#------------------------------------------------------------------------------
#$Date: 2016-02-05 00:19:48 +0200 (Fri, 05 Feb 2016) $
#$Revision: 175951 $
#$URL: svn://www.crystallography.net/cod/cif/7/22/34/7223490.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7223490
loop_
_publ_author_name
'Lei, Xiao-Wu'
'Yue, Cheng-Yang'
'Feng, Li-Juan'
'Han, Yong-Fang'
'Meng, Rong-Rong'
'Yang, Jiang-Tao'
'Ding, Hao'
'Gao, Chuan-Sheng'
'Wang, Chun-Yan'
_publ_section_title
;
 Syntheses, crystal structures and photocatalytic properties of four
 hybrid iodoargentates with zero- and two-dimensional structures
;
_journal_issue                   3
_journal_name_full               CrystEngComm
_journal_page_first              427
_journal_paper_doi               10.1039/C5CE01669J
_journal_volume                  18
_journal_year                    2016
_chemical_formula_sum            'C48 H56 Ag14 I22 N8'
_chemical_formula_weight         5046.99
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-08-14 deposited with the CCDC.
2015-12-01 downloaded from the CCDC.
;
_cell_angle_alpha                100.4410(10)
_cell_angle_beta                 94.9510(10)
_cell_angle_gamma                100.2270(10)
_cell_formula_units_Z            2
_cell_length_a                   11.3960(14)
_cell_length_b                   18.948(2)
_cell_length_c                   23.015(3)
_cell_measurement_temperature    296(2)
_cell_volume                     4773.5(10)
_computing_cell_refinement       'APEX2 Software Suite (Bruker,2005)'
_computing_data_collection       'APEX2 Software Suite (Bruker,2005)'
_computing_data_reduction        'APEX2 Software Suite (Bruker,2005)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.974
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measurement_device_type  'Bruker SMART CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0277
_diffrn_reflns_av_sigmaI/netI    0.0365
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            56436
_diffrn_reflns_theta_full        27.66
_diffrn_reflns_theta_max         27.66
_diffrn_reflns_theta_min         1.57
_exptl_absorpt_coefficient_mu    9.948
_exptl_absorpt_correction_T_max  0.6361
_exptl_absorpt_correction_T_min  0.4362
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'
_exptl_crystal_colour            'orange red'
_exptl_crystal_density_diffrn    3.511
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plane
_exptl_crystal_F_000             4448
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.884
_refine_diff_density_min         -2.356
_refine_diff_density_rms         0.181
_refine_ls_extinction_coef       0
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     859
_refine_ls_number_reflns         21694
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.023
_refine_ls_R_factor_all          0.0627
_refine_ls_R_factor_gt           0.0399
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0432P)²+18.7357P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0915
_refine_ls_wR_factor_ref         0.1003
_reflns_number_gt                15857
_reflns_number_total             21694
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5ce01669j2.cif
_cod_data_source_block           C24N4H28Ag7I11
_cod_depositor_comments
'Adding full bibliography for 7223487--7223490.cif.'
_cod_original_cell_volume        4773.6(10)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7223490
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
I22 I 0.76283(5) 0.38653(3) 0.27081(2) 0.04138(12) Uani 1 1 d .
I21 I 0.13369(5) 0.44858(3) 0.21206(3) 0.04213(13) Uani 1 1 d .
I20 I 0.64225(5) 1.08492(3) 0.46053(3) 0.04466(14) Uani 1 1 d .
I19 I 0.77795(5) 0.45497(3) 0.46311(2) 0.03979(12) Uani 1 1 d .
I18 I 0.36269(5) 0.28579(3) 0.23921(2) 0.04653(14) Uani 1 1 d .
I17 I 0.70109(5) 0.85061(3) 0.47268(3) 0.04406(13) Uani 1 1 d .
I16 I 0.71426(5) 0.95013(3) 0.29296(3) 0.04339(13) Uani 1 1 d .
I15 I 1.10797(5) 0.36288(3) 0.38518(2) 0.04077(12) Uani 1 1 d .
I14 I 0.79896(5) 0.34475(3) 0.07247(2) 0.04306(13) Uani 1 1 d .
I13 I 0.45391(5) 0.09949(3) 0.27969(3) 0.04756(14) Uani 1 1 d .
I12 I 0.35717(5) 0.87390(3) 0.35319(3) 0.04672(14) Uani 1 1 d .
I11 I -0.02999(5) 0.19647(3) 0.19641(2) 0.04174(13) Uani 1 1 d .
I10 I 0.93446(5) 0.78444(3) 0.33494(3) 0.04595(13) Uani 1 1 d .
I9 I 0.15156(5) 0.27118(3) 0.04654(2) 0.04571(13) Uani 1 1 d .
I8 I 0.54769(5) 0.69984(3) 0.27433(3) 0.04641(14) Uani 1 1 d .
I7 I 1.06043(6) 0.60489(3) 0.37702(3) 0.04966(14) Uani 1 1 d .
I6 I 0.86157(5) 0.58021(3) 0.18163(3) 0.04972(14) Uani 1 1 d .
I5 I 0.25506(6) 0.06178(3) 0.08735(3) 0.05369(16) Uani 1 1 d .
I4 I 0.37386(6) -0.13597(3) 0.15420(3) 0.04850(14) Uani 1 1 d .
I3 I 0.75880(7) 0.77852(4) 0.13199(3) 0.06074(18) Uani 1 1 d .
I2 I 0.48426(5) 0.45832(4) 0.12306(3) 0.06014(18) Uani 1 1 d .
Ag14 Ag 0.29333(7) 0.36039(4) 0.15169(4) 0.05744(19) Uani 1 1 d .
I1 I 1.06023(6) 0.97612(4) 0.22863(3) 0.06762(19) Uani 1 1 d .
Ag13 Ag 0.71083(7) 0.43601(4) 0.16384(3) 0.05206(17) Uani 1 1 d .
Ag12 Ag 0.88400(8) 0.86118(4) 0.24262(4) 0.0633(2) Uani 1 1 d .
Ag11 Ag 1.01980(7) 0.48732(4) 0.43641(4) 0.0616(2) Uani 1 1 d .
