#------------------------------------------------------------------------------
#$Date: 2016-03-25 15:40:26 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179930 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/25/7022587.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7022587
loop_
_publ_author_name
'Sha, Jing-Quan'
'Li, Meng-Ting'
'Sun, Jing-Wen'
'Zhang, Yu-Nan'
'Yan, Peng-Fei'
'Li, Guang-Ming'
_publ_section_title
;
 An unprecedented 3D POM-Ag architecture with intertwined and homological
 helical structures.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7803
_journal_page_last               7809
_journal_paper_doi               10.1039/c3dt00118k
_journal_volume                  42
_journal_year                    2013
_chemical_formula_moiety         'C18 H9 Ag6 Mo12 N14 Na O41 P'
_chemical_formula_sum            'C18 H9 Ag6 Mo12 N14 Na O41 P'
_chemical_formula_weight         2929.85
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 127.440(15)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.279(5)
_cell_length_b                   22.934(5)
_cell_length_c                   20.708(5)
_cell_measurement_temperature    293(2)
_cell_volume                     5384(3)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0657
_diffrn_reflns_av_sigmaI/netI    0.0795
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            26796
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.52
_exptl_absorpt_coefficient_mu    4.971
_exptl_absorpt_correction_T_max  0.261
_exptl_absorpt_correction_T_min  0.149
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   adabs(Sheldrick,1996)
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    3.615
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             5420.0
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.34
_exptl_crystal_size_min          0.27
_refine_diff_density_max         12.409
_refine_diff_density_min         -5.431
_refine_diff_density_rms         0.366
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.050
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     866
_refine_ls_number_reflns         9483
_refine_ls_number_restraints     128
_refine_ls_restrained_S_all      1.044
_refine_ls_R_factor_all          0.1218
_refine_ls_R_factor_gt           0.0784
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1252P)²+210.5994P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2213
_refine_ls_wR_factor_ref         0.2519
_reflns_number_gt                6055
_reflns_number_total             9483
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt00118k.txt
_cod_data_source_block           dd
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7022587
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag2A Ag 1.1016(2) 0.25947(9) 0.63304(14) 0.0368(7) Uani 0.743(4) 1 d P A 1
Ag3A Ag 0.9250(2) 0.21290(9) 0.64006(16) 0.0435(7) Uani 0.743(4) 1 d P A 1
Ag2B Ag 1.1287(6) 0.2240(3) 0.7081(4) 0.0380(19) Uani 0.257(4) 1 d P A 2
Ag3B Ag 0.9190(6) 0.2551(3) 0.5607(4) 0.0352(18) Uani 0.257(4) 1 d P A 2
Ag1 Ag 0.63587(18) 0.25872(10) 0.48914(12) 0.0537(5) Uani 1 1 d . . .
Ag4 Ag 1.0600(3) 0.27896(15) 0.4365(2) 0.0970(10) Uani 1 1 d . . .
Mo1 Mo 0.50833(16) 0.33025(9) 0.05779(11) 0.0340(5) Uani 1 1 d . . .
Mo2 Mo 0.77320(16) 0.30539(8) 0.23972(11) 0.0276(4) Uani 1 1 d . . .
Mo3 Mo 0.70667(17) 0.44080(8) 0.15715(12) 0.0298(4) Uani 1 1 d . . .
Mo4 Mo 0.48463(17) 0.53126(8) 0.14716(12) 0.0312(4) Uani 1 1 d . . .
Mo5 Mo 0.35254(19) 0.27365(9) 0.13531(12) 0.0405(5) Uani 1 1 d . . .
Mo6 Mo 0.61846(18) 0.24578(8) 0.31635(12) 0.0313(4) Uani 1 1 d . . .
Mo7 Mo 0.40877(18) 0.32866(9) 0.30764(13) 0.0372(5) Uani 1 1 d . . .
Mo8 Mo 0.34305(18) 0.47477(9) 0.21859(13) 0.0361(5) Uani 1 1 d . . .
Mo9 Mo 0.62795(17) 0.44724(9) 0.41711(11) 0.0343(5) Uani 1 1 d . . .
Mo10 Mo 0.77239(17) 0.50044(8) 0.34588(11) 0.0300(4) Uani 1 1 d . . .
Mo11 Mo 0.83331(16) 0.36488(8) 0.42870(11) 0.0320(4) Uani 1 1 d . . .
Mo12 Mo 0.28599(17) 0.42130(9) 0.04571(11) 0.0370(5) Uani 1 1 d . . .
P1 P 0.5590(4) 0.38815(19) 0.2349(3) 0.0168(9) Uani 1 1 d . . .
O1 O 0.6715(13) 0.1809(6) 0.3601(9) 0.035(3) Uani 1 1 d . A .
O2 O 0.8815(12) 0.2595(6) 0.2635(9) 0.034(3) Uani 1 1 d . . .
O3 O 0.6854(12) 0.2576(5) 0.2648(8) 0.024(3) Uani 1 1 d . A .
O4 O 0.8363(11) 0.3395(5) 0.3412(8) 0.024(3) Uani 1 1 d . A .
O5 O 0.6519(12) 0.2869(6) 0.1283(8) 0.027(3) Uani 1 1 d . . .
O6 O 0.5177(13) 0.2649(5) 0.3496(9) 0.029(3) Uani 1 1 d . . .
O7 O 0.8074(12) 0.3710(6) 0.2054(8) 0.027(3) Uani 1 1 d . . .
O9 O 0.5075(10) 0.3329(5) 0.2437(7) 0.019(3) Uani 1 1 d . A .
O10 O 0.6116(10) 0.3729(5) 0.1914(7) 0.020(3) Uani 1 1 d . A .
O11 O 0.7670(12) 0.4006(6) 0.4761(8) 0.027(3) Uani 1 1 d . A .
