#------------------------------------------------------------------------------ #$Date: 2022-11-24 12:06:42 +0200 (Thu, 24 Nov 2022) $ #$Revision: 279544 $ #$URL: file:///home/coder/svn-repositories/cod/cif/8/10/62/8106245.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_8106245 loop_ _publ_author_name 'Alotaibi, Mohammad Hayal' 'Mohamed, Hanan A.' 'Abdel-Wahab, Bakr F.' 'El-Enin, Mohammed Abu Bakr Abu' 'Ghabbour, Hazem A.' 'El-Hiti, Gamal A.' _publ_section_title ; Crystal structure of (E)-3-(3-(5-methyl-1-4-tolyl-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazol-4-yl)-1-(5-methyl-1-phenyl-1H-1,2,3-triazol-4-yl)prop-2-en-1-one, C31H26N8O ; _journal_issue 4 _journal_name_full 'Zeitschrift f\"ur Kristallographie - New Crystal Structures' _journal_page_first 647 _journal_page_last 648 _journal_paper_doi 10.1515/ncrs-2017-0420 _journal_volume 233 _journal_year 2018 _chemical_formula_sum 'C31 H26 N8 O' _chemical_formula_weight 526.60 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 61.996(2) _cell_angle_beta 80.390(3) _cell_angle_gamma 87.579(2) _cell_formula_units_Z 2 _cell_length_a 6.6046(3) _cell_length_b 15.1056(8) _cell_length_c 15.2115(8) _cell_measurement_reflns_used 4702 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 24.13 _cell_measurement_theta_min 2.63 _cell_volume 1319.97(12) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014 (Sheldrick 2014)' _computing_structure_solution 'SHELXL-2014 (Sheldrick 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1083 _diffrn_reflns_av_unetI/netI 0.0887 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 25379 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 24.998 _diffrn_reflns_theta_max 24.998 _diffrn_reflns_theta_min 2.629 _exptl_absorpt_coefficient_mu 0.085 _exptl_absorpt_correction_T_max 0.854 _exptl_absorpt_correction_T_min 0.827 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS_Bruker_2014 _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.325 _exptl_crystal_description block _exptl_crystal_F_000 552 _exptl_crystal_size_max 0.322 _exptl_crystal_size_mid 0.254 _exptl_crystal_size_min 0.112 _refine_diff_density_max 0.640 _refine_diff_density_min -0.270 _refine_diff_density_rms 0.057 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.024 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 364 _refine_ls_number_reflns 4637 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.024 _refine_ls_R_factor_all 0.1175 _refine_ls_R_factor_gt 0.0574 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0571P)^2^+0.7235P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1191 _refine_ls_wR_factor_ref 0.1431 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2881 _reflns_number_total 4637 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file suppl_ncrs-2017-0420_suppl.cif _cod_data_source_block a_A _cod_database_code 8106245 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.973 _shelx_estimated_absorpt_t_max 0.991 _shelx_res_file ; a_A.res created by SHELXL-2014/7 TITL a_a.res in P-1 REM Old TITL mo_sa309_0m in P-1 REM SHELXT solution in P-1 REM R1 0.192, Rweak 0.032, Alpha 0.070, Orientation as input REM Formula found by SHELXT: C31 N8 O CELL 0.71073 6.6046 15.1056 15.2115 61.996 80.390 87.579 ZERR 2.000 0.0003 0.0008 0.0008 0.002 0.003 0.002 LATT 1 SFAC C H N O UNIT 62 52 16 2 TEMP -273.150 SIZE 0.112 0.254 0.322 L.S. 10 BOND $H LIST 4 ACTA CONF OMIT -4 50 FMAP 2 PLAN 20 WGHT 0.057100 0.723500 FVAR 0.50647 O1 4 0.786393 0.173759 0.504890 11.00000 0.03578 0.04138 = 0.03250 -0.01275 0.00559 -0.00272 N1 3 1.289683 0.185560 0.288095 11.00000 0.01882 0.02255 = 0.02122 -0.00961 -0.00457 0.00427 N2 3 1.219019 0.263675 0.208446 11.00000 0.02703 0.02334 = 0.02168 -0.00726 -0.00891 0.00431 N3 3 1.045887 0.288729 0.246095 11.00000 0.02188 0.02442 = 0.03100 -0.01263 -0.00594 0.00429 N4 3 0.113449 0.480368 0.287062 11.00000 0.02119 0.02015 = 0.01684 -0.00614 0.00090 0.00153 N5 3 0.009753 0.446163 0.383464 11.00000 0.02091 0.02028 = 0.01844 -0.00905 0.00093 0.00028 N6 3 0.184306 0.259398 0.613692 11.00000 0.02125 0.03168 = 0.02014 -0.00825 -0.00147 0.00491 N7 3 0.079693 0.214983 0.705889 11.00000 0.01904 0.03524 = 0.02371 -0.01014 -0.00458 0.00729 N8 3 -0.106712 0.257170 0.701841 11.00000 0.01700 0.02467 = 0.01755 -0.00911 -0.00378 0.00593 C1 1 1.645485 0.192207 0.209625 11.00000 0.02703 0.02380 = 0.02368 -0.01304 -0.00134 -0.00325 AFIX 43 H1A 2 1.648642 0.263343 0.180175 11.00000 -1.20000 AFIX 0 C2 1 1.817752 0.142682 0.192669 11.00000 0.01994 0.04216 = 0.03422 -0.02527 -0.00005 -0.00168 AFIX 43 H2A 2 1.939486 0.180232 0.150745 11.00000 -1.20000 AFIX 0 C3 1 1.813005 0.039476 0.236296 11.00000 0.02721 0.04179 = 0.02956 -0.02513 -0.00879 0.01129 AFIX 43 H3A 2 1.931840 0.006172 0.224870 11.00000 -1.20000 AFIX 0 C4 1 1.635837 -0.015888 0.296698 11.00000 0.03094 0.02721 = 0.02699 -0.01355 -0.00940 0.00690 AFIX 43 H4A 2 1.633455 -0.087059 0.326774 11.00000 -1.20000 AFIX 0 C5 1 1.462068 0.032282 0.313361 11.00000 0.02415 0.02915 = 0.02248 -0.01194 -0.00467 0.00362 AFIX 43 H5A 2 1.339255 -0.005192 0.353881 11.00000 -1.20000 AFIX 0 C6 1 1.470283 0.136302 0.269854 11.00000 0.02030 0.02390 = 0.02023 -0.01121 -0.00585 0.00383 C7 1 1.211420 0.089076 0.477217 11.00000 0.02755 0.03571 = 0.02269 -0.00938 -0.00164 -0.00125 AFIX 137 H7A 2 1.359396 0.093063 0.476627 11.00000 -1.50000 H7B 2 1.170918 0.021137 0.492144 11.00000 -1.50000 H7C 2 1.136036 0.104695 0.529110 11.00000 -1.50000 AFIX 0 C8 1 1.162744 0.162386 0.376761 11.00000 0.02170 0.02414 = 0.02127 -0.01249 -0.00161 -0.00199 C9 1 1.005888 0.227902 0.348490 11.00000 0.02033 0.02256 = 0.02269 -0.01105 -0.00289 -0.00032 C10 1 0.815973 0.233429 0.412475 11.00000 0.02531 0.02536 = 0.03783 -0.01658 -0.00705 -0.00072 C11 1 0.669218 0.308534 0.363571 11.00000 0.02474 0.02651 = 0.03830 -0.01895 -0.00656 -0.00050 AFIX 43 H11A 2 0.699063 0.354839 0.293645 11.00000 -1.20000 AFIX 0 C12 1 0.492707 0.310462 0.419419 11.00000 0.01922 0.03371 = 0.04132 -0.02823 -0.00081 -0.00196 AFIX 43 H12A 2 0.474610 0.264380 0.489481 