#------------------------------------------------------------------------------
#$Date: 2016-03-26 18:10:08 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180414 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/83/7208376.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7208376
loop_
_publ_author_name
'Liu, Guang-Zhen'
'Li, Xiao-Ling'
'Xin, Ling-Yun'
'Wang, Li-Ya'
_publ_section_title
;
 Two topologically new trinodal cobalt(ii) metal--organic frameworks
 characterized as a 1D metallic oxide and a 2D → 3D penetrated
 porous solid
;
_journal_issue                   16
_journal_name_full               CrystEngComm
_journal_page_first              5315
_journal_paper_doi               10.1039/c2ce25556a
_journal_volume                  14
_journal_year                    2012
_chemical_formula_sum            'C17 H15 Co2 N O12'
_chemical_formula_weight         543.16
_chemical_name_systematic
;

?

;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                106.544(3)
_cell_angle_beta                 96.596(3)
_cell_angle_gamma                99.562(3)
_cell_formula_units_Z            2
_cell_length_a                   7.830(2)
_cell_length_b                   10.912(3)
_cell_length_c                   12.498(4)
_cell_measurement_reflns_used    3215
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      0.00
_cell_measurement_theta_min      0.00
_cell_volume                     994.4(5)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0268
_diffrn_reflns_av_sigmaI/netI    0.0400
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            7470
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         2.68
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.736
_exptl_absorpt_correction_T_max  0.7807
_exptl_absorpt_correction_T_min  0.6908
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            pink
_exptl_crystal_density_diffrn    1.814
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             548
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.17
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.997
_refine_diff_density_min         -1.433
_refine_diff_density_rms         0.103
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     298
_refine_ls_number_reflns         3657
_refine_ls_number_restraints     26
_refine_ls_restrained_S_all      1.086
_refine_ls_R_factor_all          0.0575
_refine_ls_R_factor_gt           0.0477
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0787P)²+1.4778P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1324
_refine_ls_wR_factor_ref         0.1396
_reflns_number_gt                2994
_reflns_number_total             3657
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2ce25556a.txt
_cod_data_source_block           dd
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        994.5(5)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7208376
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C16 C 0.6143(17) 0.3812(13) 0.7835(9) 0.0783(16) Uani 0.580(9) 1 d PDU A 1
H16A H 0.7329 0.3962 0.8242 0.094 Uiso 0.580(9) 1 calc PR A 1
H16B H 0.5791 0.2886 0.7422 0.094 Uiso 0.580(9) 1 calc PR A 1
C17 C 0.4900(18) 0.4146(14) 0.8733(10) 0.0843(17) Uani 0.580(9) 1 d PDU A 1
H17A H 0.5041 0.3661 0.9257 0.127 Uiso 0.580(9) 1 calc PR A 1
H17B H 0.3701 0.3915 0.8353 0.127 Uiso 0.580(9) 1 calc PR A 1
H17C H 0.5201 0.5065 0.9136 0.127 Uiso 0.580(9) 1 calc PR A 1
C16' C 0.5635(19) 0.450(2) 0.8041(9) 0.0783(16) Uani 0.420(9) 1 d PD A 2
H16C H 0.4955 0.3622 0.7895 0.094 Uiso 0.420(9) 1 calc PR A 2
H16D H 0.4814 0.5078 0.8171 0.094 Uiso 0.420(9) 1 calc PR A 2
C17' C 0.683(2) 0.481(2) 0.9147(10) 0.0843(17) Uani 0.420(9) 1 d PD A 2
H17D H 0.7709 0.4293 0.9055 0.127 Uiso 0.420(9) 1 calc PR A 2
H17E H 0.6158 0.4625 0.9699 0.127 Uiso 0.420(9) 1 calc PR A 2
H17F H 0.7385 0.5723 0.9397 0.127 Uiso 0.420(9) 1 calc PR A 2
Co1 Co 0.86215(7) 0.51850(5) 0.40173(5) 0.02508(19) Uani 1 1 d . . .
Co2 Co 0.51596(7) 0.36557(5) 0.52034(5) 0.0286(2) Uani 1 1 d . . .