O12 O 0.7165(11) 0.5056(5) 0.4106(8) 0.024(3) Uani 1 1 d . A .
O13 O 0.5833(12) 0.4920(6) 0.1262(8) 0.029(3) Uani 1 1 d . . .
O14 O 0.3520(11) 0.4961(6) 0.0512(8) 0.027(3) Uani 1 1 d . A .
O15 O 0.6261(11) 0.5329(6) 0.2577(8) 0.027(3) Uani 1 1 d . A .
O16 O 0.3954(12) 0.5400(6) 0.1860(8) 0.027(3) Uani 1 1 d . A .
O20 O 0.4819(14) 0.5985(6) 0.1167(9) 0.036(4) Uani 1 1 d . . .
O22 O 0.2814(12) 0.3457(6) 0.0835(8) 0.027(3) Uani 1 1 d . A .
O23 O 0.3137(12) 0.2854(6) 0.2083(9) 0.032(3) Uani 1 1 d . . .
O24 O 0.4726(14) 0.2217(6) 0.2160(9) 0.035(3) Uani 1 1 d . . .
O25 O 0.4363(11) 0.2821(6) 0.0922(8) 0.028(3) Uani 1 1 d . . .
O27 O 0.3924(12) 0.3853(6) 0.0296(8) 0.028(3) Uani 1 1 d . A .
O28 O 0.6042(12) 0.3923(6) 0.0634(8) 0.025(3) Uani 1 1 d . . .
O29 O 0.7823(12) 0.4689(5) 0.2659(8) 0.025(3) Uani 1 1 d . A .
O17 O 0.6539(11) 0.4138(5) 0.3193(7) 0.022(3) Uani 1 1 d . A .
O18 O 0.2385(12) 0.4559(6) 0.1060(8) 0.030(3) Uani 1 1 d . A .
O19 O 0.8630(14) 0.5573(6) 0.3793(10) 0.042(4) Uani 1 1 d . A .
O21 O 0.4876(12) 0.4813(6) 0.3241(8) 0.028(3) Uani 1 1 d . A .
O26 O 0.3397(14) 0.3164(7) 0.3489(10) 0.043(4) Uani 1 1 d . A .
O30 O 0.3334(12) 0.3993(6) 0.2479(8) 0.028(3) Uani 1 1 d . A .
O31 O 0.2542(14) 0.5115(6) 0.2295(9) 0.037(4) Uani 1 1 d . A .
O32 O 0.7307(12) 0.3002(6) 0.3984(9) 0.031(3) Uani 1 1 d . A .
O33 O 0.4589(13) 0.2995(7) -0.0306(9) 0.039(4) Uani 1 1 d . . .
O36 O 0.8794(11) 0.4412(6) 0.4209(8) 0.024(3) Uani 1 1 d . A .
O37 O 0.6296(14) 0.4730(7) 0.4933(9) 0.043(4) Uani 1 1 d . A .
O38 O 0.5341(12) 0.3775(6) 0.3862(8) 0.026(3) Uani 1 1 d . A .
Ag5 Ag 1.0469(3) -0.02671(8) 0.57097(14) 0.0721(8) Uani 1 1 d . . .
O40 O 0.4608(11) 0.4331(5) 0.1842(7) 0.021(3) Uani 1 1 d . A .
N6 N 1.0353(17) 0.0389(7) 0.6833(13) 0.040(5) Uani 1 1 d . . .
N5 N 1.0161(18) 0.0487(7) 0.6119(13) 0.038(5) Uani 1 1 d . . .
N3 N 0.9590(17) 0.1131(7) 0.4648(11) 0.039(4) Uani 1 1 d U . .
C13 C 0.9528(19) 0.1572(9) 0.4198(11) 0.032(5) Uani 1 1 d . . .
H13 H 0.9290 0.1528 0.3671 0.039 Uiso 1 1 calc R . .
C9 C 0.9939(17) 0.1363(7) 0.5335(12) 0.022(4) Uani 1 1 d . A .
N2 N 0.8716(17) 0.3728(7) 0.6989(11) 0.033(4) Uani 1 1 d . . .
N10 N 1.010(2) 0.1944(8) 0.5338(12) 0.043(5) Uani 1 1 d . . .
N12 N 1.1211(19) 0.3956(8) 0.7840(12) 0.045(5) Uani 1 1 d . . .
N8 N 1.030(2) 0.1335(7) 0.6674(12) 0.045(5) Uani 1 1 d . . .
C10 C 1.0146(17) 0.1085(8) 0.6049(13) 0.027(4) Uani 1 1 d . A .
C11 C 1.045(2) 0.0901(9) 0.7157(15) 0.038(5) Uani 1 1 d . A .
C2 C 0.766(2) 0.3521(9) 0.6432(14) 0.034(5) Uani 1 1 d . . .
C1 C 0.654(3) 0.3653(9) 0.6314(16) 0.044(6) Uani 1 1 d . A .
C7 C 1.066(2) 0.3541(8) 0.7309(13) 0.032(5) Uani 1 1 d . A .
N11 N 0.983(2) 0.2057(9) 0.4573(13) 0.051(5) Uani 1 1 d . A .
C6 C 0.944(2) 0.3420(8) 0.6863(13) 0.031(5) Uani 1 1 d . . .
N7 N 0.8816(16) 0.3047(7) 0.6270(11) 0.031(4) Uani 1 1 d . A .
N4 N 0.7649(15) 0.3108(7) 0.5967(10) 0.029(4) Uani 1 1 d . A .
C19 C 0.659(2) 0.3737(9) 0.6984(14) 0.039(6) Uani 1 1 d . . .
H19 H 0.7306 0.3716 0.7502 0.046 Uiso 1 1 calc R A .
C8 C 1.234(2) 0.3906(10) 0.8158(14) 0.036(5) Uani 1 1 d . . .