Ag10 Ag 0.77181(8) 0.70283(4) 0.22797(4) 0.0618(2) Uani 1 1 d .
Ag9 Ag 0.00292(7) 0.31671(4) 0.13420(3) 0.0596(2) Uani 1 1 d .
Ag8 Ag 0.52911(7) 0.93554(4) 0.45481(4) 0.0596(2) Uani 1 1 d .
Ag7 Ag 0.70616(8) 0.82700(5) 0.34920(4) 0.0685(2) Uani 1 1 d .
Ag6A Ag 0.99474(9) 0.34142(5) 0.26890(4) 0.0580(3) Uani 0.847(3) 1 d P
Ag6B Ag 1.1113(8) 0.3221(3) 0.2662(3) 0.092(3) Uani 0.153(3) 1 d P
Ag5 Ag 0.19809(8) 0.18904(5) 0.14908(4) 0.0748(3) Uani 1 1 d .
Ag4 Ag 0.94761(8) 0.51096(5) 0.27425(5) 0.0772(3) Uani 1 1 d .
Ag3 Ag 0.28936(8) -0.00207(5) 0.19107(4) 0.0720(2) Uani 1 1 d .
Ag2A Ag 0.49662(10) 0.83909(6) 0.25534(5) 0.0595(4) Uani 0.805(3) 1 d P
Ag2B Ag 0.5657(6) 0.8216(3) 0.2198(3) 0.087(3) Uani 0.195(3) 1 d P
Ag1A Ag 0.51912(11) 1.00515(6) 0.34626(6) 0.0689(5) Uani 0.807(3) 1 d P
Ag1B Ag 0.4443(9) 0.9573(5) 0.2830(5) 0.162(6) Uani 0.193(3) 1 d P
N6 N 0.4650(5) 0.6903(3) 0.4848(3) 0.0321(14) Uani 1 1 d .
N7 N -0.0774(6) 0.2079(3) 0.4374(3) 0.0365(15) Uani 1 1 d .
N8 N 0.1049(6) 0.0978(4) 0.3782(3) 0.0371(15) Uani 1 1 d .
N5 N 0.6123(6) 0.5865(3) 0.3906(3) 0.0366(15) Uani 1 1 d .
N4 N 0.5719(6) 0.1879(4) 0.0986(3) 0.0396(15) Uani 1 1 d .
N3 N 0.7776(6) 0.0811(3) 0.0613(3) 0.0398(16) Uani 1 1 d .
C18 C 0.5961(7) 0.1326(4) 0.0581(3) 0.0349(17) Uani 1 1 d .
C30 C 0.5211(6) 0.6317(4) 0.4781(3) 0.0329(16) Uani 1 1 d .
C25 C 0.5124(7) 0.5852(4) 0.4176(3) 0.0325(16) Uani 1 1 d .
N1 N 0.8681(7) 0.3054(5) -0.1373(4) 0.060(2) Uani 1 1 d .
N2 N 0.6956(7) 0.4073(4) -0.0640(3) 0.0483(18) Uani 1 1 d .
C37 C -0.0028(7) 0.0960(4) 0.3993(3) 0.0329(16) Uani 1 1 d .
C43 C -0.1397(8) 0.1504(4) 0.3371(4) 0.0391(18) Uani 1 1 d .
H43 H -0.1372 0.1137 0.3046 0.047 Uiso 1 1 calc .
C42 C -0.0733(7) 0.1539(4) 0.3907(4) 0.0354(17) Uani 1 1 d .
C31 C 0.5784(7) 0.6156(5) 0.5273(4) 0.0409(19) Uani 1 1 d .
H31 H 0.6182 0.5765 0.5231 0.049 Uiso 1 1 calc .
C13 C 0.6683(8) 0.0825(4) 0.0797(4) 0.0407(19) Uani 1 1 d .
C6 C 0.7973(9) 0.4134(5) -0.0906(4) 0.046(2) Uani 1 1 d .
C36 C 0.4023(8) 0.7111(5) 0.4339(4) 0.050(2) Uani 1 1 d .
H36A H 0.3689 0.7533 0.4477 0.074 Uiso 1 1 calc R
H36B H 0.3389 0.6712 0.4144 0.074 Uiso 1 1 calc R
H36C H 0.4581 0.7224 0.4064 0.074 Uiso 1 1 calc R
C34 C 0.4654(8) 0.7311(4) 0.5391(4) 0.0400(19) Uani 1 1 d .
H34 H 0.4273 0.7709 0.5431 0.048 Uiso 1 1 calc .
C39 C 0.0092(8) -0.0200(4) 0.4239(4) 0.0430(19) Uani 1 1 d .
H39 H -0.0239 -0.0600 0.4395 0.052 Uiso 1 1 calc .
C38 C -0.0522(7) 0.0371(4) 0.4209(4) 0.0390(18) Uani 1 1 d .
H38 H -0.1276 0.0347 0.4339 0.047 Uiso 1 1 calc .
C26 C 0.4078(8) 0.5394(5) 0.3923(4) 0.043(2) Uani 1 1 d .
H26 H 0.3393 0.5391 0.4114 0.052 Uiso 1 1 calc .
C40 C 0.1172(8) -0.0161(5) 0.4038(4) 0.050(2) Uani 1 1 d .
H40 H 0.1595 -0.0535 0.4056 0.060 Uiso 1 1 calc .
C45 C -0.2105(7) 0.2563(5) 0.3793(4) 0.044(2) Uani 1 1 d .
H45 H -0.2552 0.2922 0.3756 0.052 Uiso 1 1 calc .
C33 C 0.5217(8) 0.7145(5) 0.5887(4) 0.048(2) Uani 1 1 d .
H33 H 0.5212 0.7428 0.6261 0.058 Uiso 1 1 calc .
C46 C -0.1454(8) 0.2581(4) 0.4317(4) 0.045(2) Uani 1 1 d .
H46 H -0.1476 0.2946 0.4644 0.054 Uiso 1 1 calc .
C35 C 0.7270(7) 0.6365(5) 0.4141(5) 0.052(2) Uani 1 1 d .
