#------------------------------------------------------------------------------
#$Date: 2016-03-26 13:58:28 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180242 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/28/7112820.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7112820
loop_
_publ_author_name
'Strukil, Vjekoslav'
'Fábián, László'
'Reid, David G.'
'Duer, Melinda J.'
'Jackson, Graham J.'
'Eckert-Maksić, Mirjana'
'Friščić, Tomislav'
_publ_section_title
;
 Towards an environmentally-friendly laboratory: dimensionality and
 reactivity in the mechanosynthesis of metal-organic compounds.
;
_journal_issue                   48
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              9191
_journal_page_last               9193
_journal_paper_doi               10.1039/c0cc03822a
_journal_volume                  46
_journal_year                    2010
_chemical_formula_moiety         'C4 H8 Cd Cl2 N8'
_chemical_formula_sum            'C4 H8 Cd Cl2 N8'
_chemical_formula_weight         351.48
_chemical_name_common            complex12
_chemical_name_systematic        ' ?'
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_date             2009-10-30T15:17
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2009-10-30T15:17 Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 95.185(4)
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   3.76924(14)
_cell_length_b                   8.46664(23)
_cell_length_c                   17.1444(5)
_cell_measurement_temperature    298
_cell_volume                     544.89(3)
_computing_structure_refinement  GSAS
_computing_structure_solution    DASH
_diffrn_ambient_temperature      298
_diffrn_detector                 RTMS
_diffrn_detector_type            XCelerator
_diffrn_measurement_device_type  'Philips XPert Pro'
_diffrn_radiation_monochromator  'Ni filter'
_diffrn_radiation_polarisn_ratio 0.678
_diffrn_radiation_probe          x-ray
_diffrn_source                   'sealed X-ray tube'
_diffrn_source_target            Cu
_exptl_absorpt_correction_T_max  0.94031
_exptl_absorpt_correction_T_min  0.47498
_exptl_absorpt_process_details
; GSAS Absorption/surface roughness correction: function number 3
Surface roughness abs. correction (Suortti)
Terms = 0.10000E-02 0.73955E-01
Correction is not refined.
;
_exptl_crystal_density_diffrn    2.142
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             340
_pd_block_id
2009-10-30T15:17|R1|Laszlo_Fabian|Philips_Xpert_Pro
_pd_calc_method                  'Rietveld Refinement'
_pd_char_particle_morphology     'fine powder'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        59.962
_pd_meas_2theta_range_min        4.002
_pd_meas_number_of_points        2799
_pd_meas_scan_method             step
_pd_phase_name                   complex12
_pd_prep_cool_rate               0
_pd_prep_pressure                100
_pd_prep_temperature             298
_pd_proc_2theta_range_inc        0.02
_pd_proc_2theta_range_max        59.962
_pd_proc_2theta_range_min        4.002
_pd_proc_info_data_reduction     none
_pd_proc_info_datetime           2009-10-30T15:17:08
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
; GSAS Background function number 1 with 12 terms.
Shifted Chebyshev function of 1st kind
1: 743.502 2: -748.052 3: 328.325 4: -106.142
5: 22.1998 6: 2.99211 7: -22.0011 8: 24.7328
9: -16.8724 10: 3.12562 11: -0.104129 12: 0.660493
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_ls_pref_orient_corr
; March-Dollase
AXIS 1 Ratio= 0.93805 h= 0.000 k= 1.000 l= 0.000
Prefered orientation correction range: Min= 0.90853, Max= 1.21149
;
_pd_proc_ls_profile_function
;
CW Profile function number 3 with 19 terms
Pseudovoigt profile coefficients as parameterized in
P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
J. Appl. Cryst.,27,892-900.
Peak tails are ignored where the intensity is below 0.0010 times the peak
Aniso. broadening axis 0.0 0.0 1.0
;
_pd_proc_ls_prof_R_factor        0.0332
_pd_proc_ls_prof_wR_expected     0.0335
_pd_proc_ls_prof_wR_factor       0.0432
_pd_proc_number_of_points        2799
_pd_spec_mounting                ' ?'
_pd_spec_mount_mode              reflection
_pd_spec_shape                   flat_sheet
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.31
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_constraints    1
_refine_ls_number_parameters     64
_refine_ls_number_restraints     25
_refine_ls_R_Fsqd_factor         0.04118
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_refine_ls_weighting_details     1/σ(Yobs)²
_refine_ls_weighting_scheme      sigma
_reflns_d_resolution_high        1.544
_reflns_d_resolution_low         8.537
_reflns_limit_h_max              2
_reflns_limit_h_min              0
_reflns_limit_k_max              6
_reflns_limit_k_min              0
_reflns_limit_l_max              12
_reflns_limit_l_min              -11
_reflns_number_total             310
_cod_data_source_file            c0cc03822a.txt
_cod_data_source_block           R1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/usr/data/users/saulius/automatic-downloads/retrospective/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (12
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according
to
/usr/data/users/saulius/automatic-downloads/retrospective/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (22
times).