H8 H 1.2948 0.4142 0.8560 0.044 Uiso 1 1 calc R . .
N9 N 1.1395(19) 0.3210(8) 0.7273(13) 0.044(5) Uani 1 1 d . . .
N13 N 1.245(2) 0.3452(10) 0.7796(17) 0.072(8) Uani 1 1 d . A .
N1 N 0.5599(19) 0.3851(9) 0.6894(13) 0.053(5) Uani 1 1 d DU A .
C18 C 0.546(2) 0.3672(11) 0.5541(17) 0.051(7) Uani 1 1 d . . .
H18 H 0.5425 0.3616 0.5082 0.061 Uiso 1 1 calc R A .
C12 C 1.069(3) 0.0943(12) 0.7946(16) 0.070(6) Uani 1 1 d DU . .
C4 C 0.454(2) 0.3858(12) 0.6165(14) 0.062(7) Uani 1 1 d DU . .
H4 H 0.3873 0.3921 0.6140 0.074 Uiso 1 1 calc R A .
C3 C 0.440(2) 0.3778(13) 0.5457(16) 0.065(8) Uani 1 1 d D A .
O8 O 0.7776(13) 0.4773(6) 0.1286(9) 0.037(4) Uani 1 1 d . . .
O35 O 0.1600(13) 0.4214(8) -0.0482(9) 0.046(4) Uani 1 1 d . A .
O34 O 0.2487(16) 0.2251(8) 0.0725(10) 0.053(5) Uani 1 1 d . . .
Ag6A Ag 1.0584(5) -0.05058(17) 0.7246(4) 0.0732(16) Uani 0.60 1 d P . .
Ag6B Ag 0.9791(9) -0.0383(3) 0.6978(5) 0.083(2) Uani 0.40 1 d P . .
C20 C 1.094(2) 0.1464(13) 0.8325(14) 0.070(6) Uani 1 1 d DU A .
H20 H 1.0954 0.1788 0.8060 0.084 Uiso 1 1 calc R . .
C21 C 1.059(3) 0.0492(15) 0.8335(17) 0.094(8) Uani 1 1 d DU A .
H21 H 1.0256 0.0144 0.8056 0.113 Uiso 1 1 calc R . .
N14 N 1.118(2) 0.1553(11) 0.9055(13) 0.080(6) Uani 1 1 d DU . .
C15 C 1.097(4) 0.0533(16) 0.9100(17) 0.106(8) Uani 1 1 d DU . .
H15 H 1.1094 0.0203 0.9406 0.127 Uiso 1 1 calc R A .
O1W O 0.7386(14) 0.1630(7) 0.5187(10) 0.045(4) Uani 1 1 d . A .
C14 C 1.115(3) 0.1067(14) 0.941(2) 0.088(7) Uani 1 1 d DU A .
H14 H 1.1258 0.1107 0.9895 0.106 Uiso 1 1 calc R . .
Na Na 1.3954(8) 0.3115(4) 0.8132(7) 0.052(3) Uani 1 1 d . . .
O39 O 0.9619(13) 0.3391(6) 0.5092(8) 0.036(3) Uani 1 1 d . A .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N9 Ag2A N10 161.4(8) . .
N9 Ag2A Ag3A 86.7(6) . .
N10 Ag2A Ag3A 75.6(5) . .
N9 Ag2A Na 52.0(6) . .
N10 Ag2A Na 144.6(6) . .
Ag3A Ag2A Na 124.5(2) . .
N7 Ag3A N8 159.1(8) . .
N7 Ag3A O1W 105.3(6) . .
N8 Ag3A O1W 91.3(7) . .
N7 Ag3A Ag2A 79.8(5) . .
N8 Ag3A Ag2A 80.5(6) . .
O1W Ag3A Ag2A 123.1(4) . .
N9 Ag2B N8 153.7(8) . .
N9 Ag2B Ag3B 81.5(6) . .
N8 Ag2B Ag3B 79.8(5) . .
N9 Ag2B Na 54.0(6) . .
N8 Ag2B Na 151.8(6) . .
Ag3B Ag2B Na 123.7(3) . .
N7 Ag3B N10 160.1(8) . .
N7 Ag3B O39 95.1(6) . .
N10 Ag3B O39 92.6(6) . .
N7 Ag3B Ag2B 87.3(6) . .
N10 Ag3B Ag2B 72.9(6) . .
O39 Ag3B Ag2B 107.0(4) . .
N7 Ag3B Ag1 63.6(5) . .
N10 Ag3B Ag1 130.1(6) . .
O39 Ag3B Ag1 109.9(4) . .
Ag2B Ag3B Ag1 134.2(3) . .
N4 Ag1 O6 140.0(5) . .
N4 Ag1 O1W 103.0(6) . .
O6 Ag1 O1W 103.6(5) . .
N4 Ag1 Ag3B 61.5(5) . .
O6 Ag1 Ag3B 108.8(3) . .
O1W Ag1 Ag3B 60.0(4) . .
N4 Ag1 Na 171.3(5) . 4_465
O6 Ag1 Na 38.8(3) . 4_465
O1W Ag1 Na 84.8(4) . 4_465
Ag3B Ag1 Na 126.8(2) . 4_465
N14 Ag4 N11 174.2(9) 4_565 .
N14 Ag4 O34 91.0(8) 4_565 4_666
N11 Ag4 O34 94.4(7) . 4_666
O33 Mo1 O27 103.8(7) . .
O33 Mo1 O25 101.5(7) . .
O27 Mo1 O25 86.1(6) . .
O33 Mo1 O5 99.2(7) . .
O27 Mo1 O5 157.0(6) . .
O25 Mo1 O5 89.1(6) . .
O33 Mo1 O28 101.0(7) . .
O27 Mo1 O28 89.0(6) . .
O25 Mo1 O28 157.5(5) . .
O5 Mo1 O28 86.9(6) . .
