#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:11:39 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179743 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/39/7003901.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7003901
loop_
_publ_author_name
'Hill, Michael S.'
'Hitchcock, Peter B.'
'Pongtavornpinyo, Ruti'
_publ_section_title
;
 Organoiron compounds derived from the indium ‘carbene
 analogues’, [In{N(Ar)C(Me)}2CH] (Ar = dipp = 2,6-iPr2C6H3; =
 Mes = 2,4,6-Me3C6H2)
;
_journal_issue                   21
_journal_name_full               'Dalton Transactions'
_journal_page_first              2854
_journal_page_last               2860
_journal_paper_doi               10.1039/b801160e
_journal_year                    2008
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C29 H43 N2, C32 H12 B F24'
_chemical_formula_sum            'C61 H55 B F24 N2'
_chemical_formula_weight         1282.88
_chemical_name_systematic
;
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_conform_dict_location     ftp://ftp.iucr.org/pub/cif_core.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.3
_audit_creation_date             2005-06-27T11:32:04-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 98.741(5)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.4446(9)
_cell_length_b                   18.3705(14)
_cell_length_c                   19.2043(14)
_cell_measurement_reflns_used    43449
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      24.108
_cell_measurement_theta_min      3.395
_cell_measurement_wavelength     0.71073
_cell_volume                     6082.8(7)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor 1997)'
_computing_data_collection       'Collect (Nonius BV, 1997-2000)'
_computing_data_reduction
'HKL Denzo and Scalepack (Otwinowski & Minor 1997)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1986)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_device       '95mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'CCD rotation images, thick slices'
_diffrn_orient_matrix_type       'by Nonius Collect from scalepack cell'
_diffrn_orient_matrix_UB_11      0.568973E-1
_diffrn_orient_matrix_UB_12      -0.10541E-1
_diffrn_orient_matrix_UB_13      0.83727E-2
_diffrn_orient_matrix_UB_21      -0.8943E-3
_diffrn_orient_matrix_UB_22      -0.70264E-2
_diffrn_orient_matrix_UB_23      -0.517533E-1
_diffrn_orient_matrix_UB_31      0.112101E-1
_diffrn_orient_matrix_UB_32      0.529405E-1
_diffrn_orient_matrix_UB_33      -0.52017E-2
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1385
_diffrn_reflns_av_unetI/netI     0.0974
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            19000
_diffrn_reflns_theta_full        24.15
_diffrn_reflns_theta_max         24.15
_diffrn_reflns_theta_min         3.43
_diffrn_source                   'Enraf Nonius FR590'
_exptl_absorpt_coefficient_mu    0.133
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.401
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2624
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.458
_refine_diff_density_min         -0.271
_refine_diff_density_rms         0.058
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     403
_refine_ls_number_reflns         4760
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.1413
_refine_ls_R_factor_gt           0.0803
_refine_ls_shift/su_max          0
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0631P)²+19.5493P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1686
_refine_ls_wR_factor_ref         0.2016
_reflns_number_gt                2878
_reflns_number_total             4760
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b801160e.txt
_cod_data_source_block           (4)-jun2505
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7003901
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
N N -0.0286(2) 0.1657(2) 0.1261(2) 0.0414(10) Uani 1 1 d . . .
H1X H -0.033(3) 0.189(2) 0.083(3) 0.055(15) Uiso 1 1 d . . .
C1 C -0.0083(3) 0.2053(2) 0.1843(2) 0.0391(11) Uani 1 1 d . . .
C2 C 0 0.1728(3) 0.25 0.0362(15) Uani 1 2 d S . .
H2 H 0 0.1211 0.25 0.043 Uiso 1 2 calc SR . .
C3 C 0.0087(3) 0.2836(2) 0.1697(3) 0.0567(14) Uani 1 1 d . . .
H3A H 0.0213 0.288 0.1219 0.085 Uiso 1 1 calc R . .
H3B H 0.0528 0.3003 0.2037 0.085 Uiso 1 1 calc R . .
