#------------------------------------------------------------------------------
#$Date: 2017-02-04 16:04:24 +0200 (Sat, 04 Feb 2017) $
#$Revision: 191676 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/04/12/7041240.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7041240
loop_
_publ_author_name
'Bhat, Sajad A.'
'Pandey, Madhusudan K.'
'Mague, Joel T.'
'Balakrishna, Maravanji S.'
_publ_section_title
;
 Coordination of bis(azol-1-yl)methane-based bisphosphines towards Ru(II),
 Rh(I), Pd(II) and Pt(II): synthesis, structural and catalytic studies.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              227
_journal_page_last               241
_journal_paper_doi               10.1039/c6dt04094b
_journal_volume                  46
_journal_year                    2016
_chemical_formula_moiety         'C31 H26 N4 P2 Se2'
_chemical_formula_sum            'C31 H26 N4 P2 Se2'
_chemical_formula_weight         674.42
_chemical_name_systematic
'[1-({2-[diphenyl[selenylidene)-λ⁵-phosphanyl]-1H-imidazol-1-yl}methyl)-1H-imidazol-2-yl]diphenyl-λ⁵-phosphaselenone'
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-10-23 deposited with the CCDC.
2016-11-23 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 103.209(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.078(3)
_cell_length_b                   13.427(3)
_cell_length_c                   16.699(4)
_cell_measurement_reflns_used    9516
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      29.0476
_cell_measurement_theta_min      2.2043
_cell_volume                     2854.7(11)
_computing_cell_refinement       'SAINT (Bruker, 2016)'
_computing_data_collection       'APEX3 (Bruker, 2016)'
_computing_data_reduction        'SAINT (Bruker, 2016)'
_computing_molecular_graphics    'DIAMOND (Brandenburg & Putz, 2012)'
_computing_publication_material  'SHELXTL (Bruker, 2016)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2015b)'
_computing_structure_solution    'SHELXT (Sheldrick, 2015a)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 8.3660
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device_type  'Bruker Smart APEX CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0472
_diffrn_reflns_av_unetI/netI     0.0295
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.983
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            51765
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.983
_diffrn_reflns_theta_full        28.500
_diffrn_reflns_theta_max         29.090
_diffrn_reflns_theta_min         1.792
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    2.731
_exptl_absorpt_correction_T_max  0.69
_exptl_absorpt_correction_T_min  0.48
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'SADABS (Bruker, 2016)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.569
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1352
_exptl_crystal_size_max          0.242
_exptl_crystal_size_mid          0.185
_exptl_crystal_size_min          0.147
_exptl_transmission_factor_max   0.473
_exptl_transmission_factor_min   0.330
_refine_diff_density_max         0.752
_refine_diff_density_min         -0.355
_refine_diff_density_rms         0.090
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     352
_refine_ls_number_reflns         7522
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0345
_refine_ls_R_factor_gt           0.0282
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0369P)²+1.4840P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0697
_refine_ls_wR_factor_ref         0.0724
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6590
_reflns_number_total             7522
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c6dt04094b2.cif
_cod_data_source_block           MSB578_0m
_cod_depositor_comments
'Adding full bibliography for 7041235--7041247.cif.'
_cod_original_cell_volume        2854.9(12)
_cod_database_code               7041240
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.558
_shelx_estimated_absorpt_t_max   0.690
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
Se1 Se 0.41842(2) 0.03291(2) 0.60950(2) 0.02146(6) Uani 1 1 d . .
Se2 Se 0.09578(2) 0.41915(2) 0.31558(2) 0.01777(5) Uani 1 1 d . .
P1 P 0.25382(3) 0.02829(3) 0.56750(3) 0.01156(9) Uani 1 1 d . .
P2 P 0.23881(3) 0.46125(3) 0.39456(3) 0.01127(9) Uani 1 1 d . .
N1 N 0.16182(11) -0.01718(11) 0.40458(8) 0.0149(3) Uani 1 1 d . .
N2 N 0.22455(11) 0.13778(10) 0.41917(9) 0.0141(3) Uani 1 1 d . .
N3 N 0.34162(11) 0.27635(10) 0.41893(9) 0.0139(3) Uani 1 1 d . .
N4 N 0.42970(11) 0.39172(11) 0.36629(9) 0.0149(3) Uani 1 1 d . .
