a,H9b) 2.b Secondary CH2 refined with riding coordinates: C8(H8a,H8b), C36(H36a,H36b) 2.c Aromatic/amide H refined with riding coordinates: C19(H19), C20(H20), C21(H21), C33(H33), C32(H32), C31(H31), C10(H10), C11(H11), C12(H12), C41(H41), C40(H40), C39(H39), C38(H38), C6(H6a), C5(H5), C4(H4), C3(H3), C27(H27), C28(H28), C29(H29), C16(H16), C15(H15), C14(H14), C25(H25), C24(H24), C23(H23) 2.d Idealised tetrahedral OH refined as rotating group: O2(H2), O6(H6) ; _iucr_refine_fcf_details ; data_29deca_0m_a _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 11.6573(7) _cell_length_b 12.7849(8) _cell_length_c 15.4024(9) _cell_angle_alpha 66.799(2) _cell_angle_beta 71.044(2) _cell_angle_gamma 65.341(2) _cell_volume 1881.8(2) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -12 -8 1 58.794 53.531 6.805 72.424 o -12 -7 1 105.253 71.266 8.308 43.799 o -12 -7 2 242.159 220.201 9.587 17.502 o -12 -6 1 125.650 117.752 9.984 32.000 o -12 -6 2 161.700 176.074 12.590 22.039 o -12 -5 1 43.860 31.859 6.363 98.733 o -12 -5 2 22.667 26.165 5.680 151.847 o -12 -5 3 361.574 408.813 18.273 8.658 o -12 -4 1 65.658 51.478 8.175 62.166 o -12 -4 2 63.920 53.880 8.002 63.257 o -12 -4 3 1.383 -2.225 3.612 885.318 o -12 -3 1 187.635 226.979 16.950 15.840 o -12 -3 2 42.864 33.136 6.607 96.895 o -12 -3 3 141.287 111.800 11.131 28.661 o -12 -2 1 531.095 495.769 25.900 5.313 o -12 -2 2 1.184 -5.913 4.886 522.814 o -12 -2 3 179.078 143.208 14.508 20.247 o -12 -1 1 641.077 616.940 29.570 4.052 o -12 -1 2 57.651 65.964 10.742 51.015 o -12 0 1 62.591 53.413 10.189 53.853 o -11 -10 1 1321.710 1288.000 33.339 1.609 o -11 -9 1 1282.740 1326.040 33.053 1.636 o -11 -9 2 0.702 1.618 4.510 592.652 o -11 -8 1 147.870 152.800 9.407 27.569 o -11 -8 2 20.813 42.820 6.807 118.862 o -11 -8 3 1.714 3.907 4.051 609.259 o -11 -7 1 1.784 -3.169 2.205 1767.150 o -11 -7 2 82.771 91.069 7.185 50.441 o -11 -7 3 67.086 61.659 6.494 66.252 o -11 -7 4 198.058 194.032 10.722 20.278 o -11 -6 1 10.959 7.572 2.223 483.473 o -11 -6 2 71.331 78.518 5.879 61.771 o -11 -6 3 527.570 543.797 15.599 6.198 o -11 -6 4 154.801 153.762 8.478 27.657 o -11 -5 1 166.646 149.583 10.483 24.705 o -11 -5 2 27.564 25.842 5.311 145.906 o -11 -5 3 23.959 29.605 6.135 136.081 o -11 -5 4 87.515 52.884 7.062 56.262 o -11 -5 5 156.069 161.154 8.319 27.237 o -11 -4 1 10.101 12.132 4.522 295.074 o -11 -4 2 580.117 629.603 22.100 4.911 o -11 -4 3 97.533 79.846 8.743 43.639 o -11 -4 4 84.115 67.688 8.326 50.621 o -11 -4 5 4.373 0.649 4.016 575.028 o -11 -3 1 200.268 236.007 16.315 15.533 o -11 -3 2 171.645 161.310 14.662 20.009 o -11 -3 3 903.459 900.647 35.588 2.513 o -11 -3 4 281.281 273.763 14.476 12.896 o -11 -3 5 226.048 221.036 13.540 16.320 o -11 -2 1 307.662 298.376 18.371 10.611 o -11 -2 2 1.582 5.493 10.010 125.686 o -11 -2 3 230.973 250.052 17.340 13.639 o -11 -2 4 3.532 0.970 4.087 587.053 o -11 -2 5 123.207 127.701 13.162 26.960 o -11 -1 1 87.321 88.935 12.026 36.737 o -11 -1 2 437.757 473.874 24.585 6.288 o -11 -1 3 163.027 179.384 40.023 6.523 o -11 -1 4 109.322 141.334 15.508 24.341 o -11 -1 5 243.721 209.457 17.246 13.930 o -11 0 1 5.144 6.917 5.431 314.103 o -11 0 2 69.918 58.474 9.983 51.188 o -11 0 3 12.122 31.901 8.394 117.458 o -11 0 4 401.617 396.315 23.089 7.278 o -11 0 5 4.608 8.420 6.957 216.612 o -11 1 1 212.240 237.641 17.405 14.440 o -11 1 2 25.307 0.715 18.233 36.056 o -11 1 3 10.909 8.580 6.190 217.116 o -11 1 4 183.134 203.391 23.595 12.414 o -11 2 1 22.235 20.153 6.266 149.347 o -11 2 2 189.577 199.143 16.734 16.488 o -11 2 3 349.425 317.900 29.673 6.916 o -11 3 1 180.993 170.307 16.862 17.451 o -10 -11 1 1.722 -6.049 5.400 422.346 o -10 -10 1 286.503 345.386 14.700 11.676 o -10 -10 2 6.145 -0.652 9.031 147.549 o -10 -10 3 375.136 376.825 15.788 9.199 o -10 -9 1 196.605 212.472 11.278 19.421 o -10 -9 2 250.110 265.796 12.537 14.849 o -10 -9 3 139.443 100.443 8.969 32.722 o -10 -9 4 682.379 601.142 20.125 4.527 o -10 -8 1 3.630 3.090 4.749 440.151 o -10 -8 2 889.548 943.281 25.718 2.815 o -10 -8 3 352.133 364.271 14.656 9.982 o -10 -8 4 173.589 135.272 9.612 25.549 o -10 -8 5 24.565 15.886 5.693 161.052 o -10 -7 1 2445.800 2284.180 41.648 0.631 o -10 -7 2 150.910 131.459 8.509 29.471 o -10 -7 3 144.000 196.335 10.490 24.631 o -10 -7 4 37.520 50.158 6.361 95.459 o -10 -7 5 56.790 53.270 8.343 65.493 o -10 -6 1 169.018 193.844 7.420 24.875 o -10 -6 2 16.677 25.807 4.462 202.862 o -10 -6 3 100.480 112.262 7.021 42.485 o -10 -6 4 207.693 165.294 8.719 21.905 o -10 -6 5 664.364 615.646 19.302 4.639 o -10 -6 6 1.243 -2.852 3.083 1176.990 o -10 -5 1 0.630 0.188 2.786 1513.360 o -10 -5 2 336.957 337.501 9.306 11.770 o -10 -5 3 466.668 418.092 11.180 8.094 o -10 -5 4 152.449 115.623 8.359 30.494 o -10 -5 5 594.942 571.800 16.483 5.439 o -10 -5 6 100.814 109.364 7.633 41.580 o -10 -4 1 459.999 492.774 18.013 6.880 o -10 -4 2 1.766 5.291 2.761 932.398 o -10 -4 3 658.499 616.119 21.112 4.556 o -10 -4 4 101.572 96.998 4.651 48.618 o -10 -4 5 141.503 132.204 7.135 32.271 o -10 -4 6 113.522 160.326 11.503 28.566 o -10 -4 7 6.878 15.521 3.870 356.738 o -10 -3 1 127.987 124.246 11.934 28.378 o -10 -3 2 40.355 58.449 8.697 71.604 o -10 -3 3 71.090 63.610 11.791 43.563 o -10 -3 4 95.815 89.420 12.124 34.981 o -10 -3 5 1137.620 1085.160 31.022 2.028 o -10 -3 6 19.548 21.048 2.894 242.191 o -10 -3 7 424.834 450.946 14.212 8.087 o -10 -2 1 96.305 71.206 9.958 41.925 o -10 -2 2 1019.500 981.347 35.172 2.222 o -10 -2 3 83.928 67.522 10.476 43.996 o -10 -2 4 450.396 464.464 18.808 7.035 o -10 -2 5 213.986 193.966 12.477 18.201 o -10 -2 6 11.028 11.685 6.599 192.639 o -10 -2 7 37.454 67.418 8.555 71.516 o -10 -1 1 673.786 646.168 27.587 3.980 o -10 -1 2 1071.510 1104.630 38.684 1.956 o -10 -1 3 932.549 886.315 34.052 2.517 o -10 -1 4 72.843 107.681 20.378 21.422 o -10 -1 5 76.599 75.604 11.440 41.903 o -10 -1 6 496.333 513.540 24.812 5.621 o -10 -1 7 410.560 407.242 18.747 7.878 o -10 0 1 3281.430 3197.980 82.130 0.334 o -10 0 2 164.448 192.084 14.685 19.492 o -10 0 3 7.943 6.983 8.223 157.487 o -10 0 4 4.802 2.319 4.925 401.771 o -10 0 5 2.135 -0.293 15.373 56.054 o -10 0 6 34.133 26.140 11.798 62.769 o -10 0 7 25.146 21.206 8.905 99.122 o -10 1 1 132.542 172.855 17.857 19.000 o -10 1 2 1.889 -1.806 4.783 521.004 o -10 1 3 314.440 291.485 19.236 10.278 o -10 1 4 3.960 6.014 5.684 312.077 o -10 1 5 471.467 417.776 23.720 6.362 o -10 1 6 138.503 147.164 16.266 21.025 o -10 1 7 95.758 95.592 13.051 32.530 o -10 2 1 333.818 312.904 19.953 9.511 o -10 2 2 1700.490 1735.270 54.351 0.953 o -10 2 3 185.458 158.935 15.444 18.621 o -10 2 4 655.689 628.515 29.567 3.963 o -10 2 5 128.495 117.789 20.556 17.952 o -10 2 6 994.059 1108.830 42.655 1.972 o -10 3 1 6.166 4.934 5.354 319.909 o -10 3 2 70.670 59.701 17.518 28.456 o -10 3 3 1641.390 1720.450 58.631 0.952 o -10 3 4 794.750 760.330 33.228 3.043 o -10 3 5 8.646 -9.370 4.783 370.889 o -10 4 1 330.633 340.812 21.621 8.896 o -10 4 2 5.182 0.964 8.580 163.120 o -10 4 3 61.388 61.877 10.476 51.541 o -10 4 4 5.966 0.000 5.309 359.432 o -9 -12 1 43.346 51.478 6.983 84.012 o -9 -11 1 480.620 510.405 30.083 5.118 o -9 -11 2 207.486 191.829 14.765 17.140 o -9 -11 3 59.637 52.054 6.653 73.160 o -9 -10 1 191.434 230.537 17.615 15.208 o -9 -10 2 678.446 788.701 28.285 3.628 o -9 -10 3 175.404 145.135 10.030 24.515 o -9 -10 4 129.412 141.634 9.606 30.320 o -9 -9 1 544.777 535.547 17.972 5.866 o -9 -9 2 120.127 136.460 9.156 32.655 o -9 -9 3 112.552 106.857 8.254 38.088 o -9 -9 4 78.620 73.575 7.543 54.083 o -9 -9 5 195.855 240.761 11.844 18.293 o -9 -8 1 3.828 -0.409 3.635 703.169 o -9 -8 2 1865.880 1910.350 43.043 0.903 o -9 -8 3 201.781 200.515 17.099 15.709 o -9 -8 4 1037.780 1105.690 28.715 2.229 o -9 -8 5 682.259 654.886 20.390 4.365 o -9 -8 6 43.807 45.410 5.755 96.004 o -9 -7 1 2363.720 2284.030 46.482 0.641 o -9 -7 2 367.006 373.263 18.301 8.846 o -9 -7 3 1014.470 1088.140 27.597 2.314 o -9 -7 4 1020.550 1046.740 27.203 2.352 o -9 -7 5 560.226 569.562 18.616 5.546 o -9 -7 6 4.950 4.938 3.358 591.472 o -9 -7 7 564.232 578.389 19.151 5.436 o -9 -6 1 123.519 126.162 10.630 30.731 o -9 -6 2 2877.840 2743.850 47.404 0.471 o -9 -6 3 77.697 89.451 6.591 54.276 o -9 -6 4 70.906 56.023 6.494 65.684 o -9 -6 5 17.350 21.915 4.078 220.571 o -9 -6 6 100.842 110.492 10.359 35.991 o -9 -6 7 72.497 71.284 7.327 57.841 o -9 -5 1 877.201 881.158 26.589 2.905 o -9 -5 2 232.146 238.507 9.143 17.740 o -9 -5 3 0.376 -1.153 2.941 1455.540 o -9 -5 4 652.225 617.842 16.664 4.866 o -9 -5 5 450.892 446.520 14.098 7.770 