H35A H 0.7197 0.6653 0.4520 0.078 Uiso 1 1 calc R
H35B H 0.7476 0.6684 0.3869 0.078 Uiso 1 1 calc R
H35C H 0.7887 0.6088 0.4187 0.078 Uiso 1 1 calc R
C1 C 0.8066(9) 0.3580(6) -0.1429(4) 0.055(2) Uani 1 1 d .
C47 C 0.1611(8) 0.1602(5) 0.3527(5) 0.055(2) Uani 1 1 d .
H47A H 0.2365 0.1518 0.3401 0.082 Uiso 1 1 calc R
H47B H 0.1744 0.2044 0.3824 0.082 Uiso 1 1 calc R
H47C H 0.1088 0.1647 0.3192 0.082 Uiso 1 1 calc R
C27 C 0.4031(9) 0.4928(5) 0.3377(4) 0.055(2) Uani 1 1 d .
H27 H 0.3320 0.4612 0.3198 0.066 Uiso 1 1 calc .
C32 C 0.5779(8) 0.6567(5) 0.5829(4) 0.047(2) Uani 1 1 d .
H32 H 0.6157 0.6450 0.6163 0.057 Uiso 1 1 calc .
C22 C 0.5007(8) 0.2320(5) 0.0808(5) 0.052(2) Uani 1 1 d .
H22 H 0.4844 0.2702 0.1085 0.062 Uiso 1 1 calc .
C44 C -0.2101(8) 0.2017(5) 0.3319(4) 0.049(2) Uani 1 1 d .
H44 H -0.2571 0.1990 0.2962 0.059 Uiso 1 1 calc .
C21 C 0.4527(8) 0.2214(6) 0.0230(5) 0.057(3) Uani 1 1 d .
H21 H 0.4036 0.2521 0.0116 0.068 Uiso 1 1 calc .
C10 C 0.6817(10) 0.4608(6) -0.0198(4) 0.059(3) Uani 1 1 d .
H10 H 0.6125 0.4556 -0.0010 0.071 Uiso 1 1 calc .
C29 C 0.6083(9) 0.5412(5) 0.3368(4) 0.051(2) Uani 1 1 d .
H29 H 0.6769 0.5422 0.3176 0.061 Uiso 1 1 calc .
C7 C 0.8844(9) 0.4751(5) -0.0738(4) 0.057(3) Uani 1 1 d .
H7 H 0.9540 0.4798 -0.0923 0.069 Uiso 1 1 calc .
C24 C 0.6215(9) 0.2036(5) 0.1614(4) 0.055(2) Uani 1 1 d .
H24A H 0.6699 0.1686 0.1683 0.083 Uiso 1 1 calc R
H24B H 0.5571 0.2005 0.1857 0.083 Uiso 1 1 calc R
H24C H 0.6701 0.2520 0.1715 0.083 Uiso 1 1 calc R
C41 C 0.1651(8) 0.0431(5) 0.3805(4) 0.052(2) Uani 1 1 d .
H41 H 0.2394 0.0454 0.3663 0.062 Uiso 1 1 calc .
C19 C 0.5493(8) 0.1208(5) 0.0000(4) 0.048(2) Uani 1 1 d .
H19 H 0.5664 0.0825 -0.0272 0.058 Uiso 1 1 calc .
C28 C 0.5048(10) 0.4946(5) 0.3112(4) 0.062(3) Uani 1 1 d .
H28 H 0.5037 0.4635 0.2749 0.074 Uiso 1 1 calc .
C23 C 0.8314(9) 0.1302(5) 0.0241(4) 0.054(2) Uani 1 1 d .
H23A H 0.7775 0.1617 0.0158 0.082 Uiso 1 1 calc R
H23B H 0.8458 0.1018 -0.0126 0.082 Uiso 1 1 calc R
H23C H 0.9060 0.1593 0.0448 0.082 Uiso 1 1 calc R
C14 C 0.6233(9) 0.0347(5) 0.1144(4) 0.056(2) Uani 1 1 d .
H14 H 0.5481 0.0351 0.1271 0.067 Uiso 1 1 calc .
C20 C 0.4761(9) 0.1656(6) -0.0189(4) 0.058(3) Uani 1 1 d .
H20 H 0.4440 0.1582 -0.0585 0.070 Uiso 1 1 calc .
C17 C 0.8439(9) 0.0329(5) 0.0773(5) 0.064(3) Uani 1 1 d .
H17 H 0.9192 0.0326 0.0646 0.077 Uiso 1 1 calc .
C48 C -0.0086(9) 0.2129(6) 0.4959(4) 0.060(3) Uani 1 1 d .
H48A H -0.0223 0.2543 0.5234 0.090 Uiso 1 1 calc R
H48B H 0.0754 0.2186 0.4917 0.090 Uiso 1 1 calc R
H48C H -0.0344 0.1690 0.5104 0.090 Uiso 1 1 calc R
C9 C 0.7690(13) 0.5232(6) -0.0021(5) 0.074(3) Uani 1 1 d .
H9 H 0.7589 0.5602 0.0285 0.089 Uiso 1 1 calc .
C2 C 0.7591(10) 0.3636(6) -0.1998(4) 0.074(4) Uani 1 1 d .
H2 H 0.7151 0.3996 -0.2042 0.089 Uiso 1 1 calc .
C8 C 0.8686(11) 0.5303(5) -0.0293(5) 0.069(3) Uani 1 1 d .
H8 H 0.9272 0.5728 -0.0180 0.082 Uiso 1 1 calc .
C16 C 0.8001(13) -0.0149(6) 0.1119(6) 0.082(4) Uani 1 1 d .
H16 H 0.8455 -0.0478 0.1226 0.098 Uiso 1 1 calc .
C15 C 0.6921(13) -0.0143(6) 0.1303(5) 0.076(3) Uani 1 1 d .
H15 H 0.6627 -0.0468 0.1539 0.091 Uiso 1 1 calc .
C12 C 0.9204(11) 0.2976(6) -0.0789(5) 0.072(3) Uani 1 1 d .
H12A H 0.9032 0.3350 -0.0486 0.108 Uiso 1 1 calc R
H12B H 1.0059 0.3024 -0.0782 0.108 Uiso 1 1 calc R
H12C H 0.8865 0.2503 -0.0717 0.108 Uiso 1 1 calc R
C11 C 0.5966(10) 0.3432(6) -0.0837(5) 0.066(3) Uani 1 1 d .
