#------------------------------------------------------------------------------
#$Date: 2019-11-07 21:48:30 +0200 (Thu, 07 Nov 2019) $
#$Revision: 223613 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/23/28/7232816.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7232816
loop_
_publ_author_name
'Cui, Lian-sheng'
'Meng, Xiang-min'
'Li, Yong-gang'
'Huang, Ke-rui'
'Li, Yuan-cheng'
'Long, Jin-qiao'
'Yao, Peng-fei'
_publ_section_title
;
 Syntheses, structural diversity, and photocatalytic-degradation
 properties for methylene blue of Co(ii) and Ni(ii) MOFs based on
 terephthalic acid and different imidazole bridging ligands
;
_journal_issue                   25
_journal_name_full               CrystEngComm
_journal_page_first              3798
_journal_paper_doi               10.1039/C9CE00433E
_journal_volume                  21
_journal_year                    2019
_chemical_formula_sum            'C26 H22 N4 Ni O7'
_chemical_formula_weight         561.19
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2018-04-03 deposited with the CCDC.    2019-05-22 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 93.830(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   6.3774(4)
_cell_length_b                   17.5788(11)
_cell_length_c                   22.2159(16)
_cell_measurement_reflns_used    29088
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.565
_cell_measurement_theta_min      2.49
_cell_volume                     2485.0(3)
_computing_cell_refinement       'Bruker FRAMBO'
_computing_data_collection       'Bruker FRAMBO'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0490
_diffrn_reflns_av_sigmaI/netI    0.0304
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            31580
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         2.99
_exptl_absorpt_coefficient_mu    0.835
_exptl_absorpt_correction_T_max  0.7311
_exptl_absorpt_correction_T_min  0.7153
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    1.500
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1160
_exptl_crystal_size_max          0.43
_exptl_crystal_size_mid          0.42
_exptl_crystal_size_min          0.40
_refine_diff_density_max         0.360
_refine_diff_density_min         -0.655
_refine_diff_density_rms         0.063
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.068
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     343
_refine_ls_number_reflns         4629
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.068
_refine_ls_R_factor_all          0.0669
_refine_ls_R_factor_gt           0.0456
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0381P)²+3.1208P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0996
_refine_ls_wR_factor_ref         0.1083
_reflns_number_gt                3633
_reflns_number_total             4629
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c9ce00433e2.cif
_cod_data_source_block           18
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7232814--7232819.cif.
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7232816
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ni1 Ni -0.02374(6) 0.73682(2) 0.535488(15) 0.03372(13) Uani 1 1 d .
N1 N 0.2469(4) 0.92519(16) 0.45556(12) 0.0437(7) Uani 1 1 d .
N2 N 0.1102(4) 0.83766(17) 0.51192(11) 0.0430(7) Uani 1 1 d .
N3 N 1.1546(4) 0.94608(16) 0.10584(12) 0.0429(7) Uani 1 1 d .
N4 N 1.3493(4) 0.86382(16) 0.06031(11) 0.0396(6) Uani 1 1 d .
O1 O 0.0501(3) 0.75743(14) 0.62508(8) 0.0434(6) Uani 1 1 d .
O2 O 0.3964(3) 0.73637(15) 0.63187(9) 0.0492(6) Uani 1 1 d .
O3 O 0.0444(4) 0.76558(16) 0.93780(9) 0.0521(6) Uani 1 1 d .
O4 O 0.3936(3) 0.78131(13) 0.94467(8) 0.0402(5) Uani 1 1 d .
O5 O 0.5801(5) 1.06310(15) 0.25822(12) 0.0696(9) Uani 1 1 d .
O6 O -0.3128(3) 0.79423(13) 0.54517(9) 0.0427(5) Uani 1 1 d .
H6B H -0.3614 0.7805 0.5782 0.051 Uiso 1 1 d R
H6C H -0.4003 0.7806 0.5167 0.051 Uiso 1 1 d R
O7 O 0.2590(3) 0.67548(14) 0.52255(9) 0.0451(6) Uani 1 1 d .
H7B H 0.3504 0.6878 0.5504 0.054 Uiso 1 1 d R
H7C H 0.3049 0.6893 0.4892 0.054 Uiso 1 1 d R
C1 C 0.2249(5) 0.75021(18) 0.65415(12) 0.0357(7) Uani 1 1 d .