C1 C 0.19626(13) -0.09186(12) 0.58016(10) 0.0129(3) Uani 1 1 d . .
C2 C 0.23664(14) -0.17576(13) 0.54834(10) 0.0178(3) Uani 1 1 d . .
H2 H 0.2932 -0.1689 0.5218 0.021 Uiso 1 1 calc R U
C3 C 0.19397(15) -0.26904(13) 0.55567(11) 0.0207(4) Uani 1 1 d . .
H3 H 0.2205 -0.3259 0.5333 0.025 Uiso 1 1 calc R U
C4 C 0.11196(14) -0.27918(13) 0.59595(12) 0.0215(4) Uani 1 1 d . .
H4 H 0.0827 -0.3430 0.6008 0.026 Uiso 1 1 calc R U
C5 C 0.07320(13) -0.19674(13) 0.62881(11) 0.0195(4) Uani 1 1 d . .
H5 H 0.0181 -0.2043 0.6569 0.023 Uiso 1 1 calc R U
C6 C 0.11475(13) -0.10235(13) 0.62086(10) 0.0159(3) Uani 1 1 d . .
H6 H 0.0877 -0.0456 0.6430 0.019 Uiso 1 1 calc R U
C7 C 0.18440(12) 0.11941(12) 0.61513(10) 0.0122(3) Uani 1 1 d . .
C8 C 0.23588(13) 0.16951(13) 0.68625(10) 0.0151(3) Uani 1 1 d . .
H8 H 0.3088 0.1591 0.7082 0.018 Uiso 1 1 calc R U
C9 C 0.17972(14) 0.23483(13) 0.72482(11) 0.0182(3) Uani 1 1 d . .
H9 H 0.2143 0.2692 0.7732 0.022 Uiso 1 1 calc R U
C10 C 0.07317(14) 0.24964(14) 0.69249(11) 0.0182(3) Uani 1 1 d . .
H10 H 0.0350 0.2938 0.7193 0.022 Uiso 1 1 calc R U
C11 C 0.02167(13) 0.20072(13) 0.62140(11) 0.0185(3) Uani 1 1 d . .
H11 H -0.0512 0.2115 0.5996 0.022 Uiso 1 1 calc R U
C12 C 0.07735(13) 0.13597(13) 0.58242(10) 0.0160(3) Uani 1 1 d . .
H12 H 0.0427 0.1028 0.5335 0.019 Uiso 1 1 calc R U
C13 C 0.20941(12) 0.05045(12) 0.45800(10) 0.0126(3) Uani 1 1 d . .
C14 C 0.14555(14) 0.02843(13) 0.32875(10) 0.0169(3) Uani 1 1 d . .
H14 H 0.1131 -0.0023 0.2781 0.020 Uiso 1 1 calc R U
C15 C 0.18247(14) 0.12374(13) 0.33658(10) 0.0172(3) Uani 1 1 d . .
H15 H 0.1797 0.1709 0.2937 0.021 Uiso 1 1 calc R U
C16 C 0.26500(14) 0.23086(12) 0.45881(11) 0.0179(3) Uani 1 1 d . .
H16A H 0.2983 0.2179 0.5173 0.021 Uiso 1 1 calc R U
H16B H 0.2060 0.2777 0.4568 0.021 Uiso 1 1 calc R U
C17 C 0.43202(13) 0.23156(13) 0.40800(11) 0.0178(3) Uani 1 1 d . .
H17 H 0.4535 0.1647 0.4206 0.021 Uiso 1 1 calc R U
C18 C 0.48452(13) 0.30304(14) 0.37538(11) 0.0180(3) Uani 1 1 d . .
H18 H 0.5499 0.2931 0.3609 0.022 Uiso 1 1 calc R U
C19 C 0.34384(12) 0.37341(12) 0.39315(10) 0.0125(3) Uani 1 1 d . .
C20 C 0.28346(13) 0.58446(12) 0.37346(10) 0.0142(3) Uani 1 1 d . .
C21 C 0.38704(15) 0.61652(14) 0.40110(12) 0.0230(4) Uani 1 1 d . .
H21 H 0.4399 0.5707 0.4264 0.028 Uiso 1 1 calc R U
C22 C 0.41286(16) 0.71588(15) 0.39153(12) 0.0265(4) Uani 1 1 d . .
