#------------------------------------------------------------------------------
#$Date: 2016-03-26 18:01:25 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180408 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/77/7207744.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7207744
loop_
_publ_author_name
'Maxim, Catalin'
'Branzea, Diana'
'Allain, Magali'
'Andruh, Marius'
'Clérac, Rodolphe'
'Iorga, Bogdan I.'
'Avarvari, Narcis'
_publ_section_title
;
 Cyanomethylene-bis(phosphonate) as ditopical ligand: stepwise formation
 of a 2-D heterometallic Fe(iii)--Ag(i) coordination network
;
_journal_issue                   9
_journal_name_full               CrystEngComm
_journal_page_first              3096
_journal_paper_doi               10.1039/c2ce06261e
_journal_volume                  14
_journal_year                    2012
_chemical_formula_moiety         'C108 H180 Ag3 Cl3 Fe3 N9 O68 P18'
_chemical_formula_sum            'C108 H180 Ag3 Cl3 Fe3 N9 O68 P18'
_chemical_formula_weight         3847.58
_chemical_name_common
;MOLTECH ANJOU UMR CNRS 6200 2, bd Lavoisier 49045 Angers
cedex France
;
_chemical_name_systematic
;
MOLTECH ANJOU UMR CNRS 6200
2, bd Lavoisier
49045 Angers cedex
France
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.49(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   20.403(8)
_cell_length_b                   26.51(1)
_cell_length_c                   30.721(4)
_cell_measurement_reflns_used    16858
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      26.02
_cell_measurement_theta_min      2.02
_cell_volume                     16389(9)
_computing_cell_refinement
'Dirax/lsq (Duisenberg & Schreurs, 1989-2000)'
_computing_data_collection       'Collect (Nonius BV, 1997-2000)'
_computing_data_reduction        'EvalCCD (Duisenberg & Schreurs 1990-2000)'
_computing_molecular_graphics    'DIAMOND 3.2g (Crystal Impact GbR 2005)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      150(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  'horizontally mounted graphite crystal'
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.3159
_diffrn_reflns_av_sigmaI/netI    0.3815
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            206643
_diffrn_reflns_theta_full        26.02
_diffrn_reflns_theta_max         26.02
_diffrn_reflns_theta_min         2.02
_exptl_absorpt_coefficient_mu    0.925
_exptl_absorpt_correction_T_max  0.955
_exptl_absorpt_correction_T_min  0.825
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
'(SADABS (Sheldrick, Bruker, 2008))'
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.559
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             7900
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.093
_refine_diff_density_min         -1.097
_refine_diff_density_rms         0.160
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.018
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     1924
_refine_ls_number_reflns         32048
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.018
_refine_ls_R_factor_all          0.3343
_refine_ls_R_factor_gt           0.1041
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0779P)²+110.7385P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1867
_refine_ls_wR_factor_ref         0.2684
_reflns_number_gt                10011
_reflns_number_total             32048
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2ce06261e.txt
_cod_data_source_block           3
_cod_original_sg_symbol_H-M      P21/a
_cod_database_code               7207744
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x-1/2, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
O2W O 1.0901(14) 1.0441(12) 0.4299(9) 0.071(5) Uani 0.359(13) 1 d P
O21W O 1.0969(8) 1.0136(7) 0.4682(5) 0.071(5) Uani 0.641(13) 1 d P
O3W O 0.4867(7) 1.0193(6) 0.0678(5) 0.052(5) Uani 0.578(14) 1 d P
O31W O 0.429(2) 1.0510(19) 0.0780(17) 0.052(5) Uani 0.188(13) 1 d P
O32W O 0.4724(18) 0.9872(15) 0.1005(14) 0.052(5) Uani 0.234(13) 1 d P
C1A C 0.7605(6) 0.3270(5) 0.2502(4) 0.031(3) Uani 1 1 d .
C1B C 0.9064(7) 0.5907(5) 0.3356(5) 0.041(4) Uani 1 1 d .
C1C C 0.6042(7) 0.5659(5) 0.1826(4) 0.035(4) Uani 1 1 d .
C2A C 0.8773(7) 0.3089(5) 0.1598(4) 0.046(4) Uani 1 1 d .
H2A1 H 0.8777 0.2745 0.1492 0.055 Uiso 1 1 calc R
H2A2 H 0.9224 0.3217 0.1636 0.055 Uiso 1 1 calc R
C2B C 0.8581(7) 0.5630(5) 0.3091(4) 0.043(4) Uani 1 1 d .
C2C C 0.5516(6) 0.5918(4) 0.1562(4) 0.025(3) Uani 1 1 d .
C3A C 0.7648(7) 0.3181(5) 0.1220(4) 0.049(4) Uani 1 1 d .
H3A1 H 0.7347 0.3367 0.1000 0.059 Uiso 1 1 calc R
H3A2 H 0.7662 0.2836 0.1117 0.059 Uiso 1 1 calc R
C3B C 0.8391(6) 0.5858(5) 0.4515(4) 0.039(4) Uani 1 1 d .
H3B1 H 0.8598 0.6105 0.4727 0.047 Uiso 1 1 calc R
H3B2 H 0.8343 0.5545 0.4670 0.047 Uiso 1 1 calc R
C3C C 0.4166(6) 0.5306(5) 0.2218(4) 0.039(4) Uani 1 1 d .
H3C1 H 0.4181 0.4956 0.2310 0.047 Uiso 1 1 calc R
H3C2 H 0.3711 0.5385 0.2088 0.047 Uiso 1 1 calc R
C4A C 0.8336(7) 0.3408(5) 0.1256(4) 0.045(4) Uani 1 1 d .
C4B C 0.7799(7) 0.6525(4) 0.4063(5) 0.047(4) Uani 1 1 d .
H4B1 H 0.8008 0.6772 0.4275 0.056 Uiso 1 1 calc R
H4B2 H 0.7366 0.6655 0.3933 0.056 Uiso 1 1 calc R
C4C C 0.4322(6) 0.6183(4) 0.2456(4) 0.029(3) Uani 1 1 d .
H4C1 H 0.3869 0.6249 0.2315 0.035 Uiso 1 1 calc R
H4C2 H 0.4430 0.6413 0.2703 0.035 Uiso 1 1 calc R
C5A C 0.8568(8) 0.3362(6) 0.0813(4) 0.063(5) Uani 1 1 d .
H5A1 H 0.9002 0.3509 0.0832 0.094 Uiso 1 1 calc R
H5A2 H 0.8262 0.3535 0.0592 0.094 Uiso 1 1 calc R
H5A3 H 0.8588 0.3012 0.0735 0.094 Uiso 1 1 calc R
C5C C 0.4376(7) 0.5643(5) 0.2624(5) 0.042(4) Uani 1 1 d .
C6A C 0.8330(7) 0.3964(5) 0.1395(4) 0.046(4) Uani 1 1 d .
H6A1 H 0.8774 0.4096 0.1435 0.069 Uiso 1 1 calc R
H6A2 H 0.8159 0.3990 0.1668 0.069 Uiso 1 1 calc R
H6A3 H 0.8052 0.4154 0.1171 0.069 Uiso 1 1 calc R
C6B C 0.7716(7) 0.6046(5) 0.4292(4) 0.037(4) Uani 1 1 d .
C6C C 0.3883(7) 0.5563(5) 0.2934(4) 0.051(4) Uani 1 1 d .
H6C1 H 0.3916 0.5222 0.3041 0.076 Uiso 1 1 calc R
H6C2 H 0.3442 0.5623 0.2780 0.076 Uiso 1 1 calc R
H6C3 H 0.3979 0.5792 0.3178 0.076 Uiso 1 1 calc R
C7A C 0.7526(6) 0.3794(5) 0.2484(4) 0.032(4) Uani 1 1 d .
C7B C 0.7312(7) 0.6166(5) 0.4662(5) 0.051(4) Uani 1 1 d .
H7B1 H 0.7253 0.5863 0.4823 0.077 Uiso 1 1 calc R
H7B2 H 0.6885 0.6298 0.4535 0.077 Uiso 1 1 calc R
H7B3 H 0.7545 0.6411 0.4859 0.077 Uiso 1 1 calc R
C7C C 0.5073(7) 0.5506(6) 0.2843(4) 0.053(5) Uani 1 1 d .
H7C1 H 0.5085 0.5157 0.2930 0.080 Uiso 1 1 calc R
H7C2 H 0.5201 0.5713 0.3099 0.080 Uiso 1 1 calc R
H7C3 H 0.5376 0.5559 0.2639 0.080 Uiso 1 1 calc R
C8A C 0.7709(8) 0.3243(5) 0.3829(4) 0.052(5) Uani 1 1 d .
H8A1 H 0.7813 0.2910 0.3951 0.062 Uiso 1 1 calc R
H8A2 H 0.7961 0.3487 0.4025 0.062 Uiso 1 1 calc R
C8B C 0.7326(6) 0.5665(5) 0.3980(4) 0.037(4) Uani 1 1 d .
H8B1 H 0.7293 0.5353 0.4134 0.055 Uiso 1 1 calc R
H8B2 H 0.7550 0.5607 0.3734 0.055 Uiso 1 1 calc R
H8B3 H 0.6888 0.5793 0.3877 0.055 Uiso 1 1 calc R
C8C C 0.6227(6) 0.6041(5) 0.0418(4) 0.043(4) Uani 1 1 d .
H8C1 H 0.5988 0.6302 0.0235 0.052 Uiso 1 1 calc R
H8C2 H 0.6304 0.5762 0.0229 0.052 Uiso 1 1 calc R
C9A C 0.8947(6) 0.1029(5) 0.3200(4) 0.032(4) Uani 1 1 d .
C9B C 1.0488(7) 0.5172(5) 0.2850(5) 0.054(5) Uani 1 1 d .
H9B1 H 1.0478 0.4811 0.2797 0.064 Uiso 1 1 calc R
H9B2 H 1.0929 0.5260 0.3001 0.064 Uiso 1 1 calc R
C9C C 0.6740(7) 0.6686(5) 0.0922(5) 0.058(5) Uani 1 1 d .
H9C1 H 0.6502 0.6936 0.0726 0.069 Uiso 1 1 calc R
H9C2 H 0.7152 0.6837 0.1066 0.069 Uiso 1 1 calc R
C10A C 0.9406(7) 0.0700(6) 0.3445(4) 0.044(4) Uani 1 1 d .
C10B C 1.0388(7) 0.6018(5) 0.2497(5) 0.051(4) Uani 1 1 d .
H10A H 1.0827 0.6104 0.2653 0.061 Uiso 1 1 calc R
H10B H 1.0309 0.6205 0.2222 0.061 Uiso 1 1 calc R
C10C C 0.6893(6) 0.6249(5) 0.0659(4) 0.036(4) Uani 1 1 d .
C11A C 1.0235(7) 0.1723(6) 0.2546(5) 0.054(5) Uani 1 1 d .
H11D H 1.0685 0.1821 0.2670 0.065 Uiso 1 1 calc R
H11E H 1.0014 0.2014 0.2396 0.065 Uiso 1 1 calc R
C11B C 1.0341(7) 0.5454(5) 0.2407(5) 0.050(4) Uani 1 1 d .
C11C C 0.7291(8) 0.5855(6) 0.0940(6) 0.076(6) Uani 1 1 d .
H11A H 0.7384 0.5579 0.0758 0.114 Uiso 1 1 calc R
H11B H 0.7041 0.5735 0.1158 0.114 Uiso 1 1 calc R
H11C H 0.7701 0.6000 0.1085 0.114 Uiso 1 1 calc R
C12A C 0.9543(6) 0.1169(6) 0.2012(4) 0.046(4) Uani 1 1 d .
H12A H 0.9323 0.1466 0.1873 0.055 Uiso 1 1 calc R
H12B H 0.9539 0.0910 0.1788 0.055 Uiso 1 1 calc R
C12B C 0.9683(7) 0.5286(6) 0.2139(4) 0.060(5) Uani 1 1 d .