o -9 -5 6 334.721 356.799 14.105 10.550 o -9 -5 7 0.787 -3.743 3.251 1140.620 o -9 -5 8 217.473 189.251 10.498 19.326 o -9 -4 1 415.610 460.241 9.843 8.709 o -9 -4 2 20.430 22.604 2.570 238.390 o -9 -4 3 1291.140 1277.720 22.614 1.782 o -9 -4 4 416.056 383.371 10.640 9.274 o -9 -4 5 283.966 311.892 11.246 13.270 o -9 -4 6 30.094 34.733 4.607 139.277 o -9 -4 7 40.819 39.190 5.197 108.669 o -9 -4 8 949.094 987.528 26.632 2.585 o -9 -3 1 766.551 814.160 29.216 3.231 o -9 -3 2 118.959 130.783 11.241 30.110 o -9 -3 3 357.846 369.940 15.346 9.667 o -9 -3 4 110.043 113.349 5.625 42.296 o -9 -3 5 717.419 683.683 26.858 3.761 o -9 -3 6 8.089 4.713 2.579 589.617 o -9 -3 7 160.658 179.513 10.807 23.599 o -9 -3 8 21.368 21.188 4.293 195.968 o -9 -3 9 610.620 592.154 17.539 5.175 o -9 -2 1 3.044 5.070 6.435 268.633 o -9 -2 2 218.287 235.056 14.849 15.646 o -9 -2 3 56.588 57.243 9.178 60.291 o -9 -2 4 602.501 607.038 20.830 4.939 o -9 -2 5 232.564 235.319 9.891 17.474 o -9 -2 6 831.243 760.515 16.015 3.614 o -9 -2 7 88.886 87.776 5.594 52.865 o -9 -2 8 7.220 6.581 4.496 368.479 o -9 -2 9 2.479 4.897 3.994 570.801 o -9 -1 1 851.185 937.272 40.934 2.398 o -9 -1 2 43.379 51.199 7.960 77.062 o -9 -1 3 643.843 625.738 26.347 4.250 o -9 -1 4 477.367 489.386 23.211 6.064 o -9 -1 5 1885.150 1911.280 55.578 0.826 o -9 -1 6 192.349 182.458 6.287 23.897 o -9 -1 7 71.668 45.227 5.586 72.434 o -9 -1 8 58.336 74.574 7.482 63.193 o -9 -1 9 136.292 122.278 7.082 33.972 o -9 0 1 5474.750 5464.470 123.628 0.132 o -9 0 2 1.154 5.318 3.836 652.855 o -9 0 3 372.556 317.144 18.425 9.188 o -9 0 4 80.576 62.465 9.566 48.566 o -9 0 5 396.942 462.445 35.750 5.027 o -9 0 6 260.875 276.737 17.852 12.157 o -9 0 7 240.373 246.139 9.929 16.790 o -9 0 8 803.874 796.445 21.351 3.464 o -9 0 9 3.558 -1.771 3.579 734.772 o -9 1 1 61.278 43.677 8.331 65.726 o -9 1 2 1640.910 1634.210 49.391 1.049 o -9 1 3 376.525 388.472 20.717 8.091 o -9 1 4 253.017 261.729 17.084 12.899 o -9 1 5 296.327 331.623 24.131 8.813 o -9 1 6 200.735 263.192 24.668 10.844 o -9 1 7 39.032 47.515 8.837 75.183 o -9 1 8 39.714 36.397 11.950 57.098 o -9 1 9 16.910 17.196 5.986 177.563 o -9 2 1 955.478 899.313 33.797 2.463 o -9 2 2 45.468 66.498 13.228 44.414 o -9 2 3 142.107 171.181 31.979 9.403 o -9 2 4 236.587 252.527 17.915 13.155 o -9 2 5 6.742 5.418 5.684 286.441 o -9 2 6 843.814 807.147 59.882 1.866 o -9 2 7 70.978 63.420 11.300 45.281 o -9 2 8 1208.820 1169.670 43.463 1.647 o -9 3 1 4.321 10.140 5.493 300.719 o -9 3 2 316.629 375.376 21.163 8.962 o -9 3 3 875.016 898.370 35.476 2.581 o -9 3 4 442.182 427.474 23.600 6.609 o -9 3 5 10.601 -0.249 5.087 317.915 o -9 3 6 1.433 16.008 6.793 221.254 o -9 3 7 6.010 -3.075 5.899 304.911 o -9 3 8 141.244 128.318 14.774 23.189 o -9 4 1 49.254 48.685 3.627 101.843 o -9 4 2 23.774 19.309 4.231 190.882 o -9 4 3 6.285 5.013 8.759 148.769 o -9 4 4 649.285 630.481 29.776 3.972 o -9 4 5 1383.110 1435.750 53.804 1.228 o -9 4 6 3.417 23.774 7.837 157.774 o -9 4 7 12.244 13.228 7.078 169.165 o -9 5 1 440.281 420.148 16.177 7.806 o -9 5 2 300.045 295.993 22.410 9.537 o -9 5 3 360.049 393.192 14.967 9.487 o -9 5 4 10.544 -1.272 3.808 436.302 o -9 5 5 18.475 25.424 9.831 92.293 o -9 6 1 81.085 61.740 7.516 55.549 o -9 6 2 24.263 18.978 5.108 169.849 o -9 6 3 121.950 122.648 9.976 32.198 o -8 -12 1 20.286 19.877 4.577 196.716 o -8 -12 2 487.375 541.813 19.107 6.231 o -8 -11 1 364.411 380.874 15.175 9.478 o -8 -11 2 39.218 38.494 5.578 107.912 o -8 -11 3 246.511 252.749 11.831 15.556 o -8 -11 4 74.232 66.270 6.896 59.768 o -8 -10 1 139.666 151.566 9.117 28.943 o -8 -10 2 50.686 46.619 6.057 86.051 o -8 -10 3 88.104 106.817 8.140 44.031 o -8 -10 4 35.818 22.519 4.972 135.249 o -8 -10 5 607.313 632.064 19.596 4.919 o -8 -9 1 475.210 490.462 21.151 6.339 o -8 -9 2 807.052 837.118 23.550 3.297 o -8 -9 3 37.623 34.139 4.925 120.614 o -8 -9 4 176.390 222.943 13.844 18.567 o -8 -9 5 223.914 240.591 11.055 17.236 o -8 -9 6 152.210 135.732 8.360 29.190 o -8 -8 1 4553.220 4548.170 82.808 0.197 o -8 -8 2 426.478 427.485 14.999 8.120 o -8 -8 3 1670.520 1763.710 39.007 1.070 o -8 -8 4 1000.620 945.091 25.384 2.547 o -8 -8 5 451.707 527.244 17.446 6.853 o -8 -8 6 775.752 823.954 35.303 2.915 o -8 -8 7 122.370 110.309 7.846 36.489 o -8 -7 1 2549.090 2562.220 50.605 0.549 o -8 -7 2 89.313 85.640 6.928 49.818 o -8 -7 3 1230.340 1270.250 30.111 1.775 o -8 -7 4 40.882 31.097 5.731 109.353 o -8 -7 5 1302.260 1309.290 36.632 1.576 o -8 -7 6 622.306 580.923 22.141 4.798 o -8 -7 7 10.889 15.061 3.397 334.545 o -8 -7 8 0.687 -0.812 3.899 826.124 o -8 -6 1 324.856 299.982 10.400 12.410 o -8 -6 2 1052.520 1059.570 25.703 2.307 o -8 -6 3 375.961 381.116 13.619 9.563 o -8 -6 4 506.916 544.356 17.137 6.244 o -8 -6 5 667.096 697.939 20.361 4.333 o -8 -6 6 378.895 411.534 15.033 8.981 o -8 -6 7 5.317 3.879 3.397 591.110 o -8 -6 8 161.558 136.740 8.519 27.822 o -8 -5 1 480.612 491.841 12.036 7.319 o -8 -5 2 100.583 96.215 5.330 47.887 o -8 -5 3 1829.880 1835.930 34.160 0.986 o -8 -5 4 1529.280 1540.960 30.368 1.314 o -8 -5 5 239.677 253.861 11.091 16.148 o -8 -5 6 1670.090 1743.350 38.238 1.082 o -8 -5 7 224.444 157.942 9.961 20.202 o -8 -5 8 800.791 816.468 31.852 3.008 o -8 -5 9 105.952 131.104 9.272 35.254 o -8 -4 1 419.442 424.493 10.266 8.898 o -8 -4 2 142.235 146.448 6.001 32.211 o -8 -4 3 397.972 412.244 10.804 9.319 o -8 -4 4 44.037 45.366 3.936 109.532 o -8 -4 5 772.897 699.970 17.874 3.930 o -8 -4 6 154.906 185.370 8.765 25.666 o -8 -4 7 370.489 400.531 13.534 9.500 o -8 -4 8 89.484 65.224 6.770 53.884 o -8 -4 9 146.682 120.159 12.462 25.882 o -8 -3 1 333.974 371.697 17.149 9.690 o -8 -3 2 526.388 535.840 11.028 6.622 o -8 -3 3 31.116 29.547 2.957 165.039 o -8 -3 4 9.592 8.878 2.282 498.756 o -8 -3 5 152.246 111.116 5.807 33.628 o -8 -3 6 83.683 107.344 11.249 37.549 o -8 -3 7 706.778 753.362 19.425 4.045 o -8 -3 8 28.150 34.731 5.485 131.528 o -8 -3 9 602.533 612.254 24.127 4.669 o -8 -3 10 74.975 58.508 6.989 60.918 o -8 -2 1 1157.370 1166.600 35.681 1.852 o -8 -2 2 661.756 658.476 24.839 4.186 o -8 -2 3 110.710 111.708 14.479 27.119 o -8 -2 4 389.371 427.811 11.671 9.209 o -8 -2 5 499.561 529.200 13.391 6.754 o -8 -2 6 1483.740 1396.320 24.872 1.466 o -8 -2 7 371.669 378.819 12.520 9.871 o -8 -2 8 1439.640 1428.440 33.747 1.413 o -8 -2 9 324.757 331.032 12.542 11.466 o -8 -2 10 199.988 208.717 10.423 19.859 o -8 -1 1 1125.400 1065.960 34.096 2.002 o -8 -1 2 154.342 152.725 11.400 24.793 o -8 -1 3 925.965 934.170 31.914 2.547 o -8 -1 4 1010.320 983.571 52.553 1.784 o -8 -1 5 872.018 875.848 18.470 3.180 o -8 -1 6 3.203 5.864 2.158 952.348 o -8 -1 7 585.368 574.258 12.528 5.775 o -8 -1 8 829.102 815.678 18.121 3.448 o -8 -1 9 589.158 560.513 14.860 5.645 o -8 -1 10 637.376 653.865 16.877 4.834 o -8 0 1 861.552 855.924 30.030 2.861 o -8 0 2 85.812 97.058 10.890 39.018 o -8 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46.426 7.427 81.702 o -8 2 10 7.573 6.102 4.180 396.446 o -8 3 1 652.204 636.408 12.163 5.042 o -8 3 2 12.103 9.662 1.806 454.816 o -8 3 3 459.065 460.060 10.480 7.972 o -8 3 4 2.895 3.776 3.407 708.119 o -8 3 5 569.312 556.977 13.365 5.934 o -8 3 6 3.888 4.225 2.479 873.298 o -8 3 7 3.101 9.673 3.492 549.832 o -8 3 8 5.093 -5.011 3.756 612.035 o -8 3 9 318.325 343.392 17.558 10.162 o -8 4 1 14.675 26.358 3.474 241.511 o -8 4 2 231.325 213.223 8.136 18.946 o -8 4 3 3.815 -0.263 2.762 995.462 o -8 4 4 362.836 364.270 10.735 10.534 o -8 4 5 100.470 92.496 8.411 42.084 o -8 4 6 127.791 130.233 9.320 31.736 o -8 4 7 252.041 255.030 13.050 14.768 o -8 4 8 139.273 113.479 15.975 22.474 o -8 4 9 351.224 356.056 18.787 9.136 o -8 5 1 89.284 96.919 8.507 44.148 o -8 5 2 3.289 0.128 5.953 330.926 o -8 5 3 41.156 39.911 3.991 118.148 o -8 5 4 169.093 135.747 9.226 26.352 o -8 5 5 32.148 25.149 6.122 124.113 o -8 5 6 185.458 170.618 20.826 14.460 o -8 5 7 18.867 22.612 5.635 170.017 o -8 5 8 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240.050 o 7 6 5 1439.350 1325.990 24.505 1.553 o 7 6 6 576.493 562.763 11.264 5.981 o 7 6 7 1907.370 1930.720 28.430 0.944 o 7 6 8 89.046 73.453 4.342 58.673 o 7 6 9 1671.090 1699.010 33.953 1.123 o 7 6 10 282.090 231.285 15.838 12.998 o 7 6 11 1690.070 1680.320 49.678 1.007 o 7 6 12 590.162 598.352 27.142 4.532 o 7 6 13 382.942 384.368 16.371 8.889 o 7 6 14 1844.160 1941.380 46.159 0.889 o 7 6 15 39.009 40.523 9.551 72.243 o 7 6 16 446.032 441.858 19.250 7.149 o 7 6 17 5.350 9.755 5.706 277.797 o 7 7 0 37.223 40.579 6.025 104.870 o 7 7 1 78.887 71.112 7.324 55.191 o 7 7 2 