#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:59:06 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179998 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/92/7029209.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029209
loop_
_publ_author_name
'Ovsyannikov, A.'
'Ferlay, S.'
'Solovieva, S. E.'
'Antipin, I. S.'
'Konovalov, A. I.'
'Kyritsakas, N.'
'Hosseini, M. W.'
_publ_section_title
;
 Molecular tectonics: anion control of dimensionality and connectivity in
 meta-pyridyl appended tetramercaptotetrathiacalix[4]arene based silver
 coordination networks.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              158
_journal_page_last               165
_journal_paper_doi               10.1039/c3dt52654b
_journal_volume                  43
_journal_year                    2014
_chemical_formula_moiety         'C64 H68 Ag N4 S8, B F4'
_chemical_formula_sum            'C64 H68 Ag B F4 N4 S8'
_chemical_formula_weight         1344.38
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 105.167(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.1441(10)
_cell_length_b                   14.5274(10)
_cell_length_c                   19.8691(12)
_cell_measurement_reflns_used    9899
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      26.17
_cell_measurement_theta_min      2.41
_cell_volume                     6447.8(7)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.951
_diffrn_measured_fraction_theta_max 0.951
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0684
_diffrn_reflns_av_sigmaI/netI    0.0445
_diffrn_reflns_limit_h_max       32
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            121323
_diffrn_reflns_theta_full        30.00
_diffrn_reflns_theta_max         30.00
_diffrn_reflns_theta_min         1.67
_exptl_absorpt_coefficient_mu    0.626
_exptl_absorpt_correction_T_max  0.9634
_exptl_absorpt_correction_T_min  0.9458
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.385
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2784
_exptl_crystal_size_max          0.09
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.471
_refine_diff_density_min         -0.584
_refine_diff_density_rms         0.115
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.013
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     399
_refine_ls_number_reflns         8888
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.013
_refine_ls_R_factor_all          0.0899
_refine_ls_R_factor_gt           0.0544
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0934P)²+20.4299P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1546
_refine_ls_wR_factor_ref         0.1793
_reflns_number_gt                5983
_reflns_number_total             8888
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt52654b.txt
_cod_data_source_block           e2488a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/automatic-downloads/current/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029209
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.0000 -0.33498(3) 0.2500 0.04590(15) Uani 1 2 d S
S1 S 0.18091(3) 0.15565(6) 0.31205(4) 0.02559(18) Uani 1 1 d .
C1 C 0.13470(13) 0.2043(2) 0.36175(15) 0.0225(6) Uani 1 1 d .
C2 C 0.08480(13) 0.1608(2) 0.37539(15) 0.0218(6) Uani 1 1 d .
C3 C 0.05309(12) 0.2104(2) 0.41417(15) 0.0224(6) Uani 1 1 d .
C4 C 0.07211(13) 0.2968(2) 0.44164(15) 0.0234(6) Uani 1 1 d .
H4 H 0.0489 0.3292 0.4669 0.028 Uiso 1 1 calc R
C5 C 0.12412(13) 0.3366(2) 0.43286(15) 0.0226(6) Uani 1 1 d .
C6 C 0.15404(13) 0.2892(2) 0.39128(15) 0.0243(6) Uani 1 1 d .
H6 H 0.1889 0.3159 0.3828 0.029 Uiso 1 1 calc R
S2 S 0.06134(3) 0.04808(6) 0.34777(4) 0.02951(19) Uani 1 1 d .
C7 C 0.12845(15) -0.0199(2) 0.38621(19) 0.0324(7) Uani 1 1 d .
H7A H 0.1558 -0.0194 0.3553 0.039 Uiso 1 1 calc R
H7B H 0.1500 0.0059 0.4320 0.039 Uiso 1 1 calc R
C8 C 0.10794(15) -0.1162(2) 0.39462(18) 0.0301(7) Uani 1 1 d .
C9 C 0.07522(17) -0.1653(2) 0.33819(19) 0.0335(7) Uani 1 1 d .
H9 H 0.0660 -0.1364 0.2938 0.040 Uiso 1 1 calc R
N1 N 0.05561(15) -0.2512(2) 0.34220(18) 0.0400(7) Uani 1 1 d .
C10 C 0.0702(2) -0.2910(3) 0.4044(2) 0.0464(10) Uani 1 1 d .
H10 H 0.0565 -0.3520 0.4081 0.056 Uiso 1 1 calc R
C11 C 0.1036(2) -0.2498(3) 0.4631(2) 0.0512(11) Uani 1 1 d .
H11 H 0.1137 -0.2817 0.5063 0.061 Uiso 1 1 calc R
C12 C 0.12250(19) -0.1601(3) 0.4584(2) 0.0420(9) Uani 1 1 d .