H12F H 0.9618 0.5451 0.1858 0.090 Uiso 1 1 calc R
H12G H 0.9328 0.5373 0.2294 0.090 Uiso 1 1 calc R
H12H H 0.9689 0.4927 0.2097 0.090 Uiso 1 1 calc R
C12C C 0.7290(8) 0.6443(7) 0.0302(6) 0.094(7) Uani 1 1 d .
H12C H 0.7409 0.6163 0.0133 0.141 Uiso 1 1 calc R
H12D H 0.7685 0.6611 0.0443 0.141 Uiso 1 1 calc R
H12E H 0.7020 0.6675 0.0110 0.141 Uiso 1 1 calc R
C13A C 1.0254(7) 0.1296(6) 0.2214(5) 0.055(5) Uani 1 1 d .
C13B C 1.0928(8) 0.5327(6) 0.2148(6) 0.082(6) Uani 1 1 d .
H13A H 1.1344 0.5411 0.2328 0.123 Uiso 1 1 calc R
H13B H 1.0875 0.5520 0.1880 0.123 Uiso 1 1 calc R
H13C H 1.0921 0.4974 0.2079 0.123 Uiso 1 1 calc R
C13C C 0.2778(5) 0.5882(4) 0.0151(4) 0.020(3) Uani 1 1 d .
C14A C 1.0639(7) 0.0839(6) 0.2420(6) 0.072(6) Uani 1 1 d .
H14C H 1.0418 0.0700 0.2645 0.107 Uiso 1 1 calc R
H14D H 1.1081 0.0940 0.2547 0.107 Uiso 1 1 calc R
H14E H 1.0660 0.0589 0.2196 0.107 Uiso 1 1 calc R
C14B C 1.1615(7) 0.7550(5) 0.3155(4) 0.041(4) Uani 1 1 d .
H14A H 1.1485 0.7204 0.3082 0.049 Uiso 1 1 calc R
H14B H 1.2093 0.7574 0.3177 0.049 Uiso 1 1 calc R
C14C C 0.2270(7) 0.5570(6) -0.0101(4) 0.040(4) Uani 1 1 d .
C15A C 1.0594(8) 0.1549(7) 0.1836(5) 0.091(7) Uani 1 1 d .
H15E H 1.0361 0.1853 0.1737 0.136 Uiso 1 1 calc R
H15F H 1.0576 0.1318 0.1594 0.136 Uiso 1 1 calc R
H15G H 1.1049 0.1627 0.1951 0.136 Uiso 1 1 calc R
C15B C 1.0543(7) 0.7847(5) 0.2771(4) 0.042(4) Uani 1 1 d .
H15C H 1.0314 0.8065 0.2542 0.050 Uiso 1 1 calc R
H15D H 1.0420 0.7502 0.2691 0.050 Uiso 1 1 calc R
C15C C 0.4283(6) 0.5288(5) -0.0331(4) 0.042(4) Uani 1 1 d .
H15A H 0.4679 0.5378 -0.0126 0.050 Uiso 1 1 calc R
H15B H 0.4326 0.4938 -0.0413 0.050 Uiso 1 1 calc R
C16A C 0.7534(7) 0.0916(6) 0.3963(5) 0.056(5) Uani 1 1 d .
H16C H 0.7581 0.0993 0.4275 0.067 Uiso 1 1 calc R
H16D H 0.7148 0.1096 0.3813 0.067 Uiso 1 1 calc R
C16B C 1.1275(7) 0.7905(5) 0.2786(4) 0.047(4) Uani 1 1 d .
C16C C 0.4188(7) 0.6164(5) -0.0607(4) 0.036(4) Uani 1 1 d .
H16A H 0.4583 0.6272 -0.0410 0.043 Uiso 1 1 calc R
H16B H 0.4140 0.6368 -0.0872 0.043 Uiso 1 1 calc R
C17A C 0.7338(7) 0.0256(5) 0.3419(6) 0.073(6) Uani 1 1 d .
H17A H 0.7294 -0.0107 0.3381 0.088 Uiso 1 1 calc R
H17B H 0.6929 0.0410 0.3274 0.088 Uiso 1 1 calc R
C17B C 1.1481(7) 0.8451(6) 0.2893(5) 0.060(5) Uani 1 1 d .
H17C H 1.1952 0.8484 0.2903 0.089 Uiso 1 1 calc R
H17D H 1.1368 0.8542 0.3174 0.089 Uiso 1 1 calc R
H17E H 1.1252 0.8669 0.2668 0.089 Uiso 1 1 calc R
C17C C 0.4246(7) 0.5601(5) -0.0725(4) 0.041(4) Uani 1 1 d .
C18A C 0.7669(8) 0.0281(6) 0.1543(5) 0.069(5) Uani 1 1 d .
H18D H 0.7661 -0.0085 0.1550 0.083 Uiso 1 1 calc R
H18E H 0.8104 0.0390 0.1690 0.083 Uiso 1 1 calc R
C18B C 1.1442(8) 0.7732(6) 0.2340(4) 0.064(5) Uani 1 1 d .
H18A H 1.1316 0.7385 0.2291 0.096 Uiso 1 1 calc R
H18B H 1.1911 0.7766 0.2342 0.096 Uiso 1 1 calc R
H18C H 1.1204 0.7936 0.2108 0.096 Uiso 1 1 calc R
C18C C 0.3632(7) 0.5430(6) -0.1081(5) 0.056(5) Uani 1 1 d .
H18F H 0.3600 0.5644 -0.1336 0.084 Uiso 1 1 calc R
H18G H 0.3231 0.5457 -0.0957 0.084 Uiso 1 1 calc R
H18H H 0.3692 0.5087 -0.1165 0.084 Uiso 1 1 calc R
C19A C 0.7614(7) 0.1023(5) 0.1093(5) 0.049(4) Uani 1 1 d .
H19A H 0.8042 0.1123 0.1257 0.059 Uiso 1 1 calc R
H19B H 0.7577 0.1158 0.0796 0.059 Uiso 1 1 calc R
C19B C 1.0530(6) 0.8011(5) 0.4055(4) 0.029(3) Uani 1 1 d .
C19C C 0.4894(7) 0.5532(6) -0.0924(5) 0.070(5) Uani 1 1 d .
H19C H 0.4872 0.5737 -0.1183 0.105 Uiso 1 1 calc R
H19D H 0.4940 0.5184 -0.1000 0.105 Uiso 1 1 calc R
H19E H 0.5269 0.5632 -0.0711 0.105 Uiso 1 1 calc R
C20A C 0.7571(7) 0.0452(5) 0.1073(5) 0.051(4) Uani 1 1 d .
C20B C 1.0497(6) 0.8538(5) 0.4035(4) 0.033(4) Uani 1 1 d .
C20C C 0.1579(8) 0.6907(6) 0.0605(5) 0.063(5) Uani 1 1 d .
H20A H 0.1852 0.7138 0.0802 0.076 Uiso 1 1 calc R
H20B H 0.1239 0.7104 0.0421 0.076 Uiso 1 1 calc R
C21A C 0.8183(8) 0.0259(6) 0.0884(7) 0.097(7) Uani 1 1 d .
H21C H 0.8182 -0.0103 0.0881 0.146 Uiso 1 1 calc R
H21D H 0.8582 0.0377 0.1066 0.146 Uiso 1 1 calc R
H21E H 0.8165 0.0383 0.0589 0.146 Uiso 1 1 calc R
C21B C 1.0467(7) 0.5323(5) 0.5376(5) 0.043(4) Uani 1 1 d .
H21A H 1.0458 0.4974 0.5468 0.052 Uiso 1 1 calc R
H21B H 1.0031 0.5407 0.5216 0.052 Uiso 1 1 calc R
C21C C 0.1797(6) 0.6238(6) 0.1154(4) 0.046(4) Uani 1 1 d .
H21F H 0.2081 0.6460 0.1353 0.056 Uiso 1 1 calc R
H21G H 0.1594 0.5998 0.1330 0.056 Uiso 1 1 calc R
C22A C 0.6921(7) 0.0270(6) 0.0811(5) 0.062(5) Uani 1 1 d .
H22C H 0.6903 -0.0091 0.0824 0.093 Uiso 1 1 calc R
H22D H 0.6890 0.0376 0.0509 0.093 Uiso 1 1 calc R
H22E H 0.6558 0.0410 0.0934 0.093 Uiso 1 1 calc R
C22B C 1.0585(7) 0.6195(5) 0.5618(5) 0.045(4) Uani 1 1 d .
H22A H 1.0148 0.6264 0.5451 0.054 Uiso 1 1 calc R
H22B H 1.0660 0.6422 0.5868 0.054 Uiso 1 1 calc R
C22C C 0.1255(6) 0.6547(5) 0.0869(4) 0.040(4) Uani 1 1 d .
C23A C 0.5773(11) 0.0929(7) 0.1662(5) 0.082(6) Uani 1 1 d .
C23B C 1.0617(7) 0.5654(5) 0.5778(5) 0.043(4) Uani 1 1 d .
C23C C 0.0915(8) 0.6868(7) 0.1193(5) 0.087(6) Uani 1 1 d .
H23A H 0.0698 0.6649 0.1373 0.130 Uiso 1 1 calc R
H23B H 0.0593 0.7088 0.1027 0.130 Uiso 1 1 calc R
H23C H 0.1244 0.7065 0.1378 0.130 Uiso 1 1 calc R
C24A C 0.5716(6) 0.1394(5) 0.3086(4) 0.040(4) Uani 1 1 d .
H24A H 0.5989 0.1666 0.3227 0.048 Uiso 1 1 calc R
H24B H 0.5671 0.1142 0.3308 0.048 Uiso 1 1 calc R
C24B C 1.1278(7) 0.5540(5) 0.6077(4) 0.044(4) Uani 1 1 d .
H24F H 1.1343 0.5774 0.6319 0.065 Uiso 1 1 calc R
H24G H 1.1635 0.5572 0.5911 0.065 Uiso 1 1 calc R
H24H H 1.1269 0.5202 0.6189 0.065 Uiso 1 1 calc R
C24C C 0.0783(7) 0.6195(5) 0.0576(5) 0.064(5) Uani 1 1 d .
H24C H 0.0610 0.5948 0.0755 0.095 Uiso 1 1 calc R
H24D H 0.1019 0.6028 0.0371 0.095 Uiso 1 1 calc R
H24E H 0.0423 0.6387 0.0416 0.095 Uiso 1 1 calc R
C25A C 0.5133(7) 0.1987(5) 0.2561(5) 0.051(4) Uani 1 1 d .
H25F H 0.4704 0.2125 0.2434 0.062 Uiso 1 1 calc R
H25G H 0.5397 0.2259 0.2711 0.062 Uiso 1 1 calc R
C25B C 1.0047(7) 0.5595(6) 0.6039(5) 0.068(5) Uani 1 1 d .
H25C H 0.9635 0.5674 0.5852 0.102 Uiso 1 1 calc R
H25D H 1.0113 0.5820 0.6287 0.102 Uiso 1 1 calc R
H25E H 1.0035 0.5253 0.6142 0.102 Uiso 1 1 calc R
C25C C 0.3572(7) 0.7769(5) -0.0491(4) 0.043(4) Uani 1 1 d .
H25A H 0.3542 0.7409 -0.0551 0.051 Uiso 1 1 calc R
H25B H 0.3205 0.7932 -0.0680 0.051 Uiso 1 1 calc R
C26A C 0.5034(6) 0.1596(5) 0.2890(4) 0.035(4) Uani 1 1 d .
C26B C 1.1153(8) 0.7819(6) 0.5354(4) 0.069(6) Uani 1 1 d .
H26C H 1.1547 0.7975 0.5519 0.082 Uiso 1 1 calc R
H26D H 1.1168 0.7463 0.5426 0.082 Uiso 1 1 calc R
C26C C 0.4766(7) 0.7715(5) -0.0296(4) 0.048(4) Uani 1 1 d .
H26A H 0.4747 0.7352 -0.0340 0.057 Uiso 1 1 calc R
H26B H 0.5183 0.7835 -0.0370 0.057 Uiso 1 1 calc R
C27A C 0.4585(7) 0.1162(5) 0.2683(5) 0.058(5) Uani 1 1 d .