O33 Mo1 O10 170.6(6) . .
O27 Mo1 O10 83.8(5) . .
O25 Mo1 O10 84.2(5) . .
O5 Mo1 O10 73.3(5) . .
O28 Mo1 O10 73.4(5) . .
O2 Mo2 O7 102.2(6) . .
O2 Mo2 O4 101.7(6) . .
O7 Mo2 O4 91.8(6) . .
O2 Mo2 O5 102.2(6) . .
O7 Mo2 O5 88.5(6) . .
O4 Mo2 O5 155.4(5) . .
O2 Mo2 O3 101.3(6) . .
O7 Mo2 O3 156.5(5) . .
O4 Mo2 O3 83.4(5) . .
O5 Mo2 O3 86.5(6) . .
O2 Mo2 O10 174.0(6) . .
O7 Mo2 O10 74.4(5) . .
O4 Mo2 O10 83.4(5) . .
O5 Mo2 O10 73.0(5) . .
O3 Mo2 O10 82.3(5) . .
O8 Mo3 O13 102.1(7) . .
O8 Mo3 O28 100.7(6) . .
O13 Mo3 O28 92.1(6) . .
O8 Mo3 O29 102.5(6) . .
O13 Mo3 O29 86.1(6) . .
O28 Mo3 O29 156.6(5) . .
O8 Mo3 O7 100.0(6) . .
O13 Mo3 O7 157.9(5) . .
O28 Mo3 O7 85.1(6) . .
O29 Mo3 O7 87.8(5) . .
O8 Mo3 O10 170.2(6) . .
O13 Mo3 O10 85.8(5) . .
O28 Mo3 O10 73.0(5) . .
O29 Mo3 O10 83.6(5) . .
O7 Mo3 O10 72.4(5) . .
O20 Mo4 O16 101.5(6) . .
O20 Mo4 O14 102.6(7) . .
O16 Mo4 O14 89.3(6) . .
O20 Mo4 O15 101.5(7) . .
O16 Mo4 O15 89.0(6) . .
O14 Mo4 O15 155.6(6) . .
O20 Mo4 O13 101.5(6) . .
O16 Mo4 O13 156.9(6) . .
O14 Mo4 O13 88.1(6) . .
O15 Mo4 O13 84.0(6) . .
O20 Mo4 O40 172.4(6) . .
O16 Mo4 O40 73.0(5) . .
O14 Mo4 O40 72.5(5) . .
O15 Mo4 O40 83.8(5) . .
O13 Mo4 O40 84.4(5) . .
O34 Mo5 O25 102.6(7) . .
O34 Mo5 O22 102.9(8) . .
O25 Mo5 O22 85.3(6) . .
O34 Mo5 O24 99.5(8) . .
O25 Mo5 O24 89.3(6) . .
O22 Mo5 O24 157.6(6) . .
O34 Mo5 O23 99.4(7) . .
O25 Mo5 O23 158.0(6) . .
O22 Mo5 O23 90.6(6) . .
O24 Mo5 O23 86.2(6) . .
O34 Mo5 O9 170.2(7) . .
O25 Mo5 O9 84.0(5) . .
O22 Mo5 O9 84.7(5) . .
O24 Mo5 O9 73.0(5) . .
O23 Mo5 O9 74.2(5) . .
O1 Mo6 O3 102.8(6) . .
O1 Mo6 O24 99.6(7) . .
O3 Mo6 O24 91.1(6) . .
O1 Mo6 O32 103.9(7) . .
O3 Mo6 O32 88.2(6) . .
O24 Mo6 O32 156.0(6) . .
O1 Mo6 O6 101.2(6) . .
O3 Mo6 O6 155.9(5) . .
O24 Mo6 O6 84.3(6) . .
O32 Mo6 O6 86.6(6) . .
O1 Mo6 O9 169.8(6) . .
O3 Mo6 O9 83.8(5) . .
O24 Mo6 O9 72.3(5) . .
O32 Mo6 O9 83.8(5) . .
O6 Mo6 O9 72.3(5) . .
O1 Mo6 Na 77.1(5) . 4_465
O3 Mo6 Na 149.0(5) . 4_465
O24 Mo6 Na 58.9(4) . 4_465
O32 Mo6 Na 122.2(4) . 4_465
O6 Mo6 Na 39.3(4) . 4_465
O9 Mo6 Na 93.2(3) . 4_465
O26 Mo7 O38 101.7(7) . .
O26 Mo7 O23 102.0(7) . .
O38 Mo7 O23 156.3(6) . .
O26 Mo7 O6 102.0(6) . .
O38 Mo7 O6 88.9(6) . .
O23 Mo7 O6 86.7(6) . .
O26 Mo7 O30 101.3(7) . .
O38 Mo7 O30 85.5(6) . .
O23 Mo7 O30 89.5(6) . .
O6 Mo7 O30 156.6(5) . .
O26 Mo7 O9 172.5(6) . .
O38 Mo7 O9 83.6(5) . .
O23 Mo7 O9 72.9(5) . .
O6 Mo7 O9 72.6(5) . .
O30 Mo7 O9 84.3(5) . .
O26 Mo7 Na 75.4(6) . 4_465
O38 Mo7 Na 127.3(5) . 4_465
O23 Mo7 Na 60.2(5) . 4_465
O6 Mo7 Na 43.3(4) . 4_465
O30 Mo7 Na 147.2(5) . 4_465
O9 Mo7 Na 97.1(3) . 4_465
O31 Mo8 O30 102.4(7) . .
O31 Mo8 O21 101.0(7) . .
O30 Mo8 O21 86.7(6) . .
O31 Mo8 O18 100.8(7) . .
O30 Mo8 O18 91.7(6) . .
O21 Mo8 O18 157.9(6) . .
O31 Mo8 O16 98.2(6) . .
O30 Mo8 O16 159.4(5) . .