11.00000 -1.20000 AFIX 0 C13 1 0.323570 0.376807 0.383271 11.00000 0.01785 0.02291 = 0.02277 -0.01411 0.00137 -0.00063 C14 1 0.298965 0.440691 0.285172 11.00000 0.02077 0.02365 = 0.02581 -0.01460 0.00696 -0.00201 AFIX 43 H14A 2 0.396399 0.454304 0.226382 11.00000 -1.20000 AFIX 0 C15 1 0.135770 0.383643 0.442063 11.00000 0.01895 0.01861 = 0.02331 -0.01053 -0.00393 0.00000 C16 1 0.065485 0.328403 0.551186 11.00000 0.01777 0.01834 = 0.01975 -0.00821 -0.00314 0.00269 C17 1 -0.122519 0.329098 0.606672 11.00000 0.02070 0.01571 = 0.01753 -0.00695 -0.00534 0.00317 C18 1 -0.305661 0.390490 0.580396 11.00000 0.02195 0.02409 = 0.02052 -0.00901 -0.00310 0.00695 AFIX 137 H18A 2 -0.357525 0.409220 0.633368 11.00000 -1.50000 H18B 2 -0.412805 0.351509 0.574577 11.00000 -1.50000 H18C 2 -0.267617 0.451292 0.515889 11.00000 -1.50000 AFIX 0 C19 1 -0.260588 0.215597 0.791255 11.00000 0.02401 0.01769 = 0.01446 -0.00544 -0.00339 0.00493 C20 1 -0.450013 0.182320 0.786935 11.00000 0.02260 0.03083 = 0.01986 -0.01353 -0.00743 0.00320 AFIX 43 H20A 2 -0.479346 0.189662 0.724855 11.00000 -1.20000 AFIX 0 C21 1 -0.594570 0.138691 0.873251 11.00000 0.02105 0.02788 = 0.02407 -0.00921 -0.00462 0.00291 AFIX 43 H21A 2 -0.723987 0.116172 0.870068 11.00000 -1.20000 AFIX 0 C22 1 -0.555346 0.126905 0.964751 11.00000 0.02545 0.01656 = 0.01823 -0.00443 -0.00343 0.00828 C23 1 -0.365529 0.160176 0.967268 11.00000 0.03691 0.02494 = 0.01505 -0.00746 -0.00979 0.01071 AFIX 43 H23A 2 -0.335775 0.151974 1.029589 11.00000 -1.20000 AFIX 0 C24 1 -0.217039 0.205313 0.881042 11.00000 0.02236 0.02564 = 0.02264 -0.01066 -0.01030 0.00386 AFIX 43 H24A 2 -0.088179 0.228592 0.883960 11.00000 -1.20000 AFIX 0 C25 1 -0.717687 0.080768 1.057922 11.00000 0.03480 0.03329 = 0.02435 -0.00812 0.00068 0.00895 AFIX 137 H25A 2 -0.670047 0.085167 1.113462 11.00000 -1.50000 H25B 2 -0.743740 0.010181 1.076807 11.00000 -1.50000 H25C 2 -0.844817 0.116960 1.044073 11.00000 -1.50000 AFIX 0 C26 1 0.006101 0.538892 0.205575 11.00000 0.03087 0.01328 = 0.01797 -0.00254 -0.00016 -0.00124 C27 1 -0.179842 0.578258 0.223576 11.00000 0.02803 0.02577 = 0.01663 -0.00534 0.00202 0.00116 AFIX 43 H27A 2 -0.231553 0.569686 0.289352 11.00000 -1.20000 AFIX 0 C28 1 -0.290461 0.630054 0.145945 11.00000 0.03158 0.02356 = 0.02542 -0.00284 -0.00366 0.00467 AFIX 43 H28A 2 -0.418719 0.656344 0.158771 11.00000 -1.20000 AFIX 0 C29 1 -0.215158 0.643796 0.049550 11.00000 0.04782 0.02166 = 0.02182 -0.00120 -0.00900 0.00612 AFIX 43 H29A 2 -0.290695 0.679684 -0.003899 11.00000 -1.20000 AFIX 0 C30 1 -0.029047 0.604724 0.032070 11.00000 0.05297 0.02611 = 0.01602 -0.00634 -0.00310 0.00889 AFIX 43 H30A 2 0.022821 0.614130 -0.033993 11.00000 -1.20000 AFIX 0 C31 1 0.083166 0.552275 0.108642 11.00000 0.03695 0.02521 = 0.02548 -0.00874 0.00128 0.00522 AFIX 43 H31A 2 0.210883 0.525675 0.095625 11.00000 -1.20000 AFIX 0 HKLF 4 REM a_a.res in P-1 REM R1 = 0.0574 for 2881 Fo > 4sig(Fo) and 0.1175 for all 4637 data REM 364 parameters refined using 0 restraints END WGHT 0.0439 0.9020 REM Highest difference peak 0.640, deepest hole -0.270, 1-sigma level 0.057 Q1 1 0.5488 0.2458 0.4828 11.00000 0.05 0.64 Q2 1 0.5591 0.4454 0.0782 11.00000 0.05 0.28 Q3 1 0.6987 0.2364 0.4641 11.00000 0.05 0.22 Q4 1 -0.8666 -0.0720 1.1207 11.00000 0.05 0.21 Q5 1 -0.5517 0.1635 1.1207 11.00000 0.05 0.20 Q6 1 0.3445 0.6569 -0.0008 11.00000 0.05 0.20 Q7 1 -1.0337 0.0443 1.0399 11.00000 0.05 0.20 Q8 1 0.8091 0.2706 0.3517 11.00000 0.05 0.19 Q9 1 1.8315 0.1104 0.3394 11.00000 0.05 0.19 Q10 1 -0.3380 0.1804 0.7870 11.00000 0.05 0.18 Q11 1 -0.5319 0.6671 0.0581 11.00000 0.05 0.18 Q12 1 1.3273 -0.0413 0.3835 11.00000 0.05 0.18 Q13 1 1.5783 0.3506 0.0698 11.00000 0.05 0.18 Q14 1 1.0033 0.3548 0.2077 11.00000 0.05 0.18 Q15 1 -0.6246 0.0147 1.1620 11.00000 0.05 0.18 Q16 1 0.4080 0.4267 0.1225 11.00000 0.05 0.18 Q17 1 1.1329 -0.0031 0.4001 11.00000 0.05 0.18 Q18 1 -0.4243 0.3806 0.6174 11.00000 0.05 0.18 Q19 1 0.1767 0.1798 0.6217 11.00000 0.05 0.18 Q20 1 2.1599 0.1678 0.1710 11.00000 0.05 0.17 ; _shelx_res_checksum 59594 _shelx_hkl_file ; -1 0 0 456.85 29.10 -1 0 0 535.95 29.40 -1 0 0 531.25 28.90 -1 0 0 536.45 29.40 -1 0 0 521.65 29.10 1 0 0 513.15 29.30 1 0 0 521.45 28.90 1 0 0 517.65 29.30 1 0 0 529.75 28.60 1 0 0 476.35 29.10 -2 0 0 330.37 19.50 -2 0 0 277.47 19.10 -2 0 0 324.77 19.50 -2 0 0 317.87 18.60 -2 0 0 315.47 19.00 2 0 0 331.37 18.30 2 0 0 337.07 18.00 2 0 0 318.97 18.60 2 0 0 321.07 19.50 2 0 0 320.07 19.70 2 0 0 301.77 19.10 -3 0 0 15.70 3.30 -3 0 0 21.60 4.50 -3 0 0 8.00 3.40 -3 0 0 19.00 4.50 3 0 0 12.50 1.60 3 0 0 15.60 4.20 3 0 0 14.90 5.40 3 0 0 13.60 2.40 3 0 0 16.50 2.90 -4 0 0 31.80 5.90 -4 0 0 37.70 8.00 -4 0 0 49.20 6.90 -4 0 0 34.90 6.30 4 0 0 44.40 4.60 4 0 0 41.90 7.80 4 0 0 42.40 3.00 4 0 0 25.50 8.60 4 0 0 33.80 5.80 4 0 0 42.80 5.00 -5 0 0 5.90 6.80 -5 0 0 -5.20 5.30 -5 0 0 -6.20 5.60 5 0 0 14.90 11.10 5 0 0 12.30 4.00 5 0 0 -4.30 6.60 5 0 0 0.60 7.80 -6 0 0 52.89 11.00 -6 0 0 48.40 9.60 -6 0 0 61.99 11.30 6 0 0 56.19 10.80 6 0 0 50.39 7.70 -7 0 0 17.30 13.50 -7 0 0 -10.30 12.90 7 0 0 3.10 11.10 7 0 0 -5.20 7.60 7 0 0 2.80 6.00 -8 0 0 8.80 17.80 -8 0 0 16.70 19.10 8 0 0 -1.10 14.00 8 0 0 16.00 10.60 -9 0 0 49.50 26.60 -9 0 0 12.10 25.30 9 0 0 -8.30 18.90 -10 0 0 -1.80 35.90 10 0 0 75.29 32.50 10 0 0 -4.00 28.10 10 -1 0 24.40 32.50 10 -1 0 57.99 30.30 -10 1 0 17.10 27.70 9 -1 0 -31.60 20.30 -9 1 0 22.00 20.00 -9 1 0 40.30 26.60 8 -1 0 5.20 15.00 8 -1 0 0.60 10.40 -8 1 0 12.10 14.10 -8 1 0 34.80 17.70 7 -1 0 1.40 8.30 7 -1 0 13.50 8.00 -7 1 0 -7.00 11.40 -7 1 0 4.10 12.20 -7 1 0 18.00 10.30 6 -1 0 4.60 8.30 6 -1 0 9.50 6.20 -6 1 0 23.10 8.80 -6 1 0 7.00 8.70 -6 1 0 7.90 7.90 5 -1 0 244.78 20.30 5 -1 0 268.37 19.70 5 -1 0 273.17 17.10 -5 1 0 239.98 18.60 -5 1 0 226.28 20.60 -5 1 0 266.47 18.20 4 -1 0 1.20 2.70 4 -1 0 4.30 2.30 4 -1 0 7.00 4.00 4 -1 0 0.50 5.20 -4 1 0 4.30 3.90 -4 1 0 3.90 5.90 -4 1 0 -2.30 5.60 3 -1 0 127.09 7.60 3 -1 0 124.69 10.90 3 -1 0 127.39 9.60 3 -1 0 134.59 8.90 -3 1 0 118.09 10.60 -3 1 0 132.59 9.20 -3 1 0 125.69 9.50 -3 1 