224.428 185.898 8.621 20.022 o 7 7 3 158.876 178.094 8.358 25.979 o 7 7 4 971.921 933.502 22.722 2.696 o 7 7 5 1.294 5.351 3.247 806.772 o 7 7 6 2135.690 2009.910 71.909 0.647 o 7 7 7 1304.610 1352.750 24.234 1.698 o 7 7 8 1872.960 1832.620 30.280 0.981 o 7 7 9 1669.810 1649.140 170.333 0.339 o 7 7 10 363.416 336.476 18.200 9.231 o 7 7 11 1833.550 1855.260 53.769 0.869 o 7 7 12 661.116 699.926 28.876 3.837 o 7 7 13 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8 4 8 1138.640 1107.550 19.889 2.195 o 8 4 9 7.307 2.055 1.609 869.898 o 8 4 10 175.128 170.132 9.606 23.770 o 8 4 11 635.597 612.659 13.493 5.176 o 8 4 12 793.990 792.781 16.256 3.693 o 8 4 13 57.859 85.399 8.513 56.515 o 8 4 14 828.221 856.348 21.337 3.272 o 8 4 15 144.075 151.526 8.772 28.778 o 8 4 16 222.560 243.280 10.924 17.300 o 8 4 17 138.406 150.169 10.475 27.593 o 8 5 0 311.991 317.281 8.957 12.870 o 8 5 1 1332.060 1261.870 21.779 1.746 o 8 5 2 20.919 14.662 1.913 280.789 o 8 5 3 953.678 827.954 14.236 3.093 o 8 5 4 830.090 835.350 29.247 3.006 o 8 5 5 54.124 44.930 4.211 94.899 o 8 5 6 23.021 16.775 2.743 236.709 o 8 5 7 267.064 216.992 11.868 15.428 o 8 5 8 7.550 6.238 2.064 647.600 o 8 5 9 474.117 467.471 17.242 6.960 o 8 5 10 447.283 433.194 10.283 8.369 o 8 5 11 340.761 320.851 13.136 11.053 o 8 5 12 717.515 724.030 17.462 4.155 o 8 5 13 70.565 73.070 3.907 69.970 o 8 5 14 868.027 835.262 16.332 3.322 o 8 5 15 369.042 343.646 9.047 10.916 o 8 5 16 1099.150 1089.090 24.901 2.205 o 8 5 17 37.761 26.680 6.717 106.347 o 8 6 0 421.808 440.165 12.688 8.421 o 8 6 1 757.445 780.862 16.201 3.880 o 8 6 2 125.334 120.167 5.712 37.899 o 8 6 3 101.411 127.406 5.702 42.587 o 8 6 4 1264.750 1194.110 23.605 1.866 o 8 6 5 150.720 125.777 6.040 32.463 o 8 6 6 36.547 30.788 4.322 132.669 o 8 6 7 179.955 154.774 5.456 27.049 o 8 6 8 206.936 213.249 7.100 21.038 o 8 6 9 20.051 14.377 2.260 281.754 o 8 6 10 272.629 271.300 6.204 15.869 o 8 6 11 2034.380 1847.960 105.791 0.531 o 8 6 12 125.459 130.538 12.230 27.885 o 8 6 13 2155.910 2198.660 49.914 0.705 o 8 6 14 606.553 613.691 22.234 4.787 o 8 6 15 928.942 864.202 28.069 2.742 o 8 6 16 20.484 13.586 7.079 144.840 o 8 6 17 307.114 295.841 16.148 11.340 o 8 7 0 35.685 32.949 4.553 129.583 o 8 7 1 149.453 166.180 14.977 20.992 o 8 7 2 255.101 250.550 10.556 15.755 o 8 7 3 414.248 458.338 14.676 8.121 o 8 7 4 22.835 24.837 3.921 189.783 o 8 7 5 55.973 46.547 4.916 88.076 o 8 7 6 38.251 33.669 3.525 134.077 o 8 7 7 113.947 123.697 5.473 40.314 o 8 7 8 427.874 410.379 10.281 8.872 o 8 7 9 3.887 0.486 1.293 1674.450 o 8 7 10 135.443 151.678 12.697 25.160 o 8 7 11 618.454 609.978 26.182 4.429 o 8 7 12 576.862 633.844 27.219 4.502 o 8 7 13 949.730 926.331 28.103 2.615 o 8 7 14 87.369 88.023 9.481 43.309 o 8 7 15 1018.120 1138.940 33.593 2.127 o 8 7 16 9.412 23.649 6.193 188.114 o 8 7 17 14.136 16.590 7.112 157.051 o 8 8 0 0.488 5.253 3.139 917.687 o 8 8 1 380.943 448.041 15.129 8.632 o 8 8 2 10.048 7.327 8.468 144.518 o 8 8 3 240.573 215.438 9.850 17.594 o 8 8 4 4.385 2.417 2.206 996.593 o 8 8 5 6.941 6.491 2.743 577.725 o 8 8 6 455.126 453.397 12.320 7.879 o 8 8 7 433.982 466.301 11.871 8.142 o 8 8 8 106.140 113.901 5.511 43.409 o 8 8 9 326.974 309.772 7.450 12.819 o 8 8 10 157.431 159.585 13.020 22.588 o 8 8 11 18.592 10.010 4.367 240.492 o 8 8 12 1187.350 1221.670 57.898 1.393 o 8 8 13 0.141 2.554 4.290 652.582 o 8 8 14 513.474 504.424 29.137 5.043 o 8 8 15 66.808 67.739 10.735 47.859 o 8 8 16 215.047 274.901 20.227 12.377 o 8 8 17 2.384 8.561 4.640 422.412 o 8 9 0 685.088 698.214 20.592 4.227 o 8 9 1 988.636 1060.960 27.023 2.407 o 8 9 2 180.313 201.270 9.997 21.775 o 8 9 3 92.297 93.450 7.058 47.289 o 8 9 4 378.423 379.225 16.757 8.931 o 8 9 5 1385.340 1406.470 32.431 1.489 o 8 9 6 542.076 564.587 17.125 5.842 o 8 9 7 2802.270 2776.850 46.220 0.484 o 8 9 8 89.651 92.109 5.278 52.469 o 8 9 9 935.948 914.164 17.402 2.947 o 8 9 10 43.566 24.993 6.866 98.389 o 8 9 11 489.168 479.096 41.828 3.897 o 8 9 12 2.794 8.103 4.796 400.324 o 8 9 13 550.993 564.880 55.216 2.641 o 8 9 14 461.435 462.132 24.919 6.088 o 8 9 15 410.704 344.456 21.824 7.715 o 8 9 16 753.844 839.801 36.627 2.891 o 8 9 17 160.190 175.892 22.505 14.077 o 8 10 0 36.527 28.884 12.875 54.435 o 8 10 1 107.675 127.743 8.699 36.225 o 8 10 2 1102.970 1065.400 27.902 2.163 o 8 10 3 29.636 28.653 5.405 136.060 o 8 10 4 93.842 110.682 7.753 42.899 o 8 10 5 522.131 475.453 16.855 6.459 o 8 10 6 228.054 228.208 10.569 17.579 o 8 10 7 302.898 337.624 12.728 11.906 o 8 10 8 174.492 195.678 7.833 23.993 o 8 10 9 809.461 746.209 15.691 3.745 o 8 10 10 690.018 757.160 34.320 3.305 o 8 10 11 184.321 160.650 14.723 19.217 o 8 10 12 194.622 213.035 26.795 10.504 o 8 10 13 32.575 33.001 10.010 75.430 o 8 10 14 59.018 32.953 8.595 68.586 o 8 10 15 690.882 625.606 34.678 3.496 o 8 10 16 104.358 83.441 12.923 32.424 o 8 11 0 83.183 77.071 12.254 38.058 o 8 11 1 240.848 234.554 11.890 16.174 o 8 11 2 652.590 713.937 22.179 4.260 o 8 11 3 723.427 724.456 22.196 3.900 o 8 11 4 5.983 3.020 3.838 511.069 o 8 11 5 13.438 6.771 3.303 362.932 o 8 11 6 30.957 30.189 5.078 136.099 o 8 11 7 64.267 60.283 5.877 71.072 o 8 11 8 68.493 68.663 4.954 69.341 o 8 11 9 3.198 -1.554 5.934 334.695 o 8 11 10 571.943 578.545 27.828 4.624 o 8 11 11 16.017 22.295 7.251 141.354 o 8 11 12 4.130 3.493 4.547 451.833 o 8 11 13 19.649 6.274 9.295 110.184 o 8 11 14 66.203 51.666 10.735 50.574 o 8 11 15 50.802 50.646 10.709 56.506 o 8 11 16 425.445 481.418 42.722 4.032 o 8 12 0 628.356 635.839 34.022 3.745 o 8 12 1 20.469 25.405 5.224 169.296 o 8 12 2 179.447 176.164 12.695 20.682 o 8 12 3 1083.970 1181.290 31.575 2.027 o 8 12 4 27.311 35.401 6.659 116.240 o 8 12 5 291.370 266.988 12.672 13.311 o 8 12 6 1.908 1.653 2.926 1052.460 o 8 12 7 223.097 263.534 15.062 14.786 o 8 12 8 95.880 79.321 8.079 45.825 o 8 12 9 3.589 11.091 4.721 369.191 o 8 12 10 1040.330 1102.400 24.304 2.317 o 8 12 11 168.017 201.305 17.322 16.985 o 8 12 12 223.638 217.778 18.303 13.911 o 8 12 13 828.896 838.238 77.918 1.387 o 8 12 14 177.962 181.382 17.328 16.982 o 8 12 15 75.473 78.963 14.836 32.698 o 8 13 0 572.733 580.333 20.937 5.217 o 8 13 1 181.096 179.392 11.726 21.229 o 8 13 2 2550.310 2541.070 56.146 0.538 o 8 13 3 1.856 -4.725 3.713 807.208 o 8 13 4 789.024 841.590 26.165 3.246 o 8 13 5 156.551 148.785 10.431 25.777 o 8 13 6 37.215 25.680 5.030 128.206 o 8 13 7 29.109 38.199 6.256 116.215 o 8 13 8 44.796 32.893 5.928 100.906 o 8 13 9 94.846 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18.326 13.951 4.032 240.973 o 9 13 9 109.662 125.610 12.441 29.738 o 9 13 10 996.627 1084.920 28.294 2.337 o 9 13 11 208.631 211.696 19.264 13.974 o 9 13 12 18.079 14.618 12.513 68.458 o 9 13 13 17.728 34.367 9.116 97.358 o 9 14 4 340.694 376.388 17.203 9.511 o 9 14 5 58.581 65.671 8.211 61.988 o 9 14 6 167.202 186.206 16.503 18.019 o 9 14 7 22.282 17.993 4.876 184.520 o 9 14 8 539.085 584.200 20.974 5.441 o 9 14 9 117.905 119.560 14.710 25.669 o 9 14 10 87.498 104.617 18.928 22.613 o 9 14 11 0.573 -0.518 13.049 78.470 o 10 -4 0 28.460 18.840 7.329 118.500 o 10 -4 1 569.601 513.331 35.216 4.129 o 10 -4 2 16.255 6.291 3.937 294.246 o 10 -4 3 30.587 32.465 5.673 126.304 o 10 -4 4 322.664 328.385 22.949 8.768 o 10 -4 5 2.007 0.921 4.314 599.574 o 10 -4 6 437.676 424.578 41.734 4.198 o 10 -3 0 44.794 40.100 8.655 75.074 o 10 -3 1 112.541 110.666 13.732 28.177 o 10 -3 2 56.222 54.302 5.617 80.459 o 10 -3 3 709.966 705.404 21.483 4.041 o 10 -3 4 492.428 467.224 17.347 6.751 o 10 -3 5 3.138 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87.163 111.506 10.274 38.714 o 10 0 0 450.472 488.330 23.465 6.269 o 10 0 1 112.649 90.148 17.160 23.839 o 10 0 2 122.187 163.093 14.282 23.915 o 10 0 3 99.535 85.311 10.474 38.404 o 10 0 4 92.965 103.659 4.685 50.344 o 10 0 5 478.659 427.842 17.727 7.070 o 10 0 6 337.555 321.403 12.975 11.162 o 10 0 7 113.319 122.877 8.876 35.343 o 10 0 8 3.400 -2.037 2.871 997.406 o 10 0 9 154.857 162.814 9.772 25.898 o 10 0 10 133.814 161.496 14.126 23.209 o 10 0 11 32.058 22.740 5.134 141.397 o 10 0 12 485.416 496.491 19.446 6.424 o 10 1 0 2733.840 2671.620 70.140 0.459 o 10 1 1 2550.050 2653.580 69.267 0.495 o 10 1 2 949.375 978.055 34.389 2.378 o 10 1 3 411.251 425.057 20.717 7.419 o 10 1 4 2.684 -1.031 3.171 947.281 o 10 1 5 141.845 146.017 6.634 31.695 o 10 1 6 205.488 185.985 6.957 22.266 o 10 1 7 867.217 855.800 20.195 3.179 o 10 1 8 251.328 218.833 14.560 14.807 o 10 1 9 69.499 58.605 6.438 65.984 o 10 1 10 654.956 663.964 32.730 3.682 o 10 1 11 