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_cell_volume        544.888(35)
_cod_database_code               7112820
#BEGIN Tags that were not found in dictionaries:
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x+1/2,+y+1/2,-z+1/2
-1 -x,-y,-z
-2 +x+1/2,-y+1/2,+z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cd Cd1 0.5 0.5 0.5 1.0 Uiso 0.0438(14) 2
Cl Cl2 0.0072(21) 0.2867(4) 0.52152(34) 1.0 Uiso 0.0453(22) 4
N N3 0.5796(32) 0.5608(13) 0.6401(5) 1.0 Uiso 0.0514(30) 4
C C4 0.6927(18) 0.4966(12) 0.6960(4) 1.0 Uiso 0.0514(30) 4
N N5 0.7817(24) 0.4346(10) 0.7639(5) 1.0 Uiso 0.0514(30) 4
C C6 1.0063(26) 0.5100(9) 0.8157(4) 1.0 Uiso 0.0514(30) 4
N N7 1.1158(26) 0.4315(10) 0.8797(4) 1.0 Uiso 0.0514(30) 4
N N8 1.1118(31) 0.6551(9) 0.8064(5) 1.0 Uiso 0.0514(30) 4
H H9 1.264(4) 0.4745(19) 0.9146(7) 1.0 Uiso 0.062(4) 4
H H10 1.043(5) 0.3367(14) 0.8863(6) 1.0 Uiso 0.062(4) 4
H H11 1.259(5) 0.6982(15) 0.8413(8) 1.0 Uiso 0.062(4) 4
H H12 1.037(5) 0.7069(11) 0.7650(8) 1.0 Uiso 0.062(4) 4
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Cd 2.0 0.000 0.000 19.2214 0.59460 17.6444 6.90890 4.46100 24.7008 1.60290
87.4825 5.06940 International_Tables_Vol_C
Cl 4.0 0.000 0.000 11.4604 0.01040 7.19640 1.16620 6.25560 18.5194 1.64550
47.7784 -9.5574 International_Tables_Vol_C
N 16.0 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630
0.58260 -11.529 International_Tables_Vol_C
C 8.0 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500
51.6512 0.21560 International_Tables_Vol_C
H 16.0 0.000 0.000 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081
57.7997 0.00304 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540600 1.000 K\a~1~ 1
1.544400 0.500 K\a~2~ 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl2 Cd1 Cl2 91.28(11) 1_555 1_655 n
Cl2 Cd1 Cl2 88.72(11) 1_555 -1_566 n
Cl2 Cd1 Cl2 179.9657 1_555 -1_666 n
Cl2 Cd1 N3 91.84(29) 1_555 1_555 n
Cl2 Cd1 N3 88.16(29) 1_555 -1_666 n
Cl2 Cd1 Cl2 180.0 1_655 -1_566 n
Cl2 Cd1 N3 89.07(29) 1_655 1_555 n
Cl2 Cd1 N3 90.93(29) 1_655 -1_666 n
N3 Cd1 N3 180.0 1_555 -1_666 n
Cd1 Cl2 Cd1 91.28(11) 1_455 1_555 n
Cd1 N3 C4 136.2(7) 1_555 1_555 n
N3 C4 N5 171.39(24) 1_555 1_555 n
C4 N5 C6 120.18(13) 1_555 1_555 n
N5 C6 N7 116.48(21) 1_555 1_555 n
N5 C6 N8 123.5(4) 1_555 1_555 n
N7 C6 N8 120.02(34) 1_555 1_555 n
C6 N7 H9 120.00(26) 1_555 1_555 n
C6 N7 H10 120.0(5) 1_555 1_555 n
H9 N7 H10 120.0(4) 1_555 1_555 n
C6 N8 H11 120.0(4) 1_555 1_555 n
C6 N8 H12 120.00(35) 1_555 1_555 n
H11 N8 H12 120.0(4) 1_555 1_555 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cd1 Cl2 2.640(6) 1_555 n
Cd1 Cl2 2.632(6) 1_655 n
Cd1 N3 2.448(10) 1_555 n
N3 C4 1.1503(28) 1_555 n
C4 N5 1.2933(28) 1_555 n
N5 C6 1.3326(28) 1_555 n
C6 N7 1.3170(28) 1_555 n
C6 N8 1.3051(28) 1_555 n
N7 H9 0.8601(15) 1_555 n
N7 H10 0.8598(15) 1_555 n
N8 H11 0.8599(15) 1_555 n
N8 H12 0.8600(15) 1_555 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
5822.0 0.0 91.18420 .