H27C H 0.4532 0.0920 0.2907 0.087 Uiso 1 1 calc R
H27D H 0.4786 0.1002 0.2457 0.087 Uiso 1 1 calc R
H27E H 0.4158 0.1294 0.2555 0.087 Uiso 1 1 calc R
C27B C 0.9954(8) 0.7831(7) 0.5234(5) 0.072(6) Uani 1 1 d .
H27A H 0.9558 0.7974 0.5322 0.086 Uiso 1 1 calc R
H27B H 0.9953 0.7471 0.5289 0.086 Uiso 1 1 calc R
C27C C 0.4198(8) 0.7959(5) -0.0600(5) 0.052(5) Uani 1 1 d .
C28A C 0.4715(7) 0.1839(6) 0.3266(5) 0.077(6) Uani 1 1 d .
H28D H 0.4658 0.1586 0.3480 0.116 Uiso 1 1 calc R
H28E H 0.4290 0.1979 0.3144 0.116 Uiso 1 1 calc R
H28F H 0.4999 0.2101 0.3405 0.116 Uiso 1 1 calc R
C28C C 0.4215(8) 0.7798(6) -0.1086(4) 0.068(5) Uani 1 1 d .
H28A H 0.3853 0.7954 -0.1278 0.103 Uiso 1 1 calc R
H28B H 0.4176 0.7438 -0.1111 0.103 Uiso 1 1 calc R
H28C H 0.4628 0.7903 -0.1169 0.103 Uiso 1 1 calc R
C30C C 0.4257(8) 0.8532(5) -0.0539(5) 0.064(5) Uani 1 1 d .
H30A H 0.3889 0.8693 -0.0722 0.096 Uiso 1 1 calc R
H30B H 0.4665 0.8645 -0.0623 0.096 Uiso 1 1 calc R
H30C H 0.4253 0.8615 -0.0236 0.096 Uiso 1 1 calc R
C31C C 0.4260(7) 0.7881(5) 0.2115(4) 0.044(4) Uani 1 1 d .
H31A H 0.4540 0.8093 0.2327 0.052 Uiso 1 1 calc R
H31B H 0.4381 0.7533 0.2183 0.052 Uiso 1 1 calc R
C32C C 0.3092(7) 0.7648(5) 0.1829(4) 0.043(4) Uani 1 1 d .
H32A H 0.3178 0.7294 0.1896 0.051 Uiso 1 1 calc R
H32B H 0.2629 0.7714 0.1844 0.051 Uiso 1 1 calc R
C33C C 0.3521(7) 0.7963(6) 0.2164(4) 0.048(4) Uani 1 1 d .
C34C C 0.3345(7) 0.8526(5) 0.2087(5) 0.056(5) Uani 1 1 d .
H34A H 0.3621 0.8726 0.2305 0.085 Uiso 1 1 calc R
H34B H 0.2887 0.8578 0.2111 0.085 Uiso 1 1 calc R
H34C H 0.3418 0.8623 0.1798 0.085 Uiso 1 1 calc R
C35C C 0.3455(8) 0.7789(7) 0.2638(4) 0.083(6) Uani 1 1 d .
H35A H 0.3569 0.7438 0.2672 0.124 Uiso 1 1 calc R
H35B H 0.3006 0.7838 0.2685 0.124 Uiso 1 1 calc R
H35C H 0.3750 0.7984 0.2849 0.124 Uiso 1 1 calc R
C36C C 0.4037(6) 0.8006(4) 0.0802(4) 0.026(3) Uani 1 1 d .
C37C C 0.4030(6) 0.8541(5) 0.0786(4) 0.035(4) Uani 1 1 d .
C40A C 0.6283(6) 0.1171(5) 0.1911(5) 0.043(4) Uani 1 1 d .
C40B C 1.1836(7) 0.5943(5) 0.4740(4) 0.036(4) Uani 1 1 d .
C41A C 0.6979(7) 0.3344(6) 0.3802(4) 0.046(4) Uani 1 1 d .
C41B C 1.2336(7) 0.5670(6) 0.4995(5) 0.051(5) Uani 1 1 d .
C42A C 0.6601(7) 0.2961(6) 0.3511(4) 0.050(4) Uani 1 1 d .
H42C H 0.6128 0.3010 0.3504 0.060 Uiso 1 1 calc R
H42D H 0.6716 0.2626 0.3626 0.060 Uiso 1 1 calc R
C42B C 1.2726(7) 0.6367(6) 0.3741(4) 0.050(4) Uani 1 1 d .
H42A H 1.2421 0.6603 0.3571 0.060 Uiso 1 1 calc R
H42B H 1.2907 0.6151 0.3535 0.060 Uiso 1 1 calc R
C43A C 0.6800(7) 0.3889(5) 0.3653(5) 0.054(4) Uani 1 1 d .
H43A H 0.7045 0.4121 0.3858 0.081 Uiso 1 1 calc R
H43B H 0.6332 0.3942 0.3644 0.081 Uiso 1 1 calc R
H43C H 0.6910 0.3943 0.3365 0.081 Uiso 1 1 calc R
C44A C 0.7427(8) 0.0374(6) 0.3899(6) 0.067(6) Uani 1 1 d .
C45A C 0.8056(7) 0.0090(6) 0.4153(6) 0.082(6) Uani 1 1 d .
H45A H 0.8098 0.0158 0.4463 0.124 Uiso 1 1 calc R
H45B H 0.8447 0.0205 0.4046 0.124 Uiso 1 1 calc R
H45C H 0.8005 -0.0267 0.4103 0.124 Uiso 1 1 calc R
C46A C 0.6778(8) 0.0194(6) 0.4052(6) 0.092(7) Uani 1 1 d .
H46A H 0.6808 0.0255 0.4363 0.139 Uiso 1 1 calc R
H46B H 0.6719 -0.0160 0.3995 0.139 Uiso 1 1 calc R
H46C H 0.6407 0.0376 0.3894 0.139 Uiso 1 1 calc R
C48A C 0.6796(10) 0.3283(6) 0.4279(5) 0.086(6) Uani 1 1 d .
H48A H 0.7031 0.3531 0.4472 0.129 Uiso 1 1 calc R
H48B H 0.6919 0.2951 0.4389 0.129 Uiso 1 1 calc R
H48C H 0.6326 0.3329 0.4265 0.129 Uiso 1 1 calc R
C50B C 1.0535(8) 0.8053(6) 0.5499(5) 0.057(5) Uani 1 1 d .
C51B C 1.0537(10) 0.8614(7) 0.5437(5) 0.099(7) Uani 1 1 d .
H51A H 1.0183 0.8761 0.5565 0.148 Uiso 1 1 calc R
H51B H 1.0475 0.8692 0.5128 0.148 Uiso 1 1 calc R
H51C H 1.0954 0.8750 0.5580 0.148 Uiso 1 1 calc R
C52B C 1.0573(11) 0.7917(7) 0.5982(5) 0.108(8) Uani 1 1 d .
H52A H 1.0225 0.8087 0.6099 0.162 Uiso 1 1 calc R
H52B H 1.0996 0.8019 0.6143 0.162 Uiso 1 1 calc R
H52C H 1.0522 0.7559 0.6009 0.162 Uiso 1 1 calc R
C53B C 1.2955(8) 0.7011(6) 0.4316(5) 0.068(5) Uani 1 1 d .
H53A H 1.3304 0.7190 0.4508 0.081 Uiso 1 1 calc R
H53B H 1.2683 0.7258 0.4136 0.081 Uiso 1 1 calc R
C55B C 1.3272(7) 0.6649(6) 0.4013(5) 0.062(5) Uani 1 1 d .
C56B C 1.3634(8) 0.6994(7) 0.3727(5) 0.085(6) Uani 1 1 d .
H56A H 1.3975 0.7179 0.3913 0.128 Uiso 1 1 calc R
H56B H 1.3321 0.7225 0.3567 0.128 Uiso 1 1 calc R
H56C H 1.3830 0.6792 0.3523 0.128 Uiso 1 1 calc R
C57B C 1.3762(7) 0.6307(6) 0.4309(5) 0.071(5) Uani 1 1 d .
H57A H 1.3525 0.6104 0.4490 0.106 Uiso 1 1 calc R
H57B H 1.4084 0.6511 0.4494 0.106 Uiso 1 1 calc R
H57C H 1.3985 0.6092 0.4128 0.106 Uiso 1 1 calc R
Ag1 Ag 0.73012(5) 0.50527(4) 0.24314(3) 0.0360(3) Uani 1 1 d .
Ag2 Ag 1.02457(6) 0.97610(4) 0.39685(4) 0.0507(4) Uani 1 1 d .
Ag3 Ag 0.37397(6) 0.97175(4) 0.05539(4) 0.0447(3) Uani 1 1 d .
FeA Fe 0.76858(10) 0.18733(7) 0.25477(7) 0.0353(5) Uani 1 1 d .
FeB Fe 1.04306(9) 0.65992(7) 0.40629(6) 0.0315(5) Uani 1 1 d .
FeC Fe 0.41268(9) 0.65970(6) 0.08710(6) 0.0253(5) Uani 1 1 d .
N1A N 0.7460(5) 0.4227(5) 0.2462(4) 0.052(4) Uani 1 1 d .
N1B N 0.8132(6) 0.5445(4) 0.2865(3) 0.045(3) Uani 1 1 d .
N1C N 0.6451(6) 0.5439(4) 0.2032(3) 0.040(3) Uani 1 1 d .
N2A N 0.5294(6) 0.0756(5) 0.1421(4) 0.067(4) Uani 1 1 d .
N2B N 1.0468(6) 0.8968(4) 0.4013(4) 0.043(3) Uani 1 1 d .
N2C N 0.4006(5) 0.8970(4) 0.0748(4) 0.041(3) Uani 1 1 d .
N3A N 0.9783(6) 0.0425(5) 0.3665(4) 0.054(4) Uani 1 1 d .
N3B N 1.2798(7) 0.5427(5) 0.5195(4) 0.063(4) Uani 1 1 d .
N3C N 0.1913(6) 0.5311(4) -0.0295(4) 0.052(3) Uani 1 1 d .
O1A O 0.7688(4) 0.1366(3) 0.3022(3) 0.043(3) Uani 1 1 d .
O1B O 1.0519(4) 0.6079(3) 0.4542(3) 0.034(2) Uani 1 1 d .
O1C O 0.4196(4) 0.6093(3) 0.1355(2) 0.026(2) Uani 1 1 d .
O2A O 0.8677(4) 0.1782(3) 0.2621(3) 0.036(2) Uani 1 1 d .
O2B O 1.1411(4) 0.6615(3) 0.4121(3) 0.037(2) Uani 1 1 d .
O2C O 0.5121(4) 0.6592(3) 0.0931(3) 0.032(2) Uani 1 1 d .
O3A O 0.7588(4) 0.1323(3) 0.2103(3) 0.047(3) Uani 1 1 d .
O3B O 1.0484(4) 0.7151(3) 0.4514(2) 0.032(2) Uani 1 1 d .
O3C O 0.4074(4) 0.6055(3) 0.0406(3) 0.029(2) Uani 1 1 d .
O4A O 0.6698(4) 0.1902(3) 0.2486(3) 0.036(2) Uani 1 1 d .
O4B O 1.0403(4) 0.7134(3) 0.3596(3) 0.032(2) Uani 1 1 d .
O4C O 0.3132(4) 0.6572(3) 0.0789(2) 0.030(2) Uani 1 1 d .
O5A O 0.7737(4) 0.2434(3) 0.2987(3) 0.032(2) Uani 1 1 d .
O5B O 0.9452(4) 0.6559(3) 0.4014(3) 0.035(2) Uani 1 1 d .
O5C O 0.4054(4) 0.7111(3) 0.0397(3) 0.034(2) Uani 1 1 d .
O6A O 0.7725(4) 0.2397(3) 0.2084(3) 0.035(2) Uani 1 1 d .
O6B O 1.0375(4) 0.6078(3) 0.3586(3) 0.030(2) Uani 1 1 d .
O6C O 0.4152(4) 0.7159(3) 0.1305(2) 0.030(2) Uani 1 1 d .
O7A O 0.7081(4) 0.1228(3) 0.1306(3) 0.040(2) Uani 1 1 d .
