#------------------------------------------------------------------------------
#$Date: 2016-10-08 01:18:24 +0300 (Sat, 08 Oct 2016) $
#$Revision: 187121 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/04/03/7040341.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7040341
loop_
_publ_author_name
'Dau, Thuy Minh'
'Asamoah, Benjamin Darko'
'Belyaev, Andrey'
'Chakkaradhari, Gomathy'
'Hirva, Pipsa'
'Jänis, Janne'
'Grachova, Elena V.'
'Tunik, Sergey P.'
'Koshevoy, Igor O.'
_publ_section_title
;
 Adjustable coordination of a hybrid phosphine-phosphine oxide ligand in
 luminescent Cu, Ag and Au complexes.
;
_journal_issue                   36
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              14160
_journal_page_last               14173
_journal_paper_doi               10.1039/c6dt02435a
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C84 H66 Au2 O2 P6, 2(F6 P)'
_chemical_formula_sum            'C84 H66 Au2 F12 O2 P8'
_chemical_formula_weight         1977.06
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-08-03 deposited with the CCDC.
2016-08-05 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 126.759(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   32.139(2)
_cell_length_b                   15.1473(10)
_cell_length_c                   22.6292(14)
_cell_measurement_reflns_used    9297
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      34.94
_cell_measurement_theta_min      2.25
_cell_volume                     8825.8(10)
_computing_cell_refinement       'SAINT (Bruker AXS, 2009)'
_computing_data_collection       'APEX2 (Bruker AXS, 2010)'
_computing_data_reduction        'SAINT (Bruker AXS, 2009)'
_computing_molecular_graphics    'Diamond v.3.2g (Brandenburg, 2011)'
_computing_publication_material  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 16
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device       '62mm x 62mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  'Bruker KAPPA APEX II DUO CCD'
_diffrn_measurement_method       'φ scans and ω scans with κ offset'
_diffrn_radiation_monochromator  'curved graphite crystal'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0275
_diffrn_reflns_av_unetI/netI     0.0232
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       37
_diffrn_reflns_limit_h_min       -38
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            39646
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.498
_diffrn_reflns_theta_min         1.622
_exptl_absorpt_coefficient_mu    3.534
_exptl_absorpt_correction_T_max  0.790
_exptl_absorpt_correction_T_min  0.535
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 2008)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.488
_exptl_crystal_description       block
_exptl_crystal_F_000             3888
_exptl_crystal_preparation       ', Luminescent'
_exptl_crystal_size_max          0.202
_exptl_crystal_size_mid          0.074
_exptl_crystal_size_min          0.070
_refine_diff_density_max         4.885
_refine_diff_density_min         -2.589
_refine_diff_density_rms         0.126
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     488
_refine_ls_number_reflns         8201
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0500
_refine_ls_R_factor_gt           0.0340
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0374P)²+111.2962P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0876
_refine_ls_wR_factor_ref         0.0987
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6338
_reflns_number_total             8201
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c6dt02435a2.cif
_cod_data_source_block           3
_cod_depositor_comments
'Adding full bibliography for 7040337--7040350.cif.'
_cod_original_cell_volume        8825.9(10)
_cod_database_code               7040341
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.535
_shelx_estimated_absorpt_t_max   0.790
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
C1 C 0.4101(2) -0.0310(4) 0.1198(3) 0.0346(13) Uani 1 1 d . . .
C2 C 0.4348(3) -0.0960(4) 0.1737(4) 0.0500(18) Uani 1 1 d . . .
H2 H 0.4527 -0.0803 0.2241 0.060 Uiso 1 1 calc R U .
C3 C 0.4336(3) -0.1844(5) 0.1545(5) 0.069(2) Uani 1 1 d . . .
H3 H 0.4505 -0.2287 0.1916 0.083 Uiso 1 1 calc R U .
C4 C 0.4077(3) -0.2067(6) 0.0810(6) 0.072(3) Uani 1 1 d . . .
H4 H 0.4071 -0.2664 0.0677 0.087 Uiso 1 1 calc R U .
C5 C 0.3832(4) -0.1444(6) 0.0282(5) 0.066(2) Uani 1 1 d . . .
H5 H 0.3654 -0.1607 -0.0221 0.079 Uiso 1 1 calc R U .
C6 C 0.3837(3) -0.0543(5) 0.0465(4) 0.0527(19) Uani 1 1 d . . .
H6 H 0.3661 -0.0108 0.0089 0.063 Uiso 1 1 calc R U .
C7 C 0.3868(2) 0.1458(4) 0.0649(3) 0.0312(13) Uani 1 1 d . . .
