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#$Date: 2023-05-05 04:51:52 +0300 (Fri, 05 May 2023) $
#$Revision: 283261 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/19/7711963.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7711963
loop_
_publ_author_name
'Schulz, Jiří'
'Antala, Jakub'
'Císařová, Ivana'
'Štěpnička, Petr'
_publ_section_title
;
 Beyond phosphorus: synthesis, reactivity, coordination behaviour and
 catalytic properties of 1,1'-bis(diphenylstibino)ferrocene.
;
_journal_issue                   5
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1198
_journal_page_last               1211
_journal_paper_doi               10.1039/d2dt03770j
_journal_volume                  52
_journal_year                    2023
_chemical_formula_moiety         'C68 H56 Au Fe2 Sb4, F6 Sb'
_chemical_formula_sum            'C68 H56 Au F6 Fe2 Sb5'
_chemical_formula_weight         1904.54
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2022-11-11 deposited with the CCDC.	2022-12-15 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 108.945(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   19.3992(17)
_cell_length_b                   14.4857(12)
_cell_length_c                   23.3398(18)
_cell_measurement_reflns_used    9124
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      33.21
_cell_measurement_theta_min      2.63
_cell_volume                     6203.5(9)
_computing_cell_refinement       'SAINT V8.40A (Bruker Nano, Inc., 2019)'
_computing_data_collection       'Bruker Instrument Service vV6.2.14'
_computing_data_reduction        'SAINT V8.40A (Bruker Nano, Inc., 2019)'
_computing_molecular_graphics    'PLATON (Spek, 2017)'
_computing_publication_material  'PLATON (Spek, 2017)'
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker D8 VENTURE Kappa Duo with PHOTON 1000'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  'Quazar Mo multilayer optic'
_diffrn_radiation_source         'I\mS micro-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0231
_diffrn_reflns_av_unetI/netI     0.0142
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            102710
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.499
_diffrn_reflns_theta_min         1.845
_exptl_absorpt_coefficient_mu    5.010
_exptl_absorpt_correction_T_max  0.72
_exptl_absorpt_correction_T_min  0.52
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS-2016/2 - Bruker AXS'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.039
_exptl_crystal_description       prism
_exptl_crystal_F_000             3616
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.07
_refine_diff_density_max         0.951
_refine_diff_density_min         -0.741
_refine_diff_density_rms         0.068
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.085
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     776
_refine_ls_number_reflns         14188
_refine_ls_number_restraints     24
_refine_ls_restrained_S_all      1.088
_refine_ls_R_factor_all          0.0132
_refine_ls_R_factor_gt           0.0129
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0063P)²+5.8040P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0294
_refine_ls_wR_factor_ref         0.0296
_reflns_Friedel_coverage         0.000
_reflns_number_gt                13984
_reflns_number_total             14188
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d2dt03770j3.cif
_cod_data_source_block           js626
_cod_depositor_comments
'Adding full bibliography for 7711945--7711966.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7711963
_shelx_shelxl_version_number     2017/1
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.345
_shelx_estimated_absorpt_t_max   0.721
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.25081(2) 0.73170(2) 0.37899(2) 0.01314(2) Uani 1 1 d . . . . .
Sb1 Sb 0.21052(2) 0.60247(2) 0.44102(2) 0.01340(2) Uani 1 1 d . . . . .
Sb2 Sb 0.12856(2) 0.81657(2) 0.31889(2) 0.01338(2) Uani 1 1 d . . . . .
Sb3 Sb 0.35253(2) 0.84928(2) 0.43863(2) 0.01368(2) Uani 1 1 d . . . . .
Sb4 Sb 0.30952(2) 0.65056(2) 0.30493(2) 0.01364(2) Uani 1 1 d . . . . .
Fe1 Fe 0.02345(2) 0.66656(2) 0.38025(2) 0.01445(5) Uani 1 1 d . . . . .
Fe2 Fe 0.48530(2) 0.76973(2) 0.36245(2) 0.01432(5) Uani 1 1 d . . . . .
C1 C 0.11114(9) 0.63523(12) 0.45451(7) 0.0162(3) Uani 1 1 d . . . . .