O1 O 0.9387(4) 0.3636(3) 0.4607(2) 0.0267(6) Uani 1 1 d . . .
O2 O 0.7021(4) 0.2529(3) 0.5028(3) 0.0419(9) Uani 1 1 d . . .
O3 O 0.6531(4) -0.2210(3) 0.4501(3) 0.0369(8) Uani 1 1 d . . .
O4 O 0.8344(4) -0.3257(3) 0.3490(3) 0.0349(7) Uani 1 1 d . . .
O5 O 1.5316(6) 0.0536(5) 0.2028(4) 0.0816(16) Uani 1 1 d . . .
O6 O 1.6150(6) -0.1115(6) 0.1113(5) 0.113(3) Uani 1 1 d . . .
O7 O 1.2774(4) -0.3774(3) -0.2491(3) 0.0379(8) Uani 1 1 d . . .
O8 O 0.9905(4) -0.4375(3) -0.2658(3) 0.0379(8) Uani 1 1 d . . .
O9 O 1.1926(4) 0.0122(3) 0.2182(3) 0.0381(8) Uani 1 1 d . . .
O10 O 0.6192(6) 0.4533(4) 0.7006(4) 0.0650(10) Uani 1 1 d DU . .
H10D H 0.7257 0.4935 0.7238 0.098 Uiso 1 1 d R A .
O11 O 0.6753(4) 0.5270(3) 0.4994(2) 0.0265(6) Uani 1 1 d . . .
H11 H 0.7410 0.5742 0.5758 0.032 Uiso 1 1 calc R A .
O12 O 0.4277(5) 0.2802(3) 0.3349(3) 0.0452(9) Uani 1 1 d . . .
H1W H 0.4143 0.1976 0.3162 0.068 Uiso 1 1 d R A .
H2W H 0.4920 0.2972 0.2884 0.068 Uiso 1 1 d R . .
N1 N 1.5001(6) -0.0539(4) 0.1348(4) 0.0470(11) Uani 1 1 d . . .
C1 C 0.8860(5) 0.1306(4) 0.4032(3) 0.0231(8) Uani 1 1 d . . .
C2 C 0.8023(5) 0.0147(4) 0.4183(4) 0.0259(9) Uani 1 1 d . . .
H2 H 0.7137 0.0160 0.4619 0.031 Uiso 1 1 calc R . .
C3 C 0.8509(5) -0.1021(4) 0.3687(3) 0.0246(9) Uani 1 1 d . . .
C4 C 0.9811(6) -0.1052(4) 0.3008(4) 0.0291(9) Uani 1 1 d . . .
H4 H 1.0166 -0.1828 0.2687 0.035 Uiso 1 1 calc R . .
C5 C 1.0557(6) 0.0088(4) 0.2821(4) 0.0284(9) Uani 1 1 d . . .
C6 C 1.0130(5) 0.1273(4) 0.3337(4) 0.0274(9) Uani 1 1 d . . .
H6 H 1.0684 0.2035 0.3220 0.033 Uiso 1 1 calc R . .
C7 C 0.8369(6) 0.2571(4) 0.4601(4) 0.0266(9) Uani 1 1 d . . .
C8 C 0.7720(6) -0.2270(4) 0.3911(4) 0.0265(9) Uani 1 1 d . . .
C9 C 1.1714(6) -0.0791(4) 0.1145(4) 0.0308(10) Uani 1 1 d . . .
C10 C 1.3219(6) -0.1125(5) 0.0719(4) 0.0345(10) Uani 1 1 d . . .
C11 C 1.3070(6) -0.2055(5) -0.0326(4) 0.0365(11) Uani 1 1 d . . .
H11A H 1.4079 -0.2272 -0.0588 0.044 Uiso 1 1 calc R . .
C12 C 1.1451(6) -0.2660(5) -0.0982(4) 0.0351(10) Uani 1 1 d . . .
C13 C 0.9961(7) -0.2312(5) -0.0576(4) 0.0411(12) Uani 1 1 d . . .
H13 H 0.8859 -0.2703 -0.1017 0.049 Uiso 1 1 calc R . .