C8 C 0.4180(2) 0.1669(4) 0.0431(3) 0.0415(15) Uani 1 1 d . . .
H8 H 0.4543 0.1557 0.0749 0.050 Uiso 1 1 calc R U .
C9 C 0.3954(3) 0.2043(5) -0.0258(3) 0.056(2) Uani 1 1 d . . .
H9 H 0.4165 0.2186 -0.0409 0.067 Uiso 1 1 calc R U .
C10 C 0.3434(3) 0.2209(5) -0.0723(4) 0.057(2) Uani 1 1 d . . .
H10 H 0.3285 0.2460 -0.1195 0.068 Uiso 1 1 calc R U .
C11 C 0.3125(3) 0.2012(5) -0.0507(3) 0.0492(18) Uani 1 1 d . . .
H11 H 0.2763 0.2132 -0.0829 0.059 Uiso 1 1 calc R U .
C12 C 0.3341(2) 0.1639(4) 0.0180(3) 0.0396(15) Uani 1 1 d . . .
H12 H 0.3128 0.1507 0.0329 0.048 Uiso 1 1 calc R U .
C13 C 0.35770(19) 0.1644(4) 0.1963(3) 0.0251(11) Uani 1 1 d . . .
C14 C 0.3651(2) 0.0898(3) 0.1653(3) 0.0257(11) Uani 1 1 d . . .
C15 C 0.3305(2) 0.0190(4) 0.1409(3) 0.0324(13) Uani 1 1 d . . .
H15 H 0.3354 -0.0315 0.1208 0.039 Uiso 1 1 calc R U .
C16 C 0.2894(2) 0.0206(4) 0.1454(3) 0.0377(14) Uani 1 1 d . . .
H16 H 0.2663 -0.0281 0.1282 0.045 Uiso 1 1 calc R U .
C17 C 0.2822(2) 0.0933(4) 0.1751(3) 0.0350(14) Uani 1 1 d . . .
H17 H 0.2541 0.0947 0.1784 0.042 Uiso 1 1 calc R U .
C18 C 0.3160(2) 0.1647(4) 0.2000(3) 0.0293(12) Uani 1 1 d . . .
H18 H 0.3106 0.2147 0.2201 0.035 Uiso 1 1 calc R U .
C19 C 0.35378(19) 0.3520(3) 0.1927(3) 0.0220(11) Uani 1 1 d . . .
C20 C 0.3348(2) 0.3835(4) 0.1224(3) 0.0334(13) Uani 1 1 d . . .
H20 H 0.3465 0.3581 0.0964 0.040 Uiso 1 1 calc R U .
C21 C 0.2986(3) 0.4520(4) 0.0908(3) 0.0437(16) Uani 1 1 d . . .
H21 H 0.2856 0.4731 0.0430 0.052 Uiso 1 1 calc R U .
C22 C 0.2818(2) 0.4891(4) 0.1287(4) 0.0395(15) Uani 1 1 d . . .
H22 H 0.2576 0.5365 0.1072 0.047 Uiso 1 1 calc R U .
C23 C 0.2997(2) 0.4584(4) 0.1975(3) 0.0374(14) Uani 1 1 d . . .
H23 H 0.2875 0.4840 0.2228 0.045 Uiso 1 1 calc R U .
C24 C 0.3356(2) 0.3900(4) 0.2297(3) 0.0311(12) Uani 1 1 d . . .
H24 H 0.3478 0.3689 0.2771 0.037 Uiso 1 1 calc R U .
C25 C 0.43490(19) 0.2651(3) 0.3280(3) 0.0232(11) Uani 1 1 d . . .
C26 C 0.46954(19) 0.3344(3) 0.3729(3) 0.0216(10) Uani 1 1 d . . .
C27 C 0.4920(2) 0.3337(4) 0.4476(3) 0.0263(11) Uani 1 1 d . . .
H27 H 0.5148 0.3803 0.4777 0.032 Uiso 1 1 calc R U .
C28 C 0.4822(2) 0.2666(4) 0.4798(3) 0.0317(13) Uani 1 1 d . . .
H28 H 0.4977 0.2686 0.5310 0.038 Uiso 1 1 calc R U .
C29 C 0.4502(2) 0.1975(4) 0.4374(3) 0.0343(13) Uani 1 1 d . . .
H29 H 0.4442 0.1503 0.4592 0.041 Uiso 1 1 calc R U .
C30 C 0.4264(2) 0.1981(4) 0.3616(3) 0.0322(13) Uani 1 1 d . . .
H30 H 0.4038 0.1510 0.3320 0.039 Uiso 1 1 calc R U .
