#------------------------------------------------------------------------------
#$Date: 2024-02-04 13:07:58 +0200 (Sun, 04 Feb 2024) $
#$Revision: 289339 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/13/24/7132465.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7132465
loop_
_publ_author_name
'Haridas, Shyamkumar V.'
'von Delius, Max'
_publ_section_title
;
 Synthesis and supramolecular properties of
 all-cis-2,4,6-trifluorocyclohexane-1,3,5-triol.
;
_journal_issue                   5
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              606
_journal_page_last               609
_journal_paper_doi               10.1039/d3cc05510h
_journal_volume                  60
_journal_year                    2024
_chemical_formula_moiety         'C10 H15 F3 O4'
_chemical_formula_sum            'C10 H15 F3 O4'
_chemical_formula_weight         256.22
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_date             2023-11-06
_audit_creation_method
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_audit_update_record
;
2023-11-06 deposited with the CCDC.	2023-12-08 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 98.9640(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.47780(10)
_cell_length_b                   8.90490(10)
_cell_length_c                   19.2107(2)
_cell_measurement_reflns_used    10831
_cell_measurement_temperature    150.00(14)
_cell_measurement_theta_max      72.8400
_cell_measurement_theta_min      4.6340
_cell_volume                     1094.62(2)
_computing_cell_refinement       'CrysAlisPro 1.171.41.123a (Rigaku OD, 2022)'
_computing_data_collection       'CrysAlisPro 1.171.41.123a (Rigaku OD, 2022)'
_computing_data_reduction        'CrysAlisPro 1.171.41.123a (Rigaku OD, 2022)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      150.00(14)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 10.3385
_diffrn_detector_type            Atlas
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -84.00  37.00   1.00    1.00    --  -43.06  19.00   0.00  121
  2  ω   -117.00 -19.00   1.00    1.00    --  -43.06 -38.00-180.00   98
  3  ω     27.00  99.00   1.00    1.00    --   43.06-125.00 150.00   72
  4  ω     27.00  99.00   1.00    1.00    --   43.06-125.00 120.00   72
  5  ω     27.00  99.00   1.00    1.00    --   43.06-125.00  30.00   72
  6  ω     32.00 131.00   1.00    1.00    --  104.94 -45.00 -90.00   99
  7  ω     33.00 134.00   1.00    1.00    --  104.94 -61.00 150.00  101
  8  ω     23.00 106.00   1.00    1.00    --  104.94 -95.00  90.00   83
  9  ω     23.00 106.00   1.00    1.00    --  104.94 -95.00 150.00   83
 10  ω    103.00 178.00   1.00    1.00    --  104.94  77.00-120.00   75
 11  ω    103.00 178.00   1.00    1.00    --  104.94  77.00-150.00   75
 12  ω     29.00 133.00   1.00    1.00    --  104.94 -30.00-120.00  104
 13  ω     32.00 112.00   1.00    1.00    --  104.94-125.00 -90.00   80
 14  ω     23.00 106.00   1.00    1.00    --  104.94 -95.00  30.00   83
 15  ω     23.00 158.00   1.00    1.00    --  104.94 -15.00  60.00  135
 16  ω     23.00 106.00   1.00    1.00    --  104.94 -95.00 -60.00   83
 17  ω   -115.00 -15.00   1.00    1.00    --  -43.06 -57.00  60.00  100
 18  ω   -115.00 -15.00   1.00    1.00    --  -43.06 -57.00   0.00  100
 19  ω   -115.00 -15.00   1.00    1.00    --  -43.06 -57.00 -60.00  100
 20  ω   -115.00 -15.00   1.00    1.00    --  -43.06 -57.00-120.00  100
 21  ω   -115.00 -15.00   1.00    1.00    --  -43.06 -57.00 120.00  100
 22  ω     76.00 177.00   1.00    1.00    --  104.94  61.00-150.00  101
 23  ω     52.00 178.00   1.00    1.00    --  104.94  15.00 150.00  126
 24  ω     76.00 165.00   1.00    1.00    --  104.94  61.00  30.00   89
 25  ω     76.00 177.00   1.00    1.00    --  104.94  61.00 -30.00  101
