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Information card for entry 8102656
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| Coordinates | 8102656.cif |
|---|
| Formula | C65 H64 Ag B Cl2 F4 O4 P2 |
|---|---|
| Calculated formula | C65 H64 Ag B Cl2 F4 O4 P2 |
| Title of publication | Crystal structure of bis[(m2-5,11-bis(diphenyl- phosphanyl)25,26-dipropyloxy-27,28-bis(2- propenyl)calix[4]arene-P:P']disilver(I) bis(tetrafluoroborate) — dichloromethane (1:2), [Ag2(C64H62O4P2)2][BF4]2 · 2CH2Cl2 |
| Authors of publication | Mouhamad Awada; Catherine Jeunesse; Eric Brenner; Dominique Matt; Loïc Toupet |
| Journal of publication | Zeitschrift für Kristallographie - New Crystal Structures |
| Year of publication | 2010 |
| Journal volume | 225 |
| Journal issue | 1 |
| Pages of publication | 176 |
| a | 16.6993 ± 0.0008 Å |
| b | 23.1203 ± 0.0009 Å |
| c | 17.0133 ± 0.0007 Å |
| α | 90° |
| β | 115.197 ± 0.006° |
| γ | 90° |
| Cell volume | 5943.7 ± 0.5 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1441 |
| Residual factor for significantly intense reflections | 0.0602 |
| Weighted residual factors for significantly intense reflections | 0.1445 |
| Weighted residual factors for all reflections included in the refinement | 0.1637 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.802 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211175 (current) | 2018-09-26 | cif/ Removing _chemical_name_systematic and _chemical_name_common data items with placeholder values from 513 entries in range 8. |
8102656.cif |
| 176728 | 2016-02-18 | cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8. |
8102656.cif |
| 35911 | 2012-02-28 | cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree. |
8102656.cif |
| 13395 | 2011-03-06 | ../uploads/cif-deposit/cod/cif Adding structures of 8102656 via cif-deposit CGI script. |
8102656.cif |
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Users of the data should acknowledge the original authors of the
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