H3C H -0.0369 0.3134 0.1741 0.085 Uiso 1 1 calc R . .
C4 C -0.0580(3) 0.0914(2) 0.1245(2) 0.0414(12) Uani 1 1 d . . .
C5 C -0.1377(3) 0.0819(3) 0.1172(2) 0.0471(12) Uani 1 1 d . . .
C6 C -0.1644(3) 0.0103(3) 0.1167(3) 0.0571(14) Uani 1 1 d . . .
H6 H -0.2186 0.0011 0.1115 0.069 Uiso 1 1 calc R . .
C7 C -0.1131(4) -0.0471(3) 0.1237(3) 0.0652(16) Uani 1 1 d . . .
H7 H -0.1323 -0.0955 0.124 0.078 Uiso 1 1 calc R . .
C8 C -0.0353(4) -0.0355(3) 0.1302(3) 0.0635(16) Uani 1 1 d . . .
H8 H -0.001 -0.076 0.1359 0.076 Uiso 1 1 calc R . .
C9 C -0.0049(3) 0.0344(3) 0.1286(2) 0.0488(13) Uani 1 1 d . . .
C10 C -0.1957(3) 0.1440(3) 0.1071(3) 0.0596(15) Uani 1 1 d . . .
H10 H -0.1661 0.1903 0.1177 0.072 Uiso 1 1 calc R . .
C11 C -0.2551(4) 0.1395(3) 0.1569(4) 0.0825(19) Uani 1 1 d . . .
H11A H -0.2907 0.1809 0.1486 0.124 Uiso 1 1 calc R . .
H11B H -0.2285 0.1407 0.2056 0.124 Uiso 1 1 calc R . .
H11C H -0.2844 0.094 0.1486 0.124 Uiso 1 1 calc R . .
C12 C -0.2346(4) 0.1475(4) 0.0303(3) 0.091(2) Uani 1 1 d . . .
H12A H -0.2713 0.1883 0.0242 0.137 Uiso 1 1 calc R . .
H12B H -0.2624 0.1019 0.0176 0.137 Uiso 1 1 calc R . .
H12C H -0.195 0.1547 -0.0003 0.137 Uiso 1 1 calc R . .
C13 C 0.0812(3) 0.0460(3) 0.1299(3) 0.0604(14) Uani 1 1 d . . .
H13 H 0.0906 0.0995 0.1275 0.072 Uiso 1 1 calc R . .
C14 C 0.1083(4) 0.0106(4) 0.0660(3) 0.0816(19) Uani 1 1 d . . .
H14A H 0.164 0.0191 0.0677 0.122 Uiso 1 1 calc R . .
H14B H 0.08 0.032 0.0228 0.122 Uiso 1 1 calc R . .
H14C H 0.0982 -0.0418 0.0664 0.122 Uiso 1 1 calc R . .
C15 C 0.1286(4) 0.0174(4) 0.1970(3) 0.098(2) Uani 1 1 d . . .
H15A H 0.1838 0.0265 0.1959 0.148 Uiso 1 1 calc R . .
H15B H 0.1199 -0.0351 0.2009 0.148 Uiso 1 1 calc R . .
H15C H 0.1129 0.0422 0.2377 0.148 Uiso 1 1 calc R . .