H12 H 0.1453 -0.1290 0.4988 0.050 Uiso 1 1 calc R
C13 C 0.14825(14) 0.4280(2) 0.46661(16) 0.0276(7) Uani 1 1 d .
C14 C 0.10373(17) 0.4755(3) 0.5010(2) 0.0372(8) Uani 1 1 d .
H14A H 0.0650 0.4824 0.4666 0.056 Uiso 1 1 calc R
H14B H 0.1191 0.5363 0.5181 0.056 Uiso 1 1 calc R
H14C H 0.0987 0.4380 0.5401 0.056 Uiso 1 1 calc R
C15 C 0.1608(2) 0.4938(3) 0.4113(2) 0.0439(9) Uani 1 1 d .
H15A H 0.1898 0.4655 0.3894 0.066 Uiso 1 1 calc R
H15B H 0.1771 0.5518 0.4336 0.066 Uiso 1 1 calc R
H15C H 0.1234 0.5061 0.3756 0.066 Uiso 1 1 calc R
C16 C 0.20625(17) 0.4099(3) 0.5238(2) 0.0436(9) Uani 1 1 d .
H16A H 0.1972 0.3725 0.5608 0.065 Uiso 1 1 calc R
H16B H 0.2237 0.4687 0.5433 0.065 Uiso 1 1 calc R
H16C H 0.2348 0.3771 0.5038 0.065 Uiso 1 1 calc R
S3 S -0.00633(3) 0.16429(6) 0.44531(4) 0.02513(18) Uani 1 1 d .
C17 C -0.06017(13) 0.1123(2) 0.37565(15) 0.0231(6) Uani 1 1 d .
C18 C -0.08899(13) 0.1568(2) 0.31277(15) 0.0224(6) Uani 1 1 d .
C19 C -0.13404(13) 0.1077(2) 0.26536(15) 0.0226(6) Uani 1 1 d .
C20 C -0.15102(13) 0.0201(2) 0.28171(15) 0.0236(6) Uani 1 1 d .
H20 H -0.1820 -0.0113 0.2489 0.028 Uiso 1 1 calc R
C21 C -0.12384(13) -0.0226(2) 0.34466(15) 0.0230(6) Uani 1 1 d .
C22 C -0.07793(13) 0.0253(2) 0.39025(16) 0.0249(6) Uani 1 1 d .
H22 H -0.0579 -0.0028 0.4332 0.030 Uiso 1 1 calc R
S4 S -0.06941(4) 0.26832(6) 0.29084(4) 0.02812(19) Uani 1 1 d .
C23 C -0.08995(18) 0.3404(2) 0.35647(18) 0.0339(8) Uani 1 1 d .
H23A H -0.1249 0.3140 0.3696 0.041 Uiso 1 1 calc R
H23B H -0.0562 0.3448 0.3989 0.041 Uiso 1 1 calc R
C24 C -0.10500(15) 0.4338(2) 0.32421(16) 0.0287(7) Uani 1 1 d .
C25 C -0.06104(15) 0.4897(2) 0.31017(18) 0.0321(7) Uani 1 1 d .
H25 H -0.0210 0.4677 0.3227 0.039 Uiso 1 1 calc R
N2 N -0.07135(13) 0.5725(2) 0.28015(16) 0.0335(6) Uani 1 1 d .
C26 C -0.12780(16) 0.6027(2) 0.2628(2) 0.0362(8) Uani 1 1 d .
H26 H -0.1362 0.6610 0.2407 0.043 Uiso 1 1 calc R
C27 C -0.17428(17) 0.5527(3) 0.2758(2) 0.0419(9) Uani 1 1 d .
H27 H -0.2139 0.5766 0.2634 0.050 Uiso 1 1 calc R
C28 C -0.16273(16) 0.4674(3) 0.3070(2) 0.0371(8) Uani 1 1 d .
H28 H -0.1943 0.4322 0.3166 0.044 Uiso 1 1 calc R
C29 C -0.14169(14) -0.1191(2) 0.36375(16) 0.0275(7) Uani 1 1 d .
C30 C -0.08892(16) -0.1847(3) 0.36940(19) 0.0349(8) Uani 1 1 d .
H30A H -0.0982 -0.2444 0.3870 0.052 Uiso 1 1 calc R
H30B H -0.0530 -0.1588 0.4015 0.052 Uiso 1 1 calc R
H30C H -0.0818 -0.1928 0.3233 0.052 Uiso 1 1 calc R
C31 C -0.15707(17) -0.1134(3) 0.43441(19) 0.0364(8) Uani 1 1 d .