O21 Mo8 O16 87.7(6) . .
O18 Mo8 O16 86.1(6) . .
O31 Mo8 O40 170.1(6) . .
O30 Mo8 O40 86.0(5) . .
O21 Mo8 O40 84.5(5) . .
O18 Mo8 O40 73.4(5) . .
O16 Mo8 O40 73.7(5) . .
O37 Mo9 O12 100.9(7) . .
O37 Mo9 O11 100.5(7) . .
O12 Mo9 O11 87.8(6) . .
O37 Mo9 O21 102.2(7) . .
O12 Mo9 O21 88.6(6) . .
O11 Mo9 O21 157.3(5) . .
O37 Mo9 O38 102.3(7) . .
O12 Mo9 O38 156.7(5) . .
O11 Mo9 O38 89.4(6) . .
O21 Mo9 O38 85.0(6) . .
O37 Mo9 O17 172.1(6) . .
O12 Mo9 O17 73.4(5) . .
O11 Mo9 O17 74.1(5) . .
O21 Mo9 O17 83.4(5) . .
O38 Mo9 O17 83.6(5) . .
O19 Mo10 O29 102.2(7) . .
O19 Mo10 O15 102.4(7) . .
O29 Mo10 O15 86.1(6) . .
O19 Mo10 O36 100.5(7) . .
O29 Mo10 O36 89.5(5) . .
O15 Mo10 O36 157.1(5) . .
O19 Mo10 O12 101.9(7) . .
O29 Mo10 O12 155.8(5) . .
O15 Mo10 O12 88.1(6) . .
O36 Mo10 O12 86.7(5) . .
O19 Mo10 O17 171.0(6) . .
O29 Mo10 O17 84.4(5) . .
O15 Mo10 O17 84.1(5) . .
O36 Mo10 O17 73.1(5) . .
O12 Mo10 O17 71.7(5) . .
O39 Mo11 O32 102.3(7) . .
O39 Mo11 O36 100.5(7) . .
O32 Mo11 O36 157.1(6) . .
O39 Mo11 O11 103.1(6) . .
O32 Mo11 O11 88.8(6) . .
O36 Mo11 O11 87.4(5) . .
O39 Mo11 O4 101.1(6) . .
O32 Mo11 O4 84.7(6) . .
O36 Mo11 O4 89.5(5) . .
O11 Mo11 O4 155.8(6) . .
O39 Mo11 O17 173.1(6) . .
O32 Mo11 O17 83.6(5) . .
O36 Mo11 O17 73.8(5) . .
O11 Mo11 O17 73.2(5) . .
O4 Mo11 O17 82.9(5) . .
O35 Mo12 O18 101.6(7) . .
O35 Mo12 O22 101.4(7) . .
O18 Mo12 O22 89.7(6) . .
O35 Mo12 O14 102.2(7) . .
O18 Mo12 O14 86.9(6) . .
O22 Mo12 O14 156.4(6) . .
O35 Mo12 O27 101.8(7) . .
O18 Mo12 O27 156.6(6) . .
O22 Mo12 O27 84.8(5) . .
O14 Mo12 O27 89.0(5) . .
O35 Mo12 O40 172.6(6) . .
O18 Mo12 O40 72.5(5) . .
O22 Mo12 O40 83.3(5) . .
O14 Mo12 O40 73.4(5) . .
O27 Mo12 O40 84.2(5) . .
O10 P1 O9 108.9(7) . .
O10 P1 O40 108.9(7) . .
O9 P1 O40 109.5(7) . .
O10 P1 O17 110.4(7) . .
O9 P1 O17 109.7(7) . .
O40 P1 O17 109.3(7) . .
Mo6 O3 Mo2 151.8(7) . .
Mo2 O4 Mo11 155.0(7) . .
Mo2 O5 Mo1 124.7(7) . .
Mo7 O6 Mo6 124.8(7) . .
Mo7 O6 Na 101.1(6) . 4_465
Mo6 O6 Na 106.9(6) . 4_465
Mo7 O6 Ag1 112.9(6) . .
Mo6 O6 Ag1 106.8(6) . .
Na O6 Ag1 101.5(5) 4_465 .
Mo2 O7 Mo3 125.0(7) . .
P1 O9 Mo5 126.5(7) . .
P1 O9 Mo6 125.3(7) . .
Mo5 O9 Mo6 89.9(4) . .
P1 O9 Mo7 124.8(7) . .
Mo5 O9 Mo7 88.7(4) . .
Mo6 O9 Mo7 90.3(4) . .
P1 O10 Mo1 126.4(7) . .
P1 O10 Mo2 126.0(7) . .
Mo1 O10 Mo2 88.8(4) . .
P1 O10 Mo3 126.0(7) . .
Mo1 O10 Mo3 89.2(4) . .
Mo2 O10 Mo3 88.3(4) . .
Mo9 O11 Mo11 124.0(7) . .
Mo9 O12 Mo10 125.3(6) . .
Mo3 O13 Mo4 151.2(8) . .
Mo4 O14 Mo12 125.5(7) . .
Mo10 O15 Mo4 151.8(7) . .
Mo4 O16 Mo8 124.2(7) . .
Mo4 O20 Na 134.1(9) . 3_766
Mo5 O22 Mo12 151.6(8) . .
Mo7 O23 Mo5 124.3(7) . .
Mo7 O23 Na 83.6(5) . 4_465
Mo5 O23 Na 108.3(6) . 4_465
Mo5 O24 Mo6 124.8(7) . .
Mo5 O24 Na 104.5(6) . 4_465
Mo6 O24 Na 86.8(5) . 4_465
Mo5 O25 Mo1 150.7(7) . .
Mo1 O27 Mo12 151.1(8) . .
Mo3 O28 Mo1 124.4(7) . .
Mo10 O29 Mo3 150.1(8) . .