H11A H 0.5328 0.3481 -0.0595 0.099 Uiso 1 1 calc R
H11B H 0.6255 0.2995 -0.0798 0.099 Uiso 1 1 calc R
H11C H 0.5672 0.3404 -0.1246 0.099 Uiso 1 1 calc R
C5 C 0.8846(10) 0.2566(7) -0.1855(6) 0.090(5) Uani 1 1 d .
H5 H 0.9253 0.2193 -0.1805 0.108 Uiso 1 1 calc .
C3 C 0.7777(13) 0.3160(11) -0.2484(6) 0.114(7) Uani 1 1 d .
H3 H 0.7476 0.3194 -0.2865 0.136 Uiso 1 1 calc .
C4 C 0.8426(12) 0.2621(11) -0.2402(7) 0.119(7) Uani 1 1 d .
H4 H 0.8568 0.2296 -0.2730 0.143 Uiso 1 1 calc .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ag13 I22 Ag4 74.58(3) . .
Ag13 I22 Ag6A 108.29(3) . .
Ag4 I22 Ag6A 70.50(3) . .
Ag9 I21 Ag6B 66.54(12) . 1_455
Ag9 I21 Ag6A 63.80(3) . 1_455
Ag6B I21 Ag6A 28.81(19) 1_455 1_455
Ag9 I21 Ag14 67.48(3) . .
Ag6B I21 Ag14 75.99(18) 1_455 .
Ag6A I21 Ag14 100.90(3) 1_455 .
Ag9 I21 Ag4 104.28(3) . 1_455
Ag6B I21 Ag4 95.01(18) 1_455 1_455
Ag6A I21 Ag4 69.10(3) 1_455 1_455
Ag14 I21 Ag4 169.56(3) . 1_455
Ag8 I20 Ag1A 63.56(3) . .
Ag8 I20 Ag8 65.34(3) . 2_676
Ag1A I20 Ag8 105.77(3) . 2_676
Ag11 I19 Ag11 60.50(3) . 2_766
Ag14 I18 Ag5 70.12(3) . .
Ag14 I18 Ag6B 73.95(11) . 1_455
Ag5 I18 Ag6B 75.80(11) . 1_455
Ag8 I17 Ag7 86.49(3) . .
Ag7 I16 Ag2B 68.86(10) . .
Ag7 I16 Ag1A 97.03(3) . .
Ag2B I16 Ag1A 95.34(17) . .
Ag7 I16 Ag2A 66.18(3) . .
Ag2B I16 Ag2A 24.54(16) . .
Ag1A I16 Ag2A 71.87(4) . .
Ag7 I16 Ag12 71.33(3) . .
Ag2B I16 Ag12 74.98(17) . .
Ag1A I16 Ag12 166.83(3) . .
Ag2A I16 Ag12 97.20(4) . .
Ag7 I16 Ag1B 99.03(11) . .
Ag2B I16 Ag1B 67.2(3) . .
Ag1A I16 Ag1B 31.7(2) . .
Ag2A I16 Ag1B 47.19(19) . .
Ag12 I16 Ag1B 141.7(2) . .
Ag6B I15 Ag6A 30.3(2) . .
Ag6B I15 Ag11 122.74(17) . .
Ag6A I15 Ag11 98.88(3) . .
Ag9 I14 Ag13 101.70(3) 1_655 .
Ag1B I13 Ag1A 35.4(3) 1_545 1_545
Ag1B I13 Ag3 64.1(3) 1_545 .
Ag1A I13 Ag3 98.74(4) 1_545 .
Ag1B I12 Ag8 97.8(3) . .
Ag1B I12 Ag1A 34.6(3) . .
Ag8 I12 Ag1A 64.23(3) . .
Ag1B I12 Ag2A 51.45(19) . .
Ag8 I12 Ag2A 105.46(3) . .
Ag1A I12 Ag2A 72.23(3) . .
Ag6B I11 Ag9 67.81(13) 1_455 .
Ag6B I11 Ag6A 29.41(19) 1_455 1_455
Ag9 I11 Ag6A 63.91(3) . 1_455
Ag6B I11 Ag5 80.41(19) 1_455 .
Ag9 I11 Ag5 76.70(3) . .
Ag6A I11 Ag5 107.16(3) 1_455 .
Ag12 I10 Ag7 72.43(3) . .
Ag12 I10 Ag10 61.98(3) . .
Ag7 I10 Ag10 74.53(3) . .
Ag9 I9 Ag14 68.93(3) . .
Ag9 I9 Ag5 74.18(3) . .
Ag14 I9 Ag5 65.15(3) . .
Ag2B I8 Ag10 77.71(17) . .
Ag2B I8 Ag2A 24.75(17) . .
Ag10 I8 Ag2A 100.49(3) . .
Ag2B I8 Ag7 68.93(10) . .
Ag10 I8 Ag7 75.77(3) . .
Ag2A I8 Ag7 65.63(3) . .
Ag4 I7 Ag11 88.40(3) . .
Ag10 I6 Ag4 111.71(3) . .
Ag10 I6 Ag13 119.75(3) . .
Ag4 I6 Ag13 73.24(3) . .
Ag5 I5 Ag3 95.22(3) . .
Ag2A I4 Ag2B 25.08(16) 1_545 1_545
Ag2A I4 Ag3 105.91(4) 1_545 .
Ag2B I4 Ag3 123.79(13) 1_545 .
Ag2A I4 Ag1B 47.80(13) 1_545 1_545
Ag2B I4 Ag1B 66.8(2) 1_545 1_545
Ag3 I4 Ag1B 58.37(13) . 1_545
Ag12 I3 Ag10 63.34(3) . .
Ag12 I3 Ag2B 71.11(9) . .
Ag10 I3 Ag2B 71.12(8) . .
Ag13 I2 Ag14 113.50(3) . .
I18 Ag14 I2 113.45(3) . .
I18 Ag14 I9 115.80(3) . .
I2 Ag14 I9 111.15(3) . .
I18 Ag14 I21 102.06(3) . .
I2 Ag14 I21 107.23(3) . .
I9 Ag14 I21 106.10(3) . .
I18 Ag14 Ag5 55.14(3) . .