O7B O 0.8211(4) 0.6456(3) 0.3712(3) 0.040(2) Uani 1 1 d .
O7C O 0.3219(4) 0.7755(3) 0.1383(2) 0.030(2) Uani 1 1 d .
O8A O 0.7161(4) 0.0476(3) 0.1788(3) 0.050(3) Uani 1 1 d .
O8B O 0.8810(4) 0.5777(3) 0.4163(3) 0.029(2) Uani 1 1 d .
O8C O 0.4380(4) 0.7998(3) 0.1683(3) 0.030(2) Uani 1 1 d .
O9A O 0.5457(4) 0.1804(3) 0.2207(3) 0.047(3) Uani 1 1 d .
O9B O 0.9865(4) 0.6147(3) 0.2776(3) 0.032(2) Uani 1 1 d .
O9C O 0.3510(4) 0.7859(3) -0.0017(3) 0.038(2) Uani 1 1 d .
O10A O 0.6040(4) 0.1167(3) 0.2740(3) 0.039(2) Uani 1 1 d .
O10B O 0.9985(4) 0.5307(3) 0.3133(3) 0.041(2) Uani 1 1 d .
O10C O 0.4741(4) 0.7828(3) 0.0167(3) 0.032(2) Uani 1 1 d .
O11A O 0.7384(4) 0.3185(3) 0.1638(3) 0.039(2) Uani 1 1 d .
O11B O 1.0318(4) 0.7968(3) 0.3188(3) 0.034(2) Uani 1 1 d .
O11C O 0.4598(4) 0.5373(3) 0.1881(3) 0.031(2) Uani 1 1 d .
O12A O 0.8546(4) 0.3090(3) 0.2027(2) 0.033(2) Uani 1 1 d .
O12B O 1.1423(4) 0.7686(3) 0.3571(3) 0.031(2) Uani 1 1 d .
O12C O 0.4781(4) 0.6267(3) 0.2136(2) 0.027(2) Uani 1 1 d .
O13A O 0.7894(4) 0.0433(3) 0.3203(3) 0.045(3) Uani 1 1 d .
O13B O 0.9934(4) 0.7918(3) 0.4761(3) 0.040(3) Uani 1 1 d .
O13C O 0.3705(4) 0.5337(3) -0.0107(3) 0.035(2) Uani 1 1 d .
O14A O 0.8132(4) 0.1094(3) 0.3794(3) 0.046(3) Uani 1 1 d .
O14B O 1.1168(4) 0.7878(3) 0.4880(3) 0.046(3) Uani 1 1 d .
O14C O 0.3593(4) 0.6222(3) -0.0389(2) 0.029(2) Uani 1 1 d .
O15A O 0.9188(4) 0.0986(3) 0.2368(3) 0.031(2) Uani 1 1 d .
O15B O 1.0964(4) 0.5381(3) 0.5080(3) 0.035(2) Uani 1 1 d .
O15C O 0.2204(4) 0.5962(3) 0.0869(3) 0.033(2) Uani 1 1 d .
O16A O 0.9878(4) 0.1562(3) 0.2904(3) 0.044(3) Uani 1 1 d .
O16B O 1.1100(4) 0.6280(3) 0.5333(3) 0.040(2) Uani 1 1 d .
O16C O 0.2002(4) 0.6654(3) 0.0317(3) 0.035(2) Uani 1 1 d .
O17A O 0.7908(4) 0.3277(3) 0.3378(3) 0.043(3) Uani 1 1 d .
O17B O 1.2365(4) 0.6058(3) 0.4018(3) 0.042(3) Uani 1 1 d .
O17C O 0.5836(4) 0.5871(3) 0.0749(3) 0.026(2) Uani 1 1 d .
O18A O 0.6762(4) 0.3007(3) 0.3057(3) 0.034(2) Uani 1 1 d .
O18B O 1.2533(4) 0.6725(3) 0.4592(3) 0.044(3) Uani 1 1 d .
O18C O 0.6331(4) 0.6543(3) 0.1261(3) 0.043(3) Uani 1 1 d .
P1A P 0.78097(18) 0.29526(13) 0.20567(12) 0.0335(10) Uani 1 1 d .
P1B P 0.98610(18) 0.58694(13) 0.32277(11) 0.0301(9) Uani 1 1 d .
P1C P 0.39562(17) 0.77012(12) 0.12956(11) 0.0259(9) Uani 1 1 d .
P2A P 0.75150(17) 0.29661(14) 0.29844(12) 0.0329(10) Uani 1 1 d .
P2B P 0.89107(17) 0.61965(13) 0.38292(11) 0.0302(9) Uani 1 1 d .
P2C P 0.40852(17) 0.76691(13) 0.03419(11) 0.0275(9) Uani 1 1 d .
P3A P 0.91468(17) 0.13629(13) 0.27671(12) 0.0322(9) Uani 1 1 d .
P3B P 1.10707(19) 0.59329(13) 0.49049(12) 0.0332(10) Uani 1 1 d .
P3C P 0.25571(17) 0.62886(12) 0.05478(11) 0.0266(9) Uani 1 1 d .
P4A P 0.81350(19) 0.09971(13) 0.32907(12) 0.0347(10) Uani 1 1 d .
P4B P 1.20046(18) 0.63547(13) 0.43556(11) 0.0331(10) Uani 1 1 d .
P4C P 0.35667(18) 0.58908(12) 0.00329(11) 0.0284(9) Uani 1 1 d .
P5A P 0.70571(19) 0.10642(14) 0.17913(13) 0.0416(11) Uani 1 1 d .
P5B P 1.06591(18) 0.76658(13) 0.36027(11) 0.0300(9) Uani 1 1 d .
P5C P 0.47317(18) 0.59219(12) 0.17161(11) 0.0281(9) Uani 1 1 d .
P6A P 0.61560(19) 0.15279(15) 0.23427(13) 0.0424(11) Uani 1 1 d .
P6B P 1.05283(18) 0.77062(13) 0.45525(11) 0.0314(9) Uani 1 1 d .
P6C P 0.56648(17) 0.62494(12) 0.11110(11) 0.0259(9) Uani 1 1 d .
Cl1 Cl 0.13594(19) 0.31330(14) 0.44263(12) 0.0496(10) Uani 1 1 d .
O1P O 0.1243(6) 0.3664(4) 0.4410(4) 0.083(4) Uani 1 1 d .
O2P O 0.1990(5) 0.3030(4) 0.4294(4) 0.071(3) Uani 1 1 d .
O3P O 0.1362(6) 0.2955(4) 0.4861(3) 0.073(4) Uani 1 1 d .
O4P O 0.0853(5) 0.2879(4) 0.4135(3) 0.072(3) Uani 1 1 d .
Cl2 Cl 0.1065(2) 0.81286(16) -0.07303(14) 0.0605(12) Uani 1 1 d .
O5P O 0.1094(6) 0.8651(4) -0.0682(4) 0.098(5) Uani 1 1 d .
O6P O 0.1035(6) 0.7911(5) -0.0301(4) 0.092(4) Uani 1 1 d .
O7P O 0.2608(5) 0.6003(4) 0.2144(3) 0.077(4) Uani 1 1 d .
O8P O 0.2753(6) 0.6696(5) 0.2613(4) 0.096(4) Uani 1 1 d .
Cl3 Cl 0.2300(2) 0.63140(15) 0.24284(13) 0.0527(11) Uani 1 1 d .
O9P O 0.2126(6) 0.6010(4) 0.2782(3) 0.078(4) Uani 1 1 d .
O10P O 0.1707(6) 0.6513(4) 0.2185(3) 0.081(4) Uani 1 1 d .
O11P O 0.1671(6) 0.7967(4) -0.0862(4) 0.092(4) Uani 1 1 d .
O12P O 0.0506(6) 0.7961(7) -0.1024(4) 0.138(7) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O21W O2W Ag2 83.9(16) . .
O32W O3W O31W 86(3) . .
O32W O3W Ag3 61.3(17) . .
O31W O3W Ag3 66.4(19) . .
O3W O31W Ag3 78(2) . .
O3W O32W Ag3 86(2) . .
C7A C1A P1A 119.7(9) . .
C7A C1A P2A 118.1(10) . .
P1A C1A P2A 122.1(7) . .
C2B C1B P2B 121.7(11) . .
C2B C1B P1B 116.0(11) . .
P2B C1B P1B 121.7(9) . .
N1C C1C C2C 177.9(15) . .
O12A C2A C4A 112.6(10) . .
O12A C2A H2A1 109.1 . .
C4A C2A H2A1 109.1 . .
O12A C2A H2A2 109.1 . .
C4A C2A H2A2 109.1 . .
H2A1 C2A H2A2 107.8 . .
N1B C2B C1B 172.5(16) . .
C1C C2C P6C 119.7(9) . .
C1C C2C P5C 119.5(9) . .
P6C C2C P5C 120.8(7) . .
O11A C3A C4A 113.7(11) . .
O11A C3A H3A1 108.8 . .
C4A C3A H3A1 108.8 . .
O11A C3A H3A2 108.8 . .
C4A C3A H3A2 108.8 . .
H3A1 C3A H3A2 107.7 . .
O8B C3B C6B 107.7(10) . .
O8B C3B H3B1 110.2 . .
C6B C3B H3B1 110.2 . .
O8B C3B H3B2 110.2 . .
C6B C3B H3B2 110.2 . .
H3B1 C3B H3B2 108.5 . .
O11C C3C C5C 112.4(10) . .
O11C C3C H3C1 109.1 . .
C5C C3C H3C1 109.1 . .
O11C C3C H3C2 109.1 . .
C5C C3C H3C2 109.1 . .
H3C1 C3C H3C2 107.9 . .
C3A C4A C5A 109.0(12) . .
C3A C4A C2A 105.1(12) . .
C5A C4A C2A 109.9(12) . .
C3A C4A C6A 110.6(12) . .
C5A C4A C6A 110.3(12) . .
C2A C4A C6A 111.8(12) . .
C6B C4B O7B 111.3(9) . .
C6B C4B H4B1 109.4 . .
O7B C4B H4B1 109.4 . .
C6B C4B H4B2 109.4 . .
O7B C4B H4B2 109.4 . .
H4B1 C4B H4B2 108.0 . .
O12C C4C C5C 110.4(10) . .
O12C C4C H4C1 109.6 . .
C5C C4C H4C1 109.6 . .
O12C C4C H4C2 109.6 . .
C5C C4C H4C2 109.6 . .
H4C1 C4C H4C2 108.1 . .
C4A C5A H5A1 109.5 . .
C4A C5A H5A2 109.5 . .
H5A1 C5A H5A2 109.5 . .
C4A C5A H5A3 109.5 . .
H5A1 C5A H5A3 109.5 . .
H5A2 C5A H5A3 109.5 . .
C6C C5C C7C 111.1(12) . .
C6C C5C C4C 109.1(11) . .
C7C C5C C4C 112.9(12) . .
C6C C5C C3C 107.7(11) . .
C7C C5C C3C 109.7(12) . .
C4C C5C C3C 106.1(11) . .
C4A C6A H6A1 109.5 . .
C4A C6A H6A2 109.5 . .
H6A1 C6A H6A2 109.5 . .
C4A C6A H6A3 109.5 . .
H6A1 C6A H6A3 109.5 . .
H6A2 C6A H6A3 109.5 . .
C4B C6B C3B 109.3(12) . .
C4B C6B C8B 111.2(12) . .
C3B C6B C8B 114.0(11) . .
C4B C6B C7B 107.0(11) . .
C3B C6B C7B 106.9(11) . .
C8B C6B C7B 108.2(11) . .
C5C C6C H6C1 109.5 . .
C5C C6C H6C2 109.5 . .
H6C1 C6C H6C2 109.5 . .
C5C C6C H6C3 109.5 . .
H6C1 C6C H6C3 109.5 . .
H6C2 C6C H6C3 109.5 . .
N1A C7A C1A 179.0(14) . .
C6B C7B H7B1 109.5 . .
C6B C7B H7B2 109.5 . .
H7B1 C7B H7B2 109.5 . .
C6B C7B H7B3 109.5 . .