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at home/near, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0045832000
_diffrn_orient_matrix_UB_12      0.0083150000
_diffrn_orient_matrix_UB_13      -0.0803560000
_diffrn_orient_matrix_UB_21      -0.1133920000
_diffrn_orient_matrix_UB_22      -0.1524151000
_diffrn_orient_matrix_UB_23      -0.0086415000
_diffrn_orient_matrix_UB_31      -0.2122964000
_diffrn_orient_matrix_UB_32      0.0813510000
_diffrn_orient_matrix_UB_33      -0.0080095000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0550
_diffrn_reflns_av_unetI/netI     0.0222
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            15359
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         73.001
_diffrn_reflns_theta_min         4.661
_diffrn_source                   'micro-focus sealed X-ray tube'
_diffrn_source_type              'SuperNova (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    1.322
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.497
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.41.123a (Rigaku Oxford Diffraction, 2022)
Numerical absorption correction based on gaussian integration over
a multifaceted crystal model
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.555
_exptl_crystal_description       block
_exptl_crystal_F_000             536
_exptl_crystal_preparation       'Solvent layering/Methanol/n-hexane'
_exptl_crystal_recrystallization_method 'Solvent layering/Methanol/n-hexane'
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.344
_refine_diff_density_min         -0.216
_refine_diff_density_rms         0.048
_refine_ls_extinction_coef       0.0082(7)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.050
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     158
_refine_ls_number_reflns         2170
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.050
_refine_ls_R_factor_all          0.0339
_refine_ls_R_factor_gt           0.0324
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0481P)²+0.3943P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0883
_refine_ls_wR_factor_ref         0.0897
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2059
_reflns_number_total             2170
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d3cc05510h2.cif
_cod_data_source_block           svh22076
_cod_depositor_comments
'Adding full bibliography for 7132462--7132465.cif.'
_cod_database_code               7132465
_shelx_shelxl_version_number     2018/3
_publ_section_exptl
;
Any special experimental details
;
_chemical_oxdiff_formula         'C10 H15 F3 O4'
_chemical_oxdiff_usercomment     SVH-223
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.847
_shelx_estimated_absorpt_t_min   0.633
_reflns_odcompleteness_completeness 99.86
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_olex2_refinement_description
;
1.a Ternary CH refined with riding coordinates:
 C008(H008), C009(H009), C00B(H00B), C00C(H00C), C00D(H00D), C00E(H00E)
1.b Secondary CH2 refined with riding coordinates:
 C00F(H00A,H00F), C00G(H00G,H00H)
1.c Idealised Me refined as rotating group:
 C00H(H00I,H00J,H00K)
1.d Idealised tetrahedral OH refined as rotating group:
 O8(H8), O005(H005)
;
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.696
_oxdiff_exptl_absorpt_empirical_full_min 0.679
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
F001 F 0.33955(11) 0.21824(8) 0.75734(4) 0.0230(2) Uani 1 1 d . . . . .
F002 F 0.10272(11) 0.09815(7) 0.63555(4) 0.0236(2) Uani 1 1 d . . . . .
F003 F 0.50587(11) 0.22179(8) 0.63094(4) 0.0247(2) Uani 1 1 d . . . . .
O8 O -0.09206(12) 0.24697(9) 0.73471(4) 0.0198(2) Uani 1 1 d . . . . .
H8 H -0.205755 0.292175 0.734963 0.030 Uiso 1 1 calc R U . . .
O005 O 0.59246(13) 0.45294(9) 0.72570(5) 0.0221(2) Uani 1 1 d . . . . .
H005 H 0.604075 0.537796 0.745016 0.033 Uiso 1 1 calc R U . . .