C14 C 1.0085(6) -0.1391(5) 0.0475(4) 0.0379(11) Uani 1 1 d . . .
H14 H 0.9071 -0.1176 0.0730 0.045 Uiso 1 1 calc R . .
C15 C 1.1352(6) -0.3657(4) -0.2106(4) 0.0350(10) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O10 C16 C17 117.1(9) . .
O10 C16 H16A 108.0 . .
C17 C16 H16A 108.0 . .
O10 C16 H16B 108.0 . .
C17 C16 H16B 108.0 . .
H16A C16 H16B 107.3 . .
O10 C16' C17' 125.0(11) . .
O10 C16' H16C 106.1 . .
C17' C16' H16C 106.1 . .
O10 C16' H16D 106.1 . .
C17' C16' H16D 106.1 . .
H16C C16' H16D 106.3 . .
C16' C17' H17D 109.5 . .
C16' C17' H17E 109.5 . .
H17D C17' H17E 109.5 . .
C16' C17' H17F 109.5 . .
H17D C17' H17F 109.5 . .
H17E C17' H17F 109.5 . .
O11 Co1 O4 98.00(12) . 1_565
O11 Co1 O7 101.01(12) . 2_755
O4 Co1 O7 94.88(14) 1_565 2_755
O11 Co1 O1 92.64(12) . 2_766
O4 Co1 O1 91.46(12) 1_565 2_766
O7 Co1 O1 163.97(12) 2_755 2_766
O11 Co1 O1 89.29(11) . .
O4 Co1 O1 170.41(12) 1_565 .
O7 Co1 O1 89.80(12) 2_755 .
O1 Co1 O1 81.94(11) 2_766 .
O11 Co1 O8 159.33(12) . 2_755
O4 Co1 O8 93.72(13) 1_565 2_755
O7 Co1 O8 60.89(12) 2_755 2_755
O1 Co1 O8 104.06(12) 2_766 2_755
O1 Co1 O8 81.24(12) . 2_755
O11 Co1 C15 130.67(14) . 2_755
O4 Co1 C15 96.20(14) 1_565 2_755
O7 Co1 C15 30.65(14) 2_755 2_755
O1 Co1 C15 133.93(14) 2_766 2_755
O1 Co1 C15 83.59(14) . 2_755
O8 Co1 C15 30.28(14) 2_755 2_755
O3 Co2 O2 90.32(13) 2_656 .
O3 Co2 O11 174.15(11) 2_656 .
O2 Co2 O11 94.96(12) . .
O3 Co2 O11 94.08(12) 2_656 2_666
O2 Co2 O11 167.55(14) . 2_666
O11 Co2 O11 81.28(12) . 2_666
O3 Co2 O10 91.38(16) 2_656 .
O2 Co2 O10 90.86(16) . .
O11 Co2 O10 86.01(15) . .
O11 Co2 O10 100.66(14) 2_666 .
O3 Co2 O12 91.60(14) 2_656 .
O2 Co2 O12 87.08(14) . .
O11 Co2 O12 91.20(12) . .
O11 Co2 O12 81.16(13) 2_666 .
O10 Co2 O12 176.39(15) . .
C7 O1 Co1 124.4(3) . 2_766
C7 O1 Co1 126.9(3) . .
Co1 O1 Co1 98.06(11) 2_766 .
C7 O2 Co2 133.2(3) . .
C8 O3 Co2 130.4(3) . 2_656
C8 O4 Co1 131.6(3) . 1_545
C15 O7 Co1 91.4(3) . 2_755
C15 O8 Co1 87.1(3) . 2_755
C9 O9 C5 119.0(3) . .
C16' O10 C16 35.9(8) . .
C16' O10 Co2 137.1(7) . .
C16 O10 Co2 124.2(6) . .
C16' O10 H10D 101.2 . .
C16 O10 H10D 95.8 . .
Co2 O10 H10D 121.0 . .
Co1 O11 Co2 124.98(13) . .
Co1 O11 Co2 119.71(14) . 2_666
Co2 O11 Co2 98.72(12) . 2_666
Co1 O11 H11 103.6 . .