H31A H -0.1911 -0.0717 0.4305 0.055 Uiso 1 1 calc R
H31B H -0.1224 -0.0901 0.4699 0.055 Uiso 1 1 calc R
H31C H -0.1675 -0.1748 0.4479 0.055 Uiso 1 1 calc R
C32 C -0.19622(18) -0.1568(3) 0.3095(2) 0.0424(9) Uani 1 1 d .
H32A H -0.2077 -0.2163 0.3254 0.064 Uiso 1 1 calc R
H32B H -0.1862 -0.1649 0.2649 0.064 Uiso 1 1 calc R
H32C H -0.2296 -0.1134 0.3036 0.064 Uiso 1 1 calc R
B1 B 0.2507(3) 0.7493(10) 0.3927(6) 0.084(4) Uani 0.50 1 d P
F1 F 0.2706(3) 0.8290(5) 0.4114(3) 0.0749(19) Uani 0.50 1 d P
F2 F 0.2930(3) 0.7130(6) 0.3833(3) 0.086(2) Uani 0.50 1 d P
F3 F 0.1992(3) 0.7498(5) 0.3524(3) 0.084(2) Uani 0.50 1 d P
F4 F 0.2413(3) 0.7165(6) 0.4606(4) 0.092(2) Uani 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N1 115.89(16) . 2
N1 Ag1 N2 102.98(11) . 2_545
N1 Ag1 N2 112.88(11) 2 2_545
N1 Ag1 N2 112.88(11) . 1_545
N1 Ag1 N2 102.97(11) 2 1_545
N2 Ag1 N2 109.42(15) 2_545 1_545
C19 S1 C1 108.45(13) 2 .
C6 C1 C2 120.6(3) . .
C6 C1 S1 114.4(2) . .
C2 C1 S1 124.9(2) . .
C3 C2 C1 116.9(3) . .
C3 C2 S2 119.1(2) . .
C1 C2 S2 124.0(2) . .
C4 C3 C2 121.6(3) . .
C4 C3 S3 113.4(2) . .
C2 C3 S3 124.3(2) . .
C5 C4 C3 121.5(3) . .
C5 C4 H4 119.3 . .
C3 C4 H4 119.3 . .
C4 C5 C6 116.9(3) . .
C4 C5 C13 122.5(3) . .
C6 C5 C13 120.6(3) . .
C1 C6 C5 122.3(3) . .
C1 C6 H6 118.8 . .
C5 C6 H6 118.8 . .
C2 S2 C7 102.24(15) . .
C8 C7 S2 106.9(2) . .
C8 C7 H7A 110.3 . .
S2 C7 H7A 110.3 . .
C8 C7 H7B 110.3 . .
S2 C7 H7B 110.3 . .
H7A C7 H7B 108.6 . .
C9 C8 C12 117.4(3) . .
C9 C8 C7 121.0(3) . .
C12 C8 C7 121.6(3) . .
N1 C9 C8 123.9(3) . .
N1 C9 H9 118.1 . .
C8 C9 H9 118.1 . .
C10 N1 C9 117.1(4) . .
C10 N1 Ag1 117.8(3) . .
C9 N1 Ag1 125.2(3) . .
N1 C10 C11 123.9(4) . .
N1 C10 H10 118.1 . .
C11 C10 H10 118.1 . .
C10 C11 C12 118.4(4) . .
C10 C11 H11 120.8 . .
C12 C11 H11 120.8 . .
C8 C12 C11 119.3(4) . .
C8 C12 H12 120.3 . .
C11 C12 H12 120.3 . .
C5 C13 C16 109.0(3) . .
C5 C13 C14 112.0(3) . .
C16 C13 C14 107.7(3) . .
C5 C13 C15 110.0(3) . .
C16 C13 C15 110.0(3) . .
C14 C13 C15 108.1(3) . .
C13 C14 H14A 109.5 . .
C13 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
C13 C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
C13 C15 H15A 109.5 . .
C13 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C13 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
C13 C16 H16A 109.5 . .
C13 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C13 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C17 S3 C3 109.78(14) . .
C22 C17 C18 120.5(3) . .
C22 C17 S3 114.4(2) . .
C18 C17 S3 124.7(2) . .
C19 C18 C17 117.2(3) . .
C19 C18 S4 119.6(2) . .
C17 C18 S4 123.1(2) . .
C20 C19 C18 120.8(3) . .
C20 C19 S1 114.5(2) . 2
C18 C19 S1 124.1(2) . 2
C21 C20 C19 121.8(3) . .
C21 C20 H20 119.1 . .
C19 C20 H20 119.1 . .
C22 C21 C20 116.9(3) . .
C22 C21 C29 120.3(3) . .
C20 C21 C29 122.8(3) . .