446.319 451.293 17.227 7.380 o 10 1 12 312.267 332.392 14.704 11.196 o 10 1 13 747.413 770.509 24.585 3.589 o 10 2 0 261.682 309.718 17.713 11.763 o 10 2 1 101.080 96.890 11.424 34.966 o 10 2 2 1337.900 1334.290 41.262 1.465 o 10 2 3 235.856 231.435 14.748 15.067 o 10 2 4 399.475 403.048 19.493 7.920 o 10 2 5 343.752 309.556 10.940 11.626 o 10 2 6 484.881 461.862 11.177 7.538 o 10 2 7 2036.400 2116.350 37.977 0.807 o 10 2 8 360.653 347.567 11.834 10.566 o 10 2 9 1671.100 1739.980 34.213 1.108 o 10 2 10 30.193 43.363 4.974 125.304 o 10 2 11 587.899 590.999 21.273 5.051 o 10 2 12 405.631 391.660 15.807 8.571 o 10 2 13 156.771 198.897 11.232 22.741 o 10 2 14 14.186 15.534 4.849 232.819 o 10 3 0 1.478 -4.734 5.720 383.861 o 10 3 1 2184.680 2147.770 57.897 0.673 o 10 3 2 206.574 182.960 19.109 14.614 o 10 3 3 14.910 22.633 5.583 186.219 o 10 3 4 61.216 57.261 4.036 82.488 o 10 3 5 345.375 327.847 10.005 11.538 o 10 3 6 1287.080 1223.230 64.136 1.225 o 10 3 7 224.570 193.527 10.728 18.643 o 10 3 8 2366.860 2350.510 41.763 0.643 o 10 3 9 506.069 522.692 15.124 6.557 o 10 3 10 493.729 544.937 16.038 6.479 o 10 3 11 322.607 328.222 12.404 11.592 o 10 3 12 120.505 133.601 8.177 34.238 o 10 3 13 315.105 359.789 13.594 11.089 o 10 3 14 7.215 19.520 4.548 285.647 o 10 4 0 18.360 19.640 5.745 174.266 o 10 4 1 136.167 170.584 12.519 24.431 o 10 4 2 550.378 560.907 23.300 5.225 o 10 4 3 1347.310 1387.020 41.285 1.432 o 10 4 4 2935.280 2902.050 46.429 0.449 o 10 4 5 604.642 582.994 14.485 5.458 o 10 4 6 391.331 395.859 15.016 8.907 o 10 4 7 1691.810 1784.560 39.554 1.048 o 10 4 8 942.287 926.837 30.143 2.572 o 10 4 9 946.507 870.165 20.689 2.900 o 10 4 10 46.424 46.172 4.997 98.188 o 10 4 11 39.672 26.747 4.211 131.529 o 10 4 12 181.095 171.537 8.898 23.729 o 10 4 13 90.441 98.922 7.194 46.704 o 10 4 14 239.924 280.725 11.479 15.391 o 10 4 15 46.152 39.828 5.412 99.255 o 10 5 0 47.036 53.933 2.771 105.681 o 10 5 1 180.482 174.998 5.369 25.927 o 10 5 2 2183.290 2099.150 31.563 0.773 o 10 5 3 164.260 159.270 6.284 28.081 o 10 5 4 8810.430 8682.100 125.348 0.060 o 10 5 5 2317.420 2228.650 38.716 0.684 o 10 5 6 153.338 135.945 8.205 29.195 o 10 5 7 629.716 635.210 19.581 4.770 o 10 5 8 64.484 84.317 7.343 58.447 o 10 5 9 86.893 88.988 9.346 43.664 o 10 5 10 0.059 0.488 2.352 2240.420 o 10 5 11 434.509 417.019 30.032 5.742 o 10 5 12 19.030 9.277 3.182 285.681 o 10 5 13 3.626 2.634 3.063 790.838 o 10 5 14 147.771 170.364 8.964 27.041 o 10 5 15 48.157 43.172 9.934 63.682 o 10 6 0 876.746 977.759 19.230 2.985 o 10 6 1 1.480 -1.325 1.708 2588.430 o 10 6 2 8143.570 7804.910 92.758 0.072 o 10 6 3 1142.720 1170.150 18.955 2.143 o 10 6 4 5238.330 5169.010 70.395 0.160 o 10 6 5 284.850 284.341 9.555 14.212 o 10 6 6 152.647 149.900 9.023 27.587 o 10 6 7 55.338 32.894 5.731 90.443 o 10 6 8 673.906 649.618 19.949 4.450 o 10 6 9 125.304 142.244 9.015 31.640 o 10 6 10 815.482 833.830 23.361 3.281 o 10 6 11 278.834 284.280 9.558 14.439 o 10 6 12 473.583 507.081 12.065 7.309 o 10 6 13 257.961 283.772 8.153 15.727 o 10 6 14 76.712 72.443 5.460 61.940 o 10 6 15 337.747 342.720 16.719 10.001 o 10 6 16 17.667 35.373 6.611 135.309 o 10 7 0 288.094 297.073 13.416 12.701 o 10 7 1 2023.980 2147.150 39.197 0.801 o 10 7 2 104.525 101.162 6.657 43.559 o 10 7 3 300.933 334.081 11.557 12.321 o 10 7 4 25.682 36.539 4.528 149.268 o 10 7 5 1040.270 1066.570 23.124 2.377 o 10 7 6 1967.630 1939.040 35.476 0.885 o 10 7 7 1.692 7.708 2.500 908.603 o 10 7 8 3.952 8.062 2.407 742.018 o 10 7 9 41.214 29.513 2.984 136.888 o 10 7 10 17.857 29.716 2.764 227.831 o 10 7 11 64.583 67.461 3.534 77.306 o 10 7 12 1316.360 1241.420 19.505 1.803 o 10 7 13 210.522 224.253 17.236 14.835 o 10 7 14 927.686 973.718 38.139 2.312 o 10 7 15 61.172 63.431 8.622 59.391 o 10 7 16 331.283 338.862 17.579 9.946 o 10 8 0 1698.030 1630.140 43.196 1.065 o 10 8 1 1008.630 977.593 25.815 2.482 o 10 8 2 388.685 395.054 15.578 8.856 o 10 8 3 10.615 5.752 3.363 417.270 o 10 8 4 2.012 0.140 2.469 1445.710 o 10 8 5 139.051 134.955 7.453 32.078 o 10 8 6 1783.280 1779.390 33.465 1.031 o 10 8 7 2593.880 2720.090 46.519 0.531 o 10 8 8 717.676 758.914 21.090 3.903 o 10 8 9 330.290 334.827 9.944 11.861 o 10 8 10 185.753 189.710 6.678 23.953 o 10 8 11 228.716 208.676 5.759 20.202 o 10 8 12 19.978 11.316 8.580 118.195 o 10 8 13 210.423 227.876 24.489 11.083 o 10 8 14 364.681 388.212 22.940 7.791 o 10 8 15 0.825 -0.788 6.078 351.558 o 10 8 16 2.898 21.257 6.078 232.086 o 10 9 0 11.694 12.348 3.697 324.393 o 10 9 1 8.322 6.598 3.397 455.254 o 10 9 2 469.788 467.024 16.576 7.095 o 10 9 3 5.935 -4.150 3.235 685.202 o 10 9 4 296.838 314.483 14.092 11.994 o 10 9 5 22.819 20.067 6.415 144.903 o 10 9 6 222.678 204.596 11.493 18.014 o 10 9 7 435.627 446.349 15.517 7.787 o 10 9 8 884.523 942.820 30.717 2.670 o 10 9 9 2145.060 2007.530 39.932 0.779 o 10 9 10 650.590 587.174 14.500 5.104 o 10 9 11 443.636 497.711 40.398 4.175 o 10 9 12 28.194 21.291 6.700 126.623 o 10 9 13 82.738 108.271 16.624 26.511 o 10 9 14 17.686 17.869 6.435 161.839 o 10 9 15 172.595 202.340 17.981 16.283 o 10 9 16 85.631 80.312 13.650 33.882 o 10 10 0 2.359 7.474 3.952 537.141 o 10 10 1 515.988 486.007 17.432 6.406 o 10 10 2 196.612 207.837 11.827 19.209 o 10 10 3 220.875 271.146 12.482 15.971 o 10 10 4 167.293 162.177 10.563 23.997 o 10 10 5 5.327 6.780 3.546 516.247 o 10 10 6 215.862 199.665 10.562 19.070 o 10 10 7 244.048 277.740 14.663 13.960 o 10 10 8 2780.340 2696.820 54.920 0.480 o 10 10 9 34.460 41.954 6.037 107.637 o 10 10 10 86.149 115.675 6.611 46.789 o 10 10 11 84.691 74.603 11.145 41.015 o 10 10 12 37.571 57.016 9.671 67.293 o 10 10 13 18.999 28.600 15.730 44.815 o 10 10 14 93.667 67.441 10.912 40.448 o 10 10 15 710.163 673.048 37.180 3.210 o 10 11 0 37.982 50.371 6.164 96.506 o 10 11 1 6.653 7.986 5.337 298.938 o 10 11 2 502.289 528.102 18.980 6.171 o 10 11 3 1093.770 1104.380 29.994 2.104 o 10 11 4 217.593 201.811 11.099 18.598 o 10 11 5 2071.100 2065.810 46.008 0.772 o 10 11 6 97.103 99.688 9.172 40.340 o 10 11 7 385.553 358.818 19.278 8.467 o 10 11 8 173.049 140.888 9.192 25.706 o 10 11 9 1357.410 1341.940 26.708 1.615 o 10 11 10 1020.710 1143.240 22.263 2.354 o 10 11 11 12.010 14.974 6.216 194.834 o 10 11 12 333.360 292.342 20.674 9.501 o 10 11 13 31.891 19.890 7.793 105.942 o 10 11 14 12.520 13.102 9.831 106.351 o 10 11 15 54.017 46.554 10.174 58.778 o 10 12 0 14.401 22.883 5.731 183.527 o 10 12 1 10.253 6.480 4.140 353.284 o 10 12 2 162.992 156.726 10.709 24.497 o 10 12 3 8.351 15.697 4.982 268.968 o 10 12 4 826.774 824.691 25.262 3.187 o 10 12 5 356.914 325.312 16.689 9.805 o 10 12 6 211.475 240.146 12.562 17.086 o 10 12 7 10.442 7.983 4.020 348.783 o 10 12 8 20.721 24.728 7.485 124.432 o 10 12 9 92.039 106.519 7.993 43.373 o 10 12 10 273.878 300.470 11.587 13.694 o 10 12 11 721.998 717.103 40.398 2.943 o 10 12 12 160.863 156.726 15.807 19.779 o 10 12 13 9.362 8.743 7.450 174.984 o 10 12 14 16.812 -1.645 12.870 70.052 o 10 13 3 284.808 204.464 12.344 14.771 o 10 13 4 506.286 545.909 20.520 5.894 o 10 13 5 239.168 253.494 13.512 15.096 o 10 13 6 18.306 19.014 5.027 195.353 o 10 13 7 6.297 12.940 4.550 332.016 o 10 13 8 2.913 -4.618 3.034 982.014 o 10 13 9 27.339 16.396 12.460 63.624 o 10 13 10 959.501 946.916 25.434 2.641 o 10 13 11 184.902 181.755 18.351 15.941 o 10 13 12 597.125 669.795 33.278 3.854 o 10 14 6 48.380 38.212 6.696 87.638 o 10 14 7 236.111 249.646 13.645 15.233 o 10 14 8 244.503 216.258 17.107 13.861 o 10 14 9 35.457 42.319 6.248 103.858 o 11 -3 0 112.881 100.518 13.909 28.419 o 11 -3 1 442.502 515.892 27.078 5.733 o 11 -3 2 644.813 644.873 30.134 3.936 o 11 -3 3 95.408 84.098 12.452 34.761 o 11 -3 4 113.462 99.290 8.246 38.699 o 11 -2 0 130.670 126.178 20.914 17.321 o 11 -2 1 6.111 15.352 6.266 221.619 o 11 -2 2 797.272 836.041 49.514 2.266 o 11 -2 3 257.723 225.966 16.662 13.486 o 11 -2 4 993.713 982.324 26.041 2.505 o 11 -2 5 367.947 329.767 13.681 10.221 o 11 -2 6 291.469 289.908 17.946 11.201 o 11 -2 7 70.663 66.321 7.317 59.840 o 11 -1 0 2.355 -6.454 4.323 602.102 o 11 -1 1 4.306 1.089 5.395 367.233 o 11 -1 2 47.355 68.299 21.808 22.098 o 11 -1 3 54.608 44.578 16.088 35.054 o 11 -1 4 246.614 234.829 28.064 9.012 o 11 -1 5 250.328 218.816 8.426 17.586 o 11 -1 6 798.854 796.773 23.250 3.408 o 11 -1 7 63.961 71.567 6.940 63.377 o 11 -1 8 206.702 246.356 12.675 17.106 o 11 -1 9 0.139 -2.897 3.468 1097.390 o 11 0 0 59.372 65.195 10.328 52.287 o 11 0 1 664.049 742.041 30.943 3.616 o 11 0 2 0.056 6.809 5.395 390.096 o 11 0 3 1114.690 1211.850 45.743 1.687 o 