C2 C 0.08717(10) 0.72801(12) 0.45864(7) 0.0186(3) Uani 1 1 d . . . . .
H2 H 0.115575 0.782286 0.461506 0.022 Uiso 1 1 calc R U . . .
C3 C 0.01355(10) 0.72463(14) 0.45771(8) 0.0229(4) Uani 1 1 d . . . . .
H3 H -0.015597 0.776220 0.460164 0.027 Uiso 1 1 calc R U . . .
C4 C -0.00887(10) 0.63082(14) 0.45247(8) 0.0230(4) Uani 1 1 d . . . . .
H4 H -0.055639 0.608835 0.450752 0.028 Uiso 1 1 calc R U . . .
C5 C 0.05084(9) 0.57534(13) 0.45022(7) 0.0194(3) Uani 1 1 d . . . . .
H5 H 0.050716 0.510023 0.446521 0.023 Uiso 1 1 calc R U . . .
C6 C 0.03903(9) 0.72895(11) 0.30683(7) 0.0155(3) Uani 1 1 d . . . . .
C7 C -0.03286(9) 0.74793(13) 0.30887(7) 0.0185(3) Uani 1 1 d . . . . .
H7 H -0.052332 0.807325 0.311563 0.022 Uiso 1 1 calc R U . . .
C8 C -0.06972(9) 0.66257(13) 0.30614(8) 0.0217(4) Uani 1 1 d . . . . .
H8 H -0.118266 0.655093 0.306415 0.026 Uiso 1 1 calc R U . . .
C9 C -0.02169(10) 0.59030(13) 0.30295(8) 0.0210(4) Uani 1 1 d . . . . .
H9 H -0.032425 0.526160 0.300954 0.025 Uiso 1 1 calc R U . . .
C10 C 0.04527(9) 0.63055(12) 0.30327(7) 0.0172(3) Uani 1 1 d . . . . .
H10 H 0.086979 0.597921 0.301430 0.021 Uiso 1 1 calc R U . . .
C11 C 0.28502(9) 0.58018(12) 0.52995(7) 0.0167(3) Uani 1 1 d . . . . .
C12 C 0.31103(11) 0.49364(13) 0.55255(9) 0.0277(4) Uani 1 1 d . . . . .
H12 H 0.294098 0.439967 0.528749 0.033 Uiso 1 1 calc R U . . .
C13 C 0.36212(12) 0.48592(15) 0.61036(10) 0.0350(5) Uani 1 1 d . . . . .
H13 H 0.379046 0.426648 0.626165 0.042 Uiso 1 1 calc R U . . .
C14 C 0.38819(12) 0.56333(15) 0.64466(9) 0.0325(5) Uani 1 1 d . . . . .
H14 H 0.423508 0.557404 0.683722 0.039 Uiso 1 1 calc R U . . .
C15 C 0.36294(12) 0.65023(14) 0.62224(9) 0.0318(5) Uani 1 1 d . . . . .
H15 H 0.380710 0.703841 0.645863 0.038 Uiso 1 1 calc R U . . .
C16 C 0.31150(11) 0.65796(13) 0.56498(8) 0.0257(4) Uani 1 1 d . . . . .
H16 H 0.294172 0.717279 0.549547 0.031 Uiso 1 1 calc R U . . .
C17 C 0.18644(9) 0.46519(12) 0.40759(8) 0.0183(3) Uani 1 1 d . . . . .
C18 C 0.18589(10) 0.44443(13) 0.34923(8) 0.0218(4) Uani 1 1 d . . . . .
H18 H 0.196706 0.491212 0.324923 0.026 Uiso 1 1 calc R U . . .
C19 C 0.16954(11) 0.35530(14) 0.32626(10) 0.0307(4) Uani 1 1 d . . . . .
H19 H 0.168983 0.341515 0.286325 0.037 Uiso 1 1 calc R U . . .
C20 C 0.15418(12) 0.28727(14) 0.36156(11) 0.0349(5) Uani 1 1 d . . . . .
H20 H 0.143303 0.226495 0.345933 0.042 Uiso 1 1 calc R U . . .