C2 C 0.2176(5) 0.77422(19) 0.91539(12) 0.0359(7) Uani 1 1 d .
C3 C 0.2239(5) 0.75826(18) 0.72196(12) 0.0333(7) Uani 1 1 d .
C4 C 0.0405(5) 0.7748(2) 0.74907(13) 0.0416(8) Uani 1 1 d .
H4 H -0.0833 0.7822 0.7252 0.050 Uiso 1 1 calc R
C5 C 0.0381(5) 0.7806(2) 0.81110(13) 0.0402(8) Uani 1 1 d .
H5 H -0.0876 0.7906 0.8285 0.048 Uiso 1 1 calc R
C6 C 0.2214(5) 0.77175(18) 0.84753(12) 0.0335(7) Uani 1 1 d .
C7 C 0.4061(5) 0.7575(2) 0.82013(13) 0.0431(8) Uani 1 1 d .
H7 H 0.5314 0.7529 0.8438 0.052 Uiso 1 1 calc R
C8 C 0.4075(5) 0.7498(2) 0.75816(13) 0.0429(8) Uani 1 1 d .
H8 H 0.5327 0.7390 0.7407 0.051 Uiso 1 1 calc R
C9 C 0.1671(6) 0.8551(2) 0.45814(14) 0.0472(9) Uani 1 1 d .
H9 H 0.1535 0.8223 0.4253 0.057 Uiso 1 1 calc R
C10 C 0.1595(6) 0.9008(2) 0.54652(15) 0.0488(9) Uani 1 1 d .
H10 H 0.1393 0.9052 0.5874 0.059 Uiso 1 1 calc R
C11 C 0.2407(6) 0.9552(2) 0.51275(15) 0.0510(9) Uani 1 1 d .
H11 H 0.2842 1.0035 0.5254 0.061 Uiso 1 1 calc R
C12 C 0.3326(5) 0.95972(19) 0.40374(14) 0.0420(8) Uani 1 1 d .
C13 C 0.3139(6) 1.0367(2) 0.39412(15) 0.0472(9) Uani 1 1 d .
H13 H 0.2417 1.0667 0.4204 0.057 Uiso 1 1 calc R
C14 C 0.4025(6) 1.0695(2) 0.34543(15) 0.0467(8) Uani 1 1 d .
H14 H 0.3903 1.1216 0.3387 0.056 Uiso 1 1 calc R
C15 C 0.5083(5) 1.0250(2) 0.30701(15) 0.0442(8) Uani 1 1 d .
C16 C 0.5270(6) 0.9475(2) 0.31628(16) 0.0522(9) Uani 1 1 d .
H16 H 0.5975 0.9174 0.2897 0.063 Uiso 1 1 calc R
C17 C 0.4395(6) 0.9153(2) 0.36555(16) 0.0494(9) Uani 1 1 d .
H17 H 0.4533 0.8634 0.3728 0.059 Uiso 1 1 calc R
C18 C 1.2413(5) 0.8767(2) 0.10782(14) 0.0407(8) Uani 1 1 d .
H18 H 1.2271 0.8419 0.1388 0.049 Uiso 1 1 calc R
C19 C 1.3320(6) 0.9290(2) 0.02682(15) 0.0510(9) Uani 1 1 d .
H19 H 1.3946 0.9369 -0.0093 0.061 Uiso 1 1 calc R
C20 C 1.2114(6) 0.9802(2) 0.05361(16) 0.0565(10) Uani 1 1 d .
H20 H 1.1743 1.0286 0.0397 0.068 Uiso 1 1 calc R
C21 C 1.0081(5) 0.97520(19) 0.14663(14) 0.0423(8) Uani 1 1 d .
C22 C 0.8129(7) 0.9958(3) 0.12465(17) 0.0694(13) Uani 1 1 d .
H22 H 0.7753 0.9908 0.0837 0.083 Uiso 1 1 calc R
C23 C 0.6693(7) 1.0242(3) 0.16283(18) 0.0699(12) Uani 1 1 d .
H23 H 0.5365 1.0395 0.1477 0.084 Uiso 1 1 calc R
C24 C 0.7248(6) 1.0293(2) 0.22242(16) 0.0511(9) Uani 1 1 d .