I2 Ag14 Ag5 142.29(3) . .
I9 Ag14 Ag5 61.15(3) . .
I21 Ag14 Ag5 110.33(3) . .
I18 Ag14 Ag9 103.86(3) . .
I2 Ag14 Ag9 141.83(3) . .
I9 Ag14 Ag9 55.45(2) . .
I21 Ag14 Ag9 55.16(2) . .
Ag5 Ag14 Ag9 67.84(3) . .
Ag12 I1 Ag3 138.78(4) . 1_665
I2 Ag13 I22 124.12(3) . .
I2 Ag13 I14 110.12(3) . .
I22 Ag13 I14 106.57(3) . .
I2 Ag13 I6 103.38(3) . .
I22 Ag13 I6 104.58(3) . .
I14 Ag13 I6 106.75(3) . .
I1 Ag12 I3 112.58(3) . .
I1 Ag12 I10 117.63(4) . .
I3 Ag12 I10 118.17(3) . .
I1 Ag12 I16 97.37(3) . .
I3 Ag12 I16 104.55(3) . .
I10 Ag12 I16 102.42(3) . .
I1 Ag12 Ag10 153.87(4) . .
I3 Ag12 Ag10 58.39(3) . .
I10 Ag12 Ag10 60.53(3) . .
I16 Ag12 Ag10 108.56(3) . .
I7 Ag11 I15 114.71(3) . .
I7 Ag11 I19 112.63(3) . .
I15 Ag11 I19 114.04(3) . .
I7 Ag11 Ag11 120.54(4) . 2_766
I15 Ag11 Ag11 120.51(4) . 2_766
I19 Ag11 Ag11 62.43(3) . 2_766
I7 Ag11 I19 97.74(3) . 2_766
I15 Ag11 I19 96.48(3) . 2_766
I19 Ag11 I19 119.49(3) . 2_766
Ag11 Ag11 I19 57.06(3) 2_766 2_766
I6 Ag10 I8 125.15(3) . .
I6 Ag10 I3 104.04(3) . .
I8 Ag10 I3 105.61(3) . .
I6 Ag10 I10 108.13(3) . .
I8 Ag10 I10 99.43(3) . .
I3 Ag10 I10 115.07(3) . .
I6 Ag10 Ag12 129.01(4) . .
I8 Ag10 Ag12 105.83(3) . .
I3 Ag10 Ag12 58.27(3) . .
I10 Ag10 Ag12 57.49(3) . .
I14 Ag9 I9 106.48(3) 1_455 .
I14 Ag9 I21 110.18(3) 1_455 .
I9 Ag9 I21 108.29(3) . .
I14 Ag9 I11 117.69(3) 1_455 .
I9 Ag9 I11 102.70(3) . .
I21 Ag9 I11 110.80(3) . .
I14 Ag9 Ag6A 112.66(3) 1_455 1_455
I9 Ag9 Ag6A 140.85(4) . 1_455
I21 Ag9 Ag6A 58.79(3) . 1_455
I11 Ag9 Ag6A 58.14(3) . 1_455
I14 Ag9 Ag6B 139.41(18) 1_455 1_455
I9 Ag9 Ag6B 114.11(18) . 1_455
I21 Ag9 Ag6B 56.76(10) . 1_455
I11 Ag9 Ag6B 54.21(10) . 1_455
Ag6A Ag9 Ag6B 26.78(17) 1_455 1_455
I14 Ag9 Ag14 141.90(3) 1_455 .
I9 Ag9 Ag14 55.63(2) . .
I21 Ag9 Ag14 57.36(2) . .
I11 Ag9 Ag14 99.86(3) . .
Ag6A Ag9 Ag14 91.82(3) 1_455 .
Ag6B Ag9 Ag14 68.28(16) 1_455 .
I17 Ag8 I12 113.78(3) . .
I17 Ag8 I20 110.66(3) . .
I12 Ag8 I20 114.47(3) . .
I17 Ag8 I20 107.85(3) . 2_676
I12 Ag8 I20 94.41(3) . 2_676
I20 Ag8 I20 114.66(3) . 2_676
I17 Ag8 Ag1A 120.20(4) . .
I12 Ag8 Ag1A 58.17(3) . .
I20 Ag8 Ag1A 58.52(3) . .
I20 Ag8 Ag1A 130.81(4) 2_676 .
I17 Ag8 Ag8 127.63(4) . 2_676
I12 Ag8 Ag8 116.94(4) . 2_676
I20 Ag8 Ag8 57.84(3) . 2_676
I20 Ag8 Ag8 56.82(3) 2_676 2_676
Ag1A Ag8 Ag8 97.35(4) . 2_676
I17 Ag7 I16 117.91(3) . .
I17 Ag7 I10 103.27(3) . .
I16 Ag7 I10 104.31(3) . .
I17 Ag7 I8 118.89(4) . .
I16 Ag7 I8 109.67(3) . .
I10 Ag7 I8 99.57(3) . .
I17 Ag7 Ag2A 125.12(4) . .
I16 Ag7 Ag2A 57.64(3) . .
I10 Ag7 Ag2A 131.54(4) . .
I8 Ag7 Ag2A 57.08(3) . .
I17 Ag7 Ag2B 147.22(16) . .
I16 Ag7 Ag2B 55.64(8) . .
I10 Ag7 Ag2B 109.44(16) . .
I8 Ag7 Ag2B 54.06(8) . .
Ag2A Ag7 Ag2B 22.11(14) . .
Ag6B Ag6A I15 71.6(2) . .
Ag6B Ag6A I11 70.3(2) . 1_655
I15 Ag6A I11 116.31(4) . 1_655
Ag6B Ag6A I21 74.0(2) . 1_655
I15 Ag6A I21 106.52(4) . 1_655
I11 Ag6A I21 109.40(3) 1_655 1_655
Ag6B Ag6A I22 177.0(2) . .
I15 Ag6A I22 109.78(3) . .
I11 Ag6A I22 110.93(4) 1_655 .
I21 Ag6A I22 102.97(3) 1_655 .