0 130.09 9.70 2 -1 0 7.20 1.20 2 -1 0 5.80 1.80 2 -1 0 6.90 1.90 2 -1 0 5.50 3.00 -2 1 0 6.80 2.30 -2 1 0 5.80 2.20 -2 1 0 7.20 3.00 -2 1 0 6.90 1.00 1 -1 0 1117.89 60.79 1 -1 0 1066.49 60.99 1 -1 0 1096.39 60.59 1 -1 0 1082.59 60.99 -1 1 0 1130.19 60.99 -1 1 0 1003.80 60.99 -1 1 0 1106.89 60.89 -1 1 0 1110.59 60.59 -1 -1 0 2219.98 120.79 -1 -1 0 2180.28 120.49 -1 -1 0 2210.08 120.79 -1 -1 0 2204.08 120.79 1 1 0 2261.57 120.79 1 1 0 2143.49 120.59 1 1 0 2149.39 120.39 1 1 0 2228.18 120.79 1 1 0 2208.28 120.79 1 1 0 2121.29 120.19 1 1 0 1912.61 120.39 -2 -1 0 260.67 17.00 -2 -1 0 279.57 17.30 -2 -1 0 267.17 17.30 -2 -1 0 293.17 16.30 2 1 0 295.87 16.40 2 1 0 279.77 17.40 2 1 0 280.97 17.00 2 1 0 287.87 17.60 2 1 0 248.38 16.70 2 1 0 276.17 16.30 -3 -1 0 312.37 20.80 -3 -1 0 348.57 19.40 -3 -1 0 315.27 20.40 3 1 0 291.37 21.00 3 1 0 340.97 19.30 3 1 0 325.07 20.90 3 1 0 316.87 18.70 3 1 0 333.57 21.10 3 1 0 320.87 19.20 -4 -1 0 11.80 4.60 -4 -1 0 9.80 5.20 -4 -1 0 18.10 6.80 4 1 0 12.50 3.40 4 1 0 12.40 2.20 4 1 0 4.20 5.00 4 1 0 12.00 3.60 4 1 0 8.10 7.60 4 1 0 13.10 6.00 -5 -1 0 -10.40 6.50 -5 -1 0 -1.40 5.10 -5 -1 0 8.50 8.50 5 1 0 -1.80 1.60 5 1 0 -3.80 6.50 5 1 0 -2.70 8.00 5 1 0 2.80 4.90 5 1 0 3.70 8.00 5 1 0 -1.50 4.20 -6 -1 0 13.70 9.60 -6 -1 0 14.90 8.00 6 1 0 6.60 5.80 6 1 0 -2.20 7.60 6 1 0 18.50 8.60 -7 -1 0 86.89 16.20 -7 -1 0 75.39 16.30 7 1 0 76.29 9.60 7 1 0 60.09 9.90 7 1 0 77.99 14.00 -8 -1 0 13.20 14.10 -8 -1 0 41.70 17.90 8 1 0 50.19 10.50 8 1 0 27.70 17.10 -9 -1 0 47.70 26.90 -9 -1 0 2.30 26.70 9 1 0 -15.40 18.90 9 1 0 -28.30 20.00 -10 -1 0 50.79 38.40 10 1 0 7.20 20.80 10 1 0 -20.70 28.20 10 -2 0 -1.60 22.50 10 -2 0 -37.60 20.70 -10 2 0 49.30 36.30 9 -2 0 -20.20 17.60 -9 2 0 6.00 26.00 -9 2 0 17.10 25.10 8 -2 0 -2.70 14.20 -8 2 0 19.70 15.40 -8 2 0 -13.40 18.50 7 -2 0 -2.70 8.20 7 -2 0 1.70 10.70 -7 2 0 -15.40 12.30 -7 2 0 9.20 14.30 -7 2 0 -11.00 12.20 6 -2 0 48.50 8.00 6 -2 0 40.30 4.10 6 -2 0 36.00 8.50 -6 2 0 35.40 9.80 -6 2 0 45.70 10.10 -6 2 0 53.59 10.20 5 -2 0 12.20 8.30 5 -2 0 -1.30 4.50 5 -2 0 4.40 2.70 5 -2 0 13.20 7.00 -5 2 0 -5.00 5.60 -5 2 0 0.70 7.90 -5 2 0 14.60 8.70 -5 2 0 3.30 6.90 4 -2 0 3.40 7.40 4 -2 0 -1.40 5.00 -4 2 0 10.20 4.90 -4 2 0 2.00 4.40 -4 2 0 7.00 5.90 3 -2 0 293.47 18.80 3 -2 0 305.17 19.60 3 -2 0 313.17 18.10 -3 2 0 279.77 19.30 -3 2 0 270.77 19.00 -3 2 0 301.37 17.00 2 -2 0 22.00 2.80 2 -2 0 27.90 3.80 2 -2 0 14.60 2.70 -2 2 0 15.00 2.90 -2 2 0 18.30 2.10 -2 2 0 26.00 3.90 1 -2 0 348.37 20.00 1 -2 0 341.27 19.80 1 -2 0 356.36 19.60 1 -2 0 353.06 19.90 -1 2 0 348.57 19.80 -1 2 0 322.07 19.90 -1 2 0 341.67 19.90 0 -2 0 1302.57 71.79 0 -2 0 1303.27 72.19 0 -2 0 1293.27 71.79 0 2 0 1348.97 71.79 0 2 0 1253.17 71.79 0 2 0 1220.08 71.69 0 2 0 1334.07 72.19 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7.60 6 -7 0 3.80 3.20 -6 7 0 -2.40 4.50 -6 7 0 14.30 10.00 5 -7 0 27.60 9.60 5 -7 0 50.09 6.40 5 -7 0 31.60 13.70 -5 7 0 50.89 11.70 4 -7 0 33.90 6.60 4 -7 0 42.90 9.70 4 -7 0 28.00 5.50 -4 7 0 22.50 6.00 -4 7 0 21.70 10.00 -4 7 0 45.80 9.40 3 -7 0 -4.50 3.30 3 -7 0 2.90 4.80 -3 7 0 9.60 4.80 -3 7 0 2.30 6.40 -3 7 0 3.50 4.70 2 -7 0 120.99 8.00 2 -7 0 100.79 9.90 2 -7 0 129.09 9.10 2 -7 0 110.09 10.10 -2 7 0 98.89 9.30 -2 7 0 118.49 10.30 -2 7 0 89.39 9.40 1 -7 0 377.16 23.30 1 -7 0 388.06 22.00 1 -7 0 372.96 22.40 -1 7 0 350.56 23.10 -1 7 0 358.06 23.00 0 -7 0 28.70 5.00 0 -7 0 21.80 3.60 0 -7 0 29.60 5.20 0 7 0 26.60 6.00 0 7 0 29.40 3.40 0 7 0 30.00 5.80 0 7 0 30.50 3.80 -1 -7 0 44.30 6.30 -1 -7 0 39.40 4.20 -1 -7 0 44.10 5.90 1 7 0 44.30 3.90 1 7 0 52.69 6.50 1 7 0 41.60 4.50 1 7 0 38.50 7.30 1 7 0 45.80 5.30 -2 -7 0 99.69 10.40 -2 -7 0 94.69 10.30 2 7 0 112.29 10.40 2 7 0 122.49 11.40 2 7 0 102.69 9.90 2 7 0 102.19 11.20 2 7 0 109.59 12.40 2 7 0 111.09 8.30 -3 -7 0 23.00 7.90 -3 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31.10 7 7 -3 17.20 13.60 7 7 -3 0.50 15.30 -7 -7 3 -36.20 22.30 6 7 -3 28.90 6.00 6 7 -3 32.40 10.10 6 7 -3 16.00 12.20 -6 -7 3 7.40 17.80 -6 -7 3 32.50 13.00 5 7 -3 10.80 5.90 5 7 -3 12.20 7.20 5 7 -3 -11.70 14.40 5 7 -3 0.70 7.60 5 7 -3 4.00 9.80 -5 -7 3 10.20 10.10 -5 -7 3 0.10 10.80 4 7 -3 49.10 10.00 4 7 -3 59.49 10.20 4 7 -3 70.19 12.00 4 7 -3 66.59 7.90 -4 -7 3 82.39 11.80 -4 -7 3 88.79 16.10 3 7 -3 15.50 6.30 3 7 -3 10.60 2.80 3 7 -3 3.50 10.10 3 7 -3 14.30 5.70 3 7 -3 20.60 7.60 3 7 -3 -0.70 9.70 -3 -7 3 19.00 7.20 -3 -7 3 23.70 7.80 -3 -7 3 12.40 10.70 2 7 -3 13.70 5.40 2 7 -3 4.50 11.60 2 7 -3 5.40 7.40 2 7 -3 33.90 8.30 2 7 -3 16.20 5.50 -2 -7 3 6.30 7.00 -2 -7 3 4.90 6.60 -2 -7 3 10.60 5.80 -2 -7 3 8.20 6.30 1 7 -3 519.75 35.30 1 7 -3 523.95 31.50 1 7 -3 527.95 31.80 -1 -7 3 485.75 33.00 -1 -7 3 498.25 33.80 -1 -7 3 537.75 31.20 0 7 -3 0.50 6.60 0 7 -3 6.70 2.90 0 7 -3 6.60 4.50 0 7 -3 19.00 5.10 0 -7 3 3.60 4.70 0 -7 3 4.70 4.40 0 -7 3 1.20 5.50 -1 7 -3 11.20 8.20 -1 7 -3 10.70 5.00 -1 7 -3 -0.60 6.20 1 -7 3 8.30 2.50 1 -7 3 3.60 5.30 1 -7 3 6.40 4.30 -2 7 -3 22.00 7.70 -2 7 -3 20.70 8.40 2 -7 3 19.90 7.00 2 -7 3 16.30 4.80 -3 7 -3 14.40 6.70 3 -7 3 13.60 9.50 3 -7 3 31.20 6.10 3 -7 3 28.20 6.40 3 -7 3 22.60 6.80 -4 7 -3 32.00 7.90 4 -7 3 64.49 9.10 4 -7 3 48.90 8.70 4 -7 3 33.30 7.50 4 -7 3 42.60 13.60 4 -7 3 40.80 8.90 -5 7 -3 55.39 8.90 5 -7 3 68.19 11.10 5 -7 3 46.60 13.40 5 -7 3 72.09 11.70 5 -7 3 71.89 10.00 -6 7 -3 -13.60 12.30 6 -7 3 9.80 9.10 6 -7 3 16.10 8.70 6 -7 3 16.20 9.90 -7 7 -3 -8.60 17.70 7 -7 3 4.60 10.00 7 -7 3 11.90 12.60 -8 7 -3 -6.60 17.60 8 -7 3 -16.50 13.40 -9 7 -3 31.40 32.80 9 -7 3 -39.00 23.70 9 6 -3 -19.90 28.20 -9 -6 3 -8.50 42.30 8 6 -3 -1.10 17.70 -8 -6 3 -12.90 30.40 7 6 -3 15.50 14.10 7 6 -3 4.50 12.80 -7 -6 3 5.70 20.20 6 6 -3 16.70 10.70 6 6 -3 17.30 2.80 6 6 -3 13.20 2.10 6 6 -3 14.40 9.70 -6 -6 3 -0.80 11.50 -6 -6 3 20.30 18.40 5 6 -3 85.49 9.30 5 6 -3 111.49 15.80 5 6 -3 105.29 13.30 5 6 -3 107.19 11.50 5 6 -3 89.59 10.00 -5 -6 3 105.19 13.60 -5 -6 3 95.59 15.80 4 6 -3 149.29 11.70 4 6 -3 152.78 15.10 4 6 -3 141.19 13.70 4 6 -3 145.79 11.10 4 6 -3 163.08 17.20 -4 -6 3 134.69 16.90 -4 -6 