5852.0 0.0 112.45080 .
5700.0 0.0 133.53273 .
5776.0 0.0 154.43076 .
5685.0 0.0 175.14584 .
5700.0 0.0 195.67905 .
5730.0 0.0 216.03174 .
5595.0 0.0 236.20512 .
5610.0 0.0 256.20065 .
5476.0 0.0 276.01779 .
5685.0 0.0 295.65967 .
5373.0 0.0 315.12680 .
5446.0 0.0 334.42014 .
5329.0 0.0 353.54056 .
5417.0 0.0 372.48972 .
5358.0 0.0 391.26749 .
5242.0 0.0 409.87708 .
5184.0 0.0 428.31815 .
5227.0 0.0 446.59164 .
4956.0 0.0 464.69928 .
5041.0 0.0 482.64191 .
4998.0 0.0 500.42053 .
4928.0 0.0 518.03577 .
4928.0 0.0 535.48944 .
4858.0 0.0 552.78308 .
4775.0 0.0 569.91614 .
4692.0 0.0 586.89087 .
4816.0 0.0 603.70728 .
4665.0 0.0 620.36737 .
4679.0 0.0 636.87195 .
4556.0 0.0 653.22162 .
4502.0 0.0 669.41730 .
4502.0 0.0 685.46118 .
4422.0 0.0 701.35272 .
4422.0 0.0 717.09406 .
4343.0 0.0 732.68530 .
4330.0 0.0 748.12848 .
4316.0 0.0 763.42328 .
4330.0 0.0 778.57190 .
4199.0 0.0 793.57477 .
4277.0 0.0 808.43280 .
4160.0 0.0 823.14679 .
4045.0 0.0 837.71771 .
4147.0 0.0 852.14734 .
4122.0 0.0 866.43573 .
4020.0 0.0 880.58392 .
3956.0 0.0 894.59308 .
4032.0 0.0 908.46436 .
4032.0 0.0 922.19824 .
3770.0 0.0 935.79572 .
3894.0 0.0 949.25775 .
3856.0 0.0 962.58539 .
3844.0 0.0 975.77844 .
3819.0 0.0 988.84015 .
3733.0 0.0 1001.76953 .
3770.0 0.0 1014.56781 .
3697.0 0.0 1027.23596 .
3684.0 0.0 1039.77490 .
3782.0 0.0 1052.18591 .
3624.0 0.0 1064.46887 .
3636.0 0.0 1076.62598 .
3733.0 0.0 1088.65710 .
3564.0 0.0 1100.56360 .
3576.0 0.0 1112.34534 .
3552.0 0.0 1124.00464 .
3434.0 0.0 1135.54102 .
3528.0 0.0 1146.95654 .
3552.0 0.0 1158.25073 .
3422.0 0.0 1169.42542 .
3422.0 0.0 1180.48132 .
3540.0 0.0 1191.41870 .
3481.0 0.0 1202.23877 .
3399.0 0.0 1212.94263 .
3399.0 0.0 1223.53015 .
3352.0 0.0 1234.00378 .
3352.0 0.0 1244.36194 .
3272.0 0.0 1254.60693 .
3306.0 0.0 1264.73999 .
3295.0 0.0 1274.76086 .
3295.0 0.0 1284.67102 .
3226.0 0.0 1294.47009 .
3249.0 0.0 1304.16040 .
3215.0 0.0 1313.74182 .
3181.0 0.0 1323.21521 .
3170.0 0.0 1332.58118 .
3204.0 0.0 1341.84131 .
3170.0 0.0 1350.99573 .
3069.0 0.0 1360.04431 .
3091.0 0.0 1368.98962 .
3204.0 0.0 1377.83118 .
3147.0 0.0 1386.56970 .
3025.0 0.0 1395.20642 .
3091.0 0.0 1403.74182 .
3058.0 0.0 1412.17688 .
3091.0 0.0 1420.51172 .
2948.0 0.0 1428.74805 .
3025.0 0.0 1436.88525 .
2992.0 0.0 1444.92444 .
2894.0 0.0 1452.86731 .
3036.0 0.0 1460.71387 .
2981.0 0.0 1468.46484 .
2992.0 0.0 1476.12024 .
2905.0 0.0 1483.68176 .
2884.0 0.0 1491.15002 .
2905.0 0.0 1498.52405 .
2938.0 0.0 1505.80701 .
2894.0 0.0 1512.99817 .
2862.0 0.0 1520.09827 .
2767.0 0.0 1527.10852 .