H22 H 0.4836 0.7375 0.4096 0.032 Uiso 1 1 calc R U
C23 C 0.33563(17) 0.78318(14) 0.35569(11) 0.0245(4) Uani 1 1 d . .
H23 H 0.3531 0.8512 0.3506 0.029 Uiso 1 1 calc R U
C24 C 0.23303(16) 0.75135(14) 0.32729(12) 0.0242(4) Uani 1 1 d . .
H24 H 0.1804 0.7975 0.3021 0.029 Uiso 1 1 calc R U
C25 C 0.20678(14) 0.65208(13) 0.33557(11) 0.0192(3) Uani 1 1 d . .
H25 H 0.1365 0.6304 0.3154 0.023 Uiso 1 1 calc R U
C26 C 0.23543(13) 0.46485(12) 0.50300(10) 0.0124(3) Uani 1 1 d . .
C27 C 0.32813(14) 0.48041(14) 0.56259(12) 0.0201(4) Uani 1 1 d . .
H27 H 0.3928 0.4884 0.5465 0.024 Uiso 1 1 calc R U
C28 C 0.32605(16) 0.48420(15) 0.64532(12) 0.0250(4) Uani 1 1 d . .
H28 H 0.3891 0.4947 0.6858 0.030 Uiso 1 1 calc R U
C29 C 0.23158(16) 0.47262(14) 0.66868(11) 0.0228(4) Uani 1 1 d . .
H29 H 0.2301 0.4749 0.7253 0.027 Uiso 1 1 calc R U
C30 C 0.13902(15) 0.45774(13) 0.60956(11) 0.0201(4) Uani 1 1 d . .
H30 H 0.0744 0.4503 0.6258 0.024 Uiso 1 1 calc R U
C31 C 0.14077(13) 0.45375(13) 0.52660(11) 0.0160(3) Uani 1 1 d . .
H31 H 0.0775 0.4435 0.4862 0.019 Uiso 1 1 calc R U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C7 P1 C13 104.76(7)
C7 P1 C1 106.66(8)
C13 P1 C1 102.59(7)
C7 P1 Se1 114.22(6)
C13 P1 Se1 113.48(5)
C1 P1 Se1 114.03(6)
C19 P2 C20 108.17(8)
C19 P2 C26 102.74(7)
C20 P2 C26 104.51(8)
C19 P2 Se2 112.60(6)
C20 P2 Se2 113.72(6)
C26 P2 Se2 114.19(6)
C13 N1 C14 105.32(14)
C13 N2 C15 106.74(14)
C13 N2 C16 126.42(14)
C15 N2 C16 126.43(14)
C19 N3 C17 107.02(14)
C19 N3 C16 127.30(14)
C17 N3 C16 125.37(15)
C19 N4 C18 105.19(14)
C6 C1 C2 120.00(15)
C6 C1 P1 122.01(13)
C2 C1 P1 117.99(13)
C3 C2 C1 119.92(17)
C3 C2 H2 120.0
C1 C2 H2 120.0
C2 C3 C4 119.93(17)
C2 C3 H3 120.0
C4 C3 H3 120.0
C5 C4 C3 120.31(16)
C5 C4 H4 119.8
C3 C4 H4 119.8
C4 C5 C6 120.19(17)
C4 C5 H5 119.9
C6 C5 H5 119.9
C1 C6 C5 119.64(16)
C1 C6 H6 120.2
C5 C6 H6 120.2
C8 C7 C12 120.02(15)
C8 C7 P1 120.39(12)
C12 C7 P1 119.53(12)
C9 C8 C7 119.59(15)
C9 C8 H8 120.2
C7 C8 H8 120.2
C10 C9 C8 119.91(16)
C10 C9 H9 120.0
C8 C9 H9 120.0
C11 C10 C9 120.80(16)
C11 C10 H10 119.6
C9 C10 H10 119.6
C12 C11 C10 119.55(16)
C12 C11 H11 120.2
C10 C11 H11 120.2
C11 C12 C7 120.12(16)
C11 C12 H12 119.9
C7 C12 H12 119.9
N1 C13 N2 111.28(14)
N1 C13 P1 124.05(13)
N2 C13 P1 124.62(12)
C15 C14 N1 110.61(15)