3 124.49 14.20 3 6 -3 45.40 7.80 3 6 -3 49.40 7.80 3 6 -3 38.40 5.50 3 6 -3 53.79 10.80 3 6 -3 43.40 9.70 3 6 -3 28.10 11.30 3 6 -3 33.60 4.20 3 6 -3 37.30 11.70 -3 -6 3 35.60 6.90 -3 -6 3 32.70 8.80 2 6 -3 21.50 6.10 2 6 -3 21.60 6.60 2 6 -3 20.50 8.80 2 6 -3 31.60 5.30 2 6 -3 21.40 1.90 2 6 -3 13.90 8.40 2 6 -3 25.30 5.50 -2 -6 3 16.00 7.30 -2 -6 3 12.50 6.10 -2 -6 3 27.10 6.10 -2 -6 3 23.80 5.20 1 6 -3 105.29 9.00 1 6 -3 113.09 12.30 1 6 -3 98.49 8.90 -1 -6 3 97.09 11.80 -1 -6 3 106.49 9.20 -1 -6 3 97.59 8.20 -1 -6 3 95.99 9.10 0 6 -3 47.50 9.20 0 6 -3 54.09 6.80 0 6 -3 41.90 5.80 0 -6 3 48.90 5.60 0 -6 3 36.10 6.70 0 -6 3 49.60 6.30 -1 6 -3 -15.10 4.80 -1 6 -3 1.00 1.60 -1 6 -3 -4.10 6.60 1 -6 3 0.60 2.10 1 -6 3 6.00 4.20 1 -6 3 -8.80 4.40 -2 6 -3 91.09 10.50 -2 6 -3 78.69 6.50 -2 6 -3 96.69 10.60 2 -6 3 96.19 7.60 2 -6 3 74.59 8.90 2 -6 3 92.99 9.10 2 -6 3 81.29 10.20 -3 6 -3 40.80 6.90 3 -6 3 24.80 6.40 3 -6 3 31.80 6.00 3 -6 3 34.80 7.80 3 -6 3 31.00 6.40 -4 6 -3 15.10 6.00 4 -6 3 16.40 7.70 4 -6 3 16.00 5.60 4 -6 3 11.30 6.30 4 -6 3 17.30 6.20 4 -6 3 18.60 11.80 5 -6 3 3.70 8.40 5 -6 3 18.30 8.20 5 -6 3 -3.10 6.10 5 -6 3 9.30 12.20 -6 6 -3 17.20 4.80 -6 6 -3 24.60 12.50 6 -6 3 17.00 10.20 6 -6 3 15.80 7.20 6 -6 3 14.00 7.60 -7 6 -3 27.60 11.60 7 -6 3 1.20 11.20 7 -6 3 5.30 9.00 7 -6 3 -23.50 12.60 -8 6 -3 -1.90 21.10 8 -6 3 1.90 17.00 -9 6 -3 -13.90 23.00 9 -6 3 -55.69 21.80 9 5 -3 -7.80 26.80 9 5 -3 -26.10 24.80 -9 -5 3 20.70 40.60 8 5 -3 24.40 19.70 -8 -5 3 23.50 29.50 7 5 -3 22.60 12.70 7 5 -3 20.40 11.90 -7 -5 3 -10.50 22.30 6 5 -3 12.00 9.60 6 5 -3 20.90 13.70 6 5 -3 25.20 10.10 -6 -5 3 6.70 16.00 5 5 -3 -0.10 6.90 5 5 -3 -0.30 10.20 5 5 -3 2.30 3.70 5 5 -3 10.40 8.40 5 5 -3 -5.40 12.70 -5 -5 3 3.30 8.00 -5 -5 3 -5.40 11.50 4 5 -3 1.90 5.70 4 5 -3 -0.50 4.60 4 5 -3 -8.50 11.50 4 5 -3 -1.80 7.90 4 5 -3 1.10 3.50 4 5 -3 3.90 9.30 -4 -5 3 -1.20 9.50 -4 -5 3 0.50 6.30 3 5 -3 130.09 13.40 3 5 -3 150.68 16.30 3 5 -3 161.48 12.90 3 5 -3 143.19 12.40 3 5 -3 152.68 12.70 3 5 -3 155.08 10.40 3 5 -3 192.58 18.70 3 5 -3 163.98 14.10 -3 -5 3 161.18 13.30 -3 -5 3 133.79 16.10 2 5 -3 381.36 24.20 2 5 -3 398.96 22.90 2 5 -3 399.46 21.70 2 5 -3 365.56 24.90 2 5 -3 406.36 24.60 2 5 -3 384.16 23.80 2 5 -3 397.66 23.90 2 5 -3 391.16 27.30 -2 -5 3 370.06 23.80 -2 -5 3 361.26 24.10 -2 -5 3 360.66 26.40 -2 -5 3 341.87 23.10 1 5 -3 205.28 15.30 1 5 -3 190.08 13.30 1 5 -3 185.08 12.90 -1 -5 3 194.38 14.30 -1 -5 3 204.18 16.00 -1 -5 3 193.58 12.80 -1 -5 3 201.98 13.20 0 5 -3 112.79 8.90 0 5 -3 95.69 8.40 0 5 -3 112.59 10.10 0 -5 3 113.99 8.60 0 -5 3 103.69 9.20 -1 5 -3 24.30 4.60 -1 5 -3 17.20 5.90 -1 5 -3 17.90 4.20 -1 5 -3 16.00 2.50 1 -5 3 13.30 2.80 1 -5 3 11.50 4.80 1 -5 3 13.70 4.20 1 -5 3 18.90 4.20 -2 5 -3 -1.00 5.30 -2 5 -3 -2.70 4.60 -2 5 -3 1.50 2.60 2 -5 3 2.70 3.30 2 -5 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16.00 9.80 6 2 -4 8.60 9.50 -6 -2 4 4.30 10.20 -6 -2 4 7.30 12.40 5 2 -4 13.30 12.20 5 2 -4 -2.70 6.20 5 2 -4 20.30 7.80 5 2 -4 14.30 8.00 -5 -2 4 20.20 8.40 -5 -2 4 13.10 11.20 -5 -2 4 9.80 5.90 4 2 -4 10.30 7.80 4 2 -4 1.70 4.40 4 2 -4 6.50 7.90 4 2 -4 1.40 10.60 4 2 -4 3.80 7.10 4 2 -4 0.70 5.70 -4 -2 4 -6.70 4.60 -4 -2 4 -0.30 8.40 -4 -2 4 -9.20 5.00 -4 -2 4 -0.10 6.20 3 2 -4 79.39 9.10 3 2 -4 71.69 6.30 3 2 -4 74.49 8.90 3 2 -4 105.59 12.50 3 2 -4 72.99 7.60 3 2 -4 89.39 10.40 -3 -2 4 70.19 7.50 -3 -2 4 64.09 10.80 -3 -2 4 68.39 8.60 -3 -2 4 79.19 9.40 2 2 -4 32.70 6.40 2 2 -4 17.90 4.50 2 2 -4 28.30 2.80 2 2 -4 18.60 2.80 2 2 -4 24.40 4.10 2 2 -4 18.70 7.00 -2 -2 4 27.80 5.30 -2 -2 4 18.30 5.20 -2 -2 4 16.10 3.30 -2 -2 4 24.20 4.00 1 2 -4 221.98 14.80 1 2 -4 202.88 12.20 1 2 -4 214.38 13.80 -1 -2 4 211.78 13.70 -1 -2 4 201.88 12.30 -1 -2 4 203.78 12.30 -1 -2 4 222.18 13.60 0 2 -4 -1.40 2.10 0 2 -4 3.10 2.70 0 -2 4 3.20 3.20 0 -2 4 4.50 1.90 0 -2 4 3.20 2.20 -1 2 -4 218.78 14.10 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22.90 -4 -11 -21 -4.80 27.90 4 11 21 38.20 25.40 -5 -11 -21 -1.00 23.40 5 11 21 19.10 26.80 -6 -11 -21 7.60 38.70 6 11 21 -2.20 22.40 3 -12 -21 4.40 35.60 -3 12 21 -24.40 36.50 2 -12 -21 24.70 31.60 -2 12 21 -7.90 30.40 -2 12 21 31.30 28.90 1 -12 -21 26.20 28.70 -1 12 21 42.80 25.50 -1 12 21 25.90 28.50 -1 12 21 42.10 26.80 0 -12 -21 25.50 25.20 0 12 21 -10.50 23.70 0 12 21 5.00 25.50 0 12 21 -18.10 20.90 -1 -12 -21 9.00 25.30 1 12 21 -17.80 19.60 1 12 21 42.30 25.00 1 12 21 -2.40 22.50 -2 -12 -21 -0.20 24.50 -2 -12 -21 -37.80 22.00 2 12 21 18.10 23.00 2 12 21 -0.80 22.80 2 12 21 -24.80 21.00 -3 -12 -21 -0.50 18.80 3 12 21 -4.00 21.50 3 12 21 -4.80 22.20 -4 -12 -21 17.20 27.90 4 12 21 -31.80 23.20 4 12 21 -5.50 22.90 -5 -12 -21 20.50 30.70 5 12 21 20.40 25.00 -6 -12 -21 -4.00 37.70 6 12 21 2.10 31.30 3 -13 -21 9.60 39.30 -3 13 21 -7.80 37.20 -3 13 21 -16.50 28.10 2 -13 -21 -56.79 56.69 -2 13 21 46.50 34.90 -2 13 21 29.20 33.00 1 -13 -21 11.30 29.70 -1 13 21 24.50 27.20 -1 13 21 -17.10 26.90 0 -13 -21 50.29 27.50 0 13 21 15.60 25.40 0 13 21 17.30 27.80 0 13 21 48.70 23.60 -1 -13 -21 -4.60 24.80 1 13 21 -1.50 22.50 1 13 21 0.10 22.70 1 13 21 -28.90 21.90 -2 -13 -21 14.60 22.70 -2 -13 -21 5.50 25.70 2 13 21 23.10 23.20 2 13 21 -17.50 21.10 2 13 21 34.10 23.10 -3 -13 -21 21.80 26.60 3 13 21 13.10 24.10 3 13 21 20.20 22.40 -4 -13 -21 1.10 20.50 4 13 21 -31.30 24.50 4 13 21 -8.60 22.40 -5 -13 -21 0.20 33.50 5 13 21 -19.10 29.50 5 13 21 40.30 28.10 2 -14 -21 16.00 33.00 -2 14 21 -2.90 25.00 -2 14 21 92.79 32.40 1 -14 -21 19.30 29.10 -1 14 21 15.40 28.20 -1 14 21 -16.30 26.90 -1 14 21 -27.30 25.80 0 -14 -21 29.10 47.60 0 -14 -21 22.30 28.20 0 14 21 2.10 19.80 0 14 21 -5.00 24.20 -1 -14 -21 3.80 26.80 -1 -14 -21 8.50 26.20 1 14 21 -7.20 23.30 1 14 21 21.90 25.80 -2 -14 -21 60.09 25.90 -2 -14 -21 22.40 25.20 2 14 21 24.00 22.90 2 14 21 26.20 24.80 -3 -14 -21 -44.70 19.10 3 14 21 -25.00 23.40 3 14 21 5.30 17.60 -4 -14 -21 3.20 29.70 4 14 21 17.90 25.90 4 14 21 37.70 25.00 -5 -14 -21 -38.50 24.10 5 14 21 -49.99 29.00 5 14 21 -45.90 29.70 2 -15 -21 63.29 37.90 -2 15 21 12.70 35.20 -2 15 