2830.0 0.0 1534.02869 .
2884.0 0.0 1540.85999 .
2798.0 0.0 1547.60352 .
2756.0 0.0 1554.25891 .
2746.0 0.0 1560.82727 .
2798.0 0.0 1567.30945 .
2673.0 0.0 1573.70593 .
2746.0 0.0 1580.01709 .
2714.0 0.0 1586.24414 .
2746.0 0.0 1592.38745 .
2725.0 0.0 1598.44727 .
2663.0 0.0 1604.42407 .
2704.0 0.0 1610.31958 .
2611.0 0.0 1616.13318 .
2683.0 0.0 1621.86633 .
2632.0 0.0 1627.51990 .
2673.0 0.0 1633.09290 .
2570.0 0.0 1638.58740 .
2632.0 0.0 1644.00354 .
2540.0 0.0 1649.34180 .
2642.0 0.0 1654.60303 .
2570.0 0.0 1659.78748 .
2570.0 0.0 1664.89563 .
2540.0 0.0 1669.92883 .
2520.0 0.0 1674.88696 .
2673.0 0.0 1679.77063 .
2510.0 0.0 1684.58057 .
2570.0 0.0 1689.31738 .
2490.0 0.0 1693.98193 .
2480.0 0.0 1698.57410 .
2480.0 0.0 1703.09436 .
2450.0 0.0 1707.54407 .
2450.0 0.0 1711.92334 .
2470.0 0.0 1716.23267 .
2560.0 0.0 1720.47290 .
2391.0 0.0 1724.64368 .
2440.0 0.0 1728.74683 .
2421.0 0.0 1732.78223 .
2421.0 0.0 1736.75049 .
2401.0 0.0 1740.65137 .
2323.0 0.0 1744.48706 .
2401.0 0.0 1748.25623 .
2352.0 0.0 1751.96045 .
2362.0 0.0 1755.60034 .
2391.0 0.0 1759.17639 .
2352.0 0.0 1762.68860 .
2401.0 0.0 1766.13696 .
2411.0 0.0 1769.52319 .
2372.0 0.0 1772.84778 .
2275.0 0.0 1776.11035 .
2285.0 0.0 1779.31165 .
2256.0 0.0 1782.45300 .
2294.0 0.0 1785.53357 .
2304.0 0.0 1788.55469 .
2266.0 0.0 1791.51672 .
2275.0 0.0 1794.41956 .
2256.0 0.0 1797.26477 .
2275.0 0.0 1800.05261 .
2209.0 0.0 1802.78223 .
2144.0 0.0 1805.45557 .
2181.0 0.0 1808.07214 .
2237.0 0.0 1810.63281 .
2218.0 0.0 1813.13879 .
2172.0 0.0 1815.58887 .
2190.0 0.0 1817.98474 .
2172.0 0.0 1820.32715 .
2134.0 0.0 1822.61475 .
2098.0 0.0 1824.84985 .
2134.0 0.0 1827.03223 .
2134.0 0.0 1829.16223 .
2172.0 0.0 1831.23975 .
2200.0 0.0 1833.26648 .
2088.0 0.0 1835.24182 .
2070.0 0.0 1837.16711 .
2134.0 0.0 1839.04187 .
2070.0 0.0 1840.86694 .
2134.0 0.0 1842.64270 .
2134.0 0.0 1844.36951 .
2070.0 0.0 1846.04773 .
2172.0 0.0 1847.67798 .
2098.0 0.0 1849.26025 .
2043.0 0.0 1850.79565 .
2025.0 0.0 1852.28406 .
2052.0 0.0 1853.72595 .
1989.0 0.0 1855.12183 .
2016.0 0.0 1856.47205 .
1989.0 0.0 1857.77698 .
2034.0 0.0 1859.03699 .
2007.0 0.0 1860.25269 .
1998.0 0.0 1861.42395 .
2025.0 0.0 1862.55164 .
2016.0 0.0 1863.63635 .
1971.0 0.0 1864.67773 .
1918.0 0.0 1865.67651 .
1998.0 0.0 1866.63281 .
2061.0 0.0 1867.54797 .
1962.0 0.0 1868.42102 .
1998.0 0.0 1869.25378 .
2007.0 0.0 1870.04504 .
1927.0 0.0 1870.79639 .
1945.0 0.0 1871.50732 .
1910.0 0.0 1872.17896 .
1980.0 0.0 1872.81140 .
1918.0 0.0 1873.40466 .
1918.0 0.0 1873.95923 .
1936.0 0.0 1874.47620 .
1832.0 0.0 1874.95447 .
1849.0 0.0 1875.39563 .
1927.0 0.0 1875.79968 .
