#------------------------------------------------------------------------------
#$Date: 2019-11-23 12:56:55 +0200 (Sat, 23 Nov 2019) $
#$Revision: 233380 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/23/58/7235846.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7235846
loop_
_publ_author_name
'Gong, Kaining'
'Wang, Weijie'
'Yan, Jinshuang'
'Han, Zhangang'
_publ_section_title
;
 Highly reduced molybdophosphate as a noble-metal-free catalyst for the
 reduction of chromium using formic acid as a reducing agent
;
_journal_issue                   11
_journal_name_full               'Journal of Materials Chemistry A'
_journal_page_first              6019
_journal_paper_doi               10.1039/C4TA06830K
_journal_volume                  3
_journal_year                    2015
_chemical_formula_sum            'C48 H110 Co5 Mo12 N8 Na2 O87 P8'
_chemical_formula_weight         3931.11
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2014-12-05 deposited with the CCDC.
2015-02-16 downloaded from the CCDC.
;
_cell_angle_alpha                105.9200(10)
_cell_angle_beta                 110.0210(10)
_cell_angle_gamma                101.5370(10)
_cell_formula_units_Z            1
_cell_length_a                   14.2222(8)
_cell_length_b                   15.0491(14)
_cell_length_c                   16.4125(8)
_cell_measurement_reflns_used    9962
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.25
_cell_measurement_theta_min      2.37
_cell_volume                     3001.3(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0117
_diffrn_reflns_av_sigmaI/netI    0.0221
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            14396
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.80
_exptl_absorpt_coefficient_mu    2.105
_exptl_absorpt_correction_T_max  0.699
_exptl_absorpt_correction_T_min  0.625
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.175
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1931
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.17
_refine_diff_density_max         1.302
_refine_diff_density_min         -0.495
_refine_diff_density_rms         0.098
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     858
_refine_ls_number_reflns         10396
_refine_ls_number_restraints     19
_refine_ls_restrained_S_all      1.073
_refine_ls_R_factor_all          0.0265
_refine_ls_R_factor_gt           0.0245
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0365P)²+7.9837P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0733
_refine_ls_wR_factor_ref         0.0747
_reflns_number_gt                9744
_reflns_number_total             10396
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4ta06830k1.cif
_cod_data_source_block           37
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_exptl_crystal_density_meas' value 'none' was changed to
'?' -- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      'P-1   '
_cod_database_code               7235846
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Mo1 Mo 0.66303(2) 0.40899(2) 0.17926(2) 0.01689(8) Uani 1 1 d .
Mo2 Mo 0.25854(2) 0.29875(2) -0.04762(2) 0.01735(8) Uani 1 1 d .
Mo3 Mo 0.39373(2) 0.35865(2) 0.12518(2) 0.01698(8) Uani 1 1 d .
Mo4 Mo 0.45662(2) 0.68253(2) 0.18359(2) 0.01705(8) Uani 1 1 d .
Mo5 Mo 0.72856(2) 0.39214(2) 0.04835(2) 0.01710(8) Uani 1 1 d .
Mo6 Mo 0.65656(2) 0.72450(2) 0.22524(2) 0.01884(8) Uani 1 1 d .
Co1 Co 0.5000 0.5000 0.0000 0.01662(14) Uani 1 2 d S
Co2 Co 0.27846(4) 0.95778(4) 0.03952(4) 0.02103(12) Uani 1 1 d .
Co3 Co 0.63122(4) 0.11923(4) 0.34739(4) 0.02450(12) Uani 1 1 d .
Na1 Na 0.64472(16) 0.01511(12) 0.14360(12) 0.0406(4) Uani 1 1 d .
P1 P 0.54863(8) 0.28904(7) 0.28163(7) 0.0214(2) Uani 1 1 d .
P2 P 0.15335(8) 0.09521(7) -0.23928(7) 0.0256(2) Uani 1 1 d .
P3 P 0.47849(7) 0.23259(6) -0.02834(6) 0.01534(18) Uani 1 1 d .
P4 P 0.28240(8) 0.79272(7) 0.12455(7) 0.0194(2) Uani 1 1 d .
O1 O 0.6355(2) 0.46392(18) 0.08027(17) 0.0183(5) Uani 1 1 d .
O2 O 0.3860(2) 0.41478(18) 0.02789(17) 0.0190(5) Uani 1 1 d .
O3 O 0.53644(19) 0.60746(17) 0.13237(17) 0.0179(5) Uani 1 1 d .
O4 O 0.6966(2) 0.6935(2) 0.3190(2) 0.0305(6) Uani 1 1 d .
O5 O 0.7480(2) 0.66431(18) 0.16333(18) 0.0202(5) Uani 1 1 d .
H5A H 0.7200 0.5966 0.1385 0.047(15) Uiso 1 1 d R
O6 O 0.7808(2) 0.8530(2) 0.2795(2) 0.0307(7) Uani 1 1 d .
O7 O 0.5715(2) 0.80601(18) 0.24798(18) 0.0227(6) Uani 1 1 d .
O8 O 0.43415(19) 0.72236(17) 0.05500(17) 0.0178(5) Uani 1 1 d .
O9 O 0.4521(2) 0.6396(2) 0.26661(19) 0.0267(6) Uani 1 1 d .
O10 O 0.3186(2) 0.57617(18) 0.07364(17) 0.0193(5) Uani 1 1 d .
H10A H 0.3395 0.5244 0.0660 0.043(14) Uiso 1 1 d R
O11 O 0.3582(2) 0.76206(19) 0.19472(18) 0.0236(6) Uani 1 1 d .
O12 O 0.3389(2) 0.89104(19) 0.12790(19) 0.0239(6) Uani 1 1 d .