C25 C 0.9171(7) 1.0072(3) 0.24528(17) 0.0758(14) Uani 1 1 d .
H25 H 0.9524 1.0105 0.2865 0.091 Uiso 1 1 calc R
C26 C 1.0611(6) 0.9795(3) 0.20660(17) 0.0691(13) Uani 1 1 d .
H26 H 1.1937 0.9640 0.2218 0.083 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N4 Ni1 O1 87.72(10) 4_476 .
N4 Ni1 N2 178.63(11) 4_476 .
O1 Ni1 N2 91.30(10) . .
N4 Ni1 O4 92.86(9) 4_476 4_575
O1 Ni1 O4 178.07(9) . 4_575
N2 Ni1 O4 88.15(9) . 4_575
N4 Ni1 O6 91.24(10) 4_476 .
O1 Ni1 O6 87.83(8) . .
N2 Ni1 O6 89.68(10) . .
O4 Ni1 O6 90.32(8) 4_575 .
N4 Ni1 O7 87.27(10) 4_476 .
O1 Ni1 O7 94.53(9) . .
N2 Ni1 O7 91.85(10) . .
O4 Ni1 O7 87.34(8) 4_575 .
O6 Ni1 O7 177.16(9) . .
C9 N1 C11 106.2(3) . .
C9 N1 C12 126.1(3) . .
C11 N1 C12 127.6(3) . .
C9 N2 C10 104.7(3) . .
C9 N2 Ni1 125.6(2) . .
C10 N2 Ni1 129.7(2) . .
C18 N3 C20 107.1(3) . .
C18 N3 C21 126.0(3) . .
C20 N3 C21 126.5(3) . .
C18 N4 C19 105.4(3) . .
C18 N4 Ni1 127.2(2) . 4_775
C19 N4 Ni1 126.9(2) . 4_775
C1 O1 Ni1 128.32(19) . .
C2 O4 Ni1 130.07(19) . 4_676
C15 O5 C24 120.7(3) . .
Ni1 O6 H6B 108.7 . .
Ni1 O6 H6C 108.7 . .
H6B O6 H6C 107.7 . .
Ni1 O7 H7B 108.5 . .
Ni1 O7 H7C 108.4 . .
H7B O7 H7C 107.6 . .
O2 C1 O1 125.7(3) . .
O2 C1 C3 118.2(3) . .
O1 C1 C3 116.0(3) . .
O3 C2 O4 125.7(3) . .
O3 C2 C6 117.9(3) . .
O4 C2 C6 116.3(3) . .
C4 C3 C8 118.5(3) . .
C4 C3 C1 120.9(3) . .
C8 C3 C1 120.6(3) . .
C3 C4 C5 121.0(3) . .
C3 C4 H4 119.5 . .
C5 C4 H4 119.5 . .
C4 C5 C6 120.6(3) . .
C4 C5 H5 119.7 . .
C6 C5 H5 119.7 . .
C7 C6 C5 118.2(3) . .
C7 C6 C2 121.0(3) . .
C5 C6 C2 120.7(3) . .
C8 C7 C6 121.1(3) . .
C8 C7 H7 119.4 . .
C6 C7 H7 119.4 . .
C3 C8 C7 120.4(3) . .
C3 C8 H8 119.8 . .
C7 C8 H8 119.8 . .
N2 C9 N1 112.7(3) . .
N2 C9 H9 123.7 . .
N1 C9 H9 123.7 . .
C11 C10 N2 110.2(3) . .
C11 C10 H10 124.9 . .
N2 C10 H10 124.9 . .
C10 C11 N1 106.2(3) . .
C10 C11 H11 126.9 . .
N1 C11 H11 126.9 . .
C17 C12 C13 120.5(3) . .
C17 C12 N1 119.1(3) . .
C13 C12 N1 120.4(3) . .
C12 C13 C14 119.8(3) . .
C12 C13 H13 120.1 . .
C14 C13 H13 120.1 . .
C15 C14 C13 119.7(3) . .
C15 C14 H14 120.2 . .
C13 C14 H14 120.2 . .
C14 C15 O5 114.6(3) . .
C14 C15 C16 120.8(3) . .
O5 C15 C16 124.5(3) . .