C21 C 0.15454(12) 0.30706(14) 0.41972(10) 0.0321(4) Uani 1 1 d . . . . .
H21 H 0.144115 0.259790 0.443908 0.039 Uiso 1 1 calc R U . . .
C22 C 0.17017(10) 0.39628(13) 0.44288(9) 0.0243(4) Uani 1 1 d . . . . .
H22 H 0.169730 0.409996 0.482562 0.029 Uiso 1 1 calc R U . . .
C23 C 0.11107(9) 0.85917(12) 0.22803(7) 0.0177(3) Uani 1 1 d . . . . .
C24 C 0.16110(11) 0.91896(13) 0.21632(9) 0.0253(4) Uani 1 1 d . . . . .
H24 H 0.200212 0.943282 0.248856 0.030 Uiso 1 1 calc R U . . .
C25 C 0.15372(12) 0.94313(15) 0.15674(10) 0.0332(5) Uani 1 1 d . . . . .
H25 H 0.187860 0.983757 0.148620 0.040 Uiso 1 1 calc R U . . .
C26 C 0.09666(13) 0.90780(15) 0.10966(9) 0.0338(5) Uani 1 1 d . . . . .
H26 H 0.091872 0.923992 0.069106 0.041 Uiso 1 1 calc R U . . .
C27 C 0.04670(12) 0.84940(15) 0.12091(9) 0.0316(4) Uani 1 1 d . . . . .
H27 H 0.007466 0.825835 0.088151 0.038 Uiso 1 1 calc R U . . .
C28 C 0.05335(10) 0.82459(13) 0.18016(8) 0.0241(4) Uani 1 1 d . . . . .
H28 H 0.018716 0.784318 0.187860 0.029 Uiso 1 1 calc R U . . .
C29 C 0.09650(9) 0.93517(11) 0.35764(8) 0.0180(3) Uani 1 1 d . . . . .
C30 C 0.03189(10) 0.98206(13) 0.32830(8) 0.0225(4) Uani 1 1 d . . . . .
H30 H 0.001691 0.962355 0.289429 0.027 Uiso 1 1 calc R U . . .
C31 C 0.01168(12) 1.05752(14) 0.35588(10) 0.0304(4) Uani 1 1 d . . . . .
H31 H -0.032256 1.089600 0.335825 0.036 Uiso 1 1 calc R U . . .
C32 C 0.05555(13) 1.08604(14) 0.41260(11) 0.0355(5) Uani 1 1 d . . . . .
H32 H 0.041065 1.137040 0.431609 0.043 Uiso 1 1 calc R U . . .
C33 C 0.12024(13) 1.04098(15) 0.44184(10) 0.0358(5) Uani 1 1 d . . . . .
H33 H 0.150511 1.061404 0.480498 0.043 Uiso 1 1 calc R U . . .
C34 C 0.14065(11) 0.96544(13) 0.41417(9) 0.0271(4) Uani 1 1 d . . . . .
H34 H 0.185105 0.934318 0.434072 0.032 Uiso 1 1 calc R U . . .
C51 C 0.45628(9) 0.81723(12) 0.43422(7) 0.0157(3) Uani 1 1 d . . . . .
C52 C 0.49080(9) 0.72867(12) 0.44762(7) 0.0171(3) Uani 1 1 d . . . . .
H52 H 0.469731 0.674185 0.457392 0.021 Uiso 1 1 calc R U . . .
C53 C 0.56214(10) 0.73686(13) 0.44368(8) 0.0205(4) Uani 1 1 d . . . . .
H53 H 0.597229 0.688795 0.450744 0.025 Uiso 1 1 calc R U . . .
C54 C 0.57199(9) 0.82907(13) 0.42741(8) 0.0219(4) Uani 1 1 d . . . . .
H54 H 0.614585 0.853237 0.421276 0.026 Uiso 1 1 calc R U . . .
C55 C 0.50711(9) 0.87903(12) 0.42188(8) 0.0199(3) Uani 1 1 d . . . . .
H55 H 0.498946 0.942511 0.411737 0.024 Uiso 1 1 calc R U . . .