Co2 O11 H11 103.6 . .
Co2 O11 H11 103.6 2_666 .
Co2 O12 H1W 109.5 . .
Co2 O12 H2W 121.4 . .
H1W O12 H2W 100.9 . .
O6 N1 O5 121.0(5) . .
O6 N1 C10 118.4(4) . .
O5 N1 C10 120.3(4) . .
C6 C1 C2 119.6(4) . .
C6 C1 C7 120.3(4) . .
C2 C1 C7 120.0(4) . .
C3 C2 C1 120.3(4) . .
C3 C2 H2 119.8 . .
C1 C2 H2 119.8 . .
C2 C3 C4 120.1(4) . .
C2 C3 C8 121.2(4) . .
C4 C3 C8 118.6(4) . .
C5 C4 C3 118.8(4) . .
C5 C4 H4 120.6 . .
C3 C4 H4 120.6 . .
C4 C5 C6 122.0(4) . .
C4 C5 O9 121.0(4) . .
C6 C5 O9 116.7(4) . .
C5 C6 C1 119.0(4) . .
C5 C6 H6 120.5 . .
C1 C6 H6 120.5 . .
O2 C7 O1 124.5(4) . .
O2 C7 C1 118.1(4) . .
O1 C7 C1 117.4(4) . .
O3 C8 O4 126.9(4) . .
O3 C8 C3 116.7(4) . .
O4 C8 C3 116.4(4) . .
O9 C9 C14 123.2(4) . .
O9 C9 C10 118.7(4) . .
C14 C9 C10 118.1(4) . .
C11 C10 C9 120.8(4) . .
C11 C10 N1 116.5(4) . .
C9 C10 N1 122.6(4) . .
C12 C11 C10 120.9(4) . .
C12 C11 H11A 119.5 . .
C10 C11 H11A 119.5 . .
C11 C12 C13 118.5(4) . .
C11 C12 C15 119.1(4) . .
C13 C12 C15 122.4(4) . .
C14 C13 C12 121.4(5) . .
C14 C13 H13 119.3 . .
C12 C13 H13 119.3 . .
C9 C14 C13 120.3(4) . .
C9 C14 H14 119.9 . .
C13 C14 H14 119.9 . .
O8 C15 O7 120.4(4) . .
O8 C15 C12 121.2(4) . .
O7 C15 C12 118.3(4) . .
O8 C15 Co1 62.6(2) . 2_755
O7 C15 Co1 58.0(2) . 2_755
C12 C15 Co1 175.2(3) . 2_755
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C16 O10 1.470(8) .
C16 C17 1.573(9) .
C16 H16A 0.9700 .
C16 H16B 0.9700 .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C16' O10 1.421(9) .
C16' C17' 1.493(10) .
C16' H16C 0.9700 .
C16' H16D 0.9700 .
C17' H17D 0.9600 .
C17' H17E 0.9600 .
C17' H17F 0.9600 .
Co1 O11 2.008(3) .
Co1 O4 2.024(3) 1_565
Co1 O7 2.120(3) 2_755
Co1 O1 2.122(3) 2_766
Co1 O1 2.168(3) .
Co1 O8 2.221(3) 2_755
Co1 C15 2.499(5) 2_755
Co2 O3 2.032(3) 2_656
Co2 O2 2.050(3) .
Co2 O11 2.082(3) .
Co2 O11 2.084(3) 2_666
Co2 O10 2.177(4) .
Co2 O12 2.215(4) .
O1 C7 1.294(5) .
O1 Co1 2.122(3) 2_766
O2 C7 1.236(5) .
O3 C8 1.250(5) .
O3 Co2 2.032(3) 2_656
O4 C8 1.260(5) .
O4 Co1 2.024(3) 1_545
O5 N1 1.203(6) .
O6 N1 1.198(6) .
O7 C15 1.274(6) .
O7 Co1 2.120(3) 2_755
O8 C15 1.262(6) .
O8 Co1 2.221(3) 2_755
O9 C9 1.363(5) .
O9 C5 1.410(5) .
O10 H10D 0.8500 .