P1 O17 Mo9 127.0(7) . .
P1 O17 Mo11 125.9(7) . .
Mo9 O17 Mo11 88.7(4) . .
P1 O17 Mo10 125.3(7) . .
Mo9 O17 Mo10 89.5(4) . .
Mo11 O17 Mo10 88.4(4) . .
Mo8 O18 Mo12 124.5(7) . .
Mo8 O21 Mo9 150.7(8) . .
Mo8 O30 Mo7 150.2(8) . .
Mo11 O32 Mo6 149.0(8) . .
Mo1 O33 Na 148.5(9) . 1_454
Mo11 O36 Mo10 124.7(7) . .
Mo7 O38 Mo9 151.8(8) . .
N5 Ag5 N3 162.2(7) . 3_756
N5 Ag5 Ag5 88.7(6) . 3_756
N3 Ag5 Ag5 99.2(5) 3_756 3_756
N5 Ag5 Ag6A 68.1(5) . .
N3 Ag5 Ag6A 99.2(5) 3_756 .
Ag5 Ag5 Ag6A 151.47(18) 3_756 .
N5 Ag5 Ag6B 60.7(5) . .
N3 Ag5 Ag6B 103.6(6) 3_756 .
Ag5 Ag5 Ag6B 135.7(3) 3_756 .
Ag6A Ag5 Ag6B 16.66(16) . .
P1 O40 Mo8 125.6(7) . .
P1 O40 Mo12 126.5(7) . .
Mo8 O40 Mo12 89.6(4) . .
P1 O40 Mo4 125.9(7) . .
Mo8 O40 Mo4 89.0(4) . .
Mo12 O40 Mo4 88.4(4) . .
C11 N6 N5 107.4(17) . .
C11 N6 Ag6B 129.0(16) . .
N5 N6 Ag6B 118.0(14) . .
C11 N6 Ag6A 134.3(17) . .
N5 N6 Ag6A 118.0(14) . .
Ag6B N6 Ag6A 25.9(3) . .
N6 N5 C10 105.1(16) . .
N6 N5 Ag5 110.8(13) . .
C10 N5 Ag5 140.9(14) . .
C9 N3 C13 105.7(16) . .
C9 N3 Ag5 132.7(15) . 3_756
C13 N3 Ag5 119.7(13) . 3_756
N11 C13 N3 112.4(19) . .
N3 C9 N10 111.0(18) . .
N3 C9 C10 129.3(17) . .
N10 C9 C10 119.7(17) . .
C2 N2 C6 103.7(17) . .
C2 N2 Ag6A 135.5(14) . 2_756
C6 N2 Ag6A 118.7(14) . 2_756
C9 N10 N11 104.3(16) . .
C9 N10 Ag3B 120.0(14) . .
N11 N10 Ag3B 111.8(14) . .
C9 N10 Ag2A 132.2(15) . .
N11 N10 Ag2A 121.6(13) . .
Ag3B N10 Ag2A 56.2(5) . .
C7 N12 C8 106.8(19) . .
C7 N12 Ag6B 120.6(17) . 2_756
C8 N12 Ag6B 132.5(15) . 2_756
C10 N8 C11 105.6(17) . .
C10 N8 Ag3A 115.4(14) . .
C11 N8 Ag3A 125.6(15) . .
C10 N8 Ag2B 116.6(15) . .
C11 N8 Ag2B 127.0(16) . .
Ag3A N8 Ag2B 61.9(5) . .
N8 C10 N5 110.5(18) . .
N8 C10 C9 128.1(18) . .
N5 C10 C9 121.3(18) . .
N6 C11 N8 111(2) . .
N6 C11 C12 121(2) . .
N8 C11 C12 128(2) . .
N2 C2 N4 113.4(18) . .
N2 C2 C1 128(2) . .
N4 C2 C1 119(2) . .
C19 C1 C18 120(2) . .
C19 C1 C2 118(2) . .
C18 C1 C2 122(2) . .
N12 C7 N9 112(2) . .
N12 C7 C6 125(2) . .
N9 C7 C6 123.2(19) . .
C13 N11 N10 106.5(19) . .
C13 N11 Ag4 125.3(17) . .
N10 N11 Ag4 122.4(14) . .
N7 C6 N2 110.1(19) . .
N7 C6 C7 127.7(19) . .
N2 C6 C7 122.1(18) . .
C6 N7 N4 107.8(16) . .
C6 N7 Ag3B 132.3(15) . .
N4 N7 Ag3B 118.4(12) . .
C6 N7 Ag3A 122.7(15) . .
N4 N7 Ag3A 109.2(12) . .
Ag3B N7 Ag3A 51.9(4) . .
C2 N4 N7 104.9(16) . .
C2 N4 Ag1 138.8(15) . .
N7 N4 Ag1 116.2(11) . .
N1 C19 C1 120(2) . .
N12 C8 N13 108(2) . .
N12 C8 Na 140.4(15) . .
N13 C8 Na 33.0(13) . .
N13 N9 C7 104.8(19) . .
N13 N9 Ag2A 122.8(17) . .
C7 N9 Ag2A 129.7(17) . .
N13 N9 Ag2B 118.7(16) . .
C7 N9 Ag2B 126.9(16) . .
Ag2A N9 Ag2B 41.6(4) . .
N13 N9 Na 33.3(12) . .
C7 N9 Na 137.6(15) . .
Ag2A N9 Na 92.0(7) . .
Ag2B N9 Na 87.7(7) . .
N9 N13 C8 109(2) . .
N9 N13 Na 125.1(17) . .
C8 N13 Na 125.2(19) . .
C19 N1 C4 122(2) . .
C1 C18 C3 120(2) . .
C20 C12 C21 114(3) . .
C20 C12 C11 120(2) . .
C21 C12 C11 125(3) . .
N1 C4 C3 122(3) . .