C15 C16 C17 119.0(3) . .
C15 C16 H16 120.5 . .
C17 C16 H16 120.5 . .
C12 C17 C16 120.2(3) . .
C12 C17 H17 119.9 . .
C16 C17 H17 119.9 . .
N4 C18 N3 111.5(3) . .
N4 C18 H18 124.2 . .
N3 C18 H18 124.2 . .
C20 C19 N4 110.3(3) . .
C20 C19 H19 124.8 . .
N4 C19 H19 124.8 . .
C19 C20 N3 105.7(3) . .
C19 C20 H20 127.1 . .
N3 C20 H20 127.1 . .
C26 C21 C22 120.1(3) . .
C26 C21 N3 120.6(3) . .
C22 C21 N3 119.2(3) . .
C21 C22 C23 120.3(4) . .
C21 C22 H22 119.8 . .
C23 C22 H22 119.8 . .
C24 C23 C22 119.0(4) . .
C24 C23 H23 120.5 . .
C22 C23 H23 120.5 . .
C23 C24 C25 121.3(3) . .
C23 C24 O5 116.7(4) . .
C25 C24 O5 121.8(4) . .
C24 C25 C26 119.3(4) . .
C24 C25 H25 120.3 . .
C26 C25 H25 120.3 . .
C21 C26 C25 119.8(4) . .
C21 C26 H26 120.1 . .
C25 C26 H26 120.1 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ni1 N4 2.037(3) 4_476
Ni1 O1 2.0469(19) .
Ni1 N2 2.051(3) .
Ni1 O4 2.0756(19) 4_575
Ni1 O6 2.125(2) .
Ni1 O7 2.137(2) .
N1 C9 1.335(4) .
N1 C11 1.379(4) .
N1 C12 1.441(4) .
N2 C9 1.308(4) .
N2 C10 1.375(4) .
N3 C18 1.339(4) .
N3 C20 1.376(4) .
N3 C21 1.438(4) .
N4 C18 1.318(4) .
N4 C19 1.366(4) .
N4 Ni1 2.037(3) 4_775
O1 C1 1.257(4) .
O2 C1 1.254(4) .
O3 C2 1.250(4) .
O4 C2 1.265(4) .
O4 Ni1 2.0756(19) 4_676
O5 C15 1.378(4) .
O5 C24 1.391(4) .
O6 H6B 0.8501 .
O6 H6C 0.8500 .
O7 H7B 0.8501 .
O7 H7C 0.8500 .
C1 C3 1.513(4) .
C2 C6 1.510(4) .
C3 C4 1.382(4) .
C3 C8 1.384(4) .
C4 C5 1.383(4) .
C4 H4 0.9300 .
C5 C6 1.385(4) .
C5 H5 0.9300 .
C6 C7 1.384(4) .
C7 C8 1.384(4) .
C7 H7 0.9300 .
C8 H8 0.9300 .
C9 H9 0.9300 .
C10 C11 1.341(5) .
C10 H10 0.9300 .
C11 H11 0.9300 .
C12 C17 1.368(5) .
C12 C13 1.375(5) .
C13 C14 1.379(5) .
C13 H13 0.9300 .
C14 C15 1.369(5) .
C14 H14 0.9300 .
C15 C16 1.382(5) .
C16 C17 1.382(5) .
C16 H16 0.9300 .
C17 H17 0.9300 .
C18 H18 0.9300 .
C19 C20 1.349(5) .
C19 H19 0.9300 .
C20 H20 0.9300 .
C21 C26 1.355(5) .
C21 C22 1.356(5) .
C22 C23 1.382(5) .
C22 H22 0.9300 .
C23 C24 1.350(5) .
C23 H23 0.9300 .
C24 C25 1.353(6) .
C25 C26 1.387(5) .
C25 H25 0.9300 .
C26 H26 0.9300 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
N4 Ni1 N2 C9 118(4) 4_476
O1 Ni1 N2 C9 162.1(3) .
O4 Ni1 N2 C9 -19.8(3) 4_575
O6 Ni1 N2 C9 -110.1(3) .
O7 Ni1 N2 C9 67.5(3) .
N4 Ni1 N2 C10 -63(5) 4_476
O1 Ni1 N2 C10 -18.3(3) .