B B 0.5 0.0703(4) 0.25 0.0339(17) Uani 1 2 d S . 1
C16 C 0.4383(3) 0.0153(2) 0.2800(2) 0.0367(11) Uani 1 1 d . A 1
C17 C 0.4368(3) 0.0029(2) 0.3512(2) 0.0379(11) Uani 1 1 d . A 1
H17 H 0.4713 0.0296 0.3849 0.045 Uiso 1 1 calc R A 1
C18 C 0.3862(3) -0.0477(2) 0.3753(2) 0.0391(11) Uani 1 1 d . A 1
C19 C 0.3369(3) -0.0884(2) 0.3275(3) 0.0426(12) Uani 1 1 d . A 1
H19 H 0.303 -0.123 0.3435 0.051 Uiso 1 1 calc R A 1
C20 C 0.3372(3) -0.0785(2) 0.2563(2) 0.0393(11) Uani 1 1 d . A 1
C21 C 0.3875(3) -0.0284(2) 0.2336(2) 0.0402(11) Uani 1 1 d . A 1
H21 H 0.3878 -0.0234 0.1844 0.048 Uiso 1 1 calc R A 1
C22 C 0.3896(3) -0.0586(3) 0.4525(3) 0.0484(13) Uani 1 1 d . A 1
C23 C 0.2890(3) -0.1257(3) 0.2051(3) 0.0591(14) Uani 1 1 d . A 1
C24 C 0.5416(3) 0.1253(2) 0.3114(2) 0.0346(11) Uani 1 1 d . B 1
C25 C 0.4954(3) 0.1690(2) 0.3480(2) 0.0383(11) Uani 1 1 d . B 1
H25 H 0.4407 0.1625 0.3393 0.046 Uiso 1 1 calc R B 1
C26 C 0.5260(3) 0.2211(2) 0.3964(2) 0.0378(11) Uani 1 1 d . B 1
C27 C 0.6046(3) 0.2333(2) 0.4097(2) 0.0433(12) Uani 1 1 d . B 1
H27 H 0.6256 0.269 0.4429 0.052 Uiso 1 1 calc R B 1
C28 C 0.6526(3) 0.1923(2) 0.3737(2) 0.0391(11) Uani 1 1 d . B 1
C29 C 0.6214(3) 0.1393(2) 0.3263(2) 0.0388(11) Uani 1 1 d . B 1
H29 H 0.6556 0.1114 0.3029 0.047 Uiso 1 1 calc R B 1
C30 C 0.4723(3) 0.2638(3) 0.4339(3) 0.0480(13) Uani 1 1 d . B 1
C31 C 0.7374(3) 0.2035(3) 0.3877(3) 0.0533(13) Uani 1 1 d . B 1
F1 F 0.3970(2) 0.00217(17) 0.48933(16) 0.0877(12) Uani 1 1 d . A 1
F2 F 0.3273(2) -0.0912(2) 0.46902(17) 0.0911(12) Uani 1 1 d . A 1
F3 F 0.4502(2) -0.0985(2) 0.48007(17) 0.0944(12) Uani 1 1 d . A 1
F4 F 0.2684(2) -0.09631(18) 0.14267(18) 0.0868(11) Uani 1 1 d . A 1
F5 F 0.2230(2) -0.14658(18) 0.22625(19) 0.0862(11) Uani 1 1 d . A 1
F6 F 0.3244(2) -0.18873(17) 0.1948(2) 0.1002(14) Uani 1 1 d . A 1
F7 F 0.4149(2) 0.29494(17) 0.39074(16) 0.0784(10) Uani 1 1 d . B 1
F8 F 0.50689(19) 0.31741(16) 0.47384(16) 0.0719(9) Uani 1 1 d . B 1
F9 F 0.4381(2) 0.22285(15) 0.47794(17) 0.0731(10) Uani 1 1 d . B 1
F10 F 0.7588(2) 0.26855(18) 0.4152(2) 0.0902(12) Uani 1 1 d . B 1
F11 F 0.7722(2) 0.1985(2) 0.33165(19) 0.1088(14) Uani 1 1 d . B 1
F12 F 0.7753(2) 0.1575(2) 0.4346(2) 0.1009(13) Uani 1 1 d . B 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 N C4 125.1(4) . . ?
C1 N H1X 118(3) . . ?
C4 N H1X 116(3) . . ?
N C1 C2 120.5(4) . . ?
N C1 C3 113.5(4) . . ?
C2 C1 C3 125.9(4) . . ?
C1 C2 C1 128.9(6) . 2 ?
C1 C2 H2 115.5 . . ?