C56 C 0.40378(9) 0.70865(12) 0.29336(7) 0.0167(3) Uani 1 1 d . . . . .
C57 C 0.47162(9) 0.66102(13) 0.30394(7) 0.0193(3) Uani 1 1 d . . . . .
H57 H 0.480704 0.598000 0.315093 0.023 Uiso 1 1 calc R U . . .
C58 C 0.52288(10) 0.72468(14) 0.29479(8) 0.0235(4) Uani 1 1 d . . . . .
H58 H 0.572066 0.711342 0.298403 0.028 Uiso 1 1 calc R U . . .
C59 C 0.48799(10) 0.81142(14) 0.27935(8) 0.0248(4) Uani 1 1 d . . . . .
H59 H 0.509828 0.866330 0.271083 0.030 Uiso 1 1 calc R U . . .
C60 C 0.41460(10) 0.80209(13) 0.27838(8) 0.0206(3) Uani 1 1 d . . . . .
H60 H 0.378966 0.849665 0.269345 0.025 Uiso 1 1 calc R U . . .
C61 C 0.38450(9) 0.88091(11) 0.53287(7) 0.0167(3) Uani 1 1 d . . . . .
C62 C 0.33369(10) 0.91476(13) 0.55825(8) 0.0232(4) Uani 1 1 d . . . . .
H62 H 0.284510 0.923595 0.533502 0.028 Uiso 1 1 calc R U . . .
C63 C 0.35475(11) 0.93565(14) 0.61973(9) 0.0271(4) Uani 1 1 d . . . . .
H63 H 0.320258 0.959781 0.636826 0.033 Uiso 1 1 calc R U . . .
C64 C 0.42602(12) 0.92116(13) 0.65578(8) 0.0278(4) Uani 1 1 d . . . . .
H64 H 0.440306 0.935217 0.697770 0.033 Uiso 1 1 calc R U . . .
C65 C 0.47682(11) 0.88638(13) 0.63137(8) 0.0261(4) Uani 1 1 d . . . . .
H65 H 0.525534 0.875694 0.656608 0.031 Uiso 1 1 calc R U . . .
C66 C 0.45621(10) 0.86707(12) 0.56957(8) 0.0202(3) Uani 1 1 d . . . . .
H66 H 0.491194 0.844418 0.552502 0.024 Uiso 1 1 calc R U . . .
C67 C 0.33795(9) 0.98483(12) 0.40108(8) 0.0189(3) Uani 1 1 d . . . . .
C68 C 0.32272(12) 0.99408(14) 0.33903(9) 0.0302(4) Uani 1 1 d . . . . .
H68 H 0.321322 0.940796 0.314946 0.036 Uiso 1 1 calc R U . . .
C69 C 0.30947(13) 1.08060(16) 0.31168(10) 0.0366(5) Uani 1 1 d . . . . .
H69 H 0.299879 1.086458 0.269262 0.044 Uiso 1 1 calc R U . . .
C70 C 0.31033(12) 1.15749(15) 0.34638(11) 0.0378(5) Uani 1 1 d . . . . .
H70 H 0.300087 1.216526 0.327820 0.045 Uiso 1 1 calc R U . . .
C71 C 0.32601(15) 1.14897(15) 0.40788(12) 0.0461(6) Uani 1 1 d . . . . .
H71 H 0.327420 1.202427 0.431814 0.055 Uiso 1 1 calc R U . . .
C72 C 0.33984(13) 1.06269(14) 0.43547(10) 0.0357(5) Uani 1 1 d . . . . .
H72 H 0.350593 1.057463 0.478052 0.043 Uiso 1 1 calc R U . . .
C73 C 0.24330(9) 0.62548(12) 0.21352(7) 0.0178(3) Uani 1 1 d . . . . .
C74 C 0.23092(10) 0.69914(13) 0.17293(8) 0.0225(4) Uani 1 1 d . . . . .
H74 H 0.254111 0.756812 0.185754 0.027 Uiso 1 1 calc R U . . .
C75 C 0.18470(11) 0.68828(14) 0.11374(8) 0.0272(4) Uani 1 1 d . . . . .