1962.0 0.0 1876.16663 .
1918.0 0.0 1876.49719 .
1910.0 0.0 1876.79138 .
1971.0 0.0 1877.04993 .
1971.0 0.0 1877.27283 .
1892.0 0.0 1877.46082 .
1945.0 0.0 1877.61389 .
1858.0 0.000538 1877.73206 1877.73230
1918.0 0.000521 1877.81628 1877.81677
1918.0 0.000521 1877.86682 1877.86707
1927.0 0.000519 1877.88367 1877.88379
1884.0 0.000531 1877.86731 1877.86707
1901.0 0.000526 1877.81775 1877.81799
1866.0 0.000536 1877.73596 1877.73596
1815.0 0.000551 1877.62158 1877.62146
1823.0 0.000549 1877.47534 1877.47534
1884.0 0.000531 1877.29736 1877.29712
1849.0 0.000541 1877.08801 1877.08789
1936.0 0.000517 1876.84753 1876.84729
1866.0 0.000536 1876.57666 1876.57629
1936.0 0.000517 1876.27478 1876.27441
1892.0 0.000529 1875.94299 1875.94275
1927.0 0.000519 1875.58118 1875.58093
1884.0 0.000531 1875.19006 1875.18958
1901.0 0.000526 1874.76941 1874.76904
1901.0 0.000526 1874.32007 1874.31946
1901.0 0.000526 1873.84180 1873.84094
1866.0 0.000536 1873.33484 1873.33435
1884.0 0.000531 1872.80005 1872.79932
1849.0 0.000541 1872.23718 1872.23669
1866.0 0.000536 1871.64697 1871.64624
1892.0 0.000529 1871.02942 1871.02856
1884.0 0.000531 1870.38464 1870.38391
1884.0 0.000531 1869.71326 1869.71252
1884.0 0.000531 1869.01538 1869.01453
1866.0 0.000536 1868.29150 1868.29065
1892.0 0.000529 1867.54126 1867.54053
1875.0 0.000533 1866.76538 1866.76453
1858.0 0.000538 1865.96460 1865.96350
1901.0 0.000526 1865.13818 1865.13708
1849.0 0.000541 1864.28711 1864.28613
1866.0 0.000536 1863.41138 1863.41052
1901.0 0.000526 1862.51123 1862.51025
1798.0 0.000556 1861.58667 1861.58582
1832.0 0.000546 1860.63904 1863.39160
1892.0 0.000529 1859.66724 1863.88208
1840.0 0.000543 1858.67224 1863.04688
1832.0 0.000546 1857.65430 1862.19751
1866.0 0.000536 1856.61328 1861.33569
1884.0 0.000531 1855.54980 1860.46216
1954.0 0.000512 1854.46399 1859.57776
1832.0 0.000546 1853.35596 1858.68396
1892.0 0.000529 1852.22607 1857.78259
1910.0 0.000524 1851.07483 1856.87390
1875.0 0.000533 1849.90137 1855.96045
1892.0 0.000529 1848.70752 1855.04407
1849.0 0.000541 1847.49280 1854.12598
1901.0 0.000526 1846.25720 1853.20923
1815.0 0.000551 1845.00085 1852.29480
1884.0 0.000531 1843.72473 1851.38708
1832.0 0.000546 1842.42834 1850.48767
1798.0 0.000556 1841.11255 1849.60071
1866.0 0.000536 1839.77673 1848.72949
1849.0 0.000541 1838.42163 1847.87817
1858.0 0.000538 1837.04736 1847.05237
1849.0 0.000541 1835.65466 1846.25696
1798.0 0.000556 1834.24329 1845.49878
1849.0 0.000541 1832.81335 1844.78479
1840.0 0.000543 1831.36487 1844.12439
1815.0 0.000551 1829.89880 1843.52698
1849.0 0.000541 1828.41467 1843.00537
1866.0 0.000536 1826.91321 1842.57312
1823.0 0.000549 1825.39429 1842.24792
1823.0 0.000549 1823.85803 1842.04944
1849.0 0.000541 1822.30481 1842.00378
1823.0 0.000549 1820.73511 1842.14124
1832.0 0.000546 1819.14893 1842.50049
1875.0 0.000533 1817.54602 1843.12927
1858.0 0.000538 1815.92725 1844.08948
1849.0 0.000541 1814.29236 1845.46045
1884.0 0.000531 1812.64185 1847.34802
1823.0 0.000549 1810.97559 1849.89368
1875.0 0.000533 1809.29443 1853.29407
1840.0 0.000543 1807.59753 1857.83167
1901.0 0.000526 1805.88599 1863.92529
1910.0 0.000524 1804.15979 1872.24451
1832.0 0.000546 1802.41882 1883.98035
1918.0 0.000521 1800.66333 1901.54163
2034.0 0.000492 1798.89404 1929.74988
1954.0 0.000512 1797.11035 1976.10645
2007.0 0.000498 1795.31299 2041.73438