C31 C 0.4420(2) 0.5149(3) 0.3182(3) 0.0249(11) Uani 1 1 d . . .
C32 C 0.4269(3) 0.5732(4) 0.2618(4) 0.0426(15) Uani 1 1 d . . .
H32 H 0.4375 0.5644 0.2309 0.051 Uiso 1 1 calc R U .
C33 C 0.3958(3) 0.6454(5) 0.2505(4) 0.057(2) Uani 1 1 d . . .
H33 H 0.3854 0.6863 0.2121 0.069 Uiso 1 1 calc R U .
C34 C 0.3799(3) 0.6580(5) 0.2946(4) 0.057(2) Uani 1 1 d . . .
H34 H 0.3590 0.7075 0.2866 0.068 Uiso 1 1 calc R U .
C35 C 0.3942(2) 0.5994(4) 0.3496(4) 0.0424(16) Uani 1 1 d . . .
H35 H 0.3827 0.6074 0.3793 0.051 Uiso 1 1 calc R U .
C36 C 0.4256(2) 0.5282(4) 0.3619(3) 0.0314(13) Uani 1 1 d . . .
H36 H 0.4359 0.4880 0.4007 0.038 Uiso 1 1 calc R U .
C37 C 0.54880(19) 0.4654(3) 0.4195(3) 0.0222(11) Uani 1 1 d . . .
C38 C 0.5546(2) 0.5455(3) 0.4535(3) 0.0264(11) Uani 1 1 d . . .
H38 H 0.5254 0.5828 0.4347 0.032 Uiso 1 1 calc R U .
C39 C 0.6035(2) 0.5711(4) 0.5153(3) 0.0318(12) Uani 1 1 d . . .
H39 H 0.6075 0.6260 0.5386 0.038 Uiso 1 1 calc R U .
C40 C 0.6458(2) 0.5172(4) 0.5428(3) 0.0362(14) Uani 1 1 d . . .
H40 H 0.6789 0.5346 0.5853 0.043 Uiso 1 1 calc R U .
C41 C 0.6403(2) 0.4372(4) 0.5086(3) 0.0413(15) Uani 1 1 d . . .
H41 H 0.6697 0.4003 0.5276 0.050 Uiso 1 1 calc R U .
C42 C 0.5918(2) 0.4112(4) 0.4468(3) 0.0332(13) Uani 1 1 d . . .
H42 H 0.5879 0.3567 0.4231 0.040 Uiso 1 1 calc R U .
O1 O 0.43106(13) 0.2621(2) 0.20092(19) 0.0243(8) Uani 1 1 d . . .
F1 F 0.32483(14) 0.2481(3) 0.3507(2) 0.0535(10) Uani 1 1 d . . .
F2 F 0.21231(17) 0.3005(3) 0.3022(3) 0.0681(13) Uani 1 1 d . . .
F3 F 0.29314(17) 0.3020(3) 0.4087(2) 0.0603(11) Uani 1 1 d . . .
F4 F 0.24314(16) 0.2414(3) 0.2440(2) 0.0606(12) Uani 1 1 d . . .
F5 F 0.27574(18) 0.3707(3) 0.3080(2) 0.0615(12) Uani 1 1 d . . .
F7 F 0.26055(18) 0.1764(3) 0.3460(3) 0.0676(12) Uani 1 1 d . . .
P1 P 0.41462(5) 0.08340(9) 0.14943(7) 0.0249(3) Uani 1 1 d . . .
P2 P 0.39849(5) 0.26147(9) 0.22786(7) 0.0213(3) Uani 1 1 d . . .
P3 P 0.48691(5) 0.42633(9) 0.33814(7) 0.0198(3) Uani 1 1 d . . .
P10 P 0.26854(6) 0.27056(12) 0.32582(9) 0.0382(4) Uani 1 1 d . . .
Au1 Au 0.5000 0.10418(2) 0.2500 0.02036(8) Uani 1 2 d S T P
Au2 Au 0.5000 0.39961(2) 0.2500 0.02760(9) Uani 1 2 d S T P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
C6 C1 C2 119.4(6) .
C6 C1 P1 122.5(5) .
C2 C1 P1 118.1(5) .
C1 C2 C3 120.6(7) .
C1 C2 H2 119.7 .
C3 C2 H2 119.7 .
C4 C3 C2 119.4(8) .
C4 C3 H3 120.3 .
C2 C3 H3 120.3 .
C5 C4 C3 120.5(7) .
C5 C4 H4 119.7 .
C3 C4 H4 119.7 .
C4 C5 C6 120.9(7) .
C4 C5 H5 119.6 .
C6 C5 H5 119.6 .
C1 C6 C5 119.1(8) .