C1 C2 H2 115.5 2 . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C5 C4 C9 124.0(4) . . ?
C5 C4 N 117.7(4) . . ?
C9 C4 N 118.3(4) . . ?
C4 C5 C6 116.7(5) . . ?
C4 C5 C10 123.8(4) . . ?
C6 C5 C10 119.5(5) . . ?
C7 C6 C5 120.7(5) . . ?
C7 C6 H6 119.7 . . ?
C5 C6 H6 119.7 . . ?
C8 C7 C6 120.9(5) . . ?
C8 C7 H7 119.6 . . ?
C6 C7 H7 119.6 . . ?
C7 C8 C9 121.4(5) . . ?
C7 C8 H8 119.3 . . ?
C9 C8 H8 119.3 . . ?
C8 C9 C4 116.3(5) . . ?
C8 C9 C13 120.6(5) . . ?
C4 C9 C13 123.1(4) . . ?
C11 C10 C5 112.6(5) . . ?
C11 C10 C12 111.5(5) . . ?
C5 C10 C12 110.2(4) . . ?
C11 C10 H10 107.4 . . ?
C5 C10 H10 107.4 . . ?
C12 C10 H10 107.4 . . ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C10 C12 H12A 109.5 . . ?
C10 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C10 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C9 C13 C15 112.2(5) . . ?
C9 C13 C14 110.8(4) . . ?
C15 C13 C14 110.0(5) . . ?
C9 C13 H13 107.9 . . ?
C15 C13 H13 107.9 . . ?
C14 C13 H13 107.9 . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C13 C15 H15A 109.5 . . ?
C13 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C13 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C24 B C24 103.7(5) 2_655 . ?
C24 B C16 113.0(2) 2_655 . ?
C24 B C16 111.7(2) . . ?
C24 B C16 111.7(2) 2_655 2_655 ?
C24 B C16 113.0(2) . 2_655 ?
C16 B C16 104.1(5) . 2_655 ?
C17 C16 C21 115.2(4) . . ?
C17 C16 B 123.8(3) . . ?
C21 C16 B 120.7(3) . . ?
C16 C17 C18 122.5(4) . . ?
C16 C17 H17 118.7 . . ?
C18 C17 H17 118.7 . . ?
C19 C18 C17 119.9(4) . . ?
C19 C18 C22 121.1(4) . . ?
C17 C18 C22 118.9(4) . . ?
C18 C19 C20 119.5(4) . . ?
C18 C19 H19 120.3 . . ?
C20 C19 H19 120.3 . . ?
C19 C20 C21 119.7(4) . . ?
C19 C20 C23 119.7(4) . . ?
C21 C20 C23 120.3(5) . . ?
C20 C21 C16 123.1(4) . . ?
C20 C21 H21 118.4 . . ?
C16 C21 H21 118.4 . . ?
F1 C22 F2 105.8(4) . . ?
F1 C22 F3 104.3(4) . . ?
F2 C22 F3 106.7(4) . . ?
F1 C22 C18 114.0(4) . . ?
F2 C22 C18 113.0(4) . . ?
F3 C22 C18 112.3(4) . . ?
F4 C23 F5 105.5(5) . . ?
F4 C23 F6 106.8(5) . . ?
F5 C23 F6 103.6(4) . . ?
F4 C23 C20 114.6(4) . . ?
F5 C23 C20 113.4(5) . . ?
F6 C23 C20 112.1(5) . . ?
C25 C24 C29 114.9(4) . . ?
C25 C24 B 119.4(4) . . ?
C29 C24 B 125.3(3) . . ?
C26 C25 C24 122.8(5) . . ?
C26 C25 H25 118.6 . . ?
C24 C25 H25 118.6 . . ?
C27 C26 C25 120.6(4) . . ?
C27 C26 C30 120.5(4) . . ?
C25 C26 C30 118.9(4) . . ?
C26 C27 C28 118.7(4) . . ?
C26 C27 H27 120.6 . . ?
