Crystallography Open Database

Information card for entry 7708950

Preview

Coordinates	7708950.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H40 Li2 N6
Calculated formula	C16 H40 Li2 N6
SMILES	[N]1(CC[N]23CC[N](C)(C)[Li]34[N]([Li]123)(CC[N]4(C)C)CC[N]3(C)C)(C)C
Title of publication	A Monomeric (Trimethylsilyl)methyl Lithium Complex: Synthesis, Structure, Decomposition and Preliminary Reactivity Studies New Talent: Europe themed issue of Dalton Transactions
Authors of publication	Davison, Nathan; Waddell, Paul G.; Dixon, Casey; Wills, Corinne; Penfold, Thomas; Lu, Erli
Journal of publication	Dalton Transactions
Year of publication	2021
a	15.6022 ± 0.0003 Å
b	10.092 ± 0.0002 Å
c	14.6868 ± 0.0003 Å
α	90°
β	111.323 ± 0.002°
γ	90°
Cell volume	2154.24 ± 0.08 Å³
Cell temperature	150 ± 0.2 K
Ambient diffraction temperature	150 ± 0.2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0444
Residual factor for significantly intense reflections	0.0398
Weighted residual factors for significantly intense reflections	0.1065
Weighted residual factors for all reflections included in the refinement	0.111
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
270894 (current)	2021-11-27	cif/ Adding structures of 7708948, 7708949, 7708950, 7708951 via cif-deposit CGI script.	7708950.cif