O13 O 0.1931(2) 0.8079(2) 0.1565(2) 0.0298(6) Uani 1 1 d .
H13A H 0.1546 0.7660 0.1495 0.09(3) Uiso 1 1 d R
O14 O 0.7653(2) 0.4999(2) 0.26919(19) 0.0278(6) Uani 1 1 d .
O15 O 0.8478(2) 0.4777(2) 0.1067(2) 0.0277(6) Uani 1 1 d .
O16 O 0.7702(2) 0.28680(19) -0.02646(19) 0.0232(6) Uani 1 1 d .
O17 O 0.7223(2) 0.31551(18) 0.12558(18) 0.0211(5) Uani 1 1 d .
O18 O 0.5450(2) 0.46010(18) 0.20607(18) 0.0195(5) Uani 1 1 d .
H18A H 0.5481 0.5134 0.1942 0.057(17) Uiso 1 1 d R
O19 O 0.50452(19) 0.29830(18) 0.07263(17) 0.0179(5) Uani 1 1 d .
O20 O 0.37302(19) 0.23797(18) -0.09400(17) 0.0182(5) Uani 1 1 d .
O21 O 0.6379(2) 0.3207(2) 0.25260(19) 0.0247(6) Uani 1 1 d .
O22 O 0.5798(3) 0.3571(2) 0.3837(2) 0.0418(8) Uani 1 1 d .
H22 H 0.5879 0.4135 0.3866 0.063 Uiso 1 1 calc R
O23 O 0.5347(2) 0.1867(2) 0.28052(19) 0.0263(6) Uani 1 1 d .
O24 O 0.4440(2) 0.2919(2) 0.21668(19) 0.0255(6) Uani 1 1 d .
O25 O 0.2907(2) 0.23223(18) 0.03896(18) 0.0205(5) Uani 1 1 d .
O26 O 0.3283(2) 0.4167(2) 0.1773(2) 0.0269(6) Uani 1 1 d .
O27 O 0.1631(2) 0.3424(2) -0.0331(2) 0.0267(6) Uani 1 1 d .
O28 O 0.1606(2) 0.16419(19) -0.14798(19) 0.0252(6) Uani 1 1 d .
O29 O 0.0345(3) 0.0592(3) -0.3115(2) 0.0500(9) Uani 1 1 d .
H29 H 0.0171 0.1064 -0.3184 0.075 Uiso 1 1 calc R
O30 O 0.4706(2) 0.12964(18) -0.03430(18) 0.0203(5) Uani 1 1 d .
O31 O 0.1797(3) 0.0064(2) -0.2300(3) 0.0511(9) Uani 1 1 d .
C1 C 0.0753(4) 0.7901(3) -0.1074(3) 0.0349(10) Uani 1 1 d .
C2 C -0.0313(4) 0.7342(3) -0.1506(4) 0.0432(12) Uani 1 1 d .
C3 C -0.0927(4) 0.7611(4) -0.1054(4) 0.0471(13) Uani 1 1 d .
C4 C -0.0484(4) 0.8409(4) -0.0223(4) 0.0410(11) Uani 1 1 d .
C5 C 0.0585(3) 0.8927(3) 0.0157(3) 0.0286(9) Uani 1 1 d .
C6 C 0.1120(3) 0.9781(3) 0.1038(3) 0.0294(9) Uani 1 1 d .
C7 C 0.0639(4) 1.0096(4) 0.1620(4) 0.0442(12) Uani 1 1 d .
C8 C 0.1203(5) 1.0909(4) 0.2430(4) 0.0508(14) Uani 1 1 d .
C9 C 0.2240(4) 1.1409(4) 0.2671(4) 0.0424(11) Uani 1 1 d .
C10 C 0.2672(4) 1.1047(3) 0.2069(3) 0.0349(10) Uani 1 1 d .
C11 C -0.0739(5) 0.6498(5) -0.2416(5) 0.0701(18) Uani 1 1 d .
H11A H -0.1453 0.6134 -0.2569 0.105 Uiso 1 1 calc R
H11B H -0.0309 0.6082 -0.2363 0.105 Uiso 1 1 calc R
H11C H -0.0729 0.6738 -0.2899 0.105 Uiso 1 1 calc R
C12 C 0.2907(5) 1.2306(5) 0.3543(4) 0.0684(18) Uani 1 1 d .
H12A H 0.3580 1.2240 0.3857 0.103 Uiso 1 1 calc R
H12B H 0.2554 1.2380 0.3950 0.103 Uiso 1 1 calc R
H12C H 0.3012 1.2872 0.3379 0.103 Uiso 1 1 calc R
C13 C 0.8129(4) 0.3016(4) 0.5000(4) 0.0432(12) Uani 1 1 d .
C14 C 0.8719(4) 0.3733(4) 0.5878(4) 0.0525(14) Uani 1 1 d .
C15 C 0.8305(5) 0.3752(4) 0.6529(4) 0.0593(16) Uani 1 1 d .
C16 C 0.7345(5) 0.3094(4) 0.6299(4) 0.0542(14) Uani 1 1 d .
C17 C 0.6790(4) 0.2401(3) 0.5390(3) 0.0354(10) Uani 1 1 d .
C18 C 0.5751(4) 0.1676(3) 0.5063(3) 0.0363(10) Uani 1 1 d .
C19 C 0.5161(5) 0.1676(4) 0.5582(4) 0.0527(14) Uani 1 1 d .
C20 C 0.4165(5) 0.0999(4) 0.5201(4) 0.0545(14) Uani 1 1 d D
C21 C 0.3748(4) 0.0328(4) 0.4301(3) 0.0412(11) Uani 1 1 d .