C1 C6 H6 120.4 .
C5 C6 H6 120.4 .
C12 C7 C8 119.4(5) .
C12 C7 P1 121.0(5) .
C8 C7 P1 119.2(5) .
C9 C8 C7 119.2(6) .
C9 C8 H8 120.4 .
C7 C8 H8 120.4 .
C10 C9 C8 121.3(7) .
C10 C9 H9 119.4 .
C8 C9 H9 119.4 .
C9 C10 C11 119.8(6) .
C9 C10 H10 120.1 .
C11 C10 H10 120.1 .
C10 C11 C12 120.1(7) .
C10 C11 H11 120.0 .
C12 C11 H11 120.0 .
C7 C12 C11 120.2(6) .
C7 C12 H12 119.9 .
C11 C12 H12 119.9 .
C18 C13 C14 118.9(5) .
C18 C13 P2 118.0(4) .
C14 C13 P2 123.1(4) .
C15 C14 C13 118.5(5) .
C15 C14 P1 117.4(4) .
C13 C14 P1 124.0(4) .
C16 C15 C14 121.6(6) .
C16 C15 H15 119.2 .
C14 C15 H15 119.2 .
C17 C16 C15 119.7(5) .
C17 C16 H16 120.2 .
C15 C16 H16 120.2 .
C16 C17 C18 120.0(6) .
C16 C17 H17 120.0 .
C18 C17 H17 120.0 .
C17 C18 C13 121.3(6) .
C17 C18 H18 119.4 .
C13 C18 H18 119.4 .
C24 C19 C20 119.0(5) .
C24 C19 P2 124.0(4) .
C20 C19 P2 117.0(4) .
C21 C20 C19 119.9(6) .
C21 C20 H20 120.0 .
C19 C20 H20 120.0 .
C22 C21 C20 120.1(6) .
C22 C21 H21 120.0 .
C20 C21 H21 120.0 .
C21 C22 C23 120.7(6) .
C21 C22 H22 119.6 .
C23 C22 H22 119.6 .
C22 C23 C24 120.0(6) .
C22 C23 H23 120.0 .
C24 C23 H23 120.0 .
C23 C24 C19 120.3(5) .
C23 C24 H24 119.8 .
C19 C24 H24 119.8 .
C30 C25 C26 118.4(5) .
C30 C25 P2 117.8(4) .
C26 C25 P2 123.7(4) .
C27 C26 C25 118.7(5) .
C27 C26 P3 117.2(4) .
C25 C26 P3 124.2(4) .
C26 C27 C28 121.9(5) .
C26 C27 H27 119.1 .
C28 C27 H27 119.1 .
C29 C28 C27 120.0(5) .
C29 C28 H28 120.0 .
C27 C28 H28 120.0 .
C28 C29 C30 118.7(5) .
C28 C29 H29 120.6 .
C30 C29 H29 120.6 .
C25 C30 C29 122.2(5) .
C25 C30 H30 118.9 .
C29 C30 H30 118.9 .
C32 C31 C36 119.6(5) .
C32 C31 P3 119.3(4) .
C36 C31 P3 121.0(4) .
C31 C32 C33 119.0(6) .
C31 C32 H32 120.5 .
C33 C32 H32 120.5 .
C34 C33 C32 120.7(6) .
C34 C33 H33 119.6 .
C32 C33 H33 119.6 .
C35 C34 C33 120.2(6) .
C35 C34 H34 119.9 .
C33 C34 H34 119.9 .
C34 C35 C36 119.7(6) .
C34 C35 H35 120.1 .
C36 C35 H35 120.1 .
C35 C36 C31 120.8(6) .
C35 C36 H36 119.6 .
C31 C36 H36 119.6 .
C38 C37 C42 120.1(5) .
C38 C37 P3 123.3(4) .
C42 C37 P3 116.7(4) .
C37 C38 C39 119.8(5) .
C37 C38 H38 120.1 .
C39 C38 H38 120.1 .
C40 C39 C38 120.2(5) .
C40 C39 H39 119.9 .
C38 C39 H39 119.9 .
C39 C40 C41 120.3(5) .
C39 C40 H40 119.8 .
C41 C40 H40 119.8 .
C40 C41 C42 119.9(6) .
C40 C41 H41 120.1 .
C42 C41 H41 120.1 .
C41 C42 C37 119.7(5) .
C41 C42 H42 120.1 .
C37 C42 H42 120.1 .
C7 P1 C1 103.1(3) .
C7 P1 C14 104.0(3) .
C1 P1 C14 103.5(3) .
C7 P1 Au1 120.79(19) .