21 -65.19 33.60 1 -15 -21 16.80 32.10 -1 15 21 8.60 32.30 -1 15 21 -19.30 24.70 0 -15 -21 32.20 29.70 0 15 21 11.80 28.40 0 15 21 2.90 31.90 -1 -15 -21 -10.60 27.50 -1 -15 -21 32.60 27.60 -1 -15 -21 -0.80 25.20 1 15 21 -5.20 19.30 1 15 21 35.60 24.10 -2 -15 -21 -25.90 29.60 -2 -15 -21 30.30 27.70 2 15 21 17.80 24.90 2 15 21 -14.20 18.10 -3 -15 -21 -19.20 27.00 3 15 21 24.50 26.00 3 15 21 50.29 25.40 -4 -15 -21 -11.70 29.20 4 15 21 -13.00 25.10 4 15 21 13.80 25.00 -5 -15 -21 41.90 36.80 5 15 21 54.09 32.30 5 15 21 41.20 31.10 -2 16 21 53.09 38.60 1 -16 -21 48.50 35.90 -1 16 21 -31.00 27.50 -1 16 21 -7.10 32.60 0 -16 -21 -34.00 30.70 0 -16 -21 33.40 32.40 0 16 21 2.10 27.30 0 16 21 4.80 30.10 -1 -16 -21 -48.90 30.60 -1 -16 -21 -17.80 19.90 1 16 21 12.90 25.90 1 16 21 12.90 26.30 -2 -16 -21 2.80 30.00 -2 -16 -21 28.70 28.50 2 16 21 25.50 26.10 2 16 21 5.40 26.60 -3 -16 -21 24.50 31.60 3 16 21 -59.79 26.50 3 16 21 2.50 19.30 -4 -16 -21 -21.00 31.40 4 16 21 32.70 30.10 4 16 21 20.90 28.60 -5 -16 -21 -84.19 37.50 5 16 21 30.40 35.80 5 16 21 -24.30 32.80 1 -17 -21 -61.49 52.39 -1 17 21 36.70 34.90 -1 17 21 15.30 32.30 0 -17 -21 -18.60 32.10 0 17 21 3.50 31.10 0 17 21 -2.50 52.49 -1 -17 -21 -34.30 26.80 -1 -17 -21 -18.70 34.20 1 17 21 33.50 28.00 1 17 21 19.90 29.60 -2 -17 -21 5.60 33.00 -2 -17 -21 22.50 28.60 2 17 21 -58.49 25.30 2 17 21 65.99 29.00 -3 -17 -21 68.09 33.90 -3 -17 -21 -43.20 34.30 3 17 21 -6.00 27.50 3 17 21 -43.80 27.80 -4 -17 -21 -13.10 36.60 4 17 21 7.60 31.10 4 17 21 20.00 31.60 1 -18 -21 -5.40 37.30 -1 18 21 12.60 39.00 -1 18 21 -7.50 34.00 0 -18 -21 26.10 39.90 0 -18 -21 -44.50 30.60 0 18 21 -17.70 29.90 0 18 21 8.20 33.40 -1 -18 -21 -24.50 50.19 -1 -18 -21 -21.20 29.70 1 18 21 38.30 32.30 1 18 21 30.70 29.50 -2 -18 -21 -34.90 30.10 -2 -18 -21 -52.59 34.90 2 18 21 12.30 28.30 2 18 21 -41.20 29.30 -3 -18 -21 -31.30 34.10 -3 -18 -21 -17.30 38.50 3 18 21 30.00 31.20 3 18 21 30.50 31.00 0 -19 -21 -11.70 37.10 0 -19 -21 -30.70 38.50 0 19 21 -10.90 32.60 -1 -19 -21 9.10 38.90 -1 -19 -21 -36.80 33.40 1 19 21 -51.49 31.10 1 19 21 29.10 34.30 -2 -19 -21 20.20 36.10 -2 -19 -21 -49.50 41.60 2 19 21 -9.50 33.10 2 19 21 -39.70 30.10 -1 -3 -22 3.80 38.50 -2 -3 -22 -62.09 35.50 -2 -3 -22 51.99 34.20 2 3 22 3.50 28.30 -3 -3 -22 -21.50 37.00 3 3 22 10.60 30.20 0 -4 -22 -0.60 27.90 0 4 22 89.39 39.80 -1 -4 -22 -31.90 34.30 -2 -4 -22 20.30 30.00 -2 -4 -22 6.80 35.50 2 4 22 -54.09 48.20 -3 -4 -22 10.50 34.50 -3 -4 -22 38.30 30.50 3 4 22 12.50 28.00 -4 -4 -22 15.60 36.40 4 4 22 1.90 27.40 1 -5 -22 29.20 37.90 -1 5 22 75.29 41.90 0 -5 -22 1.90 36.60 0 5 22 14.20 36.50 -1 -5 -22 40.20 35.90 1 5 22 21.50 25.30 -2 -5 -22 -41.20 35.70 -2 -5 -22 -3.50 30.60 2 5 22 25.20 28.00 -3 -5 -22 -12.70 29.20 -3 -5 -22 -46.70 31.80 3 5 22 5.60 26.70 -4 -5 -22 4.50 35.30 4 5 22 39.10 29.40 1 -6 -22 -5.40 36.40 -1 6 22 -15.80 38.00 0 -6 -22 31.60 36.00 0 6 22 61.99 38.30 -1 -6 -22 22.30 34.10 1 6 22 -6.60 25.40 -2 -6 -22 -84.99 26.30 -2 -6 -22 -3.90 34.10 2 6 22 -13.80 26.20 -3 -6 -22 -36.90 32.20 -3 -6 -22 19.80 31.00 3 6 22 11.00 26.10 -4 -6 -22 -29.30 33.90 4 6 22 -14.00 28.30 1 -7 -22 20.50 36.00 -1 7 22 22.60 37.00 0 -7 -22 76.89 33.70 0 7 22 39.60 35.10 -1 -7 -22 55.99 32.90 1 7 22 51.89 25.90 1 7 22 76.39 32.10 -2 -7 -22 -13.30 25.60 -2 -7 -22 20.00 33.00 2 7 22 -29.70 23.60 -3 -7 -22 -9.80 30.20 -3 -7 -22 21.70 30.90 3 7 22 -13.30 25.30 -4 -7 -22 28.70 33.30 4 7 22 -31.20 27.70 -5 -7 -22 82.39 37.60 5 7 22 45.80 28.90 2 -8 -22 0.00 35.60 -2 8 22 32.20 42.30 1 -8 -22 86.69 36.10 -1 8 22 -43.80 34.20 0 -8 -22 -1.60 29.40 0 8 22 16.00 34.30 -1 -8 -22 16.20 28.90 1 8 22 -12.90 30.70 1 8 22 -31.70 22.90 -2 -8 -22 -10.70 30.90 -2 -8 -22 40.50 25.50 2 8 22 24.70 24.90 -3 -8 -22 3.00 30.20 3 8 22 -9.70 25.80 -4 -8 -22 42.70 30.30 4 8 22 59.39 27.30 -5 -8 -22 -17.40 36.70 5 8 22 65.39 31.40 2 -9 -22 -21.50 37.70 -2 9 22 39.80 38.80 1 -9 -22 26.90 32.40 -1 9 22 60.09 34.40 0 -9 -22 -26.70 27.60 0 9 22 10.50 30.00 0 9 22 40.70 36.30 -1 -9 -22 39.50 30.30 1 9 22 -23.50 23.40 1 9 22 59.29 28.40 -2 -9 -22 71.19 30.90 -2 -9 -22 -37.00 24.20 2 9 22 -1.00 24.30 -3 -9 -22 -26.80 29.30 3 9 22 -0.50 25.80 -4 -9 -22 40.20 25.80 4 9 22 24.00 25.60 -5 -9 -22 72.19 38.80 5 9 22 1.40 28.50 2 -10 -22 -4.10 36.30 -2 10 22 41.20 36.40 1 -10 -22 46.30 32.60 -1 10 22 45.40 34.30 0 -10 -22 -13.00 29.00 0 10 22 22.10 29.80 0 10 22 23.30 23.60 -1 -10 -22 -47.40 29.30 1 10 22 -4.20 23.40 1 10 22 18.70 30.00 -2 -10 -22 -28.10 25.80 -2 -10 -22 29.90 27.10 2 10 22 16.50 24.00 -3 -10 -22 -40.80 27.00 3 10 22 -11.20 22.30 -4 -10 -22 -7.50 29.80 4 10 22 -29.30 27.60 -5 -10 -22 32.40 36.40 5 10 22 -32.00 30.20 2 -11 -22 30.40 37.20 -2 11 22 -40.30 38.40 1 -11 -22 -7.60 32.40 -1 11 22 -28.20 31.60 0 -11 -22 75.89 32.60 0 11 22 49.30 30.00 0 11 22 61.49 27.10 -1 -11 -22 -1.30 29.10 1 11 22 -38.00 23.30 1 11 22 -36.70 29.40 -2 -11 -22 -62.79 25.90 -2 -11 -22 53.29 30.10 2 11 22 39.40 26.30 -3 -11 -22 22.40 21.90 3 11 22 51.69 26.20 -4 -11 -22 -12.80 31.60 4 11 22 25.30 26.60 -5 -11 -22 -18.10 33.20 5 11 22 -27.80 27.60 2 -12 -22 -2.70 35.80 -2 12 22 22.80 37.10 1 -12 -22 -14.00 32.40 -1 12 22 -5.60 36.90 0 -12 -22 2.10 30.70 0 12 22 -45.00 28.30 0 12 22 -61.49 28.60 0 12 22 8.40 27.20 -1 -12 -22 7.40 28.90 1 12 22 34.80 27.00 1 12 22 -19.70 25.10 1 12 22 43.80 21.80 -2 -12 -22 23.50 31.70 -2 -12 -22 23.70 19.10 2 12 22 22.60 19.90 2 12 22 12.80 24.70 -3 -12 -22 11.90 28.60 3 12 22 -19.40 26.20 3 12 22 -4.70 26.80 -4 -12 -22 31.60 31.50 4 12 22 -1.20 28.20 -5 -12 -22 -17.90 31.80 5 12 22 1.60 30.50 2 -13 -22 -5.50 39.90 -2 13 22 -30.60 37.30 -2 13 22 31.70 28.70 1 -13 -22 99.19 34.40 -1 13 22 -7.20 31.70 -1 13 22 65.89 34.50 0 -13 -22 -2.00 33.20 0 13 22 33.40 28.80 0 13 22 -29.60 28.20 0 13 22 6.60 22.30 -1 -13 -22 -30.00 29.20 1 13 22 -19.10 24.90 1 13 22 6.20 28.60 1 13 22 16.10 27.50 -2 -13 -22 29.80 46.50 -2 -13 -22 0.80 27.50 2 13 22 -1.50 27.10 2 13 22 4.90 25.70 2 13 22 -89.39 44.60 -3 -13 -22 6.70 28.80 3 13 22 13.10 25.00 3 13 22 -8.10 24.00 -4 -13 -22 22.80 25.10 4 13 22 -0.80 