11 0 4 0.186 -2.094 4.290 718.613 o 11 0 5 215.247 188.685 6.234 21.730 o 11 0 6 120.972 119.598 9.292 33.652 o 11 0 7 78.654 68.559 5.971 60.315 o 11 0 8 28.996 31.037 5.099 139.325 o 11 0 9 198.750 237.690 12.475 17.846 o 11 0 10 6.022 5.062 3.766 490.629 o 11 1 0 829.065 843.298 33.334 2.835 o 11 1 1 626.195 649.446 28.392 4.131 o 11 1 2 1217.710 1279.230 42.579 1.594 o 11 1 3 355.711 377.285 20.509 8.508 o 11 1 4 489.103 498.776 23.720 5.864 o 11 1 5 477.376 509.289 12.592 7.198 o 11 1 6 31.480 30.503 3.143 160.102 o 11 1 7 852.170 756.116 18.572 3.458 o 11 1 8 3.196 -1.384 2.492 1207.800 o 11 1 9 203.905 229.249 10.318 19.037 o 11 1 10 8.232 7.840 4.242 365.175 o 11 1 11 433.866 407.263 16.521 7.928 o 11 1 12 93.332 117.007 18.478 22.409 o 11 2 0 7.146 8.987 5.431 282.862 o 11 2 1 120.233 104.568 14.658 26.243 o 11 2 2 354.618 406.650 21.122 8.183 o 11 2 3 45.925 22.464 6.097 104.639 o 11 2 4 120.710 124.922 11.847 29.341 o 11 2 5 136.457 127.892 13.406 25.304 o 11 2 6 632.627 624.013 20.158 4.748 o 11 2 7 135.531 137.886 6.936 32.984 o 11 2 8 480.881 448.256 13.851 7.398 o 11 2 9 986.901 932.967 22.402 2.666 o 11 2 10 383.998 435.247 14.648 8.766 o 11 2 11 354.097 363.419 13.776 10.139 o 11 2 12 1472.270 1470.740 32.602 1.375 o 11 3 0 53.150 71.193 10.434 52.981 o 11 3 1 20.113 12.987 5.749 180.036 o 11 3 2 1.045 7.908 4.165 536.360 o 11 3 3 232.946 246.603 15.979 14.288 o 11 3 4 195.949 200.264 13.897 18.084 o 11 3 5 171.377 144.355 8.281 26.508 o 11 3 6 387.726 394.387 12.150 9.472 o 11 3 7 6.337 8.709 4.665 350.914 o 11 3 8 541.629 530.180 18.767 5.840 o 11 3 9 0.606 -1.104 3.293 1140.620 o 11 3 10 1492.890 1388.310 47.215 1.243 o 11 3 11 346.746 363.165 13.326 10.393 o 11 3 12 485.539 559.189 17.358 6.355 o 11 3 13 0.269 1.223 4.954 518.742 o 11 4 0 423.225 470.144 22.646 6.731 o 11 4 1 105.007 108.965 12.126 32.032 o 11 4 2 88.777 77.819 10.236 42.196 o 11 4 3 407.321 464.027 21.923 7.043 o 11 4 4 6.754 1.085 3.659 545.307 o 11 4 5 850.140 850.252 17.957 3.313 o 11 4 6 496.362 478.722 16.959 6.693 o 11 4 7 1688.410 1768.450 39.933 1.052 o 11 4 8 341.076 325.275 13.995 10.787 o 11 4 9 1702.360 1645.610 38.982 1.087 o 11 4 10 154.947 146.617 7.796 28.726 o 11 4 11 189.015 195.998 12.482 19.587 o 11 4 12 7.181 9.654 3.575 428.462 o 11 4 13 199.791 204.670 10.572 19.911 o 11 4 14 9.730 2.938 3.841 418.981 o 11 5 0 7.644 14.225 4.513 310.731 o 11 5 1 228.437 242.239 12.331 16.353 o 11 5 2 33.312 20.651 4.541 149.922 o 11 5 3 289.240 268.873 15.872 12.239 o 11 5 4 908.256 867.837 17.662 3.097 o 11 5 5 375.891 397.289 11.577 9.766 o 11 5 6 932.355 929.609 20.953 2.850 o 11 5 7 237.687 231.991 11.657 16.487 o 11 5 8 1288.740 1287.930 32.245 1.662 o 11 5 9 311.236 359.829 14.949 10.833 o 11 5 10 287.804 259.839 12.954 13.448 o 11 5 11 1200.150 1124.350 44.887 1.656 o 11 5 12 15.647 25.351 4.356 212.294 o 11 5 13 5.804 -0.618 4.696 433.474 o 11 5 14 495.850 457.237 15.496 6.981 o 11 6 0 142.308 154.750 6.269 31.326 o 11 6 1 125.792 140.475 5.158 36.394 o 11 6 2 236.944 202.988 6.796 19.464 o 11 6 3 637.277 564.403 20.193 4.901 o 11 6 4 1238.210 1199.150 21.622 1.926 o 11 6 5 560.834 530.271 12.800 6.175 o 11 6 6 653.974 664.540 20.704 4.473 o 11 6 7 170.827 154.820 11.118 23.505 o 11 6 8 43.162 39.761 5.891 98.997 o 11 6 9 15.880 11.682 4.381 253.419 o 11 6 10 170.141 177.200 14.541 19.718 o 11 6 11 0.456 -0.492 3.679 943.630 o 11 6 12 411.087 419.423 15.858 8.270 o 11 6 13 12.015 7.687 4.592 294.077 o 11 6 14 421.107 452.980 23.788 6.660 o 11 6 15 13.942 3.376 6.114 218.009 o 11 7 0 1.324 8.126 5.424 356.129 o 11 7 1 605.597 608.581 12.523 5.469 o 11 7 2 0.552 -1.969 1.739 3470.060 o 11 7 3 358.690 362.248 12.524 10.311 o 11 7 4 434.913 430.769 13.555 8.177 o 11 7 5 947.355 900.778 21.177 2.842 o 11 7 6 1.864 1.116 2.531 1326.480 o 11 7 7 220.944 214.675 9.097 19.087 o 11 7 8 300.687 292.440 10.888 13.145 o 11 7 9 37.959 40.281 4.386 119.949 o 11 7 10 40.102 32.619 3.805 128.622 o 11 7 11 108.445 101.818 7.038 41.773 o 11 7 12 64.951 68.724 4.797 72.207 o 11 7 13 8.616 11.035 2.281 495.871 o 11 7 14 640.858 563.185 35.929 3.696 o 11 7 15 199.927 208.367 17.455 15.405 o 11 8 0 119.353 121.693 8.442 35.072 o 11 8 1 42.788 25.443 5.744 110.593 o 11 8 2 286.517 295.399 11.387 13.415 o 11 8 3 71.295 50.835 5.312 71.950 o 11 8 4 133.771 139.386 7.705 32.251 o 11 8 5 3.338 1.108 2.848 952.841 o 11 8 6 1433.660 1444.750 29.389 1.453 o 11 8 7 430.039 438.527 13.438 8.208 o 11 8 8 87.040 87.299 5.942 52.820 o 11 8 9 444.978 467.120 13.277 7.812 o 11 8 10 86.585 124.024 7.018 44.601 o 11 8 11 805.848 854.906 18.179 3.459 o 11 8 12 0.767 9.786 2.644 855.554 o 11 8 13 2212.820 2217.520 65.981 0.625 o 11 8 14 343.020 331.195 63.636 2.627 o 11 8 15 365.803 380.027 33.784 5.762 o 11 9 0 1.252 -2.306 3.661 876.279 o 11 9 1 198.646 169.538 10.168 21.471 o 11 9 2 134.391 156.831 9.463 28.871 o 11 9 3 27.039 28.522 5.194 145.761 o 11 9 4 182.365 192.027 10.425 21.662 o 11 9 5 120.119 105.744 13.043 28.701 o 11 9 6 265.842 308.287 13.312 13.250 o 11 9 7 73.993 89.991 7.526 52.776 o 11 9 8 729.976 761.830 21.937 3.803 o 11 9 9 61.950 69.185 5.830 69.901 o 11 9 10 321.370 366.916 11.139 11.418 o 11 9 11 533.857 527.936 12.125 6.503 o 11 9 12 811.393 827.075 62.188 1.819 o 11 9 13 544.045 521.488 91.324 1.306 o 11 9 14 424.929 385.870 23.243 7.053 o 11 9 15 331.040 360.426 36.644 5.568 o 11 10 0 25.067 37.884 7.165 111.081 o 11 10 1 1197.420 1101.650 71.136 1.212 o 11 10 2 47.381 32.976 6.131 95.974 o 11 10 3 183.123 199.374 11.188 20.791 o 11 10 4 2.586 9.433 3.648 546.831 o 11 10 5 216.031 220.439 11.394 18.000 o 11 10 6 1.026 1.984 3.251 982.774 o 11 10 7 636.222 683.211 21.013 4.500 o 11 10 8 434.437 382.072 16.080 8.167 o 11 10 9 364.927 344.526 13.046 10.262 o 11 10 10 344.650 285.808 11.272 11.844 o 11 10 11 55.111 78.205 11.706 46.134 o 11 10 12 76.819 72.579 11.507 42.003 o 11 10 13 27.502 30.922 11.440 67.577 o 11 10 14 136.391 136.035 16.403 21.387 o 11 11 0 21.928 50.997 6.864 109.849 o 11 11 1 96.803 75.235 8.546 44.948 o 11 11 2 380.475 364.096 15.665 9.242 o 11 11 3 11.160 16.384 4.288 277.154 o 11 11 4 60.412 60.103 7.190 67.391 o 11 11 5 997.137 1045.680 28.835 2.362 o 11 11 6 300.040 327.770 19.880 10.012 o 11 11 7 1141.960 1079.720 29.099 2.062 o 11 11 8 210.319 189.213 10.612 19.706 o 11 11 9 1935.100 1927.060 42.984 0.868 o 11 11 10 1.034 -1.346 6.971 267.612 o 11 11 11 221.094 188.449 28.940 9.396 o 11 11 12 210.410 232.150 19.242 13.606 o 11 11 13 66.901 112.203 20.020 22.167 o 11 11 14 148.631 134.595 16.186 20.858 o 11 12 2 115.284 138.275 10.700 30.924 o 11 12 3 0.853 -6.519 3.738 878.975 o 11 12 4 246.384 267.145 14.055 14.325 o 11 12 5 230.984 193.814 17.415 14.546 o 11 12 6 91.268 99.396 8.929 42.301 o 11 12 7 492.915 453.804 28.779 5.378 o 11 12 8 91.507 98.069 9.211 41.731 o 11 12 9 24.453 33.613 5.426 142.067 o 11 12 10 941.733 974.371 78.797 1.264 o 11 12 11 159.633 144.942 15.077 20.923 o 11 12 12 45.386 58.420 10.646 57.455 o 11 13 5 213.435 198.730 19.458 13.919 o 11 13 6 4.698 5.553 5.943 286.727 o 11 13 7 43.325 27.523 5.536 110.354 o 11 13 8 111.268 121.353 9.288 35.150 o 11 13 9 129.322 114.505 9.075 33.053 o 11 13 10 373.772 384.391 14.726 9.364 o 12 -1 0 6.195 5.685 6.443 242.222 o 12 -1 1 278.016 292.570 23.059 9.741 o 12 -1 2 331.509 345.268 21.877 8.784 o 12 -1 3 116.813 102.624 13.480 28.558 o 12 -1 4 798.959 902.743 36.547 2.708 o 12 -1 5 23.054 23.563 8.239 109.544 o 12 0 0 2.198 0.645 4.959 471.801 o 12 0 1 179.482 194.457 41.453 6.033 o 12 0 2 4.853 9.478 8.223 162.963 o 12 0 3 91.055 83.264 11.772 37.185 o 12 0 4 31.491 27.742 9.831 79.739 o 12 0 5 121.713 158.851 19.305 18.520 o 12 0 6 55.464 61.237 9.413 58.741 o 12 0 7 272.722 260.068 9.968 15.025 o 12 0 8 1.251 -3.645 3.130 1146.160 o 12 1 0 11.053 5.460 5.493 260.762 o 12 1 1 79.072 70.749 11.591 41.444 o 12 1 2 33.689 32.755 7.817 95.539 o 12 1 3 36.689 40.053 15.015 42.515 o 12 1 4 7.986 3.497 6.256 247.955 o 12 1 5 5.618 -0.323 5.291 366.581 o 12 1 6 390.199 410.122 16.998 8.456 o 12 1 7 70.337 70.207 6.514 62.125 o 12 1 8 48.579 41.113 7.327 81.459 o 12 1 9 255.800 265.213 13.359 14.309 o 12 2 0 1.513 2.153 5.408 404.254 o 12 2 1 531.846 523.561 25.959 5.209 o 12 2 2 185.064 177.777 19.645 15.128 o 12 2 3 84.674 108.046 14.479 30.301 o 12 2 4 21.116 3.218 6.435 174.863 o 12 2 5 3.705 -3.016 3.484 753.320 o 12 2 6 6.660 4.494 3.202 559.756 o 12 2 7 67.768 49.502 6.173 70.965 o 12 2 8 36.424 39.337 6.521 101.800 o 12 2 9 81.880 88.724 6.946 51.825 o 12 2 10 205.404 