C4 C3 C18 116(3) . .
Mo5 O34 Ag4 139.4(10) . 4_465
Ag6B Ag6A N2 121.6(8) . 2_746
Ag6B Ag6A N6 69.4(7) . .
N2 Ag6A N6 161.7(8) 2_746 .
Ag6B Ag6A Ag5 92.7(6) . .
N2 Ag6A Ag5 127.0(5) 2_746 .
N6 Ag6A Ag5 62.2(5) . .
Ag6A Ag6B N6 84.7(7) . .
Ag6A Ag6B N12 110.7(8) . 2_746
N6 Ag6B N12 161.6(9) . 2_746
Ag6A Ag6B Ag5 70.6(6) . .
N6 Ag6B Ag5 58.9(6) . .
N12 Ag6B Ag5 134.7(6) 2_746 .
N14 C20 C12 125(3) . .
C15 C21 C12 122(3) . .
C14 N14 C20 114(3) . .
C14 N14 Ag4 107.1(18) . 4_566
C20 N14 Ag4 127.0(18) . 4_566
C14 C15 C21 117(3) . .
Ag1 O1W Ag3A 87.3(5) . .
C15 C14 N14 124(3) . .
N13 Na O6 151.5(9) . 4_666
N13 Na O20 96.3(8) . 3_766
O6 Na O20 108.6(6) 4_666 3_766
N13 Na O33 87.9(10) . 1_656
O6 Na O33 84.0(6) 4_666 1_656
O20 Na O33 78.0(5) 3_766 1_656
N13 Na O23 100.7(8) . 4_666
O6 Na O23 61.2(5) 4_666 4_666
O20 Na O23 155.2(6) 3_766 4_666
O33 Na O23 120.4(6) 1_656 4_666
N13 Na O24 130.3(10) . 4_666
O6 Na O24 59.2(5) 4_666 4_666
O20 Na O24 100.9(5) 3_766 4_666
O33 Na O24 141.2(6) 1_656 4_666
O23 Na O24 54.3(4) 4_666 4_666
N13 Na N9 21.6(7) . .
O6 Na N9 133.1(6) 4_666 .
O20 Na N9 117.4(6) 3_766 .
O33 Na N9 96.7(6) 1_656 .
O23 Na N9 79.2(5) 4_666 .
O24 Na N9 116.9(6) 4_666 .
N13 Na C8 21.8(8) . .
O6 Na C8 157.4(7) 4_666 .
O20 Na C8 76.4(6) 3_766 .
O33 Na C8 75.4(6) 1_656 .
O23 Na C8 122.3(6) 4_666 .
O24 Na C8 142.8(7) 4_666 .
N9 Na C8 43.2(6) . .
N13 Na Mo7 116.9(8) . 4_666
O6 Na Mo7 35.6(4) 4_666 4_666
O20 Na Mo7 143.3(5) 3_766 4_666
O33 Na Mo7 87.6(4) 1_656 4_666
O23 Na Mo7 36.1(3) 4_666 4_666
O24 Na Mo7 70.1(3) 4_666 4_666
N9 Na Mo7 97.5(4) . 4_666
C8 Na Mo7 132.4(5) . 4_666
N13 Na Mo6 164.5(10) . 4_666
O6 Na Mo6 33.9(4) 4_666 4_666
O20 Na Mo6 89.5(4) 3_766 4_666
O33 Na Mo6 107.4(4) 1_656 4_666
O23 Na Mo6 69.8(3) 4_666 4_666
O24 Na Mo6 34.3(3) 4_666 4_666
N9 Na Mo6 147.4(5) . 4_666
C8 Na Mo6 164.8(6) . 4_666
Mo7 Na Mo6 62.72(15) 4_666 4_666
N13 Na Ag1 135.3(10) . 4_666
O6 Na Ag1 39.7(4) 4_666 4_666
O20 Na Ag1 83.1(4) 3_766 4_666
O33 Na Ag1 48.1(4) 1_656 4_666
O23 Na Ag1 97.0(4) 4_666 4_666
O24 Na Ag1 93.1(4) 4_666 4_666
N9 Na Ag1 136.8(5) . 4_666
C8 Na Ag1 122.8(6) . 4_666
Mo7 Na Ag1 62.64(18) 4_666 4_666
Mo6 Na Ag1 59.53(15) 4_666 4_666
N13 Na Ag2B 58.9(7) . .
O6 Na Ag2B 95.0(5) 4_666 .
O20 Na Ag2B 155.1(5) 3_766 .
O33 Na Ag2B 97.1(4) 1_656 .
O23 Na Ag2B 46.4(3) 4_666 .
O24 Na Ag2B 98.0(4) 4_666 .
N9 Na Ag2B 38.2(4) . .
C8 Na Ag2B 78.7(5) . .
Mo7 Na Ag2B 59.41(19) 4_666 .
Mo6 Na Ag2B 115.2(3) 4_666 .
Ag1 Na Ag2B 112.0(3) 4_666 .
Mo11 O39 Ag3B 107.4(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag2A N9 2.193(18) .
Ag2A N10 2.211(18) .
Ag2A Ag3A 2.822(4) .
Ag2A Na 3.730(10) .
Ag3A N7 2.165(16) .
Ag3A N8 2.204(18) .
Ag3A O1W 2.564(17) .
Ag2B N9 2.249(18) .
Ag2B N8 2.36(2) .
Ag2B Ag3B 2.771(10) .
Ag2B Na 3.632(11) .
Ag3B N7 2.088(17) .
Ag3B N10 2.19(2) .
Ag3B O39 2.452(17) .
Ag3B Ag1 3.356(7) .
Ag1 N4 2.190(16) .
Ag1 O6 2.300(14) .
Ag1 O1W 2.500(17) .
Ag1 Na 3.528(11) 4_465
Ag4 N14 2.00(2) 4_565
Ag4 N11 2.19(2) .
