Crystallography Open Database

Information card for entry 7708952

Preview

Coordinates	7708952.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C96 H168 Cl2 F2 N16 Ni4 O20 Rh2 S4
Calculated formula	C96 H168 Cl2 F2 N16 Ni4 O20 Rh2 S4
Title of publication	Stable thiolate adducts of Rh<sub>2</sub>(OAc)<sub>4</sub> - assembly of hexametallic Ni<sub>4</sub>Rh<sub>2</sub> complexes.
Authors of publication	Schmorl, Sara; Börner, Martin; Kersting, Berthold
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	51
Journal issue	1
Pages of publication	59 - 62
a	25.546 ± 0.0002 Å
b	18.1249 ± 0.0001 Å
c	27.9275 ± 0.0002 Å
α	90°
β	108.378 ± 0.001°
γ	90°
Cell volume	12271.4 ± 0.16 Å³
Cell temperature	180 K
Ambient diffraction temperature	180 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0559
Residual factor for significantly intense reflections	0.0462
Weighted residual factors for significantly intense reflections	0.126
Weighted residual factors for all reflections included in the refinement	0.13
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	1.54186 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
272650 (current)	2022-02-04	cif/ Updating files of 7708952 Original log message: Adding full bibliography for 7708952.cif.	7708952.cif
270899	2021-11-28	cif/ Adding structures of 7708952 via cif-deposit CGI script.	7708952.cif