C22 C 0.4390(4) 0.0349(3) 0.3829(3) 0.0350(10) Uani 1 1 d .
C23 C 0.9772(5) 0.4440(5) 0.6091(5) 0.086(2) Uani 1 1 d .
H23A H 0.9660 0.4991 0.5934 0.129 Uiso 1 1 calc R
H23B H 1.0098 0.4118 0.5731 0.129 Uiso 1 1 calc R
H23C H 1.0225 0.4660 0.6745 0.129 Uiso 1 1 calc R
C24 C 0.2657(4) -0.0404(5) 0.3843(4) 0.0549(14) Uani 1 1 d .
H24A H 0.2605 -0.0805 0.4201 0.082 Uiso 1 1 calc R
H24B H 0.2521 -0.0807 0.3222 0.082 Uiso 1 1 calc R
H24C H 0.2147 -0.0068 0.3811 0.082 Uiso 1 1 calc R
N1 N 0.1197(3) 0.8666(2) -0.0273(3) 0.0281(8) Uani 1 1 d .
N2 N 0.2142(3) 1.0259(2) 0.1278(3) 0.0280(8) Uani 1 1 d .
N3 N 0.7199(3) 0.2360(3) 0.4762(3) 0.0333(8) Uani 1 1 d .
N4 N 0.5366(3) 0.1001(3) 0.4193(2) 0.0301(8) Uani 1 1 d .
O1W O 0.3363(2) 0.88330(19) -0.05440(19) 0.0242(6) Uani 1 1 d .
H1WB H 0.3996 0.8823 -0.0162 0.08(2) Uiso 1 1 d R
H1WA H 0.3097 0.8179 -0.0823 0.043(14) Uiso 1 1 d R
O2W O 0.4363(2) 1.0607(2) 0.0977(2) 0.0284(6) Uani 1 1 d .
H2WA H 0.4507 1.0990 0.0681 0.08(2) Uiso 1 1 d R
H2WB H 0.4637 1.1031 0.1531 0.029(12) Uiso 1 1 d R
O3W O 0.2387(3) 1.0377(2) -0.0446(2) 0.0360(7) Uani 1 1 d .
H3WA H 0.2638 1.0984 -0.0204 0.049(16) Uiso 1 1 d R
H3WB H 0.2048 1.0202 -0.1081 0.060(18) Uiso 1 1 d R
O4W O 0.7211(2) 0.1678(2) 0.2736(2) 0.0319(7) Uani 1 1 d .
H4WA H 0.7028 0.2190 0.2598 0.10(3) Uiso 1 1 d R
H4WB H 0.7957 0.1822 0.2966 0.058(17) Uiso 1 1 d R
O5W O 0.7429(3) 0.0474(3) 0.3902(2) 0.0443(8) Uani 1 1 d .
H5WA H 0.7438 -0.0026 0.3486 0.08(2) Uiso 1 1 d R
H5WB H 0.8049 0.0790 0.4383 0.09(2) Uiso 1 1 d R
O6W O 0.5512(2) -0.01999(19) 0.23770(19) 0.0272(6) Uani 1 1 d .
H6WA H 0.4845 -0.0420 0.1953 0.051(16) Uiso 1 1 d R
H6WB H 0.5569 -0.0736 0.2408 0.043(15) Uiso 1 1 d R
O7W O 0.1404(5) 0.5141(4) 0.1182(4) 0.0912(17) Uani 1 1 d .
H7WA H 0.1999 0.5192 0.1145 0.109 Uiso 1 1 d R
H7WB H 0.0777 0.4742 0.0939 0.109 Uiso 1 1 d R
O8W O 0.9350(5) 0.1379(5) 0.5315(5) 0.0490(18) Uani 0.50 1 d PU
H8WA H 0.9643 0.1801 0.5156 0.059 Uiso 0.50 1 d PR
H8WB H 0.9498 0.1197 0.5769 0.059 Uiso 0.50 1 d PR
O9W O 0.8820(7) 0.8986(6) 0.4903(5) 0.066(2) Uani 0.50 1 d PU
H9WA H 0.8247 0.9074 0.4842 0.079 Uiso 0.50 1 d PR
H9WB H 0.9175 0.9527 0.4942 0.079 Uiso 0.50 1 d PR
O10W O 0.8836(10) 0.7174(10) 0.5178(8) 0.112(4) Uani 0.50 1 d PU
H10C H 0.8260 0.6767 0.4814 0.134 Uiso 0.50 1 d PR
H10D H 0.9104 0.7547 0.4954 0.134 Uiso 0.50 1 d PR
O11W O 0.6177(14) 0.5464(6) 0.4142(6) 0.134(5) Uani 0.50 1 d PU
H11E H 0.6302 0.5452 0.4600 0.161 Uiso 0.50 1 d PR
H11D H 0.5557 0.5425 0.4001 0.161 Uiso 0.50 1 d PR
O12W O 0.9263(3) 0.1921(3) 0.3240(4) 0.0742(13) Uani 1 1 d U
H12E H 0.9692 0.2225 0.3812 0.089 Uiso 1 1 d R
H12D H 0.9021 0.1299 0.2956 0.089 Uiso 1 1 d R
O13W O 0.0451(3) 0.6548(3) 0.1363(3) 0.0633(11) Uani 1 1 d .
H13C H -0.0097 0.6683 0.1318 0.076 Uiso 1 1 d R
H13D H 0.0457 0.6021 0.0989 0.076 Uiso 1 1 d R
O14W O 0.0210(4) 0.2583(4) 0.7178(3) 0.0822(15) Uani 1 1 d .