H7B1 C7B H7B3 109.5 . .
H7B2 C7B H7B3 109.5 . .
C5C C7C H7C1 109.5 . .
C5C C7C H7C2 109.5 . .
H7C1 C7C H7C2 109.5 . .
C5C C7C H7C3 109.5 . .
H7C1 C7C H7C3 109.5 . .
H7C2 C7C H7C3 109.5 . .
C41A C8A O17A 110.6(10) . .
C41A C8A H8A1 109.5 . .
O17A C8A H8A1 109.5 . .
C41A C8A H8A2 109.5 . .
O17A C8A H8A2 109.5 . .
H8A1 C8A H8A2 108.1 . .
C6B C8B H8B1 109.5 . .
C6B C8B H8B2 109.5 . .
H8B1 C8B H8B2 109.5 . .
C6B C8B H8B3 109.5 . .
H8B1 C8B H8B3 109.5 . .
H8B2 C8B H8B3 109.5 . .
O17C C8C C10C 108.4(10) . .
O17C C8C H8C1 110.0 . .
C10C C8C H8C1 110.0 . .
O17C C8C H8C2 110.0 . .
C10C C8C H8C2 110.0 . .
H8C1 C8C H8C2 108.4 . .
C10A C9A P3A 121.2(10) . .
C10A C9A P4A 117.1(10) . .
P3A C9A P4A 120.7(8) . .
O10B C9B C11B 110.2(10) . .
O10B C9B H9B1 109.6 . .
C11B C9B H9B1 109.6 . .
O10B C9B H9B2 109.6 . .
C11B C9B H9B2 109.6 . .
H9B1 C9B H9B2 108.1 . .
C10C C9C O18C 112.2(11) . .
C10C C9C H9C1 109.2 . .
O18C C9C H9C1 109.2 . .
C10C C9C H9C2 109.2 . .
O18C C9C H9C2 109.2 . .
H9C1 C9C H9C2 107.9 . .
N3A C10A C9A 177.6(14) . .
O9B C10B C11B 107.2(10) . .
O9B C10B H10A 110.3 . .
C11B C10B H10A 110.3 . .
O9B C10B H10B 110.3 . .
C11B C10B H10B 110.3 . .
H10A C10B H10B 108.5 . .
C9C C10C C11C 111.9(13) . .
C9C C10C C8C 107.1(11) . .
C11C C10C C8C 112.3(13) . .
C9C C10C C12C 107.9(13) . .
C11C C10C C12C 110.0(12) . .
C8C C10C C12C 107.4(12) . .
O16A C11A C13A 110.5(11) . .
O16A C11A H11D 109.6 . .
C13A C11A H11D 109.6 . .
O16A C11A H11E 109.6 . .
C13A C11A H11E 109.6 . .
H11D C11A H11E 108.1 . .
C10B C11B C12B 114.2(13) . .
C10B C11B C9B 108.6(13) . .
C12B C11B C9B 111.3(12) . .
C10B C11B C13B 105.6(11) . .
C12B C11B C13B 109.9(13) . .
C9B C11B C13B 106.8(13) . .
C10C C11C H11A 109.5 . .
C10C C11C H11B 109.5 . .
H11A C11C H11B 109.5 . .
C10C C11C H11C 109.5 . .
H11A C11C H11C 109.5 . .
H11B C11C H11C 109.5 . .
O15A C12A C13A 108.6(10) . .
O15A C12A H12A 110.0 . .
C13A C12A H12A 110.0 . .
O15A C12A H12B 110.0 . .
C13A C12A H12B 110.0 . .
H12A C12A H12B 108.4 . .
C11B C12B H12F 109.5 . .
C11B C12B H12G 109.5 . .
H12F C12B H12G 109.5 . .
C11B C12B H12H 109.5 . .
H12F C12B H12H 109.5 . .
H12G C12B H12H 109.5 . .
C10C C12C H12C 109.5 . .
C10C C12C H12D 109.5 . .
H12C C12C H12D 109.5 . .
C10C C12C H12E 109.5 . .
H12C C12C H12E 109.5 . .
H12D C12C H12E 109.5 . .
C12A C13A C14A 112.7(13) . .
C12A C13A C11A 108.0(13) . .
C14A C13A C11A 112.5(14) . .
C12A C13A C15A 107.2(13) . .
C14A C13A C15A 112.3(14) . .
C11A C13A C15A 103.6(12) . .
C11B C13B H13A 109.5 . .
C11B C13B H13B 109.5 . .
H13A C13B H13B 109.5 . .
C11B C13B H13C 109.5 . .
H13A C13B H13C 109.5 . .
H13B C13B H13C 109.5 . .
C14C C13C P4C 120.9(9) . .
C14C C13C P3C 118.8(8) . .
P4C C13C P3C 120.1(7) . .
C13A C14A H14C 109.5 . .
C13A C14A H14D 109.5 . .
H14C C14A H14D 109.5 . .
C13A C14A H14E 109.5 . .
H14C C14A H14E 109.5 . .
H14D C14A H14E 109.5 . .
O12B C14B C16B 110.0(10) . .
O12B C14B H14A 109.7 . .
C16B C14B H14A 109.7 . .
O12B C14B H14B 109.7 . .
C16B C14B H14B 109.7 . .
H14A C14B H14B 108.2 . .
N3C C14C C13C 175.5(15) . .
C13A C15A H15E 109.5 . .
C13A C15A H15F 109.5 . .
H15E C15A H15F 109.5 . .
C13A C15A H15G 109.5 . .
H15E C15A H15G 109.5 . .
H15F C15A H15G 109.5 . .
O11B C15B C16B 113.9(11) . .
O11B C15B H15C 108.8 . .
C16B C15B H15C 108.8 . .
O11B C15B H15D 108.8 . .
C16B C15B H15D 108.8 . .
H15C C15B H15D 107.7 . .
C17C C15C O13C 113.9(11) . .
C17C C15C H15A 108.8 . .
O13C C15C H15A 108.8 . .
C17C C15C H15B 108.8 . .
O13C C15C H15B 108.8 . .
H15A C15C H15B 107.7 . .
C44A C16A O14A 112.2(11) . .
C44A C16A H16C 109.2 . .
O14A C16A H16C 109.2 . .
C44A C16A H16D 109.2 . .
O14A C16A H16D 109.2 . .
H16C C16A H16D 107.9 . .
C15B C16B C17B 110.1(12) . .
C15B C16B C18B 108.0(13) . .
C17B C16B C18B 112.3(12) . .
C15B C16B C14B 106.6(12) . .
C17B C16B C14B 110.3(13) . .
C18B C16B C14B 109.3(11) . .
O14C C16C C17C 107.9(9) . .
O14C C16C H16A 110.1 . .
C17C C16C H16A 110.1 . .
O14C C16C H16B 110.1 . .
C17C C16C H16B 110.1 . .
H16A C16C H16B 108.4 . .
O13A C17A C44A 113.5(13) . .
O13A C17A H17A 108.9 . .
C44A C17A H17A 108.9 . .
O13A C17A H17B 108.9 . .
C44A C17A H17B 108.9 . .
H17A C17A H17B 107.7 . .
C16B C17B H17C 109.5 . .
C16B C17B H17D 109.5 . .
H17C C17B H17D 109.5 . .
C16B C17B H17E 109.5 . .
H17C C17B H17E 109.5 . .
H17D C17B H17E 109.5 . .
C15C C17C C16C 110.4(11) . .
C15C C17C C19C 109.2(13) . .
C16C C17C C19C 108.0(11) . .
C15C C17C C18C 109.7(12) . .
C16C C17C C18C 110.7(12) . .
C19C C17C C18C 108.8(11) . .
O8A C18A C20A 113.2(12) . .
O8A C18A H18D 108.9 . .
C20A C18A H18D 108.9 . .
O8A C18A H18E 108.9 . .
C20A C18A H18E 108.9 . .
H18D C18A H18E 107.8 . .
C16B C18B H18A 109.5 . .
C16B C18B H18B 109.5 . .
H18A C18B H18B 109.5 . .
C16B C18B H18C 109.5 . .
H18A C18B H18C 109.5 . .
H18B C18B H18C 109.5 . .
C17C C18C H18F 109.5 . .
C17C C18C H18G 109.5 . .
H18F C18C H18G 109.5 . .
C17C C18C H18H 109.5 . .
H18F C18C H18H 109.5 . .
H18G C18C H18H 109.5 . .
O7A C19A C20A 110.2(10) . .
O7A C19A H19A 109.6 . .
C20A C19A H19A 109.6 . .
O7A C19A H19B 109.6 . .
C20A C19A H19B 109.6 . .
H19A C19A H19B 108.1 . .
C20B C19B P5B 120.5(10) . .
C20B C19B P6B 119.9(9) . .
P5B C19B P6B 119.2(7) . .
C17C C19C H19C 109.5 . .
C17C C19C H19D 109.5 . .
H19C C19C H19D 109.5 . .
C17C C19C H19E 109.5 . .
H19C C19C H19E 109.5 . .
H19D C19C H19E 109.5 . .
C18A C20A C22A 112.5(14) . .
C18A C20A C19A 105.5(13) . .
C22A C20A C19A 112.3(13) . .
C18A C20A C21A 105.9(14) . .
C22A C20A C21A 112.7(13) . .
C19A C20A C21A 107.5(12) . .
N2B C20B C19B 179.2(16) . .
C22C C20C O16C 112.9(11) . .
C22C C20C H20A 109.0 . .
O16C C20C H20A 109.0 . .
C22C C20C H20B 109.0 . .
O16C C20C H20B 109.0 . .
H20A C20C H20B 107.8 . .
C20A C21A H21C 109.5 . .
C20A C21A H21D 109.5 . .
H21C C21A H21D 109.5 . .
C20A C21A H21E 109.5 . .
H21C C21A H21E 109.5 . .
H21D C21A H21E 109.5 . .
O15B C21B C23B 112.2(10) . .
O15B C21B H21A 109.2 . .
C23B C21B H21A 109.2 . .
O15B C21B H21B 109.2 . .
C23B C21B H21B 109.2 . .
H21A C21B H21B 107.9 . .
O15C C21C C22C 110.3(10) . .
O15C C21C H21F 109.6 . .
C22C C21C H21F 109.6 . .
O15C C21C H21G 109.6 . .
C22C C21C H21G 109.6 . .
H21F C21C H21G 108.1 . .
C20A C22A H22C 109.5 . .
C20A C22A H22D 109.5 . .
H22C C22A H22D 109.5 . .
C20A C22A H22E 109.5 . .
H22C C22A H22E 109.5 . .
H22D C22A H22E 109.5 . .
O16B C22B C23B 109.7(10) . .
O16B C22B H22A 109.7 . .
C23B C22B H22A 109.7 . .
O16B C22B H22B 109.7 . .
C23B C22B H22B 109.7 . .
H22A C22B H22B 108.2 . .
C20C C22C C24C 111.4(13) . .
C20C C22C C21C 108.3(12) . .
C24C C22C C21C 109.7(12) . .
C20C C22C C23C 106.5(13) . .
C24C C22C C23C 114.1(13) . .
C21C C22C C23C 106.5(12) . .
N2A C23A C40A 174(2) . .
C21B C23B C22B 107.1(12) . .
C21B C23B C25B 107.6(13) . .
C22B C23B C25B 105.8(11) . .
C21B C23B C24B 114.6(11) . .
C22B C23B C24B 111.7(12) . .
C25B C23B C24B 109.6(12) . .
C22C C23C H23A 109.5 . .
C22C C23C H23B 109.5 . .
H23A C23C H23B 109.5 . .
C22C C23C H23C 109.5 . .
H23A C23C H23C 109.5 . .
H23B C23C H23C 109.5 . .
O10A C24A C26A 110.5(10) . .
O10A C24A H24A 109.6 . .
C26A C24A H24A 109.6 . .
O10A C24A H24B 109.6 . .
C26A C24A H24B 109.6 . .
H24A C24A H24B 108.1 . .
C23B C24B H24F 109.5 . .
C23B C24B H24G 109.5 . .
H24F C24B H24G 109.5 . .
C23B C24B H24H 109.5 . .