O006 O 0.18642(14) 0.24387(9) 0.51633(4) 0.0213(2) Uani 1 1 d . . . . .
O007 O 0.22460(15) 0.46037(10) 0.45924(5) 0.0274(2) Uani 1 1 d . . . . .
C008 C 0.38634(18) 0.43546(13) 0.68844(6) 0.0175(3) Uani 1 1 d . . . . .
H008 H 0.327077 0.538023 0.677589 0.021 Uiso 1 1 calc R U . . .
C009 C 0.24714(18) 0.35528(12) 0.73341(6) 0.0178(3) Uani 1 1 d . . . . .
H009 H 0.233143 0.419542 0.775112 0.021 Uiso 1 1 calc R U . . .
C00A C 0.21242(18) 0.32494(14) 0.45868(6) 0.0205(3) Uani 1 1 d . . . . .
C00B C 0.17818(18) 0.32841(13) 0.57984(6) 0.0178(3) Uani 1 1 d . . . . .
H00B H 0.113008 0.427934 0.565920 0.021 Uiso 1 1 calc R U . . .
C00C C 0.03093(17) 0.32715(12) 0.69202(6) 0.0171(3) Uani 1 1 d . . . . .
H00C H -0.036811 0.427033 0.680930 0.021 Uiso 1 1 calc R U . . .
C00D C 0.39717(18) 0.35700(13) 0.61878(6) 0.0186(3) Uani 1 1 d . . . . .
H00D H 0.473148 0.423204 0.589196 0.022 Uiso 1 1 calc R U . . .
C00E C 0.03543(18) 0.24590(13) 0.62243(6) 0.0181(3) Uani 1 1 d . . . . .
H00E H -0.109142 0.244420 0.595075 0.022 Uiso 1 1 calc R U . . .
C00F C 0.2240(2) 0.22591(16) 0.39640(6) 0.0282(3) Uani 1 1 d . . . . .
H00A H 0.245680 0.289148 0.355777 0.034 Uiso 1 1 calc R U . . .
H00F H 0.089116 0.172820 0.383711 0.034 Uiso 1 1 calc R U . . .
C00G C 0.3996(2) 0.11034(15) 0.41007(7) 0.0314(3) Uani 1 1 d . . . . .
H00G H 0.371436 0.041834 0.448081 0.038 Uiso 1 1 calc R U . . .
H00H H 0.400073 0.049522 0.366957 0.038 Uiso 1 1 calc R U . . .
C00H C 0.6133(2) 0.18046(19) 0.43092(8) 0.0393(4) Uani 1 1 d . . . . .
H00I H 0.646275 0.243309 0.392240 0.059 Uiso 1 1 calc R U . . .
H00J H 0.718466 0.101060 0.440906 0.059 Uiso 1 1 calc R U . . .
H00K H 0.613353 0.242396 0.473088 0.059 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
0 0 12 0.0543
0 0 -12 0.0723
4 -3 -6 0.1899
4 -3 0 0.1937
-4 0 3 0.1838
4 1 -3 0.1794
0 -6 4 0.1048
-3 4 -1 0.1437
3 4 -4 0.1581
0 4 9 0.0669
-4 0 -4 0.1555
3 2 8 0.1268
0 -4 -9 0.0852
0 4 -9 0.0837
1 -4 8 0.1218
-3 3 -1 0.1512
0 6 0 0.0836
2 5 -1 0.1340
0 -6 0 0.0990
3 4 4 0.1197
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C00C O8 H8 109.5 . . ?
C008 O005 H005 109.5 . . ?
C00A O006 C00B 116.07(9) . . ?
O005 C008 H008 107.8 . . ?
O005 C008 C009 111.03(9) . . ?
O005 C008 C00D 108.95(9) . . ?
C009 C008 H008 107.8 . . ?
C009 C008 C00D 113.39(9) . . ?
C00D C008 H008 107.8 . . ?
F001 C009 C008 109.49(9) . . ?