H14C H 0.0299 0.3180 0.7143 0.099 Uiso 1 1 d R
H14D H -0.0061 0.2657 0.7550 0.099 Uiso 1 1 d R
O15W O 0.457(2) 0.5506(16) 0.4216(12) 0.240(13) Uani 0.50 1 d P
H15C H 0.4936 0.6091 0.4553 0.289 Uiso 0.50 1 d PR
H15D H 0.3901 0.5186 0.3961 0.289 Uiso 0.50 1 d PR
H1 H 0.116(4) 0.774(3) -0.139(3) 0.032(12) Uiso 1 1 d .
H2 H -0.164(5) 0.729(4) -0.132(4) 0.054(16) Uiso 1 1 d .
H3 H -0.090(5) 0.862(4) 0.009(4) 0.054(16) Uiso 1 1 d .
H4 H 0.002(5) 0.976(4) 0.147(4) 0.047(16) Uiso 1 1 d .
H5 H 0.075(5) 1.107(4) 0.276(4) 0.067(18) Uiso 1 1 d .
H6 H 0.339(4) 1.130(3) 0.220(3) 0.030(12) Uiso 1 1 d .
H7 H 0.842(4) 0.294(4) 0.454(4) 0.052(16) Uiso 1 1 d .
H8 H 0.873(7) 0.420(6) 0.725(6) 0.12(3) Uiso 1 1 d .
H9 H 0.707(5) 0.319(4) 0.682(4) 0.068(18) Uiso 1 1 d .
H10 H 0.548(5) 0.210(5) 0.616(5) 0.08(2) Uiso 1 1 d .
H11 H 0.388(6) 0.103(6) 0.565(4) 0.10(3) Uiso 1 1 d D
H12 H 0.418(4) -0.021(4) 0.318(4) 0.042(14) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O14 Mo1 O17 106.24(13) . .
O14 Mo1 O1 102.03(12) . .
O17 Mo1 O1 95.78(10) . .
O14 Mo1 O21 96.74(12) . .
O17 Mo1 O21 85.47(11) . .
O1 Mo1 O21 159.99(11) . .
O14 Mo1 O18 95.73(12) . .
O17 Mo1 O18 156.97(10) . .
O1 Mo1 O18 86.10(10) . .
O21 Mo1 O18 85.18(10) . .
O14 Mo1 O19 168.04(12) . .
O17 Mo1 O19 85.06(10) . .
O1 Mo1 O19 80.26(9) . .
O21 Mo1 O19 79.96(10) . .
O18 Mo1 O19 72.61(9) . .
O14 Mo1 Mo5 101.14(10) . .
O17 Mo1 Mo5 48.24(7) . .
O1 Mo1 Mo5 49.19(7) . .
O21 Mo1 Mo5 133.36(8) . .
O18 Mo1 Mo5 134.46(7) . .
O19 Mo1 Mo5 89.27(6) . .
O27 Mo2 O25 104.96(12) . .
O27 Mo2 O2 102.05(12) . .
O25 Mo2 O2 95.59(10) . .
O27 Mo2 O28 97.01(12) . .
O25 Mo2 O28 86.70(11) . .
O2 Mo2 O28 159.47(11) . .
O27 Mo2 O5 95.96(12) . 2_665
O25 Mo2 O5 157.83(10) . 2_665
O2 Mo2 O5 86.98(10) . 2_665
O28 Mo2 O5 83.51(10) . 2_665
O27 Mo2 O20 169.70(12) . .
O25 Mo2 O20 83.95(10) . .
O2 Mo2 O20 81.88(10) . .
O28 Mo2 O20 78.07(10) . .
O5 Mo2 O20 74.60(9) 2_665 .
O27 Mo2 Mo3 100.04(10) . .
O25 Mo2 Mo3 48.03(8) . .
O2 Mo2 Mo3 49.23(7) . .
O28 Mo2 Mo3 134.35(8) . .
O5 Mo2 Mo3 135.54(7) 2_665 .
O20 Mo2 Mo3 89.76(6) . .
O26 Mo3 O25 105.01(12) . .
O26 Mo3 O2 101.09(12) . .
O25 Mo3 O2 95.08(10) . .
O26 Mo3 O24 97.14(12) . .
O25 Mo3 O24 86.96(11) . .
O2 Mo3 O24 160.43(11) . .
O26 Mo3 O18 98.35(12) . .
O25 Mo3 O18 155.54(10) . .
O2 Mo3 O18 87.36(10) . .
O24 Mo3 O18 82.98(10) . .
O26 Mo3 O19 171.27(12) . .
O25 Mo3 O19 83.45(10) . .
O2 Mo3 O19 79.98(9) . .
O24 Mo3 O19 80.92(10) . .
O18 Mo3 O19 72.99(9) . .
O26 Mo3 Mo2 99.33(10) . .
O25 Mo3 Mo2 47.96(7) . .
O2 Mo3 Mo2 48.77(7) . .
O24 Mo3 Mo2 134.63(8) . .
O18 Mo3 Mo2 135.06(7) . .
O19 Mo3 Mo2 87.92(6) . .
O9 Mo4 O7 105.64(13) . .
O9 Mo4 O3 101.00(12) . .
O7 Mo4 O3 95.55(11) . .
O9 Mo4 O11 96.00(12) . .
O7 Mo4 O11 86.74(11) . .
O3 Mo4 O11 161.51(10) . .
O9 Mo4 O10 96.85(12) . .
O7 Mo4 O10 156.42(10) . .
O3 Mo4 O10 86.88(10) . .
O11 Mo4 O10 83.91(10) . .
O9 Mo4 O8 170.16(12) . .
O7 Mo4 O8 83.76(10) . .
O3 Mo4 O8 80.61(9) . .
O11 Mo4 O8 81.42(10) . .
O10 Mo4 O8 73.48(9) . .