H24F C24B H24H 109.5 . .
H24G C24B H24H 109.5 . .
C22C C24C H24C 109.5 . .
C22C C24C H24D 109.5 . .
H24C C24C H24D 109.5 . .
C22C C24C H24E 109.5 . .
H24C C24C H24E 109.5 . .
H24D C24C H24E 109.5 . .
O9A C25A C26A 114.1(11) . .
O9A C25A H25F 108.7 . .
C26A C25A H25F 108.7 . .
O9A C25A H25G 108.7 . .
C26A C25A H25G 108.7 . .
H25F C25A H25G 107.6 . .
C23B C25B H25C 109.5 . .
C23B C25B H25D 109.5 . .
H25C C25B H25D 109.5 . .
C23B C25B H25E 109.5 . .
H25C C25B H25E 109.5 . .
H25D C25B H25E 109.5 . .
C27C C25C O9C 112.5(11) . .
C27C C25C H25A 109.1 . .
O9C C25C H25A 109.1 . .
C27C C25C H25B 109.1 . .
O9C C25C H25B 109.1 . .
H25A C25C H25B 107.8 . .
C25A C26A C24A 107.3(11) . .
C25A C26A C27A 112.2(12) . .
C24A C26A C27A 110.0(12) . .
C25A C26A C28A 109.8(12) . .
C24A C26A C28A 108.7(11) . .
C27A C26A C28A 108.8(12) . .
O14B C26B C50B 113.4(12) . .
O14B C26B H26C 108.9 . .
C50B C26B H26C 108.9 . .
O14B C26B H26D 108.9 . .
C50B C26B H26D 108.9 . .
H26C C26B H26D 107.7 . .
O10C C26C C27C 111.5(10) . .
O10C C26C H26A 109.3 . .
C27C C26C H26A 109.3 . .
O10C C26C H26B 109.3 . .
C27C C26C H26B 109.3 . .
H26A C26C H26B 108.0 . .
C26A C27A H27C 109.5 . .
C26A C27A H27D 109.5 . .
H27C C27A H27D 109.5 . .
C26A C27A H27E 109.5 . .
H27C C27A H27E 109.5 . .
H27D C27A H27E 109.5 . .
C50B C27B O13B 112.4(12) . .
C50B C27B H27A 109.1 . .
O13B C27B H27A 109.1 . .
C50B C27B H27B 109.1 . .
O13B C27B H27B 109.1 . .
H27A C27B H27B 107.9 . .
C25C C27C C26C 108.8(12) . .
C25C C27C C30C 111.7(12) . .
C26C C27C C30C 108.3(14) . .
C25C C27C C28C 106.4(14) . .
C26C C27C C28C 109.7(12) . .
C30C C27C C28C 111.9(12) . .
C26A C28A H28D 109.5 . .
C26A C28A H28E 109.5 . .
H28D C28A H28E 109.5 . .
C26A C28A H28F 109.5 . .
H28D C28A H28F 109.5 . .
H28E C28A H28F 109.5 . .
C27C C28C H28A 109.5 . .
C27C C28C H28B 109.5 . .
H28A C28C H28B 109.5 . .
C27C C28C H28C 109.5 . .
H28A C28C H28C 109.5 . .
H28B C28C H28C 109.5 . .
C27C C30C H30A 109.5 . .
C27C C30C H30B 109.5 . .
H30A C30C H30B 109.5 . .
C27C C30C H30C 109.5 . .
H30A C30C H30C 109.5 . .
H30B C30C H30C 109.5 . .
O8C C31C C33C 112.2(11) . .
O8C C31C H31A 109.2 . .
C33C C31C H31A 109.2 . .
O8C C31C H31B 109.2 . .
C33C C31C H31B 109.2 . .
H31A C31C H31B 107.9 . .
O7C C32C C33C 111.3(11) . .
O7C C32C H32A 109.4 . .
C33C C32C H32A 109.4 . .
O7C C32C H32B 109.4 . .
C33C C32C H32B 109.4 . .
H32A C32C H32B 108.0 . .
C32C C33C C34C 109.9(13) . .
C32C C33C C35C 110.3(12) . .
C34C C33C C35C 112.1(12) . .
C32C C33C C31C 108.9(11) . .
C34C C33C C31C 109.0(12) . .
C35C C33C C31C 106.5(13) . .
C33C C34C H34A 109.5 . .
C33C C34C H34B 109.5 . .
H34A C34C H34B 109.5 . .
C33C C34C H34C 109.5 . .
H34A C34C H34C 109.5 . .
H34B C34C H34C 109.5 . .
C33C C35C H35A 109.5 . .
C33C C35C H35B 109.5 . .
H35A C35C H35B 109.5 . .
C33C C35C H35C 109.5 . .
H35A C35C H35C 109.5 . .
H35B C35C H35C 109.5 . .
C37C C36C P2C 120.1(9) . .
C37C C36C P1C 119.3(9) . .
P2C C36C P1C 120.6(6) . .
N2C C37C C36C 176.0(16) . .
C23A C40A P6A 120.7(12) . .
C23A C40A P5A 117.1(13) . .
P6A C40A P5A 122.1(9) . .
C41B C40B P4B 121.3(11) . .
C41B C40B P3B 116.5(10) . .
P4B C40B P3B 121.1(8) . .
C42A C41A C8A 109.0(13) . .
C42A C41A C43A 112.9(13) . .
C8A C41A C43A 111.6(12) . .
C42A C41A C48A 108.0(12) . .
C8A C41A C48A 108.3(13) . .
C43A C41A C48A 106.9(12) . .
N3B C41B C40B 175.6(14) . .
C41A C42A O18A 109.5(11) . .
C41A C42A H42C 109.8 . .
O18A C42A H42C 109.8 . .
C41A C42A H42D 109.8 . .
O18A C42A H42D 109.8 . .
H42C C42A H42D 108.2 . .
O17B C42B C55B 111.0(11) . .
O17B C42B H42A 109.4 . .
C55B C42B H42A 109.4 . .
O17B C42B H42B 109.4 . .
C55B C42B H42B 109.4 . .
H42A C42B H42B 108.0 . .
C41A C43A H43A 109.5 . .
C41A C43A H43B 109.5 . .
H43A C43A H43B 109.5 . .
C41A C43A H43C 109.5 . .
H43A C43A H43C 109.5 . .
H43B C43A H43C 109.5 . .
C16A C44A C17A 109.4(14) . .
C16A C44A C46A 112.1(14) . .
C17A C44A C46A 105.4(16) . .
C16A C44A C45A 108.2(16) . .
C17A C44A C45A 110.2(15) . .
C46A C44A C45A 111.6(13) . .
C44A C45A H45A 109.5 . .
C44A C45A H45B 109.5 . .
H45A C45A H45B 109.5 . .
C44A C45A H45C 109.5 . .
H45A C45A H45C 109.5 . .
H45B C45A H45C 109.5 . .
C44A C46A H46A 109.5 . .
C44A C46A H46B 109.5 . .
H46A C46A H46B 109.5 . .
C44A C46A H46C 109.5 . .
H46A C46A H46C 109.5 . .
H46B C46A H46C 109.5 . .
C41A C48A H48A 109.5 . .
C41A C48A H48B 109.5 . .
H48A C48A H48B 109.5 . .
C41A C48A H48C 109.5 . .
H48A C48A H48C 109.5 . .
H48B C48A H48C 109.5 . .
C27B C50B C51B 110.5(17) . .
C27B C50B C52B 111.0(13) . .
C51B C50B C52B 111.0(14) . .
C27B C50B C26B 108.0(14) . .
C51B C50B C26B 110.2(13) . .
C52B C50B C26B 106.0(16) . .
C50B C51B H51A 109.5 . .
C50B C51B H51B 109.5 . .
H51A C51B H51B 109.5 . .
C50B C51B H51C 109.5 . .
H51A C51B H51C 109.5 . .
H51B C51B H51C 109.5 . .
C50B C52B H52A 109.5 . .
C50B C52B H52B 109.5 . .
H52A C52B H52B 109.5 . .
C50B C52B H52C 109.5 . .
H52A C52B H52C 109.5 . .
H52B C52B H52C 109.5 . .
O18B C53B C55B 111.1(11) . .
O18B C53B H53A 109.4 . .
C55B C53B H53A 109.4 . .
O18B C53B H53B 109.4 . .
C55B C53B H53B 109.4 . .
H53A C53B H53B 108.0 . .
C42B C55B C57B 113.1(14) . .
C42B C55B C56B 111.4(13) . .
C57B C55B C56B 111.3(13) . .
C42B C55B C53B 107.6(12) . .
C57B C55B C53B 107.8(13) . .
C56B C55B C53B 105.1(14) . .
C55B C56B H56A 109.5 . .
C55B C56B H56B 109.5 . .
H56A C56B H56B 109.5 . .
C55B C56B H56C 109.5 . .
H56A C56B H56C 109.5 . .
H56B C56B H56C 109.5 . .
C55B C57B H57A 109.5 . .
C55B C57B H57B 109.5 . .
H57A C57B H57B 109.5 . .
C55B C57B H57C 109.5 . .
H57A C57B H57C 109.5 . .
H57B C57B H57C 109.5 . .
N1C Ag1 N1A 125.4(4) . .
N1C Ag1 N1B 124.5(4) . .
N1A Ag1 N1B 110.1(4) . .
N3A Ag2 N2B 155.0(4) 1_565 .
N3A Ag2 O2W 74.8(8) 1_565 .
N2B Ag2 O2W 128.2(8) . .
N2C Ag3 N3C 156.0(4) . 2
N2C Ag3 O32W 80.6(11) . .
N3C Ag3 O32W 121.9(11) 2 .
N2C Ag3 O31W 130.2(13) . .
N3C Ag3 O31W 72.4(12) 2 .
O32W Ag3 O31W 49.7(16) . .
N2C Ag3 O3W 103.5(5) . .
N3C Ag3 O3W 100.4(5) 2 .
O32W Ag3 O3W 32.2(11) . .
O31W Ag3 O3W 35.2(11) . .
O1A FeA O3A 89.7(4) . .
O1A FeA O4A 88.6(4) . .
O3A FeA O4A 88.7(4) . .
O1A FeA O5A 90.8(3) . .
O3A FeA O5A 177.2(4) . .
O4A FeA O5A 88.6(3) . .
O1A FeA O6A 177.3(4) . .
O3A FeA O6A 91.8(4) . .
O4A FeA O6A 93.7(3) . .
O5A FeA O6A 87.8(3) . .
O1A FeA O2A 87.4(3) . .
O3A FeA O2A 88.5(4) . .
O4A FeA O2A 175.2(3) . .
O5A FeA O2A 94.2(3) . .
O6A FeA O2A 90.4(3) . .
O2B FeB O5B 178.0(4) . .
O2B FeB O1B 89.0(3) . .
O5B FeB O1B 89.2(3) . .
O2B FeB O6B 90.9(3) . .
O5B FeB O6B 88.5(3) . .
O1B FeB O6B 92.8(3) . .
O2B FeB O3B 89.0(4) . .
O5B FeB O3B 91.8(3) . .
O1B FeB O3B 90.4(3) . .
O6B FeB O3B 176.8(3) . .
O2B FeB O4B 87.6(3) . .
O5B FeB O4B 94.3(3) . .
O1B FeB O4B 176.3(3) . .
O6B FeB O4B 88.5(3) . .
O3B FeB O4B 88.3(3) . .
O5C FeC O1C 178.7(3) . .
O5C FeC O6C 88.1(3) . .
O1C FeC O6C 90.6(3) . .
O5C FeC O4C 88.8(3) . .
O1C FeC O4C 91.0(3) . .
O6C FeC O4C 91.3(3) . .
O5C FeC O2C 91.4(3) . .
O1C FeC O2C 88.9(3) . .
O6C FeC O2C 91.7(3) . .
O4C FeC O2C 177.0(3) . .
O5C FeC O3C 88.9(3) . .
O1C FeC O3C 92.3(3) . .
O6C FeC O3C 176.7(3) . .
O4C FeC O3C 87.3(3) . .
O2C FeC O3C 89.7(3) . .
C7A N1A Ag1 178.0(10) . .