O11 Co2 2.084(3) 2_666
O11 H11 0.9800 .
O12 H1W 0.8500 .
O12 H2W 0.8500 .
N1 C10 1.462(6) .
C1 C6 1.392(6) .
C1 C2 1.398(6) .
C1 C7 1.496(5) .
C2 C3 1.385(6) .
C2 H2 0.9300 .
C3 C4 1.398(6) .
C3 C8 1.515(6) .
C4 C5 1.378(6) .
C4 H4 0.9300 .
C5 C6 1.384(6) .
C6 H6 0.9300 .
C9 C14 1.386(7) .
C9 C10 1.408(6) .
C10 C11 1.386(6) .
C11 C12 1.375(7) .
C11 H11A 0.9300 .
C12 C13 1.392(6) .
C12 C15 1.496(6) .
C13 C14 1.390(7) .
C13 H13 0.9300 .
C14 H14 0.9300 .
C15 Co1 2.499(5) 2_755
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O10 H10D O8 0.85 2.06 2.887(6) 163.7 1_566
O12 H1W O5 0.85 2.20 2.856(5) 134.1 1_455
O12 H1W O9 0.85 2.35 3.040(5) 138.0 1_455
O12 H2W O7 0.85 2.05 2.830(5) 152.7 2_755
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O11 Co1 O1 C7 52.2(3) . .
O4 Co1 O1 C7 -168.2(6) 1_565 .
O7 Co1 O1 C7 -48.9(3) 2_755 .
O1 Co1 O1 C7 144.9(4) 2_766 .
O8 Co1 O1 C7 -109.4(3) 2_755 .
C15 Co1 O1 C7 -78.9(3) 2_755 .
O11 Co1 O1 Co1 -92.77(12) . 2_766
O4 Co1 O1 Co1 46.9(7) 1_565 2_766
O7 Co1 O1 Co1 166.22(12) 2_755 2_766
O1 Co1 O1 Co1 0.0 2_766 2_766
O8 Co1 O1 Co1 105.67(13) 2_755 2_766
C15 Co1 O1 Co1 136.14(15) 2_755 2_766
O3 Co2 O2 C7 162.1(5) 2_656 .
O11 Co2 O2 C7 -20.5(5) . .
O11 Co2 O2 C7 51.3(8) 2_666 .
O10 Co2 O2 C7 -106.5(5) . .
O12 Co2 O2 C7 70.5(5) . .
C17' C16' O10 C16 71(2) . .
C17' C16' O10 Co2 157.1(13) . .
C17 C16 O10 C16' 13.3(13) . .
C17 C16 O10 Co2 -111.5(10) . .
O3 Co2 O10 C16' -20.3(13) 2_656 .
O2 Co2 O10 C16' -110.6(13) . .
O11 Co2 O10 C16' 154.5(13) . .
O11 Co2 O10 C16' 74.2(13) 2_666 .
O12 Co2 O10 C16' -166(2) . .
O3 Co2 O10 C16 24.8(7) 2_656 .
O2 Co2 O10 C16 -65.5(7) . .
O11 Co2 O10 C16 -160.4(7) . .
O11 Co2 O10 C16 119.2(6) 2_666 .
O12 Co2 O10 C16 -121(2) . .
O4 Co1 O11 Co2 145.39(18) 1_565 .
O7 Co1 O11 Co2 48.8(2) 2_755 .
O1 Co1 O11 Co2 -122.76(17) 2_766 .
O1 Co1 O11 Co2 -40.86(18) . .
O8 Co1 O11 Co2 21.5(5) 2_755 .
C15 Co1 O11 Co2 40.0(3) 2_755 .
O4 Co1 O11 Co2 17.64(18) 1_565 2_666
O7 Co1 O11 Co2 -78.96(17) 2_755 2_666
O1 Co1 O11 Co2 109.49(16) 2_766 2_666
O1 Co1 O11 Co2 -168.61(16) . 2_666
O8 Co1 O11 Co2 -106.3(3) 2_755 2_666
C15 Co1 O11 Co2 -87.7(2) 2_755 2_666
O3 Co2 O11 Co1 -173.7(12) 2_656 .