C15 C14 H14 124.7
N1 C14 H14 124.7
C14 C15 N2 106.05(15)
C14 C15 H15 127.0
N2 C15 H15 127.0
N2 C16 N3 111.60(13)
N2 C16 H16A 109.3
N3 C16 H16A 109.3
N2 C16 H16B 109.3
N3 C16 H16B 109.3
H16A C16 H16B 108.0
C18 C17 N3 105.77(15)
C18 C17 H17 127.1
N3 C17 H17 127.1
C17 C18 N4 110.78(15)
C17 C18 H18 124.6
N4 C18 H18 124.6
N4 C19 N3 111.24(14)
N4 C19 P2 125.93(13)
N3 C19 P2 122.81(12)
C25 C20 C21 119.52(16)
C25 C20 P2 116.88(13)
C21 C20 P2 123.22(13)
C22 C21 C20 119.96(18)
C22 C21 H21 120.0
C20 C21 H21 120.0
C23 C22 C21 120.13(18)
C23 C22 H22 119.9
C21 C22 H22 119.9
C24 C23 C22 120.03(18)
C24 C23 H23 120.0
C22 C23 H23 120.0
C23 C24 C25 120.23(18)
C23 C24 H24 119.9
C25 C24 H24 119.9
C24 C25 C20 120.09(17)
C24 C25 H25 120.0
C20 C25 H25 120.0
C31 C26 C27 119.87(16)
C31 C26 P2 120.28(13)
C27 C26 P2 119.84(13)
C28 C27 C26 120.19(17)
C28 C27 H27 119.9
C26 C27 H27 119.9
C29 C28 C27 119.80(17)
C29 C28 H28 120.1
C27 C28 H28 120.1
C28 C29 C30 120.22(17)
C28 C29 H29 119.9
C30 C29 H29 119.9
C29 C30 C31 120.17(17)
C29 C30 H30 119.9
C31 C30 H30 119.9
C26 C31 C30 119.75(16)
C26 C31 H31 120.1
C30 C31 H31 120.1
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Se1 P1 2.1072(7)
Se2 P2 2.1049(6)
P1 C7 1.8121(17)
P1 C13 1.8123(17)
P1 C1 1.8130(17)
P2 C19 1.8147(17)
P2 C20 1.8155(17)
P2 C26 1.8222(18)
N1 C13 1.325(2)
N1 C14 1.379(2)
N2 C13 1.376(2)
N2 C15 1.376(2)
N2 C16 1.456(2)
N3 C19 1.375(2)
N3 C17 1.375(2)
N3 C16 1.458(2)
N4 C19 1.324(2)
N4 C18 1.380(2)
C1 C6 1.396(2)
C1 C2 1.399(2)
C2 C3 1.388(3)
C2 H2 0.9500
C3 C4 1.397(3)
C3 H3 0.9500
C4 C5 1.382(3)
C4 H4 0.9500
C5 C6 1.397(2)
C5 H5 0.9500
C6 H6 0.9500
C7 C8 1.397(2)
C7 C12 1.399(2)
C8 C9 1.393(2)
C8 H8 0.9500
C9 C10 1.389(2)
C9 H9 0.9500
C10 C11 1.389(2)
C10 H10 0.9500
C11 C12 1.388(2)
C11 H11 0.9500
C12 H12 0.9500
C14 C15 1.363(3)
C14 H14 0.9500
C15 H15 0.9500
C16 H16A 0.9900
C16 H16B 0.9900
C17 C18 1.364(3)
C17 H17 0.9500
C18 H18 0.9500
C20 C25 1.393(2)
C20 C21 1.396(2)
C21 C22 1.394(3)
C21 H21 0.9500
C22 C23 1.385(3)
C22 H22 0.9500
C23 C24 1.385(3)
C23 H23 0.9500
C24 C25 1.391(3)
C24 H24 0.9500
C25 H25 0.9500
C26 C31 1.390(2)
C26 C27 1.397(2)
C27 C28 1.389(3)
C27 H27 0.9500
C28 C29 1.387(3)
C28 H28 0.9500
C29 C30 1.391(3)
C29 H29 0.9500
C30 C31 1.392(2)
C30 H30 0.9500