Ag4 O34 2.443(18) 4_666
Mo1 O33 1.666(14) .
Mo1 O27 1.870(14) .
Mo1 O25 1.918(14) .
Mo1 O5 1.920(13) .
Mo1 O28 1.928(13) .
Mo1 O10 2.413(12) .
Mo2 O2 1.679(13) .
Mo2 O7 1.852(13) .
Mo2 O4 1.880(13) .
Mo2 O5 1.909(13) .
Mo2 O3 1.958(12) .
Mo2 O10 2.432(12) .
Mo3 O8 1.674(14) .
Mo3 O13 1.876(14) .
Mo3 O28 1.922(13) .
Mo3 O29 1.923(13) .
Mo3 O7 1.971(13) .
Mo3 O10 2.437(12) .
Mo4 O20 1.657(14) .
Mo4 O16 1.887(12) .
Mo4 O14 1.899(14) .
Mo4 O15 1.924(13) .
Mo4 O13 1.931(13) .
Mo4 O40 2.468(12) .
Mo5 O34 1.668(16) .
Mo5 O25 1.887(13) .
Mo5 O22 1.894(13) .
Mo5 O24 1.915(15) .
Mo5 O23 1.920(14) .
Mo5 O9 2.396(12) .
Mo6 O1 1.665(14) .
Mo6 O3 1.835(13) .
Mo6 O24 1.923(16) .
Mo6 O32 1.925(14) .
Mo6 O6 1.985(13) .
Mo6 O9 2.421(12) .
Mo6 Na 3.409(9) 4_465
Mo7 O26 1.675(14) .
Mo7 O38 1.888(13) .
Mo7 O23 1.914(14) .
Mo7 O6 1.916(14) .
Mo7 O30 1.921(13) .
Mo7 O9 2.454(11) .
Mo7 Na 3.227(9) 4_465
Mo8 O31 1.649(14) .
Mo8 O30 1.868(13) .
Mo8 O21 1.891(14) .
Mo8 O18 1.902(14) .
Mo8 O16 1.965(13) .
Mo8 O40 2.389(12) .
Mo9 O37 1.670(14) .
Mo9 O12 1.902(13) .
Mo9 O11 1.906(14) .
Mo9 O21 1.909(14) .
Mo9 O38 1.929(13) .
Mo9 O17 2.396(12) .
Mo10 O19 1.663(14) .
Mo10 O29 1.889(13) .
Mo10 O15 1.901(13) .
Mo10 O36 1.925(13) .
Mo10 O12 1.936(13) .
Mo10 O17 2.446(13) .
Mo11 O39 1.667(14) .
Mo11 O32 1.903(14) .
Mo11 O36 1.911(13) .
Mo11 O11 1.913(13) .
Mo11 O4 1.929(13) .
Mo11 O17 2.428(13) .
Mo12 O35 1.663(15) .
Mo12 O18 1.918(13) .
Mo12 O22 1.920(13) .
Mo12 O14 1.928(14) .
Mo12 O27 1.929(14) .
Mo12 O40 2.413(12) .
P1 O10 1.525(12) .
P1 O9 1.530(12) .
P1 O40 1.530(13) .
P1 O17 1.535(13) .
O6 Na 2.255(15) 4_465
O20 Na 2.519(17) 3_766
O23 Na 2.819(16) 4_465
O24 Na 2.924(17) 4_465
O33 Na 2.792(19) 1_454
Ag5 N5 2.088(17) .
Ag5 N3 2.099(16) 3_756
Ag5 Ag5 2.674(5) 3_756
Ag5 Ag6A 3.131(5) .
Ag5 Ag6B 3.315(7) .
N6 C11 1.31(3) .
N6 N5 1.35(3) .
N6 Ag6B 2.041(18) .
N6 Ag6A 2.170(17) .
N5 C10 1.38(3) .
N3 C9 1.30(2) .
N3 C13 1.34(3) .
N3 Ag5 2.099(16) 3_756
C13 N11 1.27(3) .
C9 N10 1.35(2) .
C9 C10 1.47(3) .
N2 C2 1.31(3) .
N2 C6 1.40(3) .
N2 Ag6A 2.162(17) 2_756
N10 N11 1.41(3) .
N12 C7 1.30(3) .
N12 C8 1.32(3) .
N12 Ag6B 2.27(2) 2_756
N8 C10 1.30(3) .
N8 C11 1.33(3) .
C11 C12 1.46(3) .
C2 N4 1.34(3) .
C2 C1 1.49(3) .
C1 C19 1.36(3) .
C1 C18 1.39(4) .
C7 N9 1.34(3) .
C7 C6 1.41(3) .
C6 N7 1.30(3) .
N7 N4 1.39(2) .
C19 N1 1.34(3) .
C8 N13 1.34(3) .
C8 Na 2.96(2) .
N9 N13 1.33(3) .
N9 Na 2.94(2) .
N13 Na 1.97(3) .
N1 C4 1.340(18) .
C18 C3 1.44(3) .
C12 C20 1.353(19) .
C12 C21 1.367(19) .
C4 C3 1.365(18) .
O34 Ag4 2.443(18) 4_465
Ag6A Ag6B 0.952(9) .
Ag6A N2 2.162(17) 2_746
Ag6B N12 2.27(2) 2_746
C20 N14 1.349(18) .
C21 C15 1.333(19) .
N14 C14 1.347(19) .
N14 Ag4 2.00(2) 4_566
C15 C14 1.330(19) .
Na O6 2.255(15) 4_666
Na O20 2.519(17) 3_766
Na O33 2.792(19) 1_656
Na O23 2.819(17) 4_666
Na O24 2.924(17) 4_666
Na Mo7 3.227(9) 4_666
Na Mo6 3.409(9) 4_666
Na Ag1 3.528(11) 4_666