H75 H 0.176317 0.738577 0.086199 0.033 Uiso 1 1 calc R U . . .
C76 C 0.15081(10) 0.60422(15) 0.09484(8) 0.0283(4) Uani 1 1 d . . . . .
H76 H 0.119486 0.596873 0.054301 0.034 Uiso 1 1 calc R U . . .
C77 C 0.16254(10) 0.53111(14) 0.13487(9) 0.0270(4) Uani 1 1 d . . . . .
H77 H 0.139173 0.473631 0.121753 0.032 Uiso 1 1 calc R U . . .
C78 C 0.20856(10) 0.54127(13) 0.19449(8) 0.0215(4) Uani 1 1 d . . . . .
H78 H 0.216182 0.491009 0.221996 0.026 Uiso 1 1 calc R U . . .
C79 C 0.35588(9) 0.51991(12) 0.33673(8) 0.0183(3) Uani 1 1 d . . . . .
C80 C 0.37822(10) 0.50555(13) 0.39910(9) 0.0237(4) Uani 1 1 d . . . . .
H80 H 0.368587 0.551149 0.424760 0.028 Uiso 1 1 calc R U . . .
C81 C 0.41446(12) 0.42504(15) 0.42401(10) 0.0351(5) Uani 1 1 d . . . . .
H81 H 0.430111 0.415886 0.466612 0.042 Uiso 1 1 calc R U . . .
C82 C 0.42766(13) 0.35838(15) 0.38666(12) 0.0406(5) Uani 1 1 d . . . . .
H82 H 0.452882 0.303511 0.403661 0.049 Uiso 1 1 calc R U . . .
C83 C 0.40430(13) 0.37109(14) 0.32446(11) 0.0363(5) Uani 1 1 d . . . . .
H83 H 0.412697 0.324333 0.298957 0.044 Uiso 1 1 calc R U . . .
C84 C 0.36867(11) 0.45181(13) 0.29920(9) 0.0253(4) Uani 1 1 d . . . . .
H84 H 0.353084 0.460587 0.256559 0.030 Uiso 1 1 calc R U . . .
Sb5 Sb 0.76370(2) 0.76344(2) 0.37544(2) 0.02212(3) Uani 1 1 d . . . . .
F1A F 0.83410(10) 0.82092(13) 0.43876(7) 0.0509(5) Uani 0.867(2) 1 d . . P . .
F2A F 0.81870(8) 0.65417(10) 0.39152(8) 0.0400(4) Uani 0.867(2) 1 d . . P . .
F3A F 0.69507(9) 0.70078(14) 0.31054(8) 0.0519(5) Uani 0.867(2) 1 d . . P . .
F4A F 0.70528(10) 0.86792(11) 0.35728(9) 0.0554(6) Uani 0.867(2) 1 d . . P . .
F1B F 0.7627(6) 0.8801(7) 0.4189(5) 0.042(3) Uani 0.133(2) 1 d . U P . .
F2B F 0.8481(6) 0.7348(9) 0.4421(6) 0.055(3) Uani 0.133(2) 1 d . U P . .
F3B F 0.7660(8) 0.6599(9) 0.3383(6) 0.063(4) Uani 0.133(2) 1 d . U P . .
F4B F 0.6833(7) 0.8072(10) 0.3165(6) 0.060(3) Uani 0.133(2) 1 d . U P . .
F5 F 0.71377(7) 0.72266(9) 0.42706(6) 0.0388(3) Uani 1 1 d . . . . .
F6 F 0.81317(8) 0.80490(10) 0.32355(7) 0.0451(3) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Sb2 Au1 Sb4 111.399(7) . . ?
Sb2 Au1 Sb1 104.337(6) . . ?
Sb4 Au1 Sb1 108.176(7) . . ?
Sb2 Au1 Sb3 111.700(7) . . ?
Sb4 Au1 Sb3 103.046(7) . . ?
Sb1 Au1 Sb3 118.259(6) . . ?
C1 Sb1 C17 99.35(7) . . ?
C1 Sb1 C11 104.62(6) . . ?