C28 C27 H27 120.6 . . ?
C29 C28 C27 120.1(4) . . ?
C29 C28 C31 120.0(4) . . ?
C27 C28 C31 119.9(4) . . ?
C28 C29 C24 122.8(4) . . ?
C28 C29 H29 118.6 . . ?
C24 C29 H29 118.6 . . ?
F7 C30 F8 105.8(4) . . ?
F7 C30 F9 105.6(4) . . ?
F8 C30 F9 104.9(4) . . ?
F7 C30 C26 113.3(4) . . ?
F8 C30 C26 113.9(4) . . ?
F9 C30 C26 112.6(4) . . ?
F11 C31 F12 105.4(5) . . ?
F11 C31 F10 104.4(4) . . ?
F12 C31 F10 102.6(4) . . ?
F11 C31 C28 114.6(4) . . ?
F12 C31 C28 114.5(4) . . ?
F10 C31 C28 114.1(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
N C1 1.334(5) . ?
N C4 1.457(6) . ?
N H1X 0.92(5) . ?
C1 C2 1.383(5) . ?
C1 C3 1.504(6) . ?
C2 C1 1.383(5) 2 ?
C2 H2 0.95 . ?
C3 H3A 0.98 . ?
C3 H3B 0.98 . ?
C3 H3C 0.98 . ?
C4 C5 1.387(7) . ?
C4 C9 1.393(7) . ?
C5 C6 1.393(6) . ?
C5 C10 1.518(7) . ?
C6 C7 1.377(7) . ?
C6 H6 0.95 . ?
C7 C8 1.362(8) . ?
C7 H7 0.95 . ?
C8 C9 1.391(7) . ?
C8 H8 0.95 . ?
C9 C13 1.513(7) . ?
C10 C11 1.515(7) . ?
C10 C12 1.528(8) . ?
C10 H10 1 . ?
C11 H11A 0.98 . ?
C11 H11B 0.98 . ?
C11 H11C 0.98 . ?
C12 H12A 0.98 . ?
C12 H12B 0.98 . ?
C12 H12C 0.98 . ?
C13 C15 1.516(8) . ?
C13 C14 1.526(7) . ?
C13 H13 1 . ?
C14 H14A 0.98 . ?
C14 H14B 0.98 . ?
C14 H14C 0.98 . ?
C15 H15A 0.98 . ?
C15 H15B 0.98 . ?
C15 H15C 0.98 . ?
B C24 1.636(6) 2_655 ?
B C24 1.636(6) . ?
B C16 1.642(6) . ?
B C16 1.642(6) 2_655 ?
C16 C17 1.391(6) . ?
C16 C21 1.409(6) . ?
C17 C18 1.408(6) . ?
C17 H17 0.95 . ?
C18 C19 1.379(6) . ?
C18 C22 1.489(6) . ?
C19 C20 1.382(6) . ?
C19 H19 0.95 . ?
C20 C21 1.387(6) . ?
C20 C23 1.474(7) . ?
C21 H21 0.95 . ?
C22 F1 1.317(5) . ?
C22 F2 1.321(6) . ?
C22 F3 1.328(6) . ?
C23 F4 1.314(6) . ?
C23 F5 1.335(6) . ?
C23 F6 1.342(6) . ?
C24 C25 1.400(6) . ?
C24 C29 1.403(6) . ?
C25 C26 1.384(6) . ?
C25 H25 0.95 . ?
C26 C27 1.374(7) . ?
C26 C30 1.487(6) . ?
C27 C28 1.386(6) . ?
C27 H27 0.95 . ?
C28 C29 1.386(6) . ?
C28 C31 1.477(7) . ?
C29 H29 0.95 . ?
C30 F7 1.329(6) . ?
C30 F8 1.336(5) . ?
C30 F9 1.338(5) . ?
C31 F11 1.317(6) . ?
C31 F12 1.334(6) . ?
C31 F10 1.337(5) . ?
