Crystallography Open Database

Information card for entry 7708948

Preview

Coordinates	7708948.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H41 Li N4 Si
Calculated formula	C16 H41 Li N4 Si
Title of publication	A Monomeric (Trimethylsilyl)methyl Lithium Complex: Synthesis, Structure, Decomposition and Preliminary Reactivity Studies New Talent: Europe themed issue of Dalton Transactions
Authors of publication	Davison, Nathan; Waddell, Paul G.; Dixon, Casey; Wills, Corinne; Penfold, Thomas; Lu, Erli
Journal of publication	Dalton Transactions
Year of publication	2021
a	10.891 ± 0.0003 Å
b	18.7942 ± 0.0005 Å
c	10.9483 ± 0.0003 Å
α	90°
β	94.108 ± 0.003°
γ	90°
Cell volume	2235.22 ± 0.11 Å³
Cell temperature	150 ± 0.2 K
Ambient diffraction temperature	150 ± 0.2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0805
Residual factor for significantly intense reflections	0.059
Weighted residual factors for significantly intense reflections	0.1466
Weighted residual factors for all reflections included in the refinement	0.1637
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
270894 (current)	2021-11-27	cif/ Adding structures of 7708948, 7708949, 7708950, 7708951 via cif-deposit CGI script.	7708948.cif