O9 Mo4 Mo6 99.46(10) . .
O7 Mo4 Mo6 48.27(8) . .
O3 Mo4 Mo6 49.05(7) . .
O11 Mo4 Mo6 134.85(8) . .
O10 Mo4 Mo6 135.10(7) . .
O8 Mo4 Mo6 88.94(6) . .
O15 Mo5 O17 105.34(13) . .
O15 Mo5 O1 102.50(12) . .
O17 Mo5 O1 95.51(10) . .
O15 Mo5 O16 97.72(12) . .
O17 Mo5 O16 87.17(11) . .
O1 Mo5 O16 158.07(11) . .
O15 Mo5 O10 97.63(12) . 2_665
O17 Mo5 O10 156.30(10) . 2_665
O1 Mo5 O10 84.98(10) . 2_665
O16 Mo5 O10 84.00(10) . 2_665
O15 Mo5 O8 170.00(12) . 2_665
O17 Mo5 O8 83.68(10) . 2_665
O1 Mo5 O8 80.52(9) . 2_665
O16 Mo5 O8 78.15(10) . 2_665
O10 Mo5 O8 73.00(9) 2_665 2_665
O15 Mo5 Mo1 100.79(10) . .
O17 Mo5 Mo1 48.12(7) . .
O1 Mo5 Mo1 49.02(7) . .
O16 Mo5 Mo1 134.69(8) . .
O10 Mo5 Mo1 133.05(7) 2_665 .
O8 Mo5 Mo1 88.41(6) 2_665 .
O4 Mo6 O7 105.06(13) . .
O4 Mo6 O3 102.41(13) . .
O7 Mo6 O3 95.84(11) . .
O4 Mo6 O6 96.41(13) . .
O7 Mo6 O6 86.49(12) . .
O3 Mo6 O6 159.69(11) . .
O4 Mo6 O5 96.70(12) . .
O7 Mo6 O5 157.15(10) . .
O3 Mo6 O5 86.04(10) . .
O6 Mo6 O5 84.22(11) . .
O4 Mo6 O20 170.11(12) . 2_665
O7 Mo6 O20 83.99(10) . 2_665
O3 Mo6 O20 80.24(9) . 2_665
O6 Mo6 O20 79.95(10) . 2_665
O5 Mo6 O20 73.86(9) . 2_665
O4 Mo6 Mo4 100.10(10) . .
O7 Mo6 Mo4 48.29(8) . .
O3 Mo6 Mo4 49.32(7) . .
O6 Mo6 Mo4 134.46(9) . .
O5 Mo6 Mo4 134.65(7) . .
O20 Mo6 Mo4 88.86(6) 2_665 .
O2 Co1 O2 180.0 2_665 .
O2 Co1 O3 95.37(9) 2_665 .
O2 Co1 O3 84.63(9) . .
O2 Co1 O3 84.63(9) 2_665 2_665
O2 Co1 O3 95.37(9) . 2_665
O3 Co1 O3 180.0 . 2_665
O2 Co1 O1 96.77(9) 2_665 2_665
O2 Co1 O1 83.23(9) . 2_665
O3 Co1 O1 95.97(9) . 2_665
O3 Co1 O1 84.04(9) 2_665 2_665
O2 Co1 O1 83.23(9) 2_665 .
O2 Co1 O1 96.77(9) . .
O3 Co1 O1 84.04(9) . .
O3 Co1 O1 95.96(9) 2_665 .
O1 Co1 O1 180.0 2_665 .
O12 Co2 O3W 171.93(12) . .
O12 Co2 N1 99.18(12) . .
O3W Co2 N1 88.81(13) . .
O12 Co2 N2 90.73(12) . .
O3W Co2 N2 92.04(13) . .
N1 Co2 N2 78.18(14) . .
O12 Co2 O1W 89.73(11) . .
O3W Co2 O1W 87.87(12) . .
N1 Co2 O1W 99.03(12) . .
N2 Co2 O1W 177.20(12) . .
O12 Co2 O2W 87.46(11) . .
O3W Co2 O2W 84.54(12) . .
N1 Co2 O2W 173.35(12) . .
N2 Co2 O2W 102.08(12) . .
O1W Co2 O2W 80.70(11) . .
O23 Co3 N3 98.41(13) . .
O23 Co3 N4 88.88(13) . .
N3 Co3 N4 78.18(15) . .
O23 Co3 O6W 94.42(11) . .
N3 Co3 O6W 165.70(13) . .
N4 Co3 O6W 95.84(13) . .
O23 Co3 O5W 166.25(13) . .
N3 Co3 O5W 88.22(14) . .
N4 Co3 O5W 104.32(14) . .
O6W Co3 O5W 80.63(13) . .
O23 Co3 O4W 80.76(11) . .
N3 Co3 O4W 96.75(13) . .
N4 Co3 O4W 167.74(12) . .
O6W Co3 O4W 91.51(11) . .
O5W Co3 O4W 86.53(13) . .
O23 Co3 Na1 87.46(9) . .
N3 Co3 Na1 140.18(11) . .
N4 Co3 Na1 141.55(11) . .
O6W Co3 Na1 46.43(8) . .
O5W Co3 Na1 79.82(10) . .
O4W Co3 Na1 45.10(8) . .
O30 Na1 O4W 161.66(14) 2_655 .
O30 Na1 O1W 103.84(11) 2_655 2_665
O4W Na1 O1W 84.05(11) . 2_665
O30 Na1 O6W 84.56(11) 2_655 .
O4W Na1 O6W 79.26(11) . .
O1W Na1 O6W 141.64(13) 2_665 .