2043.0 0.000489 1793.50183 2116.92285
2116.0 0.000473 1791.67773 2226.99951
2218.0 0.000451 1789.83948 2367.37573
2237.0 0.000447 1787.98865 2506.19434
2401.0 0.000416 1786.12488 2703.78247
2694.0 0.000371 1784.24866 2925.08398
3003.0 0.0003330 1782.35913 3203.40845
3387.0 0.0002952 1780.45776 3556.33472
3944.0 0.0002535 1778.54382 3976.38135
4382.0 0.0002282 1776.61804 4440.50488
4692.0 0.0002131 1774.67993 4757.61279
4529.0 0.0002208 1772.73059 4518.47266
3832.0 0.0002610 1770.76965 3763.36548
2948.0 0.0003392 1768.79712 2982.36401
2440.0 0.000410 1766.81311 2477.48926
2125.0 0.000471 1764.81860 2213.61084
1892.0 0.000529 1762.81323 2074.52612
1945.0 0.000514 1760.79663 1993.32422
1849.0 0.000541 1758.76953 1940.73804
1866.0 0.000536 1756.73230 1904.18970
1927.0 0.000519 1754.68469 1877.52942
1849.0 0.000541 1752.62708 1857.33948
1858.0 0.000538 1750.55945 1841.56995
1875.0 0.000533 1748.48193 1828.92969
1806.0 0.000554 1746.39453 1818.57166
1840.0 0.000543 1744.29785 1809.92188
1815.0 0.000551 1742.19214 1802.58069
1866.0 0.000536 1740.07703 1796.26270
1815.0 0.000551 1737.95276 1790.76074
1772.0 0.000564 1735.81995 1785.92188
1789.0 0.000559 1733.67786 1781.63135
1806.0 0.000554 1731.52747 1777.80225
1731.0 0.000578 1729.36865 1774.36938
1731.0 0.000578 1727.20142 1771.28247
1764.0 0.000567 1725.02612 1768.50476
1832.0 0.000546 1722.84229 1766.00732
1772.0 0.000564 1720.65149 1763.77173
1756.0 0.000569 1718.45227 1761.78333
1772.0 0.000564 1716.24536 1760.03601
1764.0 0.000567 1714.03125 1758.52637
1772.0 0.000564 1711.80994 1757.25842
1689.0 0.000592 1709.58105 1756.23914
1823.0 0.000549 1707.34534 1755.48193
1608.0 0.000622 1705.10278 1755.00391
1673.0 0.000598 1702.85303 1754.82935
1731.0 0.000578 1700.59668 1754.98877
1772.0 0.000564 1698.33386 1755.52124
1756.0 0.000569 1696.06458 1756.47375
1781.0 0.000561 1693.78918 1757.90686
1781.0 0.000561 1691.50745 1759.89380
1764.0 0.000567 1689.21960 1762.52722
1781.0 0.000561 1686.92603 1765.92212
1789.0 0.000559 1684.62634 1770.22583
1815.0 0.000551 1682.32092 1775.62427
1798.0 0.000556 1680.01050 1782.36060
1840.0 0.000543 1677.69409 1790.75330
1858.0 0.000538 1675.37256 1801.22974
1901.0 0.000526 1673.04565 1814.37695
1954.0 0.000512 1670.71387 1831.02173
1989.0 0.000503 1668.37720 1852.37268
1989.0 0.000503 1666.03516 1880.27710
2079.0 0.000481 1663.68872 1917.78723
2025.0 0.000494 1661.33765 1970.78857
2190.0 0.000457 1658.98206 2052.57495
2314.0 0.000432 1656.62183 2190.67480
2490.0 0.000402 1654.25769 2420.77832
2642.0 0.000379 1651.88904 2724.07983
3047.0 0.0003282 1649.51660 3135.45068
3318.0 0.0003014 1647.14014 3721.44189
3982.0 0.0002511 1644.75964 4328.96729
4692.0 0.0002131 1642.37512 5211.12109
5837.0 0.0001713 1639.98755 6169.47412
7379.0 0.0001355 1637.59607 7521.99951
9254.0 0.0001081 1635.20129 9128.66602
11109.0 0.0000900 1632.80286 11215.82227
12611.0 0.0000793 1630.40125 12913.83008
12232.0 0.0000818 1627.99670 12680.73242
10140.0 0.0000986 1625.58887 9924.57031
6906.0 0.0001448 1623.17834 6683.50000
4516.0 0.0002214 1620.76501 4378.40674
3114.0 0.0003211 1618.34851 3216.03003
2550.0 0.000392 1615.92957 2660.06689
2228.0 0.000449 1613.50806 2361.64526
2134.0 0.000469 1611.08398 2177.43213
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1901.0 0.000526 1606.22876 1964.95508