Ag6B Ag6A Ag9 80.2(2) . 1_655
I15 Ag6A Ag9 150.99(4) . 1_655
I11 Ag6A Ag9 57.95(3) 1_655 1_655
I21 Ag6A Ag9 57.41(3) 1_655 1_655
I22 Ag6A Ag9 97.98(3) . 1_655
Ag6B Ag6A Ag4 123.6(2) . .
I15 Ag6A Ag4 97.47(3) . .
I11 Ag6A Ag4 146.20(4) 1_655 .
I21 Ag6A Ag4 55.99(3) 1_655 .
I22 Ag6A Ag4 53.81(3) . .
Ag9 Ag6A Ag4 92.04(3) 1_655 .
Ag6A Ag6B I15 78.0(3) . .
Ag6A Ag6B I11 80.3(3) . 1_655
I15 Ag6B I11 124.0(3) . 1_655
Ag6A Ag6B I21 77.2(3) . 1_655
I15 Ag6B I21 110.0(2) . 1_655
I11 Ag6B I21 114.5(2) 1_655 1_655
Ag6A Ag6B I18 170.6(3) . 1_655
I15 Ag6B I18 110.5(3) . 1_655
I11 Ag6B I18 97.4(2) 1_655 1_655
I21 Ag6B I18 95.7(2) 1_655 1_655
Ag6A Ag6B Ag9 73.0(3) . 1_655
I15 Ag6B Ag9 150.1(4) . 1_655
I11 Ag6B Ag9 57.98(12) 1_655 1_655
I21 Ag6B Ag9 56.70(11) 1_655 1_655
I18 Ag6B Ag9 98.0(2) 1_655 1_655
I5 Ag5 I18 121.33(4) . .
I5 Ag5 I11 124.28(4) . .
I18 Ag5 I11 101.84(3) . .
I5 Ag5 I9 101.43(3) . .
I18 Ag5 I9 108.01(3) . .
I11 Ag5 I9 96.12(3) . .
I5 Ag5 Ag14 133.14(4) . .
I18 Ag5 Ag14 54.74(2) . .
I11 Ag5 Ag14 99.53(3) . .
I9 Ag5 Ag14 53.70(2) . .
I7 Ag4 I22 124.25(4) . .
I7 Ag4 I6 115.33(4) . .
I22 Ag4 I6 104.53(3) . .
I7 Ag4 I21 107.69(3) . 1_655
I22 Ag4 I21 103.67(3) . 1_655
I6 Ag4 I21 97.58(4) . 1_655
I7 Ag4 Ag6A 112.03(4) . .
I22 Ag4 Ag6A 55.69(3) . .
I6 Ag4 Ag6A 130.80(4) . .
I21 Ag4 Ag6A 54.91(3) 1_655 .
I1 Ag3 I13 110.09(4) 1_445 .
I1 Ag3 I4 113.57(4) 1_445 .
I13 Ag3 I4 112.25(4) . .
I1 Ag3 I5 103.45(4) 1_445 .
I13 Ag3 I5 109.26(4) . .
I4 Ag3 I5 107.76(3) . .
I1 Ag3 Ag1B 104.54(14) 1_445 1_545
I13 Ag3 Ag1B 55.6(2) . 1_545
I4 Ag3 Ag1B 64.9(2) . 1_545
I5 Ag3 Ag1B 151.56(15) . 1_545
Ag2B Ag2A Ag1B 127.4(3) . .
Ag2B Ag2A I4 81.7(2) . 1_565
Ag1B Ag2A I4 73.8(3) . 1_565
Ag2B Ag2A I8 73.3(2) . .
Ag1B Ag2A I8 155.8(2) . .
I4 Ag2A I8 126.38(4) 1_565 .
Ag2B Ag2A I16 75.7(2) . .
Ag1B Ag2A I16 70.5(3) . .
I4 Ag2A I16 110.06(4) 1_565 .
I8 Ag2A I16 108.51(4) . .
Ag2B Ag2A I12 171.2(2) . .
Ag1B Ag2A I12 57.47(17) . .
I4 Ag2A I12 107.10(4) 1_565 .
I8 Ag2A I12 100.38(4) . .
I16 Ag2A I12 101.08(4) . .
Ag2B Ag2A Ag7 82.9(2) . .
Ag1B Ag2A Ag7 108.5(3) . .
I4 Ag2A Ag7 161.71(5) 1_565 .
I8 Ag2A Ag7 57.28(3) . .
I16 Ag2A Ag7 56.17(3) . .
I12 Ag2A Ag7 88.49(4) . .
Ag2A Ag2B I8 81.9(3) . .
Ag2A Ag2B I16 79.7(3) . .
I8 Ag2B I16 112.48(17) . .
Ag2A Ag2B I4 73.2(3) . 1_565
I8 Ag2B I4 126.5(2) . 1_565
I16 Ag2B I4 108.69(17) . 1_565
Ag2A Ag2B I3 176.9(3) . .
I8 Ag2B I3 97.4(2) . .
I16 Ag2B I3 97.8(2) . .
I4 Ag2B I3 109.4(2) 1_565 .
Ag2A Ag2B Ag7 75.0(2) . .
I8 Ag2B Ag7 57.01(9) . .
I16 Ag2B Ag7 55.51(9) . .
I4 Ag2B Ag7 146.7(3) 1_565 .
I3 Ag2B Ag7 102.14(18) . .
Ag2A Ag2B Ag1B 35.4(2) . .
I8 Ag2B Ag1B 116.2(3) . .
I16 Ag2B Ag1B 59.8(2) . .
I4 Ag2B Ag1B 60.4(3) 1_565 .
I3 Ag2B Ag1B 144.4(2) . .
Ag7 Ag2B Ag1B 87.8(3) . .
Ag1B Ag1A I13 71.6(2) . 1_565
Ag1B Ag1A I12 63.8(2) . .
I13 Ag1A I12 121.34(5) 1_565 .
Ag1B Ag1A I20 177.1(2) . .
I13 Ag1A I20 110.11(4) 1_565 .
I12 Ag1A I20 113.35(4) . .
Ag1B Ag1A I16 80.9(3) . .
I13 Ag1A I16 105.95(4) 1_565 .
I12 Ag1A I16 102.67(4) . .
I20 Ag1A I16 100.63(4) . .
Ag1B Ag1A Ag8 119.6(2) . .