O30 Na1 O31 109.71(12) 2_655 2_655
O4W Na1 O31 81.87(12) . 2_655
O1W Na1 O31 111.30(13) 2_665 2_655
O6W Na1 O31 100.26(13) . 2_655
O30 Na1 O3W 79.54(11) 2_655 2_665
O4W Na1 O3W 118.79(12) . 2_665
O1W Na1 O3W 68.26(10) 2_665 2_665
O6W Na1 O3W 149.38(12) . 2_665
O31 Na1 O3W 61.76(11) 2_655 2_665
O30 Na1 Co3 123.05(10) 2_655 .
O4W Na1 Co3 40.43(8) . .
O1W Na1 Co3 117.36(9) 2_665 .
O6W Na1 Co3 38.84(7) . .
O31 Na1 Co3 90.77(10) 2_655 .
O3W Na1 Co3 150.42(10) 2_665 .
O30 Na1 P3 19.23(7) 2_655 2_655
O4W Na1 P3 156.32(10) . 2_655
O1W Na1 P3 119.26(9) 2_665 2_655
O6W Na1 P3 79.24(8) . 2_655
O31 Na1 P3 92.31(9) 2_655 2_655
O3W Na1 P3 77.16(8) 2_665 2_655
Co3 Na1 P3 117.31(5) . 2_655
O23 P1 O24 108.85(16) . .
O23 P1 O21 109.93(16) . .
O24 P1 O21 111.66(15) . .
O23 P1 O22 107.10(17) . .
O24 P1 O22 109.90(18) . .
O21 P1 O22 109.29(18) . .
O31 P2 O28 112.28(19) . .
O31 P2 O6 111.6(2) . 2_665
O28 P2 O6 112.26(16) . 2_665
O31 P2 O29 106.7(2) . .
O28 P2 O29 106.52(19) . .
O6 P2 O29 107.05(18) 2_665 .
O30 P3 O8 112.47(14) . 2_665
O30 P3 O19 109.90(14) . .
O8 P3 O19 107.74(14) 2_665 .
O30 P3 O20 111.69(14) . .
O8 P3 O20 107.20(14) 2_665 .
O19 P3 O20 107.63(14) . .
O30 P3 Na1 29.52(11) . 2_655
O8 P3 Na1 115.25(10) 2_665 2_655
O19 P3 Na1 129.85(10) . 2_655
O20 P3 Na1 83.56(10) . 2_655
O12 P4 O11 110.12(16) . .
O12 P4 O16 113.36(16) . 2_665
O11 P4 O16 111.43(15) . 2_665
O12 P4 O13 105.96(16) . .
O11 P4 O13 107.92(16) . .
O16 P4 O13 107.73(16) 2_665 .
Mo1 O1 Mo5 81.79(9) . .
Mo1 O1 Co1 133.67(12) . .
Mo5 O1 Co1 134.85(13) . .
Mo2 O2 Mo3 82.00(9) . .
Mo2 O2 Co1 135.21(13) . .
Mo3 O2 Co1 134.19(13) . .
Mo6 O3 Mo4 81.63(9) . .
Mo6 O3 Co1 136.24(13) . .
Mo4 O3 Co1 134.47(13) . .
Mo2 O5 Mo6 111.84(11) 2_665 .
Mo2 O5 H5A 104.0 2_665 .
Mo6 O5 H5A 110.1 . .
P2 O6 Mo6 134.44(17) 2_665 .
Mo6 O7 Mo4 83.44(10) . .
P3 O8 Mo4 127.27(14) 2_665 .
P3 O8 Mo5 125.60(14) 2_665 2_665
Mo4 O8 Mo5 99.59(9) . 2_665
Mo4 O10 Mo5 113.19(11) . 2_665
Mo4 O10 H10A 100.6 . .
Mo5 O10 H10A 111.9 2_665 .
P4 O11 Mo4 132.56(16) . .
P4 O12 Co2 125.75(16) . .
P4 O13 H13A 117.3 . .
P4 O16 Mo5 135.83(16) 2_665 .
Mo1 O17 Mo5 83.65(10) . .
Mo3 O18 Mo1 112.74(11) . .
Mo3 O18 H18A 109.8 . .
Mo1 O18 H18A 107.3 . .
P3 O19 Mo1 126.45(14) . .
P3 O19 Mo3 127.36(14) . .
Mo1 O19 Mo3 100.87(10) . .
P3 O20 Mo2 125.49(14) . .
P3 O20 Mo6 126.66(14) . 2_665
Mo2 O20 Mo6 99.35(9) . 2_665
P1 O21 Mo1 133.54(16) . .
P1 O22 H22 109.5 . .
P1 O23 Co3 134.95(17) . .
P1 O24 Mo3 137.82(16) . .
Mo2 O25 Mo3 84.01(10) . .
P2 O28 Mo2 137.37(17) . .
P2 O29 H29 109.5 . .
P3 O30 Na1 131.25(16) . 2_655
P2 O31 Na1 131.1(2) . 2_655
N1 C1 C2 124.2(5) . .
N1 C1 H1 119(3) . .
C2 C1 H1 117(3) . .
C3 C2 C1 116.6(5) . .
C3 C2 C11 123.3(5) . .
C1 C2 C11 120.1(5) . .
C2 C3 C4 120.2(5) . .
C2 C3 H2 120(4) . .
C4 C3 H2 119(4) . .
C3 C4 C5 119.4(5) . .
C3 C4 H3 121(3) . .
C5 C4 H3 119(3) . .
N1 C5 C4 121.0(4) . .
N1 C5 C6 116.0(4) . .
C4 C5 C6 123.0(4) . .
N2 C6 C7 120.0(4) . .
N2 C6 C5 116.1(4) . .
C7 C6 C5 123.8(4) . .