22.00 4 13 22 -51.29 26.80 -5 -13 -22 -2.60 38.10 5 13 22 -42.50 29.60 1 -14 -22 28.50 34.60 -1 14 22 8.40 33.10 -1 14 22 44.20 35.60 0 -14 -22 11.60 30.60 0 14 22 -28.60 31.90 0 14 22 -71.29 28.20 0 14 22 7.50 31.40 -1 -14 -22 -10.40 30.70 1 14 22 65.89 28.00 1 14 22 59.09 30.40 1 14 22 40.50 28.90 -2 -14 -22 2.20 26.30 -2 -14 -22 11.80 30.40 2 14 22 23.90 28.90 2 14 22 12.30 25.80 2 14 22 9.90 27.00 -3 -14 -22 -0.60 28.10 3 14 22 5.80 27.40 3 14 22 31.90 29.40 -4 -14 -22 33.60 34.50 4 14 22 9.00 30.00 4 14 22 26.30 29.30 1 -15 -22 -10.10 52.99 -1 15 22 11.90 35.80 -1 15 22 44.10 35.10 0 -15 -22 7.00 32.00 0 15 22 43.40 28.20 0 15 22 -20.00 34.40 0 15 22 -19.80 30.40 -1 -15 -22 13.60 30.60 -1 -15 -22 -14.20 29.80 1 15 22 45.40 29.60 1 15 22 72.09 45.30 -2 -15 -22 36.90 31.00 2 15 22 48.70 28.60 2 15 22 14.60 29.10 -3 -15 -22 -10.50 31.80 3 15 22 -13.40 26.40 3 15 22 65.79 29.50 -4 -15 -22 18.90 26.40 4 15 22 4.70 31.10 4 15 22 18.70 29.90 -1 16 22 -7.50 28.00 0 16 22 39.00 33.50 0 16 22 78.89 67.99 -1 -16 -22 32.00 31.10 -1 -16 -22 18.30 32.50 1 16 22 -45.70 32.40 1 16 22 -20.30 29.50 -2 -16 -22 3.30 34.30 -2 -16 -22 62.19 32.20 2 16 22 -42.00 27.30 2 16 22 7.10 30.80 -3 -16 -22 -15.20 32.80 3 16 22 18.80 30.00 3 16 22 22.90 27.50 -4 -16 -22 -19.40 37.20 4 16 22 -17.00 33.20 4 16 22 33.00 32.10 0 17 22 15.80 31.40 0 17 22 15.50 26.40 -1 -17 -22 -29.50 24.70 -1 -17 -22 -34.60 38.50 1 17 22 -27.60 31.40 1 17 22 -30.40 34.00 -2 -17 -22 38.50 26.50 -2 -17 -22 32.90 42.00 2 17 22 125.89 34.40 2 17 22 18.20 27.80 -3 -17 -22 21.50 35.00 3 17 22 -11.90 31.50 3 17 22 -19.20 29.50 -1 -18 -22 39.30 42.80 -1 -18 -22 36.40 35.50 1 18 22 -20.10 38.70 1 18 22 -7.70 32.70 -2 -18 -22 -33.20 40.90 -2 -18 -22 12.20 35.80 2 18 22 -40.30 29.90 2 18 22 18.10 34.40 -1 -6 -23 -64.89 36.20 -2 -6 -23 5.00 36.60 -2 -6 -23 12.60 31.10 2 6 23 20.20 29.40 0 -7 -23 -4.10 35.70 0 7 23 -58.09 42.10 -1 -7 -23 -9.90 28.10 -2 -7 -23 11.40 28.80 -2 -7 -23 67.39 34.10 2 7 23 32.30 29.90 -3 -7 -23 41.20 34.00 3 7 23 -27.30 26.90 0 -8 -23 -12.60 28.90 0 8 23 1.00 41.80 -1 -8 -23 -32.90 33.80 1 8 23 16.40 27.30 -2 -8 -23 -25.90 32.40 -2 -8 -23 44.00 34.10 2 8 23 6.10 28.70 -3 -8 -23 5.70 25.40 3 8 23 21.70 29.30 0 -9 -23 31.50 34.30 0 9 23 -7.70 36.90 -1 -9 -23 -6.30 32.80 1 9 23 -16.20 27.60 -2 -9 -23 -9.20 33.70 -2 -9 -23 -75.99 29.60 2 9 23 2.50 29.00 -3 -9 -23 5.40 25.50 3 9 23 -14.60 29.40 -4 -9 -23 14.00 37.70 4 9 23 54.29 32.90 0 -10 -23 35.50 33.80 0 10 23 -21.40 35.70 -1 -10 -23 37.30 33.10 1 10 23 -52.29 27.00 -2 -10 -23 9.50 34.50 -2 -10 -23 -9.60 30.00 2 10 23 -9.40 28.90 -3 -10 -23 -5.20 24.60 3 10 23 7.90 29.80 -4 -10 -23 -28.90 36.60 4 10 23 -22.80 27.10 0 -11 -23 22.20 35.40 0 11 23 102.09 55.39 -1 -11 -23 34.90 35.50 1 11 23 31.40 36.00 1 11 23 2.80 28.90 -2 -11 -23 -2.20 21.90 -2 -11 -23 23.30 34.10 2 11 23 12.20 28.80 -3 -11 -23 26.70 32.60 3 11 23 -0.30 27.80 -4 -11 -23 25.60 36.60 4 11 23 -5.10 32.90 0 -12 -23 75.29 38.80 0 12 23 -20.40 34.20 -1 -12 -23 30.50 35.10 1 12 23 10.70 34.80 1 12 23 21.40 29.70 -2 -12 -23 -48.00 28.40 -2 -12 -23 -1.40 34.50 2 12 23 35.30 28.10 -3 -12 -23 35.40 35.20 3 12 23 1.90 29.90 -4 -12 -23 -2.00 35.70 4 12 23 -32.50 28.00 0 -13 -23 24.40 36.10 0 13 23 19.50 36.40 0 13 23 38.30 38.10 -1 -13 -23 -3.20 36.10 1 13 23 -19.20 35.80 1 13 23 -16.40 30.60 1 13 23 -32.20 31.80 -2 -13 -23 48.60 37.40 -2 -13 -23 27.40 31.60 2 13 23 -29.70 30.00 2 13 23 8.70 30.70 -3 -13 -23 17.50 32.00 3 13 23 -42.70 29.50 3 13 23 11.50 30.70 0 -14 -23 -1.50 37.60 0 14 23 -35.90 51.99 0 14 23 8.80 34.90 0 14 23 -38.30 34.20 -1 -14 -23 17.10 43.70 -1 -14 -23 7.90 30.30 1 14 23 22.80 31.30 1 14 23 19.90 36.80 1 14 23 -5.50 30.90 -2 -14 -23 -37.60 29.80 -2 -14 -23 -50.39 51.39 2 14 23 -54.79 30.00 2 14 23 -11.10 30.10 -3 -14 -23 29.60 34.30 3 14 23 35.40 31.60 3 14 23 17.60 32.00 -1 -15 -23 -53.59 50.79 -1 -15 -23 37.50 34.80 1 15 23 28.80 33.80 1 15 23 15.10 32.20 1 15 23 7.90 35.10 -2 -15 -23 23.00 34.30 2 15 23 10.30 32.20 2 15 23 3.50 34.00 -3 -15 -23 -12.40 36.10 3 15 23 -4.80 32.10 3 15 23 69.39 26.40 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 66604 _publcif_funding_html ; ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.7864(3) 0.17376(17) 0.50489(17) 0.0398(6) Uani 1 1 d . . . . . N1 N 1.2897(3) 0.18556(17) 0.28809(17) 0.0211(6) Uani 1 1 d . . . . . N2 N 1.2190(4) 0.26368(18) 0.20845(18) 0.0248(6) Uani 1 1 d . . . . . N3 N 1.0459(4) 0.28873(18) 0.24609(19) 0.0258(6) Uani 1 1 d . . . . . N4 N 0.1134(3) 0.48037(17) 0.28706(17) 0.0210(6) Uani 1 1 d . . . . . N5 N 0.0098(3) 0.44616(17) 0.38346(17) 0.0204(6) Uani 1 1 d . . . . . N6 N 0.1843(4) 0.25940(19) 0.61369(18) 0.0263(6) Uani 1 1 d . . . . . N7 N 0.0797(4) 0.21498(19) 0.70589(18) 0.0276(6) Uani 1 1 d . . . . . N8 N -0.1067(3) 0.25717(17) 0.70184(17) 0.0201(6) Uani 1 1 d . . . . . C1 C 1.6455(4) 0.1922(2) 0.2096(2) 0.0243(7) Uani 1 1 d . . . . . H1A H 1.6486 0.2633 0.1802 0.029 Uiso 1 1 calc R U . . . C2 C 1.8178(4) 0.1427(2) 0.1927(2) 0.0296(8) Uani 1 1 d . . . . . H2A H 1.9395 0.1802 0.1507 0.036 Uiso 1 1 calc R U . . . C3 C 1.8130(5) 0.0395(2) 0.2363(2) 0.0292(8) Uani 1 1 d . . . . . H3A H 1.9318 0.0062 0.2249 0.035 Uiso 1 1 calc R U . . . C4 C 1.6358(5) -0.0159(2) 0.2967(2) 0.0276(7) Uani 1 1 d . . . . . H4A H 1.6335 -0.0871 0.3268 0.033 Uiso 1 1 calc R U . . . C5 C 1.4621(4) 0.0323(2) 0.3134(2) 0.0253(7) Uani 1 1 d . . . . . H5A H 1.3393 -0.0052 0.3539 0.030 Uiso 1 1 calc R U . . . C6 C 1.4703(4) 0.1363(2) 0.2699(2) 0.0209(7) Uani 1 1 d . . . . . C7 C 1.2114(5) 0.0891(2) 0.4772(2) 0.0307(8) Uani 1 1 d . . . . . H7A H 1.3594 0.0931 0.4766 0.046 Uiso 1 1 calc R U . . . H7B H 1.1709 0.0211 0.4921 0.046 Uiso 1 1 calc R U . . . H7C H 1.1360 0.1047 0.5291 0.046 Uiso 1 1 calc R U . . . C8 C 1.1627(4) 0.1624(2) 0.3768(2) 0.0218(7) Uani 1 1 d . . . . . C9 C 1.0059(4) 0.2279(2) 0.3485(2) 0.0217(7) Uani 1 1 d . . . . . C10 C 0.8160(5) 0.2334(2) 0.4125(3) 0.0285(8) Uani 1 1 d . . . . . C11 C 0.6692(4) 0.3085(2) 0.3636(2) 0.0281(8) Uani 1 1 d . . . . . H11A H 0.6991 0.3548 