I13 Ag1A Ag8 155.40(5) 1_565 .
I12 Ag1A Ag8 57.60(3) . .
I20 Ag1A Ag8 57.92(3) . .
I16 Ag1A Ag8 97.75(4) . .
Ag1A Ag1B Ag2A 112.9(4) . .
Ag1A Ag1B I12 81.5(3) . .
Ag2A Ag1B I12 71.09(16) . .
Ag1A Ag1B I13 73.0(3) . 1_565
Ag2A Ag1B I13 154.9(3) . 1_565
I12 Ag1B I13 133.5(4) . 1_565
Ag1A Ag1B Ag3 131.5(4) . 1_565
Ag2A Ag1B Ag3 114.9(5) . 1_565
I12 Ag1B Ag3 121.7(4) . 1_565
I13 Ag1B Ag3 60.22(15) 1_565 1_565
Ag1A Ag1B I16 67.4(3) . .
Ag2A Ag1B I16 62.30(18) . .
I12 Ag1B I16 103.9(3) . .
I13 Ag1B I16 101.1(3) 1_565 .
Ag3 Ag1B I16 131.1(2) 1_565 .
Ag1A Ag1B I4 164.1(4) . 1_565
Ag2A Ag1B I4 58.4(3) . 1_565
I12 Ag1B I4 105.8(4) . 1_565
I13 Ag1B I4 109.2(3) 1_565 1_565
Ag3 Ag1B I4 56.8(2) 1_565 1_565
I16 Ag1B I4 96.9(2) . 1_565
Ag1A Ag1B Ag2B 114.6(4) . .
Ag2A Ag1B Ag2B 17.18(13) . .
I12 Ag1B Ag2B 88.1(2) . .
I13 Ag1B Ag2B 137.8(3) 1_565 .
Ag3 Ag1B Ag2B 108.6(4) 1_565 .
I16 Ag1B Ag2B 53.07(15) . .
I4 Ag1B Ag2B 52.87(19) 1_565 .
C34 N6 C30 120.4(7) . .
C34 N6 C36 117.5(7) . .
C30 N6 C36 122.1(7) . .
C46 N7 C42 120.7(7) . .
C46 N7 C48 118.3(7) . .
C42 N7 C48 121.0(7) . .
C41 N8 C37 120.8(7) . .
C41 N8 C47 117.9(7) . .
C37 N8 C47 121.4(7) . .
C25 N5 C29 119.4(7) . .
C25 N5 C35 123.9(7) . .
C29 N5 C35 116.6(7) . .
C22 N4 C18 119.3(7) . .
C22 N4 C24 117.7(7) . .
C18 N4 C24 123.0(7) . .
C13 N3 C17 120.5(8) . .
C13 N3 C23 123.0(7) . .
C17 N3 C23 116.5(8) . .
N4 C18 C19 120.9(8) . .
N4 C18 C13 118.0(7) . .
C19 C18 C13 121.0(7) . .
C31 C30 N6 119.1(7) . .
C31 C30 C25 122.1(7) . .
N6 C30 C25 118.8(7) . .
N5 C25 C26 120.9(7) . .
N5 C25 C30 118.3(7) . .
C26 C25 C30 120.7(7) . .
C1 N1 C5 121.4(11) . .
C1 N1 C12 121.5(8) . .
C5 N1 C12 117.2(11) . .
C10 N2 C6 120.2(8) . .
C10 N2 C11 118.5(9) . .
C6 N2 C11 121.2(8) . .
C38 C37 N8 119.4(7) . .
C38 C37 C42 120.5(7) . .
N8 C37 C42 119.5(7) . .
C42 C43 C44 119.4(8) . .
N7 C42 C43 119.4(7) . .
N7 C42 C37 119.5(7) . .
C43 C42 C37 120.9(7) . .
C30 C31 C32 120.6(7) . .
N3 C13 C14 119.8(8) . .
N3 C13 C18 118.5(7) . .
C14 C13 C18 121.5(8) . .
N2 C6 C7 120.0(9) . .
N2 C6 C1 119.7(8) . .
C7 C6 C1 119.8(9) . .
N6 C34 C33 120.6(7) . .
C40 C39 C38 118.8(8) . .
C37 C38 C39 120.5(7) . .
C25 C26 C27 120.2(8) . .
C39 C40 C41 120.1(8) . .
C46 C45 C44 119.6(8) . .
C32 C33 C34 119.9(8) . .
N7 C46 C45 121.0(8) . .
N1 C1 C2 119.3(10) . .
N1 C1 C6 120.5(9) . .
C2 C1 C6 120.0(10) . .
C28 C27 C26 118.1(9) . .
C33 C32 C31 119.4(8) . .
N4 C22 C21 121.1(8) . .
C45 C44 C43 119.8(8) . .
C22 C21 C20 120.6(9) . .
N2 C10 C9 120.5(10) . .
C28 C29 N5 120.4(8) . .
C6 C7 C8 119.4(10) . .
N8 C41 C40 120.3(8) . .
C18 C19 C20 120.4(8) . .
C27 C28 C29 121.1(9) . .
C13 C14 C15 119.0(10) . .
C21 C20 C19 117.9(9) . .
N3 C17 C16 120.2(11) . .
C8 C9 C10 119.6(10) . .
C3 C2 C1 119.7(14) . .
C9 C8 C7 120.2(10) . .
C15 C16 C17 120.1(11) . .
C16 C15 C14 120.4(11) . .
C4 C5 N1 120.2(15) . .
C2 C3 C4 118.7(13) . .
C5 C4 C3 120.6(14) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
I22 Ag13 2.8413(9) .
I22 Ag4 2.8530(11) .
I22 Ag6A 2.9200(12) .
I21 Ag9 2.8757(10) .
I21 Ag6B 2.878(6) 1_455
I21 Ag6A 2.9190(11) 1_455
I21 Ag14 2.9507(9) .
I21 Ag4 2.9569(11) 1_455
I20 Ag8 2.8689(10) .
I20 Ag1A 2.8876(16) .
I20 Ag8 2.9022(10) 2_676
I19 Ag11 2.8598(10) .
I19 Ag11 3.0205(11) 2_766
I18 Ag14 2.7990(10) .
I18 Ag5 2.8126(11) .