222.643 13.107 17.515 o 12 3 0 83.635 93.966 12.420 35.998 o 12 3 1 622.628 656.118 28.699 4.110 o 12 3 2 116.589 113.358 13.183 28.445 o 12 3 3 84.569 97.138 12.063 36.403 o 12 3 4 27.341 24.223 6.558 127.693 o 12 3 5 225.929 227.013 15.725 15.033 o 12 3 6 238.262 265.899 8.227 17.062 o 12 3 7 590.080 596.519 19.621 5.149 o 12 3 8 155.322 143.421 10.283 26.333 o 12 3 9 214.648 185.841 11.416 19.048 o 12 3 10 37.630 47.653 5.250 106.693 o 12 3 11 145.019 166.908 9.318 27.186 o 12 4 0 52.671 63.433 21.450 22.488 o 12 4 1 111.753 107.535 12.973 29.719 o 12 4 2 606.304 579.407 26.200 4.573 o 12 4 3 7.526 -4.111 8.044 176.017 o 12 4 4 195.680 171.646 13.734 19.006 o 12 4 5 58.369 61.323 9.477 57.167 o 12 4 6 14.148 24.247 3.802 242.102 o 12 4 7 1616.120 1654.550 31.951 1.190 o 12 4 8 111.907 133.151 9.553 33.608 o 12 4 9 1088.030 1077.680 29.788 2.141 o 12 4 10 23.965 7.984 4.541 208.795 o 12 4 11 564.730 526.573 20.011 5.553 o 12 4 12 228.624 224.313 15.166 15.276 o 12 5 0 30.768 40.291 6.486 109.255 o 12 5 1 14.322 26.489 5.150 192.953 o 12 5 2 22.787 16.419 4.835 186.708 o 12 5 3 40.683 38.773 7.837 85.315 o 12 5 4 324.835 338.208 30.567 6.860 o 12 5 5 151.573 184.797 13.987 21.164 o 12 5 6 79.502 78.181 5.658 58.612 o 12 5 7 45.086 50.736 5.061 96.604 o 12 5 8 7.915 14.848 4.567 300.940 o 12 5 9 100.073 97.974 15.416 27.387 o 12 5 10 609.986 650.443 21.893 4.683 o 12 5 11 133.555 135.027 14.720 23.602 o 12 5 12 272.570 283.091 21.744 10.372 o 12 5 13 1.845 2.499 3.295 860.327 o 12 6 0 230.428 257.906 18.244 13.106 o 12 6 1 335.918 395.796 16.831 9.507 o 12 6 2 92.591 79.280 8.426 45.874 o 12 6 3 104.030 113.699 9.878 36.061 o 12 6 4 233.477 246.544 7.010 18.274 o 12 6 5 89.681 122.055 5.736 46.520 o 12 6 6 26.723 28.721 4.867 151.752 o 12 6 7 35.081 30.985 5.625 119.977 o 12 6 8 228.362 255.583 12.720 15.871 o 12 6 9 37.585 35.391 6.227 105.887 o 12 6 10 498.266 526.603 19.173 6.194 o 12 6 11 41.054 43.112 6.270 96.237 o 12 6 12 260.382 243.903 22.133 10.870 o 12 6 13 11.566 9.956 5.549 237.943 o 12 7 0 156.232 126.002 6.947 30.748 o 12 7 1 245.077 285.795 10.785 15.342 o 12 7 2 801.838 797.483 19.072 3.555 o 12 7 3 51.274 46.407 3.823 99.612 o 12 7 4 310.093 298.110 14.659 11.690 o 12 7 5 35.766 54.130 6.372 95.108 o 12 7 6 37.471 31.478 4.452 128.564 o 12 7 7 64.406 89.071 7.123 58.222 o 12 7 8 35.720 31.329 4.621 130.398 o 12 7 9 1077.930 1109.190 24.738 2.229 o 12 7 10 564.828 647.098 17.231 5.328 o 12 7 11 292.040 302.536 10.724 13.309 o 12 7 12 522.079 504.305 14.156 6.578 o 12 7 13 13.501 9.702 4.378 281.803 o 12 8 0 129.613 105.858 11.620 29.766 o 12 8 1 3.175 -2.084 2.991 971.678 o 12 8 2 150.374 153.067 10.573 26.038 o 12 8 3 66.273 45.305 7.299 67.758 o 12 8 4 136.432 129.210 12.015 27.043 o 12 8 5 175.227 146.845 8.391 25.875 o 12 8 6 207.641 189.887 11.600 19.232 o 12 8 7 3.566 2.329 2.688 926.277 o 12 8 8 250.046 271.766 10.630 15.487 o 12 8 9 32.814 24.392 4.541 146.270 o 12 8 10 80.485 79.302 5.941 57.104 o 12 8 11 210.401 236.272 8.823 19.206 o 12 8 12 5.406 7.593 2.619 637.796 o 12 8 13 287.478 266.687 31.639 7.301 o 12 9 0 5.729 8.931 3.768 448.586 o 12 9 1 47.868 60.447 11.972 49.800 o 12 9 2 101.911 94.359 8.520 41.276 o 12 9 3 26.404 17.532 6.569 136.473 o 12 9 4 202.877 231.392 11.865 18.152 o 12 9 5 131.872 131.778 9.215 31.180 o 12 9 6 173.138 167.215 14.631 19.763 o 12 9 7 3.889 3.630 3.671 603.419 o 12 9 8 62.397 84.721 8.301 55.624 o 12 9 9 153.640 151.356 9.302 27.108 o 12 9 10 35.344 37.041 4.452 127.251 o 12 9 11 36.133 39.599 6.216 105.106 o 12 9 12 23.499 25.953 7.634 116.141 o 12 9 13 41.618 33.879 8.908 77.703 o 12 10 1 123.354 121.880 10.456 31.315 o 12 10 2 49.034 41.891 6.547 86.388 o 12 10 3 79.417 69.881 7.914 53.255 o 12 10 4 121.543 149.015 9.933 30.445 o 12 10 5 257.797 340.858 19.848 10.739 o 12 10 6 1.388 -0.875 7.874 209.406 o 12 10 7 148.334 132.025 9.421 28.730 o 12 10 8 72.796 110.762 9.675 43.604 o 12 10 9 796.437 863.753 24.428 3.254 o 12 10 10 28.125 25.061 4.109 165.800 o 12 10 11 771.034 763.211 20.830 3.678 o 12 10 12 169.117 209.067 17.786 16.427 o 12 10 13 20.826 1.367 6.413 180.039 o 12 11 3 52.208 41.945 6.463 84.052 o 12 11 4 46.214 47.011 6.939 83.774 o 12 11 5 59.780 94.898 12.003 41.842 o 12 11 6 159.114 181.410 19.999 15.781 o 12 11 7 13.791 11.585 5.848 207.781 o 12 11 8 183.399 165.070 14.171 19.588 o 12 11 9 325.123 342.279 22.708 8.691 o 12 11 10 125.980 137.006 8.389 32.775 o 12 11 11 578.425 614.740 30.494 4.271 o 12 11 12 22.026 17.608 11.619 73.274 o 12 12 5 84.723 65.701 8.134 51.366 o 12 12 6 153.303 162.852 11.025 24.802 o 12 12 7 0.429 -2.592 3.546 1014.780 o 12 12 8 210.240 209.047 11.873 18.357 o 12 12 9 3.542 -1.433 3.734 692.727 o 12 12 10 9.883 3.115 7.865 168.855 o 13 2 1 490.785 456.086 25.349 5.817 o 13 2 2 95.725 110.727 14.096 29.505 o 13 2 3 33.912 35.961 8.501 86.792 o 13 2 4 60.364 49.322 8.950 61.517 o 13 2 5 90.637 71.037 11.046 40.362 o 13 2 6 30.226 30.206 8.242 96.175 o 13 2 7 98.195 117.352 22.344 17.520 o 13 3 0 200.169 219.979 17.264 15.288 o 13 3 1 220.325 172.930 17.778 15.106 o 13 3 2 34.364 36.227 9.417 78.031 o 13 3 3 113.775 138.154 15.010 24.775 o 13 3 4 78.085 54.616 16.624 29.844 o 13 3 5 87.591 68.230 10.688 42.373 o 13 3 6 377.311 398.058 22.091 7.744 o 13 3 7 556.063 630.275 28.309 4.528 o 13 3 8 10.883 5.915 6.442 213.427 o 13 4 0 82.313 111.908 16.429 26.715 o 13 4 1 35.742 36.873 9.653 74.855 o 13 4 2 55.224 55.758 19.484 26.102 o 13 4 3 36.020 43.153 8.837 79.006 o 13 4 4 6.373 17.637 6.700 196.280 o 13 4 5 7.171 4.886 5.237 317.794 o 13 4 6 124.366 120.688 13.270 27.052 o 13 4 7 67.848 44.731 5.656 74.968 o 13 4 8 407.236 361.866 15.258 8.881 o 13 4 9 360.726 414.687 17.288 8.824 o 13 4 10 25.967 24.916 5.701 144.402 o 13 5 0 118.106 146.142 11.355 29.078 o 13 5 1 487.979 500.331 20.020 6.313 o 13 5 2 1.690 -5.770 3.925 746.162 o 13 5 3 3.065 4.656 5.222 377.582 o 13 5 4 301.240 309.178 33.248 6.613 o 13 5 5 1.820 -0.986 4.165 666.741 o 13 5 6 117.147 141.772 13.539 26.328 o 13 5 7 10.856 12.335 3.789 329.492 o 13 5 8 2.530 2.879 5.978 320.972 o 13 5 9 40.187 27.380 6.453 105.425 o 13 5 10 86.790 98.113 9.869 41.228 o 13 6 0 106.116 122.839 11.153 32.611 o 13 6 1 146.796 156.335 11.571 25.152 o 13 6 2 133.654 117.016 14.551 24.571 o 13 6 3 57.013 76.590 11.986 44.820 o 13 6 4 1.870 0.076 3.642 829.205 o 13 6 5 459.111 419.029 20.460 6.952 o 13 6 6 1.359 16.209 5.169 325.063 o 13 6 7 244.066 271.073 13.195 14.705 o 13 6 8 11.504 17.194 4.503 260.638 o 13 6 9 267.719 259.828 15.579 13.104 o 13 6 10 143.675 165.536 16.665 19.728 o 13 6 11 28.874 25.406 6.018 131.891 o 13 7 1 7.938 2.070 6.338 248.686 o 13 7 2 1223.380 1153.150 49.643 1.533 o 13 7 3 4.202 -2.021 4.690 472.014 o 13 7 4 2412.300 2273.900 50.525 0.617 o 13 7 5 5.065 4.394 2.672 732.701 o 13 7 6 3.114 -5.499 4.851 474.397 o 13 7 7 33.489 33.347 4.614 133.076 o 13 7 8 150.118 155.256 11.657 24.798 o 13 7 9 79.813 54.230 6.470 61.541 o 13 7 10 277.696 254.606 11.765 14.313 o 13 7 11 534.149 563.747 20.320 5.617 o 13 8 2 632.044 548.381 21.714 4.870 o 13 8 3 51.288 53.825 6.869 77.312 o 13 8 4 1373.920 1294.790 37.870 1.493 o 13 8 5 0.138 -4.895 2.946 1511.040 o 13 8 6 305.345 299.261 11.477 12.728 o 13 8 7 38.358 39.552 7.444 90.617 o 13 8 8 47.379 54.708 5.867 86.612 o 13 8 9 9.059 10.571 4.489 317.018 o 13 8 10 6.039 4.620 4.388 418.000 o 13 8 11 124.261 114.008 11.610 29.944 o 13 9 3 76.702 68.285 9.607 48.732 o 13 9 4 408.457 414.174 22.213 7.257 o 13 9 5 2.325 6.765 3.790 580.270 o 13 9 6 111.270 102.116 7.547 40.146 o 13 9 7 99.871 81.162 6.991 47.010 o 13 9 8 295.120 331.252 23.014 9.150 o 13 9 9 33.540 25.163 4.030 150.481 o 13 9 10 124.368 160.157 10.608 28.482 o 13 9 11 76.838 85.279 6.847 54.684 o 13 10 5 1.922 -6.539 3.468 896.863 o 13 10 6 7.181 2.360 3.898 478.221 o 13 10 7 390.355 396.821 16.082 8.723 o 13 10 8 77.793 76.910 17.010 27.847 o 13 10 9 450.377 446.479 16.970 7.395 o 13 10 10 18.737 5.785 4.143 264.236 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Cu1 Cu 0.42571(2) 0.35286(2) 0.272073(17) 0.01334(10) Uani 1.000000 . O1 O 0.69862(18) 0.68892(16) -0.02543(13) 0.0293(4) Uani 1.000000 . O2 O 0.6075(2) 0.54446(18) 0.02650(14) 0.0377(5) Uani 1.000000 . H2 H 0.625(3) 0.552(2) -0.0325(3) 0.0565(7) Uiso 1.000000 GR O3 O 0.65466(15) 0.33817(14) 0.21864(11) 0.0174(3) Uani 1.000000 . O4 O 0.38274(15) 0.48202(13) 0.15651(11) 0.0168(3) Uani 1.000000 . O5 O 0.23260(15) 0.31174(15) 0.32408(11) 0.0195(3) Uani 1.000000 . O6 O -0.0318(3) 0.6227(2) 0.04195(17) 0.0548(6) Uani 