0.2936 0.034 Uiso 1 1 calc R U . . . C12 C 0.4927(4) 0.3105(2) 0.4194(2) 0.0275(8) Uani 1 1 d . . . . . H12A H 0.4746 0.2644 0.4895 0.033 Uiso 1 1 calc R U . . . C13 C 0.3236(4) 0.3768(2) 0.3833(2) 0.0204(7) Uani 1 1 d . . . . . C14 C 0.2990(4) 0.4407(2) 0.2852(2) 0.0235(7) Uani 1 1 d . . . . . H14A H 0.3964 0.4543 0.2264 0.028 Uiso 1 1 calc R U . . . C15 C 0.1358(4) 0.3836(2) 0.4421(2) 0.0199(7) Uani 1 1 d . . . . . C16 C 0.0655(4) 0.3284(2) 0.5512(2) 0.0190(7) Uani 1 1 d . . . . . C17 C -0.1225(4) 0.3291(2) 0.6067(2) 0.0181(7) Uani 1 1 d . . . . . C18 C -0.3057(4) 0.3905(2) 0.5804(2) 0.0230(7) Uani 1 1 d . . . . . H18A H -0.3575 0.4092 0.6334 0.035 Uiso 1 1 calc R U . . . H18B H -0.4128 0.3515 0.5746 0.035 Uiso 1 1 calc R U . . . H18C H -0.2676 0.4513 0.5159 0.035 Uiso 1 1 calc R U . . . C19 C -0.2606(4) 0.2156(2) 0.7913(2) 0.0197(7) Uani 1 1 d . . . . . C20 C -0.4500(4) 0.1823(2) 0.7869(2) 0.0233(7) Uani 1 1 d . . . . . H20A H -0.4793 0.1897 0.7249 0.028 Uiso 1 1 calc R U . . . C21 C -0.5946(4) 0.1387(2) 0.8733(2) 0.0255(7) Uani 1 1 d . . . . . H21A H -0.7240 0.1162 0.8701 0.031 Uiso 1 1 calc R U . . . C22 C -0.5553(4) 0.1269(2) 0.9648(2) 0.0219(7) Uani 1 1 d . . . . . C23 C -0.3655(5) 0.1602(2) 0.9673(2) 0.0260(7) Uani 1 1 d . . . . . H23A H -0.3358 0.1520 1.0296 0.031 Uiso 1 1 calc R U . . . C24 C -0.2170(4) 0.2053(2) 0.8810(2) 0.0231(7) Uani 1 1 d . . . . . H24A H -0.0882 0.2286 0.8840 0.028 Uiso 1 1 calc R U . . . C25 C -0.7177(5) 0.0808(2) 1.0579(2) 0.0340(8) Uani 1 1 d . . . . . H25A H -0.6700 0.0852 1.1135 0.051 Uiso 1 1 calc R U . . . H25B H -0.7437 0.0102 1.0768 0.051 Uiso 1 1 calc R U . . . H25C H -0.8448 0.1170 1.0441 0.051 Uiso 1 1 calc R U . . . C26 C 0.0061(5) 0.5389(2) 0.2056(2) 0.0231(7) Uani 1 1 d . . . . . C27 C -0.1798(4) 0.5783(2) 0.2236(2) 0.0261(7) Uani 1 1 d . . . . . H27A H -0.2316 0.5697 0.2894 0.031 Uiso 1 1 calc R U . . . C28 C -0.2905(5) 0.6301(2) 0.1459(2) 0.0306(8) Uani 1 1 d . . . . . H28A H -0.4187 0.6563 0.1588 0.037 Uiso 1 1 calc R U . . . C29 C -0.2152(5) 0.6438(2) 0.0496(2) 0.0338(8) Uani 1 1 d . . . . . H29A H -0.2907 0.6797 -0.0039 0.041 Uiso 1 1 calc R U . . . C30 C -0.0290(5) 0.6047(2) 0.0321(2) 0.0337(8) Uani 1 1 d . . . . . H30A H 0.0228 0.6141 -0.0340 0.040 Uiso 1 1 calc R U . . . C31 C 0.0832(5) 0.5523(2) 0.1086(2) 0.0315(8) Uani 1 1 d . . . . . H31A H 0.2109 0.5257 0.0956 0.038 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0358(14) 0.0414(15) 0.0325(14) -0.0128(12) 0.0056(11) -0.0027(11) N1 0.0188(13) 0.0226(14) 0.0212(14) -0.0096(12) -0.0046(11) 0.0043(11) N2 0.0270(15) 0.0233(14) 0.0217(14) -0.0073(12) -0.0089(11) 0.0043(11) N3 0.0219(14) 0.0244(15) 0.0310(16) -0.0126(13) -0.0059(12) 0.0043(11) N4 0.0212(14) 0.0202(14) 0.0168(14) -0.0061(11) 0.0009(11) 0.0015(11) N5 0.0209(13) 0.0203(14) 0.0184(14) -0.0090(11) 0.0009(11) 0.0003(11) N6 0.0212(14) 0.0317(15) 0.0201(14) -0.0083(12) -0.0015(12) 0.0049(12) N7 0.0190(14) 0.0352(16) 0.0237(15) -0.0101(13) -0.0046(12) 0.0073(12) N8 0.0170(13) 0.0247(14) 0.0175(14) -0.0091(12) -0.0038(10) 0.0059(11) C1 0.0270(18) 0.0238(17) 0.0237(17) -0.0130(14) -0.0013(13) -0.0032(14) C2 0.0199(17) 0.042(2) 0.0342(19) -0.0253(17) 0.0000(14) -0.0017(15) C3 0.0272(18) 0.042(2) 0.0296(19) -0.0251(17) -0.0088(15) 0.0113(15) C4 0.0309(19) 0.0272(18) 0.0270(18) -0.0135(15) -0.0094(15) 0.0069(15) C5 0.0242(17) 0.0292(19) 0.0225(17) -0.0119(15) -0.0047(13) 0.0036(14) C6 0.0203(16) 0.0239(18) 0.0202(16) -0.0112(14) -0.0058(13) 0.0038(13) C7 0.0275(18) 0.036(2) 0.0227(18) -0.0094(16) -0.0016(14) -0.0013(15) C8 0.0217(16) 0.0241(17) 0.0213(17) -0.0125(14) -0.0016(13) -0.0020(13) C9 0.0203(16) 0.0226(17) 0.0227(18) -0.0110(15) -0.0029(13) -0.0003(13) C10 0.0253(18) 0.0254(18) 0.038(2) -0.0166(17) -0.0070(15) -0.0007(14) C11 0.0247(17) 0.0265(18) 0.038(2) -0.0190(16) -0.0066(15) -0.0005(14) C12 0.0192(17) 0.0337(19) 0.041(2) -0.0282(17) -0.0008(15) -0.0020(14) C13 0.0179(16) 0.0229(17) 0.0228(17) -0.0141(15) 0.0014(13) -0.0006(13) C14 0.0208(17) 0.0237(17) 0.0258(18) -0.0146(15) 0.0070(13) -0.0020(13) C15 0.0190(16) 0.0186(16) 0.0233(17) -0.0105(14) -0.0039(13) 0.0000(13) C16 0.0178(16) 0.0183(16) 0.0198(17) -0.0082(14) -0.0031(13) 0.0027(12) C17 0.0207(16) 0.0157(16) 0.0175(16) -0.0069(14) -0.0053(13) 0.0032(12) C18 0.0220(16) 0.0241(17) 0.0205(17) -0.0090(14) -0.0031(13) 0.0070(13) C19 0.0240(16) 0.0177(16) 0.0145(16) -0.0054(13) -0.0034(13) 0.0049(13) C20 0.0226(17) 0.0308(18) 0.0199(17) -0.0135(15) -0.0074(13) 0.0032(13) C21 0.0211(16) 0.0279(18) 0.0241(18) -0.0092(15) -0.0046(14) 0.0029(14) C22 0.0255(17) 0.0166(16) 0.0182(17) -0.0044(13) -0.0034(13) 0.0083(13) C23 0.0369(19) 0.0249(18) 0.0151(16) -0.0075(14) -0.0098(14) 0.0107(15) C24 0.0224(16) 0.0256(17) 0.0226(17) -0.0107(14) -0.0103(13) 0.0039(13) C25 0.0348(19) 0.0333(19) 0.0244(18) -0.0081(16) 0.0007(15) 0.0089(15) C26 0.0309(18) 0.0133(15) 0.0180(17) -0.0025(13) -0.0002(14) -0.0012(13) C27 0.0280(18) 0.0258(18) 0.0166(17) -0.0053(14) 0.0020(14) 0.0012(14) C28 0.0316(18) 0.0236(18) 0.0254(19) -0.0028(15) -0.0037(15) 0.0047(14) C29 0.048(2) 0.0217(18) 0.0218(18) -0.0012(15) -0.0090(16) 0.0061(16) C30 0.053(2) 0.0261(18) 0.0160(17) -0.0063(15) -0.0031(16) 0.0089(16) C31 0.0369(19) 0.0252(18) 0.0255(19) -0.0087(15) 0.0013(15) 0.0052(15) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C8 N1 N2 111.4(2) . . C8 N1 C6 128.8(2) . . N2 N1 C6 119.7(2) . . N3 N2 N1 106.5(2) . . N2 N3 C9 109.2(2) . . C14 N4 N5 111.9(2) . . C14 N4 C26 129.3(2) . . N5 N4 C26 118.2(2) . . C15 N5 N4 105.0(2) . . N7 N6 C16 109.1(2) . . N6 N7 N8 106.6(2) . . N7 N8 C17 111.7(2) . . N7 N8 C19 118.4(2) . . C17 N8 C19 129.6(2) . . C6 C1 C2 118.8(3) . . C6 C1 H1A 120.6 . . C2 C1 H1A 120.6 . . C3 C2 C1 120.4(3) . . C3 C2 H2A 119.8 . . C1 C2 H2A 119.8 . . C2 C3 C4 120.3(3) . . C2 C3 H3A 119.9 . . C4 C3 H3A 119.9 . . C3 C4 C5 120.1(3) . . C3 C4 H4A 120.0 . . C5 C4 H4A 120.0 . . C4 C5 C6 118.9(3) . . C4 C5 H5A 120.6 . . C6 C5 H5A 120.6 . . C1 C6 C5 121.6(3) . . C1 C6 N1 119.9(3) . . C5 C6 N1 118.5(2) . . C8 C7 H7A 109.5 . . C8 C7 