C1 P1 Au1 106.1(2) .
C14 P1 Au1 117.30(17) .
O1 P2 C19 112.7(2) .
O1 P2 C13 111.3(2) .
C19 P2 C13 104.3(2) .
O1 P2 C25 114.9(2) .
C19 P2 C25 106.1(2) .
C13 P2 C25 106.8(2) .
C31 P3 C37 103.6(2) .
C31 P3 C26 105.4(2) .
C37 P3 C26 103.9(2) .
C31 P3 Au2 116.29(18) .
C37 P3 Au2 106.13(17) .
C26 P3 Au2 119.67(17) .
F7 P10 F4 91.6(3) .
F7 P10 F1 93.0(2) .
F4 P10 F1 92.1(2) .
F7 P10 F3 88.9(2) .
F4 P10 F3 178.4(3) .
F1 P10 F3 89.3(2) .
F7 P10 F2 90.3(3) .
F4 P10 F2 89.9(2) .
F1 P10 F2 176.0(3) .
F3 P10 F2 88.6(3) .
F7 P10 F5 176.3(3) .
F4 P10 F5 91.2(2) .
F1 P10 F5 89.2(2) .
F3 P10 F5 88.2(2) .
F2 P10 F5 87.3(3) .
P1 Au1 P1 164.34(7) 2_655
P3 Au2 P3 159.80(7) 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C6 1.382(9) .
C1 C2 1.388(9) .
C1 P1 1.832(6) .
C2 C3 1.402(10) .
C2 H2 0.9500 .
C3 C4 1.383(13) .
C3 H3 0.9500 .
C4 C5 1.347(13) .
C4 H4 0.9500 .
C5 C6 1.423(11) .
C5 H5 0.9500 .
C6 H6 0.9500 .
C7 C12 1.385(8) .
C7 C8 1.395(9) .
C7 P1 1.817(6) .
C8 C9 1.387(9) .
C8 H8 0.9500 .
C9 C10 1.363(11) .
C9 H9 0.9500 .
C10 C11 1.378(11) .
C10 H10 0.9500 .
C11 C12 1.388(9) .
C11 H11 0.9500 .
C12 H12 0.9500 .
C13 C18 1.392(8) .
C13 C14 1.422(8) .
C13 P2 1.808(5) .
C14 C15 1.398(7) .
C14 P1 1.833(6) .
C15 C16 1.386(8) .
C15 H15 0.9500 .
C16 C17 1.380(9) .
C16 H16 0.9500 .
C17 C18 1.392(8) .
C17 H17 0.9500 .
C18 H18 0.9500 .
C19 C24 1.402(8) .
C19 C20 1.403(7) .
C19 P2 1.791(5) .
C20 C21 1.394(8) .
C20 H20 0.9500 .
C21 C22 1.378(9) .
C21 H21 0.9500 .
C22 C23 1.378(9) .
C22 H22 0.9500 .
C23 C24 1.388(8) .
C23 H23 0.9500 .
C24 H24 0.9500 .
C25 C30 1.388(8) .
C25 C26 1.422(7) .
C25 P2 1.826(5) .
C26 C27 1.385(7) .
C26 P3 1.842(5) .
C27 C28 1.393(8) .
C27 H27 0.9500 .
C28 C29 1.376(8) .
C28 H28 0.9500 .
C29 C30 1.401(8) .
C29 H29 0.9500 .
C30 H30 0.9500 .
C31 C32 1.380(8) .
C31 C36 1.388(8) .
C31 P3 1.818(5) .
C32 C33 1.400(9) .
C32 H32 0.9500 .
C33 C34 1.377(11) .
C33 H33 0.9500 .
C34 C35 1.366(10) .
C34 H34 0.9500 .
C35 C36 1.386(8) .
C35 H35 0.9500 .
C36 H36 0.9500 .
C37 C38 1.388(7) .
C37 C42 1.394(8) .
C37 P3 1.821(5) .
C38 C39 1.394(8) .
C38 H38 0.9500 .
C39 C40 1.376(8) .
C39 H39 0.9500 .
C40 C41 1.391(8) .
C40 H40 0.9500 .
C41 C42 1.391(8) .
C41 H41 0.9500 .
C42 H42 0.9500 .
O1 P2 1.494(4) .
F1 P10 1.576(4) .
F2 P10 1.613(5) .
F3 P10 1.610(4) .
F4 P10 1.574(4) .
F5 P10 1.621(4) .
F7 P10 1.565(4) .
P1 Au1 2.3094(13) .
P3 Au2 2.3071(13) .
Au1 P1 2.3094(13) 2_655
Au2 P3 2.3070(13) 2_655