1.000000 . H6 H -0.019(4) 0.5971(7) -0.0042(6) 0.0823(9) Uiso 1.000000 GR O7 O -0.00030(17) 0.42566(16) 0.12772(12) 0.0251(4) Uani 1.000000 . N1 N 0.51764(18) 0.22637(16) 0.19987(13) 0.0145(4) Uani 1.000000 . N2 N 0.33867(18) 0.48516(17) 0.33516(13) 0.0164(4) Uani 1.000000 . N3 N 0.44117(17) 0.22791(16) 0.40094(13) 0.0135(4) Uani 1.000000 . C1 C 0.6409(2) 0.6246(2) 0.04018(17) 0.0203(5) Uani 1.000000 . C2 C 0.6036(2) 0.6328(2) 0.14109(17) 0.0207(5) Uani 1.000000 . C3 C 0.5329(2) 0.7461(2) 0.15417(19) 0.0256(5) Uani 1.000000 . H3 H 0.5103(2) 0.8146(2) 0.10022(19) 0.0308(7) Uiso 1.000000 R C4 C 0.4956(3) 0.7597(2) 0.2451(2) 0.0304(6) Uani 1.000000 . H4 H 0.4459(3) 0.8369(2) 0.2537(2) 0.0365(7) Uiso 1.000000 R C5 C 0.5307(3) 0.6606(3) 0.3235(2) 0.0307(6) Uani 1.000000 . H5 H 0.5051(3) 0.6697(3) 0.3861(2) 0.0368(7) Uiso 1.000000 R C6 C 0.6030(3) 0.5483(2) 0.31087(18) 0.0259(5) Uani 1.000000 . H6a H 0.6276(3) 0.4810(2) 0.36498(18) 0.0311(7) Uiso 1.000000 R C7 C 0.6403(2) 0.5324(2) 0.21998(17) 0.0202(5) Uani 1.000000 . C8 C 0.7287(2) 0.4118(2) 0.20865(18) 0.0207(5) Uani 1.000000 . H8a H 0.7832(2) 0.3702(2) 0.25813(18) 0.0249(6) Uiso 1.000000 R H8b H 0.7859(2) 0.4227(2) 0.14452(18) 0.0249(6) Uiso 1.000000 R C9 C 0.7241(2) 0.2394(2) 0.18611(15) 0.0167(5) Uani 1.000000 . C10 C 0.8555(2) 0.1960(2) 0.16365(17) 0.0206(5) Uani 1.000000 . H10 H 0.9049(2) 0.2334(2) 0.17194(17) 0.0247(6) Uiso 1.000000 R C11 C 0.9176(2) 0.0955(2) 0.12813(18) 0.0237(5) Uani 1.000000 . H11 H 1.0090(2) 0.0654(2) 0.11345(18) 0.0284(6) Uiso 1.000000 R C12 C 0.8492(2) 0.0409(2) 0.11451(17) 0.0222(5) Uani 1.000000 . H12 H 0.8928(2) -0.0266(2) 0.09054(17) 0.0266(6) Uiso 1.000000 R C13 C 0.7133(2) 0.0848(2) 0.13608(16) 0.0183(5) Uani 1.000000 . C14 C 0.6373(2) 0.0363(2) 0.11810(16) 0.0201(5) Uani 1.000000 . H14 H 0.6768(2) -0.0283(2) 0.09076(16) 0.0241(6) Uiso 1.000000 R C15 C 0.5064(2) 0.0833(2) 0.14046(16) 0.0193(5) Uani 1.000000 . H15 H 0.4538(2) 0.0530(2) 0.12754(16) 0.0232(6) Uiso 1.000000 R C16 C 0.4504(2) 0.1770(2) 0.18277(16) 0.0173(5) Uani 1.000000 . H16 H 0.3593(2) 0.2066(2) 0.20013(16) 0.0207(6) Uiso 1.000000 R C17 C 0.6496(2) 0.18335(19) 0.17457(15) 0.0150(4) Uani 1.000000 . C18 C 0.3153(2) 0.5885(2) 0.17303(16) 0.0175(5) Uani 1.000000 . C19 C 0.2694(2) 0.6948(2) 0.10382(17) 0.0233(5) Uani 1.000000 . H19 H 0.2839(2) 0.6952(2) 0.03933(17) 0.0279(6) Uiso 1.000000 R C20 C 0.2006(3) 0.8034(2) 0.12810(19) 0.0288(6) Uani 1.000000 . H20 H 0.1702(3) 0.8758(2) 0.07899(19) 0.0346(7) Uiso 1.000000 R C21 C 0.1762(2) 0.8081(2) 0.21982(18) 0.0263(5) Uani 1.000000 . H21 H 0.1298(2) 0.8826(2) 0.23385(18) 0.0315(7) Uiso 1.000000 R C22 C 0.2207(2) 0.7010(2) 0.29344(17) 0.0204(5) Uani 1.000000 . C23 C 0.1995(2) 0.6938(2) 0.39083(18) 0.0224(5) Uani 1.000000 . H23 H 0.1536(2) 0.7644(2) 0.41059(18) 0.0269(6) Uiso 1.000000 R C24 C 0.2448(2) 0.5854(2) 0.45655(18) 0.0235(5) Uani 1.000000 . H24 H 0.2288(2) 0.5798(2) 0.52250(18) 0.0282(6) Uiso 1.000000 R C25 C 0.3153(2) 0.4819(2) 0.42618(17) 0.0202(5) Uani 1.000000 . H25 H 0.3474(2) 0.4070(2) 0.47251(17) 0.0242(6) Uiso 1.000000 R C26 C 0.2910(2) 0.5925(2) 0.26876(16) 0.0160(4) Uani 1.000000 . C27 C 0.5418(2) 0.1929(2) 0.44057(16) 0.0174(5) Uani 1.000000 . H27 H 0.6128(2) 0.2194(2) 0.40292(16) 0.0209(6) Uiso 1.000000 R C28 C 0.5480(2) 0.1183(2) 0.53576(17) 0.0220(5) Uani 1.000000 . H28 H 0.6205(2) 0.0970(2) 0.56242(17) 0.0264(6) Uiso 1.000000 R C29 C 0.4483(2) 0.0772(2) 0.58910(16) 0.0220(5) Uani 1.000000 . H29 H 0.4514(2) 0.0263(2) 0.65344(16) 0.0264(6) Uiso 1.000000 R C30 C 0.3400(2) 0.1095(2) 0.54958(16) 0.0184(5) Uani 1.000000 . C31 C 0.2346(2) 0.0668(2) 0.59930(17) 0.0248(5) Uani 1.000000 . H31 H 0.2351(2) 0.0122(2) 0.66263(17) 0.0298(7) Uiso 1.000000 R C32 C 0.1329(2) 0.1036(2) 0.55693(19) 0.0256(6) Uani 1.000000 . H32 H 0.0643(2) 0.0722(2) 0.59043(19) 0.0308(7) Uiso 1.000000 R C33 C 0.1273(2) 0.1874(2) 0.46413(18) 0.0217(5) Uani 1.000000 . H33 H 0.0538(2) 0.2145(2) 0.43680(18) 0.0260(6) Uiso 1.000000 R C34 C 0.2274(2) 0.2295(2) 0.41368(16) 0.0163(5) Uani 1.000000 . C35 C 0.3384(2) 0.18904(19) 0.45434(15) 0.0142(4) Uani 1.000000 . C36 C 0.1322(2) 0.3593(2) 0.26891(17) 0.0217(5) Uani 1.000000 . H36a H 0.1717(2) 0.3703(2) 0.19989(17) 0.0260(6) Uiso 1.000000 R H36b H 0.0869(2) 0.3004(2) 0.28972(17) 0.0260(6) Uiso 1.000000 R C37 C 0.0366(2) 0.4781(2) 0.28154(17) 0.0202(5) Uani 1.000000 . C38 C 0.0208(2) 0.5127(2) 0.36132(17) 0.0241(5) Uani 1.000000 . H38 H 0.0715(2) 0.4600(2) 0.40898(17) 0.0289(6) Uiso 1.000000 R C39 C -0.0669(3) 0.6219(2) 0.37236(19) 0.0305(6) Uani 1.000000 . H39 H -0.0755(3) 0.6432(2) 0.42722(19) 0.0366(7) Uiso 1.000000 R C40 C -0.1422(3) 0.7003(3) 0.3044(2) 0.0357(7) Uani 1.000000 . H40 H -0.2038(3) 0.7746(3) 0.3129(2) 0.0428(8) Uiso 1.000000 R C41 C -0.1266(3) 0.6692(2) 0.2240(2) 0.0328(6) Uani 1.000000 . H41 H -0.1774(3) 0.7229(2) 0.1765(2) 0.0393(7) Uiso 1.000000 R C42 C -0.0373(2) 0.5602(2) 0.21186(18) 0.0234(5) Uani 1.000000 . C43 C -0.0215(2) 0.5306(2) 0.12310(17) 0.0225(5) Uani 1.000000 . O8 O 0.15175(18) -0.19926(17) 0.59717(14) 0.0324(4) Uani 1.000000 . H8c H 0.148(3) -0.149(2) 0.5413(8) 0.0486(7) Uiso 1.000000 G H8d H 0.089(2) -0.164(2) 0.6341(15) 0.0486(7) Uiso 1.000000 G O9 O 0.7836(2) 0.87657(19) -0.05918(15) 0.0364(5) Uani 1.000000 . H9a H 0.8502(16) 0.857(3) -0.0370(18) 0.0546(7) Uiso 1.000000 G H9b H 0.805(3) 0.886(3) -0.1194(5) 0.0546(7) Uiso 1.000000 G O10 O 0.1309(2) -0.03341(18) 0.40767(13) 0.0368(5) Uani 1.000000 . O11 O 0.27764(18) 0.0212(2) 0.29292(15) 0.0391(5) Uani 1.000000 . O12 O 0.08176(19) 0.09367(19) 0.27327(15) 0.0415(5) Uani 1.000000 . N4 N 0.16492(18) 0.02648(17) 0.32435(14) 0.0191(4) Uani 1.000000 . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cu1 0.01690(16) 0.00991(15) 0.01061(15) -0.00352(11) -0.00236(10) -0.00173(10) O1 0.0354(10) 0.0290(10) 0.0234(9) -0.0196(8) -0.0026(8) -0.0006(8) O2 0.0449(12) 0.0366(11) 0.0305(11) -0.0146(9) -0.0049(9) -0.0098(9) O3 0.0175(8) 0.0147(8) 0.0208(8) -0.0066(6) -0.0026(6) -0.0057(7) O4 0.0212(8) 0.0124(8) 0.0131(7) -0.0036(6) -0.0016(6) -0.0034(6) O5 0.0197(8) 0.0225(8) 0.0162(8) -0.0044(7) -0.0090(6) -0.0040(7) O6 0.0772(18) 0.0454(14) 0.0400(13) -0.0147(13) -0.0207(12) -0.0094(11) O7 0.0272(9) 0.0256(10) 0.0239(9) -0.0063(7) -0.0083(7) -0.0088(7) N1 0.0173(9) 0.0118(9) 0.0107(9) -0.0048(7) -0.0033(7) 0.0009(7) N2 0.0191(10) 0.0153(9) 0.0138(9) -0.0064(8) -0.0018(7) -0.0037(8) N3 0.0147(9) 0.0114(9) 0.0142(9) -0.0039(7) -0.0033(7) -0.0036(7) C1 0.0198(12) 0.0164(11) 0.0217(12) -0.0058(9) -0.0052(9) -0.0020(10) C2 0.0206(12) 0.0197(12) 0.0242(12) -0.0111(10) -0.0022(10) -0.0060(10) C3 0.0284(13) 0.0180(12) 0.0312(14) -0.0107(10) -0.0048(11) -0.0056(11) C4 0.0294(14) 0.0269(14) 0.0419(16) -0.0127(11) -0.0001(12) -0.0191(12) C5 0.0357(15) 0.0404(16) 0.0286(14) -0.0215(13) 0.0010(11) -0.0193(12) C6 0.0334(14) 0.0292(14) 0.0226(12) -0.0172(11) -0.0076(10) -0.0061(11) C7 0.0228(12) 0.0205(12) 0.0228(12) -0.0128(10) -0.0049(9) -0.0055(10) C8 0.0228(12) 0.0180(12) 0.0247(12) -0.0103(10) -0.0078(10) -0.0033(10) C9 0.0206(12) 0.0128(11) 0.0127(10) -0.0052(9) -0.0036(9) 0.0003(9) C10 0.0200(12) 0.0194(12) 0.0201(12) -0.0069(10) -0.0060(9) -0.0015(10) C11 0.0152(12) 0.0205(12) 0.0256(13) -0.0001(9) -0.0034(9) -0.0040(10) C12 0.0210(12) 0.0169(12) 0.0215(12) -0.0012(10) -0.0020(10) -0.0059(10) C13 0.0217(12) 0.0138(11) 0.0138(11) -0.0038(9) -0.0025(9) -0.0016(9) C14 0.0262(13) 0.0130(11) 0.0185(11) -0.0039(9) -0.0031(9) -0.0058(9) C15 0.0248(12) 0.0161(11) 0.0175(11) -0.0084(10) -0.0040(9) -0.0039(9) C16 0.0196(12) 0.0142(11) 0.0145(11) -0.0055(9) -0.0036(9) -0.0008(9) C17 0.0161(11) 0.0124(10) 0.0113(10) -0.0033(9) -0.0024(8) -0.0002(8) C18 0.0183(11) 0.0133(11) 0.0181(11) -0.0042(9) -0.0017(9) -0.0045(9) C19 0.0303(13) 0.0169(12) 0.0165(12) -0.0036(10) -0.0050(10) -0.0031(10) C20 0.0347(15) 0.0140(12) 0.0264(13) 0.0006(10) -0.0092(11) -0.0014(10) C21 0.0297(14) 0.0141(12) 0.0287(13) -0.0001(10) -0.0052(11) -0.0081(10) C22 0.0191(12) 0.0179(12) 0.0234(12) -0.0060(9) -0.0013(9) -0.0080(10) C23 0.0218(12) 0.0220(12) 0.0263(13) -0.0068(10) 0.0003(10) -0.0145(10) C24 0.0262(13) 0.0285(13) 0.0190(12) -0.0096(11) -0.0017(10) -0.0118(10) C25 0.0237(12) 0.0197(12) 0.0171(11) -0.0074(10) -0.0043(9) -0.0048(10) C26 0.0162(11) 0.0131(11) 0.0171(11) -0.0052(9) -0.0012(9) -0.0042(9) C27 0.0165(11) 0.0169(11) 0.0194(11) -0.0025(9) -0.0048(9) -0.0081(9) C28 0.0224(12) 0.0202(12) 0.0227(12) 0.0046(10) -0.0128(10) -0.0114(10) C29 0.0301(13) 0.0142(11) 0.0126(11) 0.0023(10) -0.0064(10) -0.0036(9) C30 