I18 Ag6B 3.149(10) 1_455
I17 Ag8 2.7965(9) .
I17 Ag7 2.8030(11) .
I16 Ag7 2.8576(11) .
I16 Ag2B 2.862(5) .
I16 Ag1A 2.8927(12) .
I16 Ag2A 2.9059(12) .
I16 Ag12 2.9601(10) .
I16 Ag1B 3.094(9) .
I15 Ag6B 2.712(6) .
I15 Ag6A 2.7956(11) .
I15 Ag11 2.8282(10) .
I14 Ag9 2.8010(10) 1_655
I14 Ag13 2.8433(9) .
I13 Ag1B 2.693(7) 1_545
I13 Ag1A 2.7136(12) 1_545
I13 Ag3 2.8311(11) .
I12 Ag1B 2.596(6) .
I12 Ag8 2.8426(10) .
I12 Ag1A 2.8603(13) .
I12 Ag2A 2.9126(15) .
I11 Ag6B 2.765(6) 1_455
I11 Ag9 2.8902(10) .
I11 Ag6A 2.8963(11) 1_455
I11 Ag5 2.9198(11) .
I10 Ag12 2.8576(10) .
I10 Ag7 2.8850(11) .
I10 Ag10 2.9500(11) .
I9 Ag9 2.8568(10) .
I9 Ag14 2.8631(10) .
I9 Ag5 3.1116(12) .
I8 Ag2B 2.806(5) .
I8 Ag10 2.8471(10) .
I8 Ag2A 2.9002(13) .
I8 Ag7 2.9067(11) .
I7 Ag4 2.7482(11) .
I7 Ag11 2.8093(10) .
I6 Ag10 2.7779(10) .
I6 Ag4 2.8873(13) .
I6 Ag13 2.8967(10) .
I5 Ag5 2.7800(10) .
I5 Ag3 2.8929(12) .
I4 Ag2A 2.7697(12) 1_545
I4 Ag2B 2.862(5) 1_545
I4 Ag3 2.8832(11) .
I4 Ag1B 3.121(13) 1_545
I3 Ag12 2.8471(11) .
I3 Ag10 2.8507(10) .
I3 Ag2B 3.225(9) .
I2 Ag13 2.7999(10) .
I2 Ag14 2.8051(10) .
Ag14 Ag5 3.2235(13) .
Ag14 Ag9 3.2368(12) .
I1 Ag12 2.7734(11) .
I1 Ag3 2.8057(11) 1_665
Ag12 Ag10 2.9913(12) .
Ag11 Ag11 2.9658(17) 2_766
Ag11 I19 3.0206(11) 2_766
Ag9 I14 2.8010(10) 1_455
Ag9 Ag6A 3.0624(12) 1_455
Ag9 Ag6B 3.156(6) 1_455
Ag8 I20 2.9021(10) 2_676
Ag8 Ag1A 3.0320(14) .
Ag8 Ag8 3.1155(16) 2_676
Ag7 Ag2A 3.1471(13) .
Ag7 Ag2B 3.234(5) .
Ag6A Ag6B 1.443(9) .
Ag6A I11 2.8964(11) 1_655
Ag6A I21 2.9189(11) 1_655
Ag6A Ag9 3.0624(12) 1_655
Ag6A Ag4 3.3323(14) .
Ag6B I11 2.765(6) 1_655
Ag6B I21 2.878(6) 1_655
Ag6B I18 3.149(10) 1_655
Ag6B Ag9 3.156(6) 1_655
Ag4 I21 2.9570(11) 1_655
Ag3 I1 2.8057(11) 1_445
Ag3 Ag1B 2.935(11) 1_545
Ag2A Ag2B 1.227(8) .
Ag2A Ag1B 2.408(8) .
Ag2A I4 2.7697(12) 1_565
Ag2B I4 2.863(5) 1_565
Ag2B Ag1B 3.300(11) .
Ag1A Ag1B 1.644(13) .
Ag1A I13 2.7136(12) 1_565
Ag1B I13 2.693(7) 1_565
Ag1B Ag3 2.935(11) 1_565
Ag1B I4 3.121(13) 1_565
N6 C34 1.343(10) .
N6 C30 1.369(9) .
N6 C36 1.470(10) .
N7 C46 1.346(10) .
N7 C42 1.352(10) .
N7 C48 1.477(10) .
N8 C41 1.347(10) .
N8 C37 1.356(9) .
N8 C47 1.483(11) .
N5 C25 1.343(9) .
N5 C29 1.365(11) .
N5 C35 1.467(10) .
N4 C22 1.354(11) .
N4 C18 1.355(10) .
N4 C24 1.462(11) .
N3 C13 1.353(10) .
N3 C17 1.362(11) .
N3 C23 1.466(11) .
C18 C19 1.359(11) .
C18 C13 1.485(11) .
C30 C31 1.369(11) .
C30 C25 1.490(10) .
C25 C26 1.358(11) .
N1 C1 1.334(13) .
N1 C5 1.360(13) .
N1 C12 1.465(13) .
N2 C10 1.340(11) .
N2 C6 1.354(11) .
N2 C11 1.476(12) .
C37 C38 1.355(11) .
C37 C42 1.501(10) .
C43 C42 1.376(11) .
C43 C44 1.381(12) .
C31 C32 1.373(11) .
C13 C14 1.374(11) .
C6 C7 1.364(12) .
C6 C1 1.471(13) .
C34 C33 1.374(12) .
C39 C40 1.346(12) .
C39 C38 1.399(11) .
C26 C27 1.389(12) .
C40 C41 1.377(13) .
C45 C46 1.353(12) .
C45 C44 1.361(13) .
C33 C32 1.355(12) .
C1 C2 1.403(13) .
C27 C28 1.353(14) .
C22 C21 1.359(14) .
C21 C20 1.375(14) .
C10 C9 1.376(16) .
C29 C28 1.355(14) .
C7 C8 1.374(15) .
C19 C20 1.389(13) .
C14 C15 1.394(15) .
C17 C16 1.369(16) .
C9 C8 1.341(17) .
C2 C3 1.362(19) .
C16 C15 1.338(18) .
C5 C4 1.34(2) .
C3 C4 1.39(2) .