C2B N1B Ag1 177.1(12) . .
C1C N1C Ag1 176.0(12) . .
C20B N2B Ag2 170.9(11) . .
C37C N2C Ag3 164.9(12) . .
C10A N3A Ag2 162.2(12) . 1_545
C14C N3C Ag3 168.4(12) . 2_545
P4A O1A FeA 141.3(5) . .
P3B O1B FeB 133.6(5) . .
P5C O1C FeC 135.5(5) . .
P3A O2A FeA 135.2(5) . .
P4B O2B FeB 140.3(5) . .
P6C O2C FeC 136.7(5) . .
P5A O3A FeA 139.5(6) . .
P6B O3B FeB 141.0(5) . .
P4C O3C FeC 135.1(5) . .
P6A O4A FeA 133.6(5) . .
P5B O4B FeB 133.1(5) . .
P3C O4C FeC 141.3(5) . .
P2A O5A FeA 136.3(5) . .
P2B O5B FeB 137.0(5) . .
P2C O5C FeC 140.0(5) . .
P1A O6A FeA 138.3(5) . .
P1B O6B FeB 137.9(5) . .
P1C O6C FeC 136.9(5) . .
C19A O7A P5A 117.9(8) . .
C4B O7B P2B 119.4(8) . .
C32C O7C P1C 117.6(8) . .
C18A O8A P5A 117.3(8) . .
C3B O8B P2B 121.8(7) . .
C31C O8C P1C 116.3(7) . .
C25A O9A P6A 117.3(9) . .
C10B O9B P1B 120.0(8) . .
C25C O9C P2C 117.4(7) . .
C24A O10A P6A 116.6(8) . .
C9B O10B P1B 119.3(8) . .
C26C O10C P2C 116.3(8) . .
C3A O11A P1A 119.0(8) . .
C15B O11B P5B 116.0(7) . .
C3C O11C P5C 119.4(7) . .
C2A O12A P1A 120.1(8) . .
C14B O12B P5B 117.5(8) . .
C4C O12C P5C 119.6(7) . .
C17A O13A P4A 117.6(8) . .
C27B O13B P6B 116.9(9) . .
C15C O13C P4C 114.0(7) . .
C16A O14A P4A 115.6(9) . .
C26B O14B P6B 116.8(8) . .
C16C O14C P4C 117.0(7) . .
C12A O15A P3A 117.0(8) . .
C21B O15B P3B 116.9(7) . .
C21C O15C P3C 117.1(8) . .
C11A O16A P3A 117.3(8) . .
C22B O16B P3B 117.5(8) . .
C20C O16C P3C 117.1(8) . .
C8A O17A P2A 119.7(8) . .
C42B O17B P4B 116.0(8) . .
C8C O17C P6C 120.1(7) . .
C42A O18A P2A 119.5(8) . .
C53B O18B P4B 118.2(8) . .
C9C O18C P6C 118.6(8) . .
O6A P1A O11A 112.6(5) . .
O6A P1A O12A 110.9(5) . .
O11A P1A O12A 105.6(5) . .
O6A P1A C1A 113.2(5) . .
O11A P1A C1A 106.9(5) . .
O12A P1A C1A 107.2(5) . .
O6B P1B O10B 112.2(5) . .
O6B P1B O9B 111.8(5) . .
O10B P1B O9B 105.1(5) . .
O6B P1B C1B 112.3(6) . .
O10B P1B C1B 106.6(6) . .
O9B P1B C1B 108.4(6) . .
O6C P1C O8C 111.0(5) . .
O6C P1C O7C 110.1(5) . .
O8C P1C O7C 104.4(4) . .
O6C P1C C36C 113.5(5) . .
O8C P1C C36C 108.0(5) . .
O7C P1C C36C 109.6(5) . .
O5A P2A O17A 112.3(5) . .
O5A P2A O18A 111.4(5) . .
O17A P2A O18A 103.8(5) . .
O5A P2A C1A 111.9(6) . .
O17A P2A C1A 107.7(6) . .
O18A P2A C1A 109.3(5) . .
O5B P2B O8B 112.2(5) . .
O5B P2B O7B 112.9(5) . .
O8B P2B O7B 104.5(5) . .
O5B P2B C1B 112.4(6) . .
O8B P2B C1B 107.6(5) . .
O7B P2B C1B 106.7(6) . .
O5C P2C O9C 111.1(5) . .
O5C P2C O10C 110.9(5) . .
O9C P2C O10C 104.8(5) . .
O5C P2C C36C 114.8(5) . .
O9C P2C C36C 106.3(5) . .
O10C P2C C36C 108.2(5) . .
O2A P3A O16A 111.5(5) . .
O2A P3A O15A 110.4(5) . .
O16A P3A O15A 104.4(5) . .
O2A P3A C9A 113.5(5) . .
O16A P3A C9A 107.7(6) . .
O15A P3A C9A 108.9(5) . .
O1B P3B O15B 111.2(5) . .
O1B P3B O16B 112.7(5) . .
O15B P3B O16B 103.9(5) . .
O1B P3B C40B 112.6(6) . .
O15B P3B C40B 107.3(6) . .
O16B P3B C40B 108.7(6) . .
O4C P3C O16C 111.4(5) . .
O4C P3C O15C 111.9(5) . .
O16C P3C O15C 104.6(5) . .
O4C P3C C13C 112.8(5) . .
O16C P3C C13C 108.5(5) . .
O15C P3C C13C 107.3(5) . .
O1A P4A O14A 109.7(5) . .
O1A P4A O13A 112.4(5) . .
O14A P4A O13A 105.6(5) . .
O1A P4A C9A 113.2(6) . .
O14A P4A C9A 108.1(6) . .
O13A P4A C9A 107.4(5) . .
O2B P4B O18B 112.6(5) . .
O2B P4B O17B 110.2(5) . .
O18B P4B O17B 105.1(5) . .
O2B P4B C40B 113.6(6) . .
O18B P4B C40B 106.8(6) . .
O17B P4B C40B 108.0(6) . .
O3C P4C O13C 110.7(5) . .
O3C P4C O14C 111.0(5) . .
O13C P4C O14C 105.4(4) . .
O3C P4C C13C 113.8(5) . .
O13C P4C C13C 105.3(5) . .
O14C P4C C13C 110.1(5) . .
O3A P5A O7A 110.6(5) . .
O3A P5A O8A 112.1(5) . .
O7A P5A O8A 104.1(5) . .
O3A P5A C40A 112.8(6) . .
O7A P5A C40A 109.6(6) . .
O8A P5A C40A 107.3(6) . .
O4B P5B O11B 111.2(5) . .
O4B P5B O12B 112.1(5) . .
O11B P5B O12B 104.0(5) . .
O4B P5B C19B 114.2(5) . .
O11B P5B C19B 106.1(5) . .
O12B P5B C19B 108.5(5) . .
O1C P5C O12C 111.8(5) . .
O1C P5C O11C 112.0(5) . .
O12C P5C O11C 105.4(4) . .
O1C P5C C2C 113.1(5) . .
O12C P5C C2C 106.9(5) . .
O11C P5C C2C 107.3(5) . .
O4A P6A O9A 111.0(5) . .
O4A P6A O10A 111.6(5) . .
O9A P6A O10A 103.6(5) . .
O4A P6A C40A 113.7(6) . .
O9A P6A C40A 107.4(6) . .
O10A P6A C40A 109.1(6) . .
O3B P6B O13B 110.4(5) . .
O3B P6B O14B 111.8(5) . .
O13B P6B O14B 104.5(5) . .
O3B P6B C19B 113.8(5) . .
O13B P6B C19B 107.9(5) . .
O14B P6B C19B 107.9(5) . .
O2C P6C O18C 111.6(5) . .
O2C P6C O17C 111.6(5) . .
O18C P6C O17C 104.0(4) . .
O2C P6C C2C 113.5(5) . .
O18C P6C C2C 106.2(6) . .
O17C P6C C2C 109.5(5) . .
O3P Cl1 O4P 109.0(6) . .
O3P Cl1 O1P 109.7(7) . .
O4P Cl1 O1P 110.2(8) . .
O3P Cl1 O2P 109.8(7) . .
O4P Cl1 O2P 108.9(7) . .
O1P Cl1 O2P 109.2(6) . .
O5P Cl2 O12P 113.5(10) . .
O5P Cl2 O11P 107.8(7) . .
O12P Cl2 O11P 111.8(9) . .
O5P Cl2 O6P 107.7(8) . .
O12P Cl2 O6P 107.8(8) . .
O11P Cl2 O6P 107.9(8) . .
O10P Cl3 O7P 108.5(7) . .
O10P Cl3 O8P 112.7(8) . .
O7P Cl3 O8P 109.5(7) . .
O10P Cl3 O9P 108.2(7) . .
O7P Cl3 O9P 109.2(7) . .
O8P Cl3 O9P 108.7(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
O2W O21W 1.41(3) .
O2W Ag2 2.37(3) .
O3W O32W 1.39(4) .
O3W O31W 1.53(5) .
O3W Ag3 2.596(15) .
O31W Ag3 2.43(5) .
O32W Ag3 2.28(4) .
C1A C7A 1.398(16) .
C1A P1A 1.715(13) .
C1A P2A 1.723(12) .
C1B C2B 1.382(18) .
C1B P2B 1.716(14) .
C1B P1B 1.739(14) .
C1C N1C 1.124(15) .
C1C C2C 1.412(17) .
C2A O12A 1.466(14) .
C2A C4A 1.519(18) .
C2A H2A1 0.9700 .
C2A H2A2 0.9700 .
C2B N1B 1.163(15) .
C2C P6C 1.709(12) .
C2C P5C 1.742(12) .
C3A O11A 1.473(14) .
C3A C4A 1.513(19) .
C3A H3A1 0.9700 .
C3A H3A2 0.9700 .
C3B O8B 1.499(13) .
C3B C6B 1.518(17) .
C3B H3B1 0.9700 .
C3B H3B2 0.9700 .
C3C O11C 1.476(13) .
C3C C5C 1.537(18) .
C3C H3C1 0.9700 .
C3C H3C2 0.9700 .
C4A C5A 1.517(18) .
C4A C6A 1.535(18) .
C4B C6B 1.475(17) .
C4B O7B 1.484(14) .
C4B H4B1 0.9700 .
C4B H4B2 0.9700 .
C4C O12C 1.484(12) .
C4C C5C 1.518(17) .
C4C H4C1 0.9700 .
C4C H4C2 0.9700 .
C5A H5A1 0.9600 .
C5A H5A2 0.9600 .
C5A H5A3 0.9600 .
C5C C6C 1.510(17) .
C5C C7C 1.514(18) .
C6A H6A1 0.9600 .
C6A H6A2 0.9600 .
C6A H6A3 0.9600 .
C6B C8B 1.525(18) .
C6B C7B 1.544(16) .
C6C H6C1 0.9600 .
C6C H6C2 0.9600 .
C6C H6C3 0.9600 .
C7A N1A 1.156(15) .
C7B H7B1 0.9600 .
C7B H7B2 0.9600 .
C7B H7B3 0.9600 .
C7C H7C1 0.9600 .
C7C H7C2 0.9600 .
C7C H7C3 0.9600 .
C8A C41A 1.502(19) .
C8A O17A 1.510(15) .
C8A H8A1 0.9700 .
C8A H8A2 0.9700 .
C8B H8B1 0.9600 .
C8B H8B2 0.9600 .
C8B H8B3 0.9600 .
C8C O17C 1.463(13) .
C8C C10C 1.539(17) .
C8C H8C1 0.9700 .
C8C H8C2 0.9700 .
C9A C10A 1.403(18) .
C9A P3A 1.701(12) .
C9A P4A 1.728(13) .
C9B O10B 1.494(15) .
C9B C11B 1.54(2) .
C9B H9B1 0.9700 .
C9B H9B2 0.9700 .
C9C C10C 1.475(19) .
C9C O18C 1.486(15) .
C9C H9C1 0.9700 .
C9C H9C2 0.9700 .
C10A N3A 1.187(16) .
C10B O9B 1.513(13) .
C10B C11B 1.522(18) .