1858.0 0.000538 1603.79810 1899.57971
1832.0 0.000546 1601.36523 1849.59192
1840.0 0.000543 1598.93005 1810.32227
1764.0 0.000567 1596.49329 1778.75415
1772.0 0.000564 1594.05432 1752.86670
1714.0 0.000583 1591.61401 1731.26392
1781.0 0.000561 1589.17200 1712.95544
1714.0 0.000583 1586.72815 1697.22192
1722.0 0.000581 1584.28296 1683.53186
1689.0 0.000592 1581.83630 1671.48364
1739.0 0.000575 1579.38843 1660.77136
1665.0 0.000601 1576.93933 1651.15613
1706.0 0.000586 1574.48901 1642.45081
1681.0 0.000595 1572.03748 1634.50732
1706.0 0.000586 1569.58533 1627.20544
1681.0 0.000595 1567.13184 1620.44836
1648.0 0.000607 1564.67761 1614.15771
1665.0 0.000601 1562.22266 1608.26709
1624.0 0.000616 1559.76746 1602.72314
1673.0 0.000598 1557.31079 1597.48010
1632.0 0.000613 1554.85449 1592.50037
1616.0 0.000619 1552.39697 1587.75110
1624.0 0.000616 1549.93958 1583.20557
1592.0 0.000628 1547.48169 1578.83997
1568.0 0.000638 1545.02368 1574.63367
1560.0 0.000641 1542.56555 1570.57007
1560.0 0.000641 1540.10706 1566.63367
1576.0 0.000635 1537.64893 1562.81177
1600.0 0.000625 1535.19080 1559.09265
1584.0 0.000631 1532.73267 1555.46631
1537.0 0.000651 1530.27478 1551.92395
1568.0 0.000638 1527.81702 1548.45801
1576.0 0.000635 1525.35974 1545.06116
1576.0 0.000635 1522.90295 1541.72754
1608.0 0.000622 1520.44678 1538.45178
1608.0 0.000622 1517.99097 1535.22900
1544.0 0.000648 1515.53540 1532.05481
1608.0 0.000622 1513.08118 1528.92566
1576.0 0.000635 1510.62683 1525.83765
1537.0 0.000651 1508.17407 1522.78796
1537.0 0.000651 1505.72168 1519.77344
1568.0 0.000638 1503.27087 1516.79175
1552.0 0.000644 1500.82031 1513.84058
1529.0 0.000654 1498.37109 1510.91785
1576.0 0.000635 1495.92285 1508.02148
1513.0 0.000661 1493.47620 1505.15027
1513.0 0.000661 1491.03027 1494.90601
1560.0 0.000641 1488.58582 1488.58472
1529.0 0.000654 1486.14270 1486.14172
1552.0 0.000644 1483.70105 1483.70032
1505.0 0.000664 1481.26062 1481.25977
1584.0 0.000631 1478.82190 1478.82104
1498.0 0.000668 1476.38489 1476.38403
1544.0 0.000648 1473.94922 1473.94836
1482.0 0.000675 1471.51550 1471.51465
1521.0 0.000657 1469.08301 1469.08252
1513.0 0.000661 1466.65295 1466.65234
1490.0 0.000671 1464.22437 1464.22363
1513.0 0.000661 1461.79785 1461.79712
1490.0 0.000671 1459.37280 1459.37244
1467.0 0.000682 1456.95056 1456.94971
1505.0 0.000664 1454.52942 1454.52893
1459.0 0.000685 1452.11096 1452.11047
1421.0 0.000704 1449.69458 1449.69385
1467.0 0.000682 1447.28027 1447.27991
1490.0 0.000671 1444.86804 1444.86768
1482.0 0.000675 1442.45874 1442.45813
1429.0 0.000700 1440.05103 1440.05054
1490.0 0.000671 1437.64587 1437.64563
1421.0 0.000704 1435.24341 1435.24304
1414.0 0.000707 1432.84326 1432.84290
1475.0 0.000678 1430.44580 1430.44531
1429.0 0.000700 1428.05066 1428.05029
1391.0 0.000719 1425.65820 1425.70032
1490.0 0.000671 1423.26843 1423.31177
1399.0 0.000715 1420.88123 1420.94751
1429.0 0.000700 1418.49670 1418.56506
1452.0 0.000689 1416.11499 1416.18579
1391.0 0.000719 1413.73621 1413.80884
1452.0 0.000689 1411.36047 1411.43542
1399.0 0.000715 1408.98730 1409.06494
1384.0 0.000723 1406.61743 1406.69739
1369.0 0.000730 1404.25012 1404.33289
1444.0 0.000693 1401.88586 1401.97156
1429.0 0.000700 1399.52490 1399.61340
1399.0 0.000715 1397.16699 1397.25891
1362.0 0.000734 1394.81226 1394.90710
1421.0 0.000704 1392.46045 1392.55933