C8 C7 C6 119.7(5) . .
C8 C7 H4 123(4) . .
C6 C7 H4 117(4) . .
C7 C8 C9 120.5(5) . .
C7 C8 H5 111(4) . .
C9 C8 H5 128(4) . .
C8 C9 C10 116.7(5) . .
C8 C9 C12 123.5(5) . .
C10 C9 C12 119.8(5) . .
N2 C10 C9 124.1(4) . .
N2 C10 H6 113(3) . .
C9 C10 H6 123(3) . .
C2 C11 H11A 109.5 . .
C2 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
C2 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
C9 C12 H12A 109.5 . .
C9 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C9 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
N3 C13 C14 123.5(5) . .
N3 C13 H7 117(3) . .
C14 C13 H7 119(3) . .
C13 C14 C15 116.6(5) . .
C13 C14 C23 120.0(6) . .
C15 C14 C23 123.4(5) . .
C16 C15 C14 121.1(5) . .
C16 C15 H8 115(5) . .
C14 C15 H8 124(5) . .
C15 C16 C17 118.7(5) . .
C15 C16 H9 116(4) . .
C17 C16 H9 126(4) . .
N3 C17 C16 120.7(5) . .
N3 C17 C18 116.0(4) . .
C16 C17 C18 123.3(5) . .
N4 C18 C19 120.3(5) . .
N4 C18 C17 115.9(4) . .
C19 C18 C17 123.8(4) . .
C20 C19 C18 120.1(5) . .
C20 C19 H10 125(5) . .
C18 C19 H10 115(5) . .
C21 C20 C19 120.2(5) . .
C21 C20 H11 128(5) . .
C19 C20 H11 111(5) . .
C20 C21 C22 116.9(5) . .
C20 C21 C24 122.5(5) . .
C22 C21 C24 120.7(5) . .
N4 C22 C21 123.5(4) . .
N4 C22 H12 115(3) . .
C21 C22 H12 121(3) . .
C14 C23 H23A 109.5 . .
C14 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
C14 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
C21 C24 H24A 109.5 . .
C21 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C21 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C1 N1 C5 118.6(4) . .
C1 N1 Co2 126.5(3) . .
C5 N1 Co2 114.9(3) . .
C10 N2 C6 119.0(4) . .
C10 N2 Co2 126.2(3) . .
C6 N2 Co2 114.5(3) . .
C13 N3 C17 119.5(4) . .
C13 N3 Co3 125.5(3) . .
C17 N3 Co3 115.0(3) . .
C22 N4 C18 119.0(4) . .
C22 N4 Co3 125.9(3) . .
C18 N4 Co3 114.7(3) . .
Co2 O1W Na1 104.76(11) . 2_665
Co2 O1W H1WB 104.2 . .
Na1 O1W H1WB 112.5 2_665 .
Co2 O1W H1WA 119.5 . .
Na1 O1W H1WA 120.9 2_665 .
H1WB O1W H1WA 93.3 . .
Co2 O2W H2WA 119.0 . .
Co2 O2W H2WB 120.9 . .
H2WA O2W H2WB 99.3 . .
Co2 O3W Na1 95.65(12) . 2_665
Co2 O3W H3WA 118.5 . .
Na1 O3W H3WA 104.1 2_665 .
Co2 O3W H3WB 132.8 . .
Na1 O3W H3WB 64.6 2_665 .
H3WA O3W H3WB 108.1 . .
Co3 O4W Na1 94.46(12) . .
Co3 O4W H4WA 108.4 . .
Na1 O4W H4WA 114.7 . .
Co3 O4W H4WB 122.4 . .
Na1 O4W H4WB 106.4 . .
H4WA O4W H4WB 109.9 . .
Co3 O5W H5WA 119.2 . .
Co3 O5W H5WB 121.6 . .
H5WA O5W H5WB 112.8 . .
Co3 O6W Na1 94.73(11) . .
Co3 O6W H6WA 127.0 . .
Na1 O6W H6WA 100.6 . .
Co3 O6W H6WB 126.4 . .
Na1 O6W H6WB 104.7 . .
H6WA O6W H6WB 98.1 . .
H7WA O7W H7WB 140.6 . .
H8WA O8W H8WB 137.9 . .
H9WA O9W H9WB 101.2 . .
H10C O10W H10D 115.0 . .
H11E O11W H11D 97.7 . .
H12E O12W H12D 125.5 . .
H13C O13W H13D 123.2 . .
H14C O14W H14D 97.6 . .
H15C O15W H15D 134.8 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 O14 1.671(3) .
Mo1 O17 1.941(3) .
Mo1 O1 1.977(2) .
Mo1 O21 2.079(3) .
Mo1 O18 2.107(2) .
Mo1 O19 2.262(2) .
Mo1 Mo5 2.5916(4) .
Mo2 O27 1.681(3) .
Mo2 O25 1.936(3) .
Mo2 O2 1.969(3) .
Mo2 O28 2.056(3) .
Mo2 O5 2.098(3) 2_665
Mo2 O20 2.265(2) .
Mo2 Mo3 2.5929(5) .
Mo3 O26 1.679(3) .
Mo3 O25 1.938(3) .
Mo3 O2 1.983(2) .
Mo3 O24 2.038(3) .
Mo3 O18 2.084(3) .
Mo3 O19 2.264(2) .
Mo4 O9 1.674(3) .
Mo4 O7 1.940(3) .
Mo4 O3 1.979(2) .
Mo4 O11 2.037(3) .
Mo4 O10 2.098(3) .
Mo4 O8 2.286(2) .
Mo4 Mo6 2.5818(5) .
Mo5 O15 1.669(3) .
Mo5 O17 1.945(2) .