C10B H10A 0.9700 .
C10B H10B 0.9700 .
C10C C11C 1.504(19) .
C10C C12C 1.554(19) .
C11A O16A 1.481(15) .
C11A C13A 1.53(2) .
C11A H11D 0.9700 .
C11A H11E 0.9700 .
C11B C12B 1.519(19) .
C11B C13B 1.579(18) .
C11C H11A 0.9600 .
C11C H11B 0.9600 .
C11C H11C 0.9600 .
C12A O15A 1.490(13) .
C12A C13A 1.519(19) .
C12A H12A 0.9700 .
C12A H12B 0.9700 .
C12B H12F 0.9600 .
C12B H12G 0.9600 .
C12B H12H 0.9600 .
C12C H12C 0.9600 .
C12C H12D 0.9600 .
C12C H12E 0.9600 .
C13A C14A 1.52(2) .
C13A C15A 1.595(19) .
C13B H13A 0.9600 .
C13B H13B 0.9600 .
C13B H13C 0.9600 .
C13C C14C 1.446(17) .
C13C P4C 1.706(11) .
C13C P3C 1.743(11) .
C14A H14C 0.9600 .
C14A H14D 0.9600 .
C14A H14E 0.9600 .
C14B O12B 1.442(13) .
C14B C16B 1.546(18) .
C14B H14A 0.9700 .
C14B H14B 0.9700 .
C14C N3C 1.102(15) .
C15A H15E 0.9600 .
C15A H15F 0.9600 .
C15A H15G 0.9600 .
C15B O11B 1.466(14) .
C15B C16B 1.493(19) .
C15B H15C 0.9700 .
C15B H15D 0.9700 .
C15C C17C 1.460(18) .
C15C O13C 1.466(13) .
C15C H15A 0.9700 .
C15C H15B 0.9700 .
C16A C44A 1.46(2) .
C16A O14A 1.480(14) .
C16A H16C 0.9700 .
C16A H16D 0.9700 .
C16B C17B 1.526(19) .
C16B C18B 1.537(17) .
C16C O14C 1.487(13) .
C16C C17C 1.545(17) .
C16C H16A 0.9700 .
C16C H16B 0.9700 .
C17A O13A 1.481(15) .
C17A C44A 1.49(2) .
C17A H17A 0.9700 .
C17A H17B 0.9700 .
C17B H17C 0.9600 .
C17B H17D 0.9600 .
C17B H17E 0.9600 .
C17C C19C 1.555(17) .
C17C C18C 1.587(18) .
C18A O8A 1.471(16) .
C18A C20A 1.50(2) .
C18A H18D 0.9700 .
C18A H18E 0.9700 .
C18B H18A 0.9600 .
C18B H18B 0.9600 .
C18B H18C 0.9600 .
C18C H18F 0.9600 .
C18C H18G 0.9600 .
C18C H18H 0.9600 .
C19A O7A 1.464(13) .
C19A C20A 1.515(18) .
C19A H19A 0.9700 .
C19A H19B 0.9700 .
C19B C20B 1.400(17) .
C19B P5B 1.720(12) .
C19B P6B 1.730(13) .
C19C H19C 0.9600 .
C19C H19D 0.9600 .
C19C H19E 0.9600 .
C20A C22A 1.513(19) .
C20A C21A 1.548(19) .
C20B N2B 1.142(15) .
C20C C22C 1.479(19) .
C20C O16C 1.492(14) .
C20C H20A 0.9700 .
C20C H20B 0.9700 .
C21A H21C 0.9600 .
C21A H21D 0.9600 .
C21A H21E 0.9600 .
C21B O15B 1.476(14) .
C21B C23B 1.505(19) .
C21B H21A 0.9700 .
C21B H21B 0.9700 .
C21C O15C 1.494(13) .
C21C C22C 1.529(18) .
C21C H21F 0.9700 .
C21C H21G 0.9700 .
C22A H22C 0.9600 .
C22A H22D 0.9600 .
C22A H22E 0.9600 .
C22B O16B 1.490(13) .
C22B C23B 1.513(17) .
C22B H22A 0.9700 .
C22B H22B 0.9700 .
C22C C24C 1.525(19) .
C22C C23C 1.556(18) .
C23A N2A 1.21(2) .
C23A C40A 1.35(2) .
C23B C25B 1.525(17) .
C23B C24B 1.531(18) .
C23C H23A 0.9600 .
C23C H23B 0.9600 .
C23C H23C 0.9600 .
C24A O10A 1.469(13) .
C24A C26A 1.521(17) .
C24A H24A 0.9700 .
C24A H24B 0.9700 .
C24B H24F 0.9600 .
C24B H24G 0.9600 .
C24B H24H 0.9600 .
C24C H24C 0.9600 .
C24C H24D 0.9600 .
C24C H24E 0.9600 .
C25A O9A 1.445(15) .
C25A C26A 1.483(18) .
C25A H25F 0.9700 .
C25A H25G 0.9700 .
C25B H25C 0.9600 .
C25B H25D 0.9600 .
C25B H25E 0.9600 .
C25C C27C 1.461(19) .
C25C O9C 1.502(14) .
C25C H25A 0.9700 .
C25C H25B 0.9700 .
C26A C27A 1.542(18) .
C26A C28A 1.555(18) .
C26B O14B 1.470(15) .
C26B C50B 1.54(2) .
C26B H26C 0.9700 .
C26B H26D 0.9700 .
C26C O10C 1.465(14) .
C26C C27C 1.509(19) .
C26C H26A 0.9700 .
C26C H26B 0.9700 .
C27A H27C 0.9600 .
C27A H27D 0.9600 .
C27A H27E 0.9600 .
C27B C50B 1.45(2) .
C27B O13B 1.464(15) .
C27B H27A 0.9700 .
C27B H27B 0.9700 .
C27C C30C 1.531(19) .
C27C C28C 1.561(19) .
C28A H28D 0.9600 .
C28A H28E 0.9600 .
C28A H28F 0.9600 .
C28C H28A 0.9600 .
C28C H28B 0.9600 .
C28C H28C 0.9600 .
C30C H30A 0.9600 .
C30C H30B 0.9600 .
C30C H30C 0.9600 .
C31C O8C 1.424(14) .
C31C C33C 1.555(19) .
C31C H31A 0.9700 .
C31C H31B 0.9700 .
C32C O7C 1.464(13) .
C32C C33C 1.492(18) .
C32C H32A 0.9700 .
C32C H32B 0.9700 .
C33C C34C 1.543(19) .
C33C C35C 1.553(18) .
C34C H34A 0.9600 .
C34C H34B 0.9600 .
C34C H34C 0.9600 .
C35C H35A 0.9600 .
C35C H35B 0.9600 .
C35C H35C 0.9600 .
C36C C37C 1.421(16) .
C36C P2C 1.688(12) .
C36C P1C 1.749(12) .
C37C N2C 1.141(14) .
C40A P6A 1.684(15) .
C40A P5A 1.704(13) .
C40B C41B 1.384(19) .
C40B P4B 1.684(13) .
C40B P3B 1.720(13) .
C41A C42A 1.483(18) .
C41A C43A 1.541(19) .
C41A C48A 1.578(18) .
C41B N3B 1.219(18) .
C42A O18A 1.489(13) .
C42A H42C 0.9700 .
C42A H42D 0.9700 .
C42B O17B 1.465(14) .
C42B C55B 1.481(19) .
C42B H42A 0.9700 .
C42B H42B 0.9700 .
C43A H43A 0.9600 .
C43A H43B 0.9600 .
C43A H43C 0.9600 .
C44A C46A 1.55(2) .
C44A C45A 1.58(2) .
C45A H45A 0.9600 .
C45A H45B 0.9600 .
C45A H45C 0.9600 .
C46A H46A 0.9600 .
C46A H46B 0.9600 .
C46A H46C 0.9600 .
C48A H48A 0.9600 .
C48A H48B 0.9600 .
C48A H48C 0.9600 .
C50B C51B 1.50(2) .
C50B C52B 1.516(19) .
C51B H51A 0.9600 .
C51B H51B 0.9600 .
C51B H51C 0.9600 .
C52B H52A 0.9600 .
C52B H52B 0.9600 .
C52B H52C 0.9600 .
C53B O18B 1.509(16) .
C53B C55B 1.55(2) .
C53B H53A 0.9700 .
C53B H53B 0.9700 .
C55B C57B 1.53(2) .
C55B C56B 1.537(19) .
C56B H56A 0.9600 .
C56B H56B 0.9600 .
C56B H56C 0.9600 .
C57B H57A 0.9600 .
C57B H57B 0.9600 .
C57B H57C 0.9600 .
Ag1 N1C 2.205(11) .
Ag1 N1A 2.214(13) .
Ag1 N1B 2.233(13) .
Ag2 N3A 2.139(12) 1_565
Ag2 N2B 2.150(11) .
Ag3 N2C 2.116(10) .
Ag3 N3C 2.129(12) 2
FeA O1A 1.982(8) .
FeA O3A 1.987(9) .
FeA O4A 1.995(8) .
FeA O5A 1.998(8) .
FeA O6A 1.999(8) .
FeA O2A 2.012(8) .
FeB O2B 1.979(9) .
FeB O5B 1.980(8) .
FeB O1B 2.003(8) .
FeB O6B 2.003(8) .
FeB O3B 2.006(8) .
FeB O4B 2.010(8) .
FeC O5C 1.983(8) .
FeC O1C 1.986(8) .
FeC O6C 1.996(8) .
FeC O4C 2.004(8) .
FeC O2C 2.007(9) .
FeC O3C 2.016(8) .
N3A Ag2 2.139(12) 1_545
N3C Ag3 2.129(12) 2_545
O1A P4A 1.490(9) .
O1B P3B 1.499(8) .
O1C P5C 1.494(8) .
O2A P3A 1.487(9) .
O2B P4B 1.475(9) .
O2C P6C 1.469(9) .
O3A P5A 1.489(10) .
O3B P6B 1.478(8) .
O3C P4C 1.477(9) .
O4A P6A 1.496(9) .
O4B P5B 1.503(8) .
O4C P3C 1.484(8) .
O5A P2A 1.482(8) .
O5B P2B 1.504(9) .
O5C P2C 1.491(8) .
O6A P1A 1.487(9) .
O6B P1B 1.496(8) .
O6C P1C 1.490(8) .
O7A P5A 1.561(9) .
O7B P2B 1.571(9) .
O7C P1C 1.577(8) .
O8A P5A 1.573(9) .
O8B P2B 1.551(8) .
O8C P1C 1.563(9) .
O9A P6A 1.595(9) .
O9B P1B 1.572(8) .
O9C P2C 1.556(9) .
O10A P6A 1.600(9) .
O10B P1B 1.548(9) .
O10C P2C 1.579(8) .
O11A P1A 1.555(9) .
O11B P5B 1.566(8) .
O11C P5C 1.578(8) .
O12A P1A 1.563(8) .
O12B P5B 1.579(8) .
O12C P5C 1.572(8) .
O13A P4A 1.583(9) .
O13B P6B 1.565(8) .
O13C P4C 1.568(8) .
O14A P4A 1.568(9) .
O14B P6B 1.578(9) .
O14C P4C 1.574(8) .
O15A P3A 1.594(8) .
O15B P3B 1.585(8) .
O15C P3C 1.573(8) .
O16A P3A 1.572(9) .
O16B P3B 1.599(9) .
O16C P3C 1.568(9) .
O17A P2A 1.571(9) .
O17B P4B 1.576(9) .
O17C P6C 1.580(8) .
O18A P2A 1.593(8) .
O18B P4B 1.548(9) .
O18C P6C 1.568(9) .
Cl1 O3P 1.415(10) .
Cl1 O4P 1.419(10) .
Cl1 O1P 1.428(10) .
Cl1 O2P 1.439(10) .
Cl2 O5P 1.392(12) .
Cl2 O12P 1.406(12) .
Cl2 O11P 1.427(11) .
Cl2 O6P 1.451(12) .
O7P Cl3 1.421(10) .
O8P Cl3 1.424(11) .
Cl3 O10P 1.416(12) .
Cl3 O9P 1.443(11) .
