Crystallography Open Database

Information card for entry 8101347

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Coordinates	8101347.cif

Structure parameters

Formula	C36 H108 N6 O3 Si12 Yb3
Calculated formula	C32 H100 N6 O2 Si12 Yb3
SMILES	[Yb]1([O]2CCCC2)(N(=[Si](C)C)=[Si](C)C)[N]([Yb]2([N]1(=[Si](C)C)=[Si](C)C)[N]([Yb]([N]2(=[Si](C)C)=[Si](C)C)([O]1CCCC1)N(=[Si](C)C)=[Si](C)C)(=[Si](C)C)=[Si](C)C)(=[Si](C)C)=[Si](C)C
Title of publication	Crystal structure of ytterbium-bis[bis(μ-dimethylsilylamido) ytterbium-dimethylsilylamide(tetrahydrofuran)]‒tetrahydrofuran (1/1), C~32~H~100~N~6~O~2~Si~12~Yb~3~ · C~4~H~8~O
Authors of publication	Rabe, Gerd W.; Rheingold, A. L.; Incarvito, C. D.
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2000
Journal volume	215
Journal issue	4
Pages of publication	560 - 562
a	11.4205 ± 0.0017 Å
b	28.422 ± 0.005 Å
c	21.796 ± 0.004 Å
α	90°
β	96.6 ± 0.004°
γ	90°
Cell volume	7027.9 ± 1.9 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
200436 (current)	2017-09-11	cif/8/10/13/ Marking attached hydrogen atoms in entry 8101347.	8101347.cif
176728	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8101347.cif
102820	2014-02-24	cif/8/10/ (antanas@lokys.ibt.lt) Adding and updating bibliographic information: volume, authors, issue, first page, last page.	8101347.cif
100676	2014-02-06	cif/8/ (antanas@lokys.ibt.lt) Adding volume number.	8101347.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8101347.cif
5310	2011-01-02	cif/ Running cif_fix_enum with the core CIF dictionary on COD ranges 2, 8 and 9. Range 9 remained unchanged, and in ranges 2 and 8 there were 17309 modified files, most changes were fixes enumerator case.	8101347.cif
966	2010-01-30	cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated.	8101347.cif
853	2009-11-16	cif/ Reconstructing spacegroup designators from the symmetry operators were possible. The comands used can be found in the log file reformat-spacegroups-2009.11.14.log committed with the current revision. Only lines that contained spacegroup designators were changed, and all files pass vcif test after the conversion.	8101347.cif
19	2008-01-26	Changing all end-of-line codes from DOS style to UNIX style in all COD CIF files, for more convenient processing: In the cod/cif/ directory: ff \*.cif \| xargs perl -i -pe 's/\r\n/\n/'	8101347.cif
14	2008-01-14	Appending a header with SVN keywords, COD URL and copying policy to all COD CIF files.	8101347.cif
13	2008-01-13	Setting the svn:keywords property to "Author Date Revision URL Id" for all CIF files in the cod/cif directory.	8101347.cif
1	2007-11-30	Adding all .cif files from the COD, downloaded in a Cod.zip file on 2007.02.07 (and the same Cod.zip is downloadable today, on 2007.11.29)	8101347.cif