O4 Ni1 N2 C10 159.9(3) 4_575
O6 Ni1 N2 C10 69.5(3) .
O7 Ni1 N2 C10 -112.9(3) .
N4 Ni1 O1 C1 101.3(3) 4_476
N2 Ni1 O1 C1 -77.8(3) .
O4 Ni1 O1 C1 -151(3) 4_575
O6 Ni1 O1 C1 -167.4(3) .
O7 Ni1 O1 C1 14.2(3) .
Ni1 O1 C1 O2 8.2(5) .
Ni1 O1 C1 C3 -171.0(2) .
Ni1 O4 C2 O3 12.0(5) 4_676
Ni1 O4 C2 C6 -164.4(2) 4_676
O2 C1 C3 C4 178.8(3) .
O1 C1 C3 C4 -1.9(5) .
O2 C1 C3 C8 -0.5(5) .
O1 C1 C3 C8 178.8(3) .
C8 C3 C4 C5 -2.0(5) .
C1 C3 C4 C5 178.6(3) .
C3 C4 C5 C6 1.6(5) .
C4 C5 C6 C7 0.4(5) .
C4 C5 C6 C2 -177.0(3) .
O3 C2 C6 C7 -160.0(3) .
O4 C2 C6 C7 16.7(5) .
O3 C2 C6 C5 17.3(5) .
O4 C2 C6 C5 -166.0(3) .
C5 C6 C7 C8 -2.0(5) .
C2 C6 C7 C8 175.4(3) .
C4 C3 C8 C7 0.4(5) .
C1 C3 C8 C7 179.8(3) .
C6 C7 C8 C3 1.6(6) .
C10 N2 C9 N1 -0.8(4) .
Ni1 N2 C9 N1 179.0(2) .
C11 N1 C9 N2 0.1(4) .
C12 N1 C9 N2 176.8(3) .
C9 N2 C10 C11 1.2(4) .
Ni1 N2 C10 C11 -178.5(3) .
N2 C10 C11 N1 -1.2(4) .
C9 N1 C11 C10 0.7(4) .
C12 N1 C11 C10 -176.0(3) .
C9 N1 C12 C17 -34.9(5) .
C11 N1 C12 C17 141.2(4) .
C9 N1 C12 C13 147.5(4) .
C11 N1 C12 C13 -36.4(5) .
C17 C12 C13 C14 0.4(6) .
N1 C12 C13 C14 177.9(3) .
C12 C13 C14 C15 0.0(6) .
C13 C14 C15 O5 176.6(3) .
C13 C14 C15 C16 0.2(6) .
C24 O5 C15 C14 167.0(4) .
C24 O5 C15 C16 -16.8(6) .
C14 C15 C16 C17 -0.8(6) .
O5 C15 C16 C17 -176.9(4) .
C13 C12 C17 C16 -1.0(6) .
N1 C12 C17 C16 -178.6(3) .
C15 C16 C17 C12 1.2(6) .
C19 N4 C18 N3 0.7(4) .
Ni1 N4 C18 N3 -170.7(2) 4_775
C20 N3 C18 N4 -0.2(4) .
C21 N3 C18 N4 172.5(3) .
C18 N4 C19 C20 -1.0(4) .
Ni1 N4 C19 C20 170.5(3) 4_775
N4 C19 C20 N3 0.9(5) .
C18 N3 C20 C19 -0.4(4) .
C21 N3 C20 C19 -173.1(3) .
C18 N3 C21 C26 59.2(5) .
C20 N3 C21 C26 -129.4(4) .
C18 N3 C21 C22 -118.4(4) .
C20 N3 C21 C22 53.0(5) .
C26 C21 C22 C23 2.6(7) .
N3 C21 C22 C23 -179.8(4) .
C21 C22 C23 C24 -1.6(7) .
C22 C23 C24 C25 -0.2(7) .
C22 C23 C24 O5 175.7(4) .
C15 O5 C24 C23 124.0(4) .
C15 O5 C24 C25 -60.1(6) .
C23 C24 C25 C26 0.9(7) .
O5 C24 C25 C26 -174.8(4) .
C22 C21 C26 C25 -1.9(7) .
N3 C21 C26 C25 -179.5(4) .
C24 C25 C26 C21 0.2(7) .