C17 C22 C21 122.7(3) . .
C17 C22 H22 118.7 . .
C21 C22 H22 118.7 . .
C18 S4 C23 102.58(15) . .
C24 C23 S4 106.7(2) . .
C24 C23 H23A 110.4 . .
S4 C23 H23A 110.4 . .
C24 C23 H23B 110.4 . .
S4 C23 H23B 110.4 . .
H23A C23 H23B 108.6 . .
C28 C24 C25 117.2(3) . .
C28 C24 C23 121.8(3) . .
C25 C24 C23 121.0(3) . .
N2 C25 C24 124.2(3) . .
N2 C25 H25 117.9 . .
C24 C25 H25 117.9 . .
C26 N2 C25 117.3(3) . .
C26 N2 Ag1 117.2(2) . 1_565
C25 N2 Ag1 125.4(2) . 1_565
N2 C26 C27 122.6(3) . .
N2 C26 H26 118.7 . .
C27 C26 H26 118.7 . .
C26 C27 C28 119.3(3) . .
C26 C27 H27 120.4 . .
C28 C27 H27 120.4 . .
C24 C28 C27 119.4(3) . .
C24 C28 H28 120.3 . .
C27 C28 H28 120.3 . .
C30 C29 C32 108.9(3) . .
C30 C29 C21 109.0(3) . .
C32 C29 C21 112.2(3) . .
C30 C29 C31 109.7(3) . .
C32 C29 C31 108.5(3) . .
C21 C29 C31 108.6(3) . .
C29 C30 H30A 109.5 . .
C29 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C29 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C29 C31 H31A 109.5 . .
C29 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C29 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
C29 C32 H32A 109.5 . .
C29 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C29 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
F2 B1 F3 126.6(14) . .
F2 B1 F1 101.8(8) . .
F3 B1 F1 113.3(9) . .
F2 B1 F4 109.0(7) . .
F3 B1 F4 103.9(7) . .
F1 B1 F4 98.9(11) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N1 2.294(3) .
Ag1 N1 2.294(3) 2
Ag1 N2 2.326(3) 2_545
Ag1 N2 2.326(3) 1_545
S1 C19 1.776(3) 2
S1 C1 1.781(3) .
C1 C6 1.389(4) .
C1 C2 1.404(4) .
C2 C3 1.396(4) .
C2 S2 1.766(3) .
C3 C4 1.394(4) .
C3 S3 1.779(3) .
C4 C5 1.387(4) .
C4 H4 0.9500 .
C5 C6 1.391(4) .
C5 C13 1.526(4) .
C6 H6 0.9500 .
S2 C7 1.830(3) .
C7 C8 1.501(5) .
C7 H7A 0.9900 .
C7 H7B 0.9900 .
C8 C9 1.376(5) .
C8 C12 1.379(5) .
C9 N1 1.338(5) .
C9 H9 0.9500 .
N1 C10 1.325(5) .
C10 C11 1.358(7) .
C10 H10 0.9500 .
C11 C12 1.386(6) .
C11 H11 0.9500 .
C12 H12 0.9500 .
C13 C16 1.537(5) .
C13 C14 1.541(5) .
C13 C15 1.541(5) .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C16 H16A 0.9800 .
C16 H16B 0.9800 .
C16 H16C 0.9800 .
S3 C17 1.771(3) .
C17 C22 1.382(4) .
C17 C18 1.410(4) .
C18 C19 1.403(4) .
C18 S4 1.767(3) .
C19 C20 1.396(4) .
C19 S1 1.776(3) 2
C20 C21 1.390(4) .
C20 H20 0.9500 .
C21 C22 1.390(4) .
C21 C29 1.536(4) .
C22 H22 0.9500 .
S4 C23 1.830(4) .
C23 C24 1.502(5) .
C23 H23A 0.9900 .
C23 H23B 0.9900 .
C24 C28 1.379(5) .
C24 C25 1.386(5) .
C25 N2 1.336(4) .
C25 H25 0.9500 .
N2 C26 1.335(4) .
N2 Ag1 2.326(3) 1_565
C26 C27 1.377(6) .
C26 H26 0.9500 .
C27 C28 1.380(6) .
C27 H27 0.9500 .
C28 H28 0.9500 .
C29 C30 1.530(5) .
C29 C32 1.531(5) .
C29 C31 1.538(5) .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
C31 H31A 0.9800 .
C31 H31B 0.9800 .
C31 H31C 0.9800 .
C32 H32A 0.9800 .
C32 H32B 0.9800 .
C32 H32C 0.9800 .
B1 F2 1.170(12) .
B1 F3 1.251(10) .
B1 F1 1.265(15) .
B1 F4 1.498(12) .