F001 C009 H009 108.8 . . ?
F001 C009 C00C 109.81(9) . . ?
C008 C009 H009 108.8 . . ?
C00C C009 C008 111.10(9) . . ?
C00C C009 H009 108.8 . . ?
O006 C00A C00F 111.57(11) . . ?
O007 C00A O006 122.74(11) . . ?
O007 C00A C00F 125.69(11) . . ?
O006 C00B H00B 107.8 . . ?
O006 C00B C00D 110.46(9) . . ?
O006 C00B C00E 108.04(9) . . ?
C00D C00B H00B 107.8 . . ?
C00E C00B H00B 107.8 . . ?
C00E C00B C00D 114.63(9) . . ?
O8 C00C C009 109.55(9) . . ?
O8 C00C H00C 107.6 . . ?
O8 C00C C00E 110.89(9) . . ?
C009 C00C H00C 107.6 . . ?
C009 C00C C00E 113.27(9) . . ?
C00E C00C H00C 107.6 . . ?
F003 C00D C008 109.89(9) . . ?
F003 C00D C00B 110.24(9) . . ?
F003 C00D H00D 108.9 . . ?
C008 C00D H00D 108.9 . . ?
C00B C00D C008 110.05(9) . . ?
C00B C00D H00D 108.9 . . ?
F002 C00E C00B 110.76(9) . . ?
F002 C00E C00C 109.68(9) . . ?
F002 C00E H00E 108.8 . . ?
C00B C00E C00C 109.86(9) . . ?
C00B C00E H00E 108.8 . . ?
C00C C00E H00E 108.8 . . ?
C00A C00F H00A 109.0 . . ?
C00A C00F H00F 109.0 . . ?
C00A C00F C00G 112.86(10) . . ?
H00A C00F H00F 107.8 . . ?
C00G C00F H00A 109.0 . . ?
C00G C00F H00F 109.0 . . ?
C00F C00G H00G 108.9 . . ?
C00F C00G H00H 108.9 . . ?
H00G C00G H00H 107.8 . . ?
C00H C00G C00F 113.17(11) . . ?
C00H C00G H00G 108.9 . . ?
C00H C00G H00H 108.9 . . ?
C00G C00H H00I 109.5 . . ?
C00G C00H H00J 109.5 . . ?
C00G C00H H00K 109.5 . . ?
H00I C00H H00J 109.5 . . ?
H00I C00H H00K 109.5 . . ?
H00J C00H H00K 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
F001 C009 1.4047(13) . ?
F002 C00E 1.3966(13) . ?
F003 C00D 1.3960(13) . ?
O8 H8 0.8400 . ?
O8 C00C 1.4215(13) . ?
O005 H005 0.8400 . ?
O005 C008 1.4217(14) . ?
O006 C00A 1.3544(14) . ?
O006 C00B 1.4417(13) . ?
O007 C00A 1.2086(16) . ?
C008 H008 1.0000 . ?
C008 C009 1.5205(15) . ?
C008 C00D 1.5209(15) . ?
C009 H009 1.0000 . ?
C009 C00C 1.5197(15) . ?
C00A C00F 1.4975(17) . ?
C00B H00B 1.0000 . ?
C00B C00D 1.5186(16) . ?
C00B C00E 1.5165(16) . ?
C00C H00C 1.0000 . ?
C00C C00E 1.5245(16) . ?
C00D H00D 1.0000 . ?
C00E H00E 1.0000 . ?
C00F H00A 0.9900 . ?
C00F H00F 0.9900 . ?
C00F C00G 1.5258(19) . ?
C00G H00G 0.9900 . ?
C00G H00H 0.9900 . ?
C00G C00H 1.515(2) . ?
C00H H00I 0.9800 . ?
C00H H00J 0.9800 . ?
C00H H00K 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
F001 C009 C00C O8 56.45(11) . . . . ?
F001 C009 C00C C00E -67.93(11) . . . . ?