0.0240(12) 0.0112(10) 0.0140(11) -0.0018(9) -0.0009(9) -0.0044(9) C31 0.0320(14) 0.0151(11) 0.0175(12) -0.0070(10) 0.0053(10) -0.0040(10) C32 0.0232(13) 0.0211(12) 0.0313(14) -0.0114(10) 0.0094(10) -0.0140(11) C33 0.0190(12) 0.0245(12) 0.0263(13) -0.0076(10) 0.0001(10) -0.0156(11) C34 0.0182(11) 0.0147(11) 0.0173(11) -0.0035(9) -0.0030(9) -0.0087(9) C35 0.0176(11) 0.0105(10) 0.0135(10) -0.0024(8) -0.0023(8) -0.0057(8) C36 0.0193(12) 0.0253(13) 0.0201(12) -0.0028(10) -0.0093(9) -0.0071(10) C37 0.0162(11) 0.0218(12) 0.0219(12) -0.0089(10) -0.0017(9) -0.0047(10) C38 0.0258(13) 0.0288(13) 0.0189(12) -0.0109(11) -0.0021(10) -0.0083(10) C39 0.0337(15) 0.0319(15) 0.0268(14) -0.0118(12) -0.0008(11) -0.0127(12) C40 0.0377(16) 0.0274(14) 0.0386(16) -0.0015(12) -0.0048(13) -0.0185(13) C41 0.0349(15) 0.0260(14) 0.0329(15) 0.0004(12) -0.0129(12) -0.0104(12) C42 0.0211(12) 0.0235(13) 0.0244(13) -0.0077(10) -0.0031(10) -0.0068(10) C43 0.0211(12) 0.0230(13) 0.0219(12) -0.0037(10) -0.0088(10) -0.0056(10) O8 0.0307(11) 0.0266(10) 0.0340(11) -0.0054(8) -0.0115(8) -0.0036(8) O9 0.0405(12) 0.0370(11) 0.0370(11) -0.0188(10) -0.0082(9) -0.0095(10) O10 0.0598(14) 0.0362(11) 0.0211(10) -0.0308(10) -0.0043(9) -0.0023(8) O11 0.0222(10) 0.0491(13) 0.0440(12) -0.0125(9) 0.0021(9) -0.0183(10) O12 0.0352(11) 0.0409(12) 0.0428(12) 0.0020(9) -0.0237(10) -0.0097(10) N4 0.0200(11) 0.0164(10) 0.0222(10) -0.0060(8) -0.0052(8) -0.0062(8) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Cu 0.34125 1.28947 13.33800 7.16760 5.61580 1.67350 3.58280 0.24700 11.39660 64.81260 1.19099998474 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _citation_id _citation_doi _citation_year 1 10.1016/j.bioorg.2021.104772 2021 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Cu1 O3 91.40(6) . . ? O5 Cu1 O3 164.44(6) . . ? O5 Cu1 O4 96.96(6) . . ? N1 Cu1 O3 72.18(6) . . ? N1 Cu1 O4 92.61(7) . . ? N1 Cu1 O5 94.28(7) . . ? N2 Cu1 O3 105.96(6) . . ? N2 Cu1 O4 84.18(7) . . ? N2 Cu1 O5 87.99(7) . . ? N2 Cu1 N1 176.28(7) . . ? N3 Cu1 O3 96.97(6) . . ? N3 Cu1 O4 171.08(7) . . ? N3 Cu1 O5 75.61(6) . . ? N3 Cu1 N1 92.87(7) . . ? N3 Cu1 N2 90.55(7) . . ? C1 O2 H2 109.5 . . ? C8 O3 Cu1 135.53(13) . . ? C9 O3 Cu1 109.57(12) . . ? C9 O3 C8 114.77(17) . . ? C18 O4 Cu1 112.51(13) . . ? C34 O5 Cu1 111.16(13) . . ? C36 O5 Cu1 126.18(14) . . ? C36 O5 C34 122.57(18) . . ? C43 O6 H6 109.5 . . ? C16 N1 Cu1 119.94(15) . . ? C17 N1 Cu1 121.79(15) . . ? C17 N1 C16 118.08(19) . . ? C25 N2 Cu1 131.36(16) . . ? C26 N2 Cu1 109.63(14) . . ? C26 N2 C25 118.8(2) . . ? C27 N3 Cu1 121.27(15) . . ? C35 N3 Cu1 119.10(14) . . ? C35 N3 C27 119.12(19) . . ? O2 C1 O1 122.6(2) . . ? C2 C1 O1 120.9(2) . . ? C2 C1 O2 116.4(2) . . ? C3 C2 C1 117.7(2) . . ? C7 C2 C1 122.3(2) . . ? C7 C2 C3 119.9(2) . . ? H3 C3 C2 119.75(15) . . ? C4 C3 C2 120.5(2) . . ? C4 C3 H3 119.75(16) . . ? H4 C4 C3 120.08(16) . . ? C5 C4 C3 119.8(2) . . ? C5 C4 H4 120.08(16) . . ? H5 C5 C4 120.00(16) . . ? C6 C5 C4 120.0(2) . . ? C6 C5 H5 120.00(16) . . ? H6a C6 C5 119.45(16) . . ? C7 C6 C5 121.1(2) . . ? C7 C6 H6a 119.45(15) . . ? C6 C7 C2 118.6(2) . . ? C8 C7 C2 122.2(2) . . ? C8 C7 C6 119.0(2) . . ? C7 C8 O3 110.26(18) . . ? H8a C8 O3 109.60(11) . . ? H8a C8 C7 109.60(13) . . ? H8b C8 O3 109.60(11) . . ? H8b C8 C7 109.60(13) . . ? H8b C8 H8a 108.1 . . ? C10 C9 O3 124.5(2) . . ? C17 C9 O3 115.22(19) . . ? C17 C9 C10 120.3(2) . . ? H10 C10 C9 120.00(14) . . ? C11 C10 C9 120.0(2) . . ? C11 C10 H10 120.00(14) . . ? H11 C11 C10 119.37(14) . . ? C12 C11 C10 121.3(2) . . ? C12 C11 H11 119.37(14) . . ? H12 C12 C11 120.03(14) . . ? C13 C12 C11 119.9(2) . . ? C13 C12 H12 120.03(14) . . ? C14 C13 C12 122.4(2) . . ? C17 C13 C12 119.4(2) . . ? C17 C13 C14 118.2(2) . . ? H14 C14 C13 120.36(13) . . ? C15 C14 C13 119.3(2) . . ? C15 C14 H14 120.36(14) . . ? H15 C15 C14 120.40(14) . . ? C16 C15 C14 119.2(2) . . ? C16 C15 H15 120.40(14) . . ? C15 C16 N1 123.7(2) . . ? H16 C16 N1 118.17(13) . . ? H16 C16 C15 118.17(13) . . ? C9 C17 N1 119.5(2) . . ? C13 C17 N1 121.5(2) . . ? C13 C17 C9 119.0(2) . . ? C19 C18 O4 124.5(2) . . ? C26 C18 O4 117.7(2) . . ? C26 C18 C19 117.7(2) . . ? H19 C19 C18 119.81(14) . . ? C20 C19 C18 120.4(2) . . ? C20 C19 H19 119.81(14) . . ? H20 C20 C19 118.83(14) . . ? C21 C20 C19 122.3(2) . . ? C21 C20 H20 118.83(14) . . ? H21 C21 C20 120.35(14) . . ? C22 C21 C20 119.3(2) . . ? C22 C21 H21 120.35(14) . . ? C23 C22 C21 124.6(2) . . ? C26 C22 C21 118.3(2) . . ? C26 C22 C23 117.1(2) . . ? H23 C23 C22 120.02(14) . . ? C24 C23 C22 120.0(2) . . ? C24 C23 H23 120.02(14) . . ? H24 C24 C23 120.21(14) . . ? C25 C24 C23 119.6(2) . . ? C25 C24 H24 120.21(14) . . ? C24 C25 N2 122.3(2) . . ? H25 C25 N2 118.84(13) . . ? H25 C25 C24 118.84(14) . . ? C18 C26 N2 115.9(2) . . ? C22 C26 N2 122.2(2) . . ? C22 C26 C18 122.0(2) . . ? H27 C27 N3 118.56(13) . . ? C28 C27 N3 122.9(2) . . ? C28 C27 H27 118.56(14) . . ? H28 C28 C27 120.59(14) . . ? C29 C28 C27 118.8(2) . . ? C29 C28 H28 120.59(14) . . ? H29 C29 C28 119.71(14) . . ? C30 C29 C28 120.6(2) . . ? C30 C29 H29 119.71(13) . . ? C31 C30 C29 123.9(2) . . ? C35 C30 C29 117.3(2) . . ? C35 C30 C31 118.8(2) . . ? H31 C31 C30 119.79(14) . . ? C32 C31 C30 120.4(2) . . ? C32 C31 H31 119.79(14) . . ? H32 C32 C31 119.37(14) . . ? C33 C32 C31 121.3(2) . . ? C33 C32 H32 119.37(14) . . ? H33 C33 C32 120.02(14) . . ? C34 C33 C32 120.0(2) . . ? C34 C33 H33 120.02(14) . . ? C33 C34 O5 125.5(2) . . ? C35 C34 O5 114.17(19) . . ? C35 C34 C33 120.4(2) . . ? C30 C35 N3 121.2(2) . . ? C34 C35 N3 119.74(19) . . ? C34 C35 C30 119.0(2) . . ? H36a C36 O5 109.26(12) . . ? H36b C36 O5 109.26(12) . . ? H36b C36 H36a 107.9 . . ? C37 C36 O5 111.79(19) . . ? C37 C36 H36a 109.26(13) . . ? C37 C36 H36b 109.26(13) . . ? C38 C37 C36 121.7(2) . . ? C42 C37 C36 121.0(2) . . ? C42 C37 C38 117.2(2) . . ? H38 C38 C37 119.29(15) . . ? C39 C38 C37 121.4(2) . . ? C39 C38 H38 119.29(16) . . ? H39 C39 C38 119.68(16) . . ? C40 C39 C38 120.6(3) . . ? C40 C39 H39 119.68(16) . . ? H40 C40 C39 120.47(16) . . ? C41 C40 C39 119.1(3) . . ? C41 C40 H40 120.47(17) . . ? H41 C41 C40 119.73(17) . . ? C42 C41 C40 120.5(3) . . ? C42 C41 H41 119.73(16) . . ? C41 C42 C37 121.0(2) . . ? C43 C42 C37 119.9(2) . . ? C43 C42 C41 119.1(2) . . ? O7 C43 O6 123.8(2) . . ? C42 C43 O6 116.2(2) . . ? C42 C43 O7 119.9(2) . . ? H8d O8 H8c 104.5 . . ? H9b O9 H9a 109.5 . . ? O11 N4 O10 120.7(2) . . ? O12 N4 O10 118.8(2) . . ? O12 N4 O11 120.5(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O3 2.4723(15) . ? Cu1 O4 1.9285(15) . ? Cu1 O5 2.3387(16) . ? Cu1 N1 2.0487(19) . ? Cu1 N2 2.0143(19) . ? Cu1 N3 2.0045(18) . ? O1 C1 1.231(3) . ? O2 H2 0.8400 . ? O2 C1 1.343(3) . ? O3 C8 1.461(3) . ? O3 C9 1.372(3) . ? O4 C18 1.336(3) . ? O5 C34 1.367(3) . ? O5 C36 1.451(3) . ? O6 H6 0.8400 . ? O6 C43 1.335(3) . ? O7 C43 1.235(3) . ? N1 C16 1.327(3) . ? N1 C17 1.376(3) . ? N2 C25 1.326(3) . ? N2 C26 1.366(3) . ? N3 C27 1.327(3) . ? N3 C35 1.375(3) . ? C1 C2 1.506(3) . ? C2 C3 1.394(3) . ? C2 C7 1.400(3) . ? C3 H3 0.9500 . ? C3 C4 1.384(4) . ? C4 H4 0.9500 . ? C4 C5 1.383(4) . ? C5 H5 0.9500 . ? C5 C6 1.383(4) . ? C6 H6a 0.9500 . ? C6 C7 1.395(3) . ? C7 C8 1.496(3) . ? C8 H8a 0.9900 . ? C8 H8b 0.9900 . ? C9 C10 1.368(3) . ? C9 C17 1.422(3) . ? C10 H10 0.9500 . ? C10 C11 1.412(3) . ? C11 H11 0.9500 . ? C11 C12 1.362(4) . ? C12 H12 0.9500 . ? C12 C13 1.414(3) . ? C13 C14 1.414(3) . ? C13 C17 1.418(3) . ? C14 H14 0.9500 . ? C14 C15 1.365(3) . ? C15 H15 0.9500 . ? C15 C16 1.404(3) . ? C16 H16 0.9500 . ? C18 C19 1.376(3) . ? C18 C26 1.426(3) . ? C19 H19 0.9500 . ? C19 C20 1.412(3) . ? C20 H20 0.9500 . ? C20 C21 1.368(4) . ? C21 H21 0.9500 . ? C21 C22 1.413(3) . ? C22 C23 1.410(3) . ? C22 C26 1.416(3) . ? C23 H23 0.9500 . ? C23 C24 1.362(4) . ? C24 H24 0.9500 . ? C24 C25 1.405(3) . ? C25 H25 0.9500 . ? C27 H27 0.9500 . ? C27 C28 1.405(3) . ? C28 H28 0.9500 . ? C28 C29 1.361(4) . ? C29 H29 0.9500 . ? C29 C30 1.414(3) . ? C30 C31 1.418(3) . ? C30 C35 1.419(3) . ? C31 H31 0.9500 . ? C31 C32 1.360(4) . ? C32 H32 0.9500 . ? C32 C33 1.411(4) . ? C33 H33 0.9500 . ? C33 C34 1.364(3) . ? C34 C35 1.432(3) . ? C36 H36a 0.9900 . ? C36 H36b 0.9900 . ? C36 C37 1.505(3) . ? C37 C38 1.398(3) . ? C37 C42 1.398(3) . ? C38 H38 0.9500 . ? C38 C39 1.380(4) . ? C39 H39 0.9500 . ? C39 C40 1.381(4) . ? C40 H40 0.9500 . ? C40 C41 1.381(4) . ? C41 H41 0.9500 . ? C41 C42 1.389(4) . ? C42 C43 1.494(3) . ? O8 H8c 0.8500 . ? O8 H8d 0.8500 . ? O9 H9a 0.8500 . ? O9 H9b 0.8500 . ? O10 N4 1.241(3) . ? O11 N4 1.226(3) . ? O12 N4 1.251(3) . ?