O2 Co2 O11 Co1 32.0(2) . .
O11 Co2 O11 Co1 -136.0(2) 2_666 .
O10 Co2 O11 Co1 122.6(2) . .
O12 Co2 O11 Co1 -55.13(19) . .
O3 Co2 O11 Co2 -37.7(13) 2_656 2_666
O2 Co2 O11 Co2 168.04(14) . 2_666
O11 Co2 O11 Co2 0.0 2_666 2_666
O10 Co2 O11 Co2 -101.44(15) . 2_666
O12 Co2 O11 Co2 80.86(13) . 2_666
C6 C1 C2 C3 2.9(6) . .
C7 C1 C2 C3 -178.0(4) . .
C1 C2 C3 C4 -1.6(6) . .
C1 C2 C3 C8 175.3(4) . .
C2 C3 C4 C5 -1.7(6) . .
C8 C3 C4 C5 -178.7(4) . .
C3 C4 C5 C6 3.7(7) . .
C3 C4 C5 O9 177.3(4) . .
C9 O9 C5 C4 50.5(6) . .
C9 O9 C5 C6 -135.6(4) . .
C4 C5 C6 C1 -2.4(7) . .
O9 C5 C6 C1 -176.3(4) . .
C2 C1 C6 C5 -1.0(6) . .
C7 C1 C6 C5 -180.0(4) . .
Co2 O2 C7 O1 33.8(7) . .
Co2 O2 C7 C1 -145.9(3) . .
Co1 O1 C7 O2 82.7(5) 2_766 .
Co1 O1 C7 O2 -53.8(6) . .
Co1 O1 C7 C1 -97.7(4) 2_766 .
Co1 O1 C7 C1 125.9(3) . .
C6 C1 C7 O2 166.4(4) . .
C2 C1 C7 O2 -12.7(6) . .
C6 C1 C7 O1 -13.3(6) . .
C2 C1 C7 O1 167.6(4) . .
Co2 O3 C8 O4 -12.2(7) 2_656 .
Co2 O3 C8 C3 168.4(3) 2_656 .
Co1 O4 C8 O3 -30.0(7) 1_545 .
Co1 O4 C8 C3 149.3(3) 1_545 .
C2 C3 C8 O3 4.7(6) . .
C4 C3 C8 O3 -178.4(4) . .
C2 C3 C8 O4 -174.7(4) . .
C4 C3 C8 O4 2.2(6) . .
C5 O9 C9 C14 27.5(7) . .
C5 O9 C9 C10 -153.9(4) . .
O9 C9 C10 C11 179.5(4) . .
C14 C9 C10 C11 -1.9(7) . .
O9 C9 C10 N1 0.5(7) . .
C14 C9 C10 N1 179.2(5) . .
O6 N1 C10 C11 -20.8(8) . .
O5 N1 C10 C11 154.1(5) . .
O6 N1 C10 C9 158.2(6) . .
O5 N1 C10 C9 -26.9(8) . .
C9 C10 C11 C12 1.0(8) . .
N1 C10 C11 C12 -180.0(5) . .
C10 C11 C12 C13 0.4(8) . .
C10 C11 C12 C15 179.9(4) . .
C11 C12 C13 C14 -1.1(8) . .
C15 C12 C13 C14 179.5(5) . .
O9 C9 C14 C13 179.8(4) . .
C10 C9 C14 C13 1.2(7) . .
C12 C13 C14 C9 0.2(8) . .
Co1 O8 C15 O7 -4.1(4) 2_755 .
Co1 O8 C15 C12 176.6(4) 2_755 .
Co1 O7 C15 O8 4.3(5) 2_755 .
Co1 O7 C15 C12 -176.4(4) 2_755 .
C11 C12 C15 O8 169.3(5) . .
C13 C12 C15 O8 -11.3(7) . .
C11 C12 C15 O7 -10.0(7) . .
C13 C12 C15 O7 169.4(5) . .
C11 C12 C15 Co1 -49(4) . 2_755
C13 C12 C15 Co1 130(4) . 2_755