C31 H31 0.9500
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C7 P1 C1 C6 -0.53(16)
C13 P1 C1 C6 -110.37(14)
Se1 P1 C1 C6 126.50(13)
C7 P1 C1 C2 -179.93(13)
C13 P1 C1 C2 70.23(14)
Se1 P1 C1 C2 -52.90(14)
C6 C1 C2 C3 1.5(3)
P1 C1 C2 C3 -179.13(13)
C1 C2 C3 C4 -1.0(3)
C2 C3 C4 C5 -0.2(3)
C3 C4 C5 C6 1.0(3)
C2 C1 C6 C5 -0.7(2)
P1 C1 C6 C5 179.94(13)
C4 C5 C6 C1 -0.5(3)
C13 P1 C7 C8 -139.15(14)
C1 P1 C7 C8 112.54(14)
Se1 P1 C7 C8 -14.38(15)
C13 P1 C7 C12 43.84(15)
C1 P1 C7 C12 -64.46(15)
Se1 P1 C7 C12 168.62(11)
C12 C7 C8 C9 0.8(2)
P1 C7 C8 C9 -176.14(13)
C7 C8 C9 C10 0.1(3)
C8 C9 C10 C11 -0.6(3)
C9 C10 C11 C12 0.3(3)
C10 C11 C12 C7 0.7(3)
C8 C7 C12 C11 -1.2(2)
P1 C7 C12 C11 175.80(13)
C14 N1 C13 N2 -0.17(19)
C14 N1 C13 P1 -177.63(12)
C15 N2 C13 N1 0.79(19)
C16 N2 C13 N1 173.70(15)
C15 N2 C13 P1 178.23(12)
C16 N2 C13 P1 -8.9(2)
C7 P1 C13 N1 -120.81(15)
C1 P1 C13 N1 -9.55(16)
Se1 P1 C13 N1 113.94(13)
C7 P1 C13 N2 62.06(15)
C1 P1 C13 N2 173.33(14)
Se1 P1 C13 N2 -63.18(15)
C13 N1 C14 C15 -0.5(2)
N1 C14 C15 N2 1.0(2)
C13 N2 C15 C14 -1.07(18)
C16 N2 C15 C14 -173.98(15)
C13 N2 C16 N3 136.37(16)
C15 N2 C16 N3 -52.1(2)
C19 N3 C16 N2 130.43(17)
C17 N3 C16 N2 -56.8(2)
C19 N3 C17 C18 -0.57(19)
C16 N3 C17 C18 -174.53(16)
N3 C17 C18 N4 0.5(2)
C19 N4 C18 C17 -0.3(2)
C18 N4 C19 N3 -0.10(19)
C18 N4 C19 P2 -178.57(12)
C17 N3 C19 N4 0.43(19)
C16 N3 C19 N4 174.24(15)
C17 N3 C19 P2 178.96(12)
C16 N3 C19 P2 -7.2(2)
C20 P2 C19 N4 -11.76(17)
C26 P2 C19 N4 -121.91(15)
Se2 P2 C19 N4 114.78(14)
C20 P2 C19 N3 169.94(13)
C26 P2 C19 N3 59.78(15)
Se2 P2 C19 N3 -63.53(15)
C19 P2 C20 C25 151.56(13)
C26 P2 C20 C25 -99.49(14)
Se2 P2 C20 C25 25.69(15)
C19 P2 C20 C21 -35.58(18)
C26 P2 C20 C21 73.36(17)
Se2 P2 C20 C21 -161.46(14)
C25 C20 C21 C22 0.7(3)
P2 C20 C21 C22 -171.93(15)
C20 C21 C22 C23 0.9(3)
C21 C22 C23 C24 -1.7(3)
C22 C23 C24 C25 0.8(3)
C23 C24 C25 C20 0.8(3)
C21 C20 C25 C24 -1.6(3)
P2 C20 C25 C24 171.53(14)
C19 P2 C26 C31 -130.63(14)
C20 P2 C26 C31 116.49(14)
Se2 P2 C26 C31 -8.39(15)
C19 P2 C26 C27 50.39(15)
C20 P2 C26 C27 -62.49(15)
Se2 P2 C26 C27 172.63(12)
C31 C26 C27 C28 0.4(3)
P2 C26 C27 C28 179.38(14)
C26 C27 C28 C29 -0.1(3)
C27 C28 C29 C30 -0.3(3)
C28 C29 C30 C31 0.4(3)
C27 C26 C31 C30 -0.3(3)
P2 C26 C31 C30 -179.29(13)
C29 C30 C31 C26 -0.1(3)