H7B 109.5 . . H7A C7 H7B 109.5 . . C8 C7 H7C 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . N1 C8 C9 103.8(2) . . N1 C8 C7 123.6(3) . . C9 C8 C7 132.3(3) . . N3 C9 C8 109.1(2) . . N3 C9 C10 122.5(3) . . C8 C9 C10 128.3(3) . . O1 C10 C11 122.9(3) . . O1 C10 C9 119.2(3) . . C11 C10 C9 117.9(3) . . C12 C11 C10 118.4(3) . . C12 C11 H11A 120.8 . . C10 C11 H11A 120.8 . . C11 C12 C13 126.3(3) . . C11 C12 H12A 116.9 . . C13 C12 H12A 116.9 . . C14 C13 C15 103.7(3) . . C14 C13 C12 128.5(3) . . C15 C13 C12 127.6(3) . . N4 C14 C13 108.2(2) . . N4 C14 H14A 125.9 . . C13 C14 H14A 125.9 . . N5 C15 C13 111.3(2) . . N5 C15 C16 119.1(2) . . C13 C15 C16 129.4(3) . . N6 C16 C17 109.3(2) . . N6 C16 C15 121.3(2) . . C17 C16 C15 129.2(3) . . N8 C17 C16 103.2(2) . . N8 C17 C18 123.6(2) . . C16 C17 C18 133.2(3) . . C17 C18 H18A 109.5 . . C17 C18 H18B 109.5 . . H18A C18 H18B 109.5 . . C17 C18 H18C 109.5 . . H18A C18 H18C 109.5 . . H18B C18 H18C 109.5 . . C24 C19 C20 120.6(3) . . C24 C19 N8 120.1(3) . . C20 C19 N8 119.3(2) . . C21 C20 C19 119.5(3) . . C21 C20 H20A 120.3 . . C19 C20 H20A 120.3 . . C20 C21 C22 121.4(3) . . C20 C21 H21A 119.3 . . C22 C21 H21A 119.3 . . C23 C22 C21 118.1(3) . . C23 C22 C25 121.5(3) . . C21 C22 C25 120.4(3) . . C22 C23 C24 121.8(3) . . C22 C23 H23A 119.1 . . C24 C23 H23A 119.1 . . C19 C24 C23 118.7(3) . . C19 C24 H24A 120.7 . . C23 C24 H24A 120.7 . . C22 C25 H25A 109.5 . . C22 C25 H25B 109.5 . . H25A C25 H25B 109.5 . . C22 C25 H25C 109.5 . . H25A C25 H25C 109.5 . . H25B C25 H25C 109.5 . . C27 C26 C31 120.0(3) . . C27 C26 N4 119.9(3) . . C31 C26 N4 120.1(3) . . C28 C27 C26 120.1(3) . . C28 C27 H27A 120.0 . . C26 C27 H27A 120.0 . . C27 C28 C29 120.3(3) . . C27 C28 H28A 119.8 . . C29 C28 H28A 119.8 . . C30 C29 C28 119.2(3) . . C30 C29 H29A 120.4 . . C28 C29 H29A 120.4 . . C31 C30 C29 121.3(3) . . C31 C30 H30A 119.3 . . C29 C30 H30A 119.3 . . C30 C31 C26 119.0(3) . . C30 C31 H31A 120.5 . . C26 C31 H31A 120.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 O1 C10 1.249(4) . N1 C8 1.360(3) . N1 N2 1.370(3) . N1 C6 1.436(3) . N2 N3 1.314(3) . N3 C9 1.371(4) . N4 C14 1.343(4) . N4 N5 1.367(3) . N4 C26 1.426(4) . N5 C15 1.330(3) . N6 N7 1.314(3) . N6 C16 1.362(4) . N7 N8 1.359(3) . N8 C17 1.360(3) . N8 C19 1.438(3) . C1 C6 1.376(4) . C1 C2 1.390(4) . C1 H1A 0.9500 . C2 C3 1.377(4) . C2 H2A 0.9500 . C3 C4 1.384(4) . C3 H3A 0.9500 . C4 C5 1.384(4) . C4 H4A 0.9500 . C5 C6 1.389(4) . C5 H5A 0.9500 . C7 C8 1.486(4) . C7 H7A 0.9800 . C7 H7B 0.9800 . C7 H7C 0.9800 . C8 C9 1.378(4) . C9 C10 1.479(4) . C10 C11 1.461(4) . C11 C12 1.331(4) . C11 H11A 0.9500 . C12 C13 1.465(4) . C12 H12A 0.9500 . C13 C14 1.378(4) . C13 C15 1.433(4) . C14 H14A 0.9500 . C15 C16 1.464(4) . C16 C17 1.383(4) . C17 C18 1.484(4) . C18 H18A 0.9800 . C18 H18B 0.9800 . C18 H18C 0.9800 . C19 C24 1.379(4) . C19 C20 1.391(4) . C20 C21 1.375(4) . C20 H20A 0.9500 . C21 C22 1.386(4) . C21 H21A 0.9500 . C22 C23 1.383(4) . C22 C25 1.507(4) . C23 C24 1.391(4) . C23 H23A 0.9500 . C24 H24A 0.9500 . C25 H25A 0.9800 . C25 H25B 0.9800 . C25 H25C 0.9800 . C26 C27 1.384(4) . C26 C31 1.397(4) . C27 C28 1.383(4) . C27 H27A 0.9500 . C28 C29 1.386(4) . C28 H28A 0.9500 . C29 C30 1.381(4) . C29 H29A 0.9500 . C30 C31 1.380(4) . C30 H30A 0.9500 . C31 H31A 0.9500 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C8 N1 N2 N3 -1.2(3) . . . . C6 N1 N2 N3 175.3(2) . . . . N1 N2 N3 C9 0.2(3) . . . . C14 N4 N5 C15 -0.1(3) . . . . C26 N4 N5 C15 171.6(2) . . . . C16 N6 N7 N8 -0.7(3) . . . . N6 N7 N8 C17 0.0(3) . . . . N6 N7 N8 C19 174.1(2) . . . . C6 C1 C2 C3 -0.6(4) . . . . C1 C2 C3 C4 0.6(5) . . . . C2 C3 C4 C5 0.2(5) . . . . C3 C4 C5 C6 -1.0(4) . . . . C2 C1 C6 C5 -0.2(4) . . . . C2 C1 C6 N1 -179.6(3) . . . . C4 C5 C6 C1 1.0(4) . . . . C4 C5 C6 N1 -179.6(3) . . . . C8 N1 C6 C1 -134.7(3) . . . . N2 N1 C6 C1 49.4(4) . . . . C8 N1 C6 C5 45.9(4) . . . . N2 N1 C6 C5 -129.9(3) . . . . N2 N1 C8 C9 1.6(3) . . . . C6 N1 C8 C9 -174.5(3) . . . . N2 N1 C8 C7 -172.7(3) . . . . C6 N1 C8 C7 11.2(5) . . . . N2 N3 C9 C8 0.8(3) . . . . N2 N3 C9 C10 -176.6(3) . . . . N1 C8 C9 N3 -1.5(3) . . . . C7 C8 C9 N3 172.1(3) . . . . N1 C8 C9 C10 175.8(3) . . . . C7 C8 C9 C10 -10.6(5) . . . . N3 C9 C10 O1 177.9(3) . . . . C8 C9 C10 O1 0.9(5) . . . . N3 C9 C10 C11 -1.3(4) . . . . C8 C9 C10 C11 -178.3(3) . . . . O1 C10 C11 C12 -2.9(5) . . . . C9 C10 C11 C12 176.3(3) . . . . C10 C11 C12 C13 -177.1(3) . . . . C11 C12 C13 C14 8.9(5) . . . . C11 C12 C13 C15 -177.1(3) . . . . N5 N4 C14 C13 0.3(3) . . . . C26 N4 C14 C13 -170.2(3) . . . . C15 C13 C14 N4 -0.3(3) . . . . C12 C13 C14 N4 174.8(3) . . . . N4 N5 C15 C13 -0.1(3) . . . . N4 N5 C15 C16 -176.2(2) . . . . C14 C13 C15 N5 0.3(3) . . . . C12 C13 C15 N5 -174.9(3) . . . . C14 C13 C15 C16 175.9(3) . . . . C12 C13 C15 C16 0.7(5) . . . . N7 N6 C16 C17 1.1(3) . . . . N7 N6 C16 C15 -174.8(2) . . . . N5 C15 C16 N6 176.3(3) . . . . C13 C15 C16 N6 1.0(5) . . . . N5 C15 C16 C17 1.3(4) . . . . C13 C15 C16 C17 -174.0(3) . . . . N7 N8 C17 C16 0.6(3) . . . . C19 N8 C17 C16 -172.7(3) . . . . N7 N8 C17 C18 -177.6(2) . . . . C19 N8 C17 C18 9.2(4) . . . . N6 C16 C17 N8 -1.0(3) . . . . C15 C16 C17 N8 174.4(3) . . . . N6 C16 C17 C18 176.9(3) . . . . C15 C16 C17 C18 -7.6(5) . . . . N7 N8 C19 C24 54.0(4) . . . . C17 N8 C19 C24 -133.1(3) . . . . N7 N8 C19 C20 -123.4(3) . . . . C17 N8 C19 C20 49.5(4) . . . . C24 C19 C20 C21 -0.1(4) . . . . N8 C19 C20 C21 177.3(3) . . . . C19 C20 C21 C22 -0.2(4) . . . . C20 C21 C22 C23 -0.1(4) . . . . C20 C21 C22 C25 178.8(3) . . . . C21 C22 C23 C24 0.7(4) . . . . C25 C22 C23 C24 -178.2(3) . . . . C20 C19 C24 C23 0.6(4) . . . . N8 C19 C24 C23 -176.8(2) . . . . C22 C23 C24 C19 -0.9(4) . . . . C14 N4 C26 C27 -175.7(3) . . . . N5 N4 C26 C27 14.3(4) . . . . C14 N4 C26 C31 7.5(4) . . . . N5 N4 C26 C31 -162.5(3) . . . . C31 C26 C27 C28 0.6(4) . . . . N4 C26 C27 C28 -176.2(3) . . . . C26 C27 C28 C29 -0.7(5) . . . . C27 C28 C29 C30 0.3(5) . . . . C28 C29 C30 C31 0.0(5) . . . . C29 C30 C31 C26 -0.1(5) . . . . C27 C26 C31 C30 -0.2(4) . . . . N4 C26 C31 C30 176.6(3) . . . .