1354.0 0.000739 1390.11182 1390.21436
1475.0 0.000678 1387.76685 1387.87292
1384.0 0.000723 1385.42468 1385.53528
1362.0 0.000734 1383.08618 1383.20105
1362.0 0.000734 1380.75073 1380.87048
1406.0 0.000711 1378.41895 1378.54321
1406.0 0.000711 1376.09033 1376.22034
1332.0 0.000751 1373.76550 1373.90088
1347.0 0.000742 1371.44373 1371.58496
1332.0 0.000751 1369.12573 1369.27344
1325.0 0.000755 1366.81116 1366.96570
1391.0 0.000719 1364.50024 1364.66187
1296.0 0.000772 1362.19287 1362.36255
1421.0 0.000704 1359.88904 1360.06726
1362.0 0.000734 1357.58887 1357.77625
1391.0 0.000719 1355.29272 1355.48962
1384.0 0.000723 1353.00024 1353.20776
1303.0 0.000767 1350.71143 1350.92993
1362.0 0.000734 1348.42639 1348.65723
1303.0 0.000767 1346.14478 1346.38953
1325.0 0.000755 1343.86743 1344.12671
1303.0 0.000767 1341.59399 1341.86926
1267.0 0.000789 1339.32446 1339.61719
1325.0 0.000755 1337.05847 1337.37073
1282.0 0.000780 1334.79675 1335.13013
1332.0 0.000751 1332.53906 1332.89624
1318.0 0.000759 1330.28516 1330.66858
1310.0 0.000763 1328.03552 1328.44800
1325.0 0.000755 1325.78979 1326.23474
1310.0 0.000763 1323.54810 1324.02991
1303.0 0.000767 1321.31079 1321.83386
1310.0 0.000763 1319.07703 1319.64771
1325.0 0.000755 1316.84802 1317.47266
1274.0 0.000785 1314.62280 1315.30933
1340.0 0.000746 1312.40210 1313.16028
1267.0 0.000789 1310.18542 1311.02759
1340.0 0.000746 1307.97278 1308.91431
1282.0 0.000780 1305.76477 1306.82446
1260.0 0.000794 1303.56067 1304.76306
1282.0 0.000780 1301.36121 1302.73804
1282.0 0.000780 1299.16565 1300.75928
1340.0 0.000746 1296.97473 1298.84387
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1274.0 0.000785 1292.60632 1295.32092
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1225.0 0.000816 1288.25513 1292.80469
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1310.0 0.000763 1283.92188 1293.42419
1267.0 0.000789 1281.76172 1295.50183
1303.0 0.000767 1279.60608 1299.65369
1325.0 0.000755 1277.45508 1305.49182
1296.0 0.000772 1275.30859 1314.01904
1362.0 0.000734 1273.16675 1325.89746
1376.0 0.000727 1271.02917 1341.23657
1406.0 0.000711 1268.89661 1356.47461
1421.0 0.000704 1266.76831 1360.61597
1340.0 0.000746 1264.64453 1344.35706
1376.0 0.000727 1262.52539 1319.53857
1340.0 0.000746 1260.41138 1294.92859
1318.0 0.000759 1258.30151 1277.62585
1296.0 0.000772 1256.19641 1267.66113
1274.0 0.000785 1254.09595 1261.70886
1246.0 0.000803 1252.00037 1257.53516
1267.0 0.000789 1249.90930 1254.15442
1260.0 0.000794 1247.82312 1251.19080
1282.0 0.000780 1245.74133 1248.48108
1260.0 0.000794 1243.66455 1245.93823
1225.0 0.000816 1241.59241 1243.51013
1282.0 0.000780 1239.52551 1241.16553
1225.0 0.000816 1237.46265 1238.88159
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1340.0 0.000746 1233.35205 1234.44519
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1246.0 0.000803 1229.26038 1230.12915
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1190.0 0.000840 1199.19458 1199.46008
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1190.0 0.000840 1191.36401 1191.57642
1197.0 0.000835 1189.41882 1189.62000
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1024.0 0.000977 1080.22717 1080.22900
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1076.0 0.000929 1075.33533 1075.33716
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279.0 . . .