O8 C00C C00E F002 -54.54(12) . . . . ?
O8 C00C C00E C00B -176.52(8) . . . . ?
O005 C008 C009 F001 -54.72(11) . . . . ?
O005 C008 C009 C00C -176.18(9) . . . . ?
O005 C008 C00D F003 55.02(12) . . . . ?
O005 C008 C00D C00B 176.59(9) . . . . ?
O006 C00A C00F C00G -57.64(14) . . . . ?
O006 C00B C00D F003 -54.23(12) . . . . ?
O006 C00B C00D C008 -175.60(9) . . . . ?
O006 C00B C00E F002 55.74(11) . . . . ?
O006 C00B C00E C00C 177.07(8) . . . . ?
O007 C00A C00F C00G 122.22(14) . . . . ?
C008 C009 C00C O8 177.72(9) . . . . ?
C008 C009 C00C C00E 53.34(12) . . . . ?
C009 C008 C00D F003 -69.18(12) . . . . ?
C009 C008 C00D C00B 52.40(13) . . . . ?
C009 C00C C00E F002 69.11(12) . . . . ?
C009 C00C C00E C00B -52.87(12) . . . . ?
C00A O006 C00B C00D -85.52(11) . . . . ?
C00A O006 C00B C00E 148.37(9) . . . . ?
C00A C00F C00G C00H -57.97(15) . . . . ?
C00B O006 C00A O007 -1.25(16) . . . . ?
C00B O006 C00A C00F 178.61(10) . . . . ?
C00D C008 C009 F001 68.34(12) . . . . ?
C00D C008 C009 C00C -53.12(13) . . . . ?
C00D C00B C00E F002 -67.88(12) . . . . ?
C00D C00B C00E C00C 53.45(13) . . . . ?
C00E C00B C00D F003 68.09(12) . . . . ?
C00E C00B C00D C008 -53.28(13) . . . . ?
loop_
_exptl_oxdiff_crystal_face_indexfrac_h
_exptl_oxdiff_crystal_face_indexfrac_k
_exptl_oxdiff_crystal_face_indexfrac_l
_exptl_oxdiff_crystal_face_x
_exptl_oxdiff_crystal_face_y
_exptl_oxdiff_crystal_face_z
-0.1177 -0.0899 12.3610 -0.9935 -0.0798 -0.0813
0.2016 0.0289 -12.3918 0.9951 0.0798 0.0588
3.5363 -2.5102 -5.6062 0.4134 0.0301 -0.9100
3.6573 -2.6839 0.3594 -0.0680 -0.0088 -0.9976
-4.1982 -0.1181 2.6263 -0.1928 0.4713 0.8606
4.1375 0.8787 -3.0912 0.2367 -0.5764 -0.7821
-0.1571 -5.5156 3.7334 -0.3451 0.8262 -0.4452
-2.7105 4.2692 -1.1706 0.1420 -0.3332 0.9321
3.1454 3.6023 -4.2854 0.3599 -0.8687 -0.3404
-0.0819 4.1433 8.6234 -0.6581 -0.6967 0.2854
-3.6585 0.4538 -4.3032 0.3663 0.3829 0.8481
2.5109 1.9759 7.7789 -0.6202 -0.6531 -0.4346
-0.3182 -3.9517 -8.7944 0.6753 0.7144 -0.1835
0.0249 4.1317 -8.6223 0.7271 -0.5581 0.3999
0.7048 -4.2760 7.6972 -0.6573 0.5053 -0.5591
-3.3893 3.2061 -0.9694 0.1201 -0.0960 0.9881
-0.0302 5.7799 -0.2526 0.0685 -0.8753 0.4786
2.4243 4.7209 -0.6396 0.0795 -0.9889 -0.1255
-0.2348 -5.7719 0.2991 -0.0710 0.9038 -0.4221
2.7303 3.5997 4.1259 -0.3141 -0.8939 -0.3198