Mo5 O1 1.982(2) .
Mo5 O16 2.044(3) .
Mo5 O10 2.102(2) 2_665
Mo5 O8 2.305(2) 2_665
Mo6 O4 1.676(3) .
Mo6 O7 1.939(3) .
Mo6 O3 1.971(2) .
Mo6 O6 2.065(3) .
Mo6 O5 2.101(3) .
Mo6 O20 2.297(2) 2_665
Co1 O2 2.117(2) 2_665
Co1 O2 2.117(2) .
Co1 O3 2.138(2) .
Co1 O3 2.138(2) 2_665
Co1 O1 2.195(2) 2_665
Co1 O1 2.195(2) .
Co2 O12 2.035(3) .
Co2 O3W 2.079(3) .
Co2 N1 2.103(3) .
Co2 N2 2.109(4) .
Co2 O1W 2.144(3) .
Co2 O2W 2.163(3) .
Co3 O23 2.063(3) .
Co3 N3 2.098(4) .
Co3 N4 2.099(4) .
Co3 O6W 2.121(3) .
Co3 O5W 2.127(3) .
Co3 O4W 2.193(3) .
Co3 Na1 3.3709(19) .
Na1 O30 2.251(3) 2_655
Na1 O4W 2.395(3) .
Na1 O1W 2.426(3) 2_665
Na1 O6W 2.451(3) .
Na1 O31 2.550(4) 2_655
Na1 O3W 2.772(4) 2_665
Na1 P3 3.4342(19) 2_655
P1 O23 1.507(3) .
P1 O24 1.522(3) .
P1 O21 1.538(3) .
P1 O22 1.555(3) .
P2 O31 1.491(3) .
P2 O28 1.527(3) .
P2 O6 1.528(3) 2_665
P2 O29 1.570(3) .
P3 O30 1.504(3) .
P3 O8 1.547(3) 2_665
P3 O19 1.548(3) .
P3 O20 1.552(3) .
P3 Na1 3.4342(19) 2_655
P4 O12 1.512(3) .
P4 O11 1.530(3) .
P4 O16 1.531(3) 2_665
P4 O13 1.564(3) .
O5 Mo2 2.098(3) 2_665
O5 H5A 0.9285 .
O6 P2 1.528(3) 2_665
O8 P3 1.547(3) 2_665
O8 Mo5 2.305(2) 2_665
O10 Mo5 2.102(2) 2_665
O10 H10A 0.8799 .
O13 H13A 0.6998 .
O16 P4 1.531(3) 2_665
O18 H18A 0.8720 .
O20 Mo6 2.297(2) 2_665
O22 H22 0.8200 .
O29 H29 0.8200 .
O30 Na1 2.251(3) 2_655
O31 Na1 2.550(4) 2_655
C1 N1 1.327(6) .
C1 C2 1.392(7) .
C1 H1 0.92(5) .
C2 C3 1.377(8) .
C2 C11 1.498(8) .
C3 C4 1.382(8) .
C3 H2 0.91(6) .
C4 C5 1.384(6) .
C4 H3 0.96(6) .
C5 N1 1.348(5) .
C5 C6 1.469(6) .
C6 N2 1.348(5) .
C6 C7 1.392(6) .
C7 C8 1.375(8) .
C7 H4 0.83(6) .
C8 C9 1.376(8) .
C8 H5 0.99(6) .
C9 C10 1.379(7) .
C9 C12 1.507(7) .
C10 N2 1.337(6) .
C10 H6 0.94(5) .
C11 H11A 0.9600 .
C11 H11B 0.9600 .
C11 H11C 0.9600 .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 N3 1.338(6) .
C13 C14 1.379(7) .
C13 H7 0.98(6) .
C14 C15 1.383(9) .
C14 C23 1.515(8) .
C15 C16 1.374(9) .
C15 H8 1.06(9) .
C16 C17 1.395(7) .
C16 H9 1.04(6) .
C17 N3 1.339(6) .
C17 C18 1.468(7) .
C18 N4 1.348(6) .
C18 C19 1.384(7) .
C19 C20 1.380(9) .
C19 H10 0.87(7) .
C20 C21 1.376(8) .
C20 H11 0.954(10) .
C21 C22 1.387(7) .
C21 C24 1.500(7) .
C22 N4 1.346(6) .
C22 H12 1.05(5) .
C23 H23A 0.9600 .
C23 H23B 0.9600 .
C23 H23C 0.9600 .
C24 H24A 0.9600 .
C24 H24B 0.9600 .
C24 H24C 0.9600 .
O1W Na1 2.426(3) 2_665
O1W H1WB 0.9100 .
O1W H1WA 0.8975 .
O2W H2WA 0.8874 .
O2W H2WB 0.8514 .
O3W Na1 2.772(4) 2_665
O3W H3WA 0.8328 .
O3W H3WB 0.9183 .
O4W H4WA 0.9218 .
O4W H4WB 0.9497 .
O5W H5WA 0.8728 .
O5W H5WB 0.8814 .
O6W H6WA 0.8885 .
O6W H6WB 0.8409 .
O7W H7WA 0.8587 .
O7W H7WB 0.8522 .
O8W H8WA 0.8394 .
O8W H8WB 0.8378 .
O9W H9WA 0.8278 .
O9W H9WB 0.8409 .
O10W H10C 0.8160 .
O10W H10D 0.8492 .
O11W H11E 0.7177 .
O11W H11D 0.8163 .
O12W H12E 0.8505 .
O12W H12D 0.8567 .
O13W H13C 0.8293 .
O13W H13D 0.8624 .
O14W H14C 0.9032 .
O14W H14D 0.8216 .
O15W H15C 0.8406 .
O15W H15D 0.8583 .