C17 Sb1 C11 102.33(6) . . ?
C1 Sb1 Au1 111.79(5) . . ?
C17 Sb1 Au1 122.02(5) . . ?
C11 Sb1 Au1 114.45(5) . . ?
C6 Sb2 C29 101.68(6) . . ?
C6 Sb2 C23 100.65(7) . . ?
C29 Sb2 C23 102.45(6) . . ?
C6 Sb2 Au1 110.64(5) . . ?
C29 Sb2 Au1 119.18(5) . . ?
C23 Sb2 Au1 119.39(4) . . ?
C51 Sb3 C67 100.66(6) . . ?
C51 Sb3 C61 97.79(6) . . ?
C67 Sb3 C61 100.45(7) . . ?
C51 Sb3 Au1 113.34(5) . . ?
C67 Sb3 Au1 113.67(5) . . ?
C61 Sb3 Au1 126.92(4) . . ?
C56 Sb4 C79 96.54(7) . . ?
C56 Sb4 C73 101.86(6) . . ?
C79 Sb4 C73 104.29(7) . . ?
C56 Sb4 Au1 118.91(5) . . ?
C79 Sb4 Au1 113.11(5) . . ?
C73 Sb4 Au1 118.92(4) . . ?
C5 Fe1 C10 117.76(7) . . ?
C5 Fe1 C7 163.95(7) . . ?
C10 Fe1 C7 68.82(7) . . ?
C5 Fe1 C6 152.80(7) . . ?
C10 Fe1 C6 41.11(7) . . ?
C7 Fe1 C6 41.16(6) . . ?
C5 Fe1 C4 40.88(7) . . ?
C10 Fe1 C4 150.01(8) . . ?
C7 Fe1 C4 126.28(7) . . ?
C6 Fe1 C4 165.98(7) . . ?
C5 Fe1 C1 41.14(7) . . ?
C10 Fe1 C1 109.61(7) . . ?
C7 Fe1 C1 153.58(7) . . ?
C6 Fe1 C1 119.96(7) . . ?
C4 Fe1 C1 68.85(7) . . ?
C5 Fe1 C2 68.93(7) . . ?
C10 Fe1 C2 131.23(7) . . ?
C7 Fe1 C2 119.03(7) . . ?
C6 Fe1 C2 110.24(7) . . ?
C4 Fe1 C2 68.40(7) . . ?
C1 Fe1 C2 41.04(7) . . ?
C5 Fe1 C9 106.37(7) . . ?
C10 Fe1 C9 40.61(7) . . ?
C7 Fe1 C9 68.37(7) . . ?
C6 Fe1 C9 68.80(7) . . ?
C4 Fe1 C9 115.48(7) . . ?
C1 Fe1 C9 128.67(7) . . ?
C2 Fe1 C9 168.44(7) . . ?
C5 Fe1 C8 125.90(7) . . ?
C10 Fe1 C8 68.27(7) . . ?
C7 Fe1 C8 40.50(7) . . ?
C6 Fe1 C8 68.67(7) . . ?
C4 Fe1 C8 105.36(7) . . ?
C1 Fe1 C8 165.36(7) . . ?
C2 Fe1 C8 150.87(7) . . ?
C9 Fe1 C8 40.40(7) . . ?
C5 Fe1 C3 68.57(7) . . ?
C10 Fe1 C3 169.03(7) . . ?
C7 Fe1 C3 107.62(7) . . ?
C6 Fe1 C3 129.55(7) . . ?
C4 Fe1 C3 40.47(8) . . ?
C1 Fe1 C3 68.65(7) . . ?
C2 Fe1 C3 40.51(7) . . ?
C9 Fe1 C3 148.94(7) . . ?
C8 Fe1 C3 116.28(7) . . ?
C52 Fe2 C57 112.33(7) . . ?
C52 Fe2 C59 175.79(7) . . ?
C57 Fe2 C59 68.43(8) . . ?
C52 Fe2 C58 137.51(7) . . ?
C57 Fe2 C58 40.66(7) . . ?
C59 Fe2 C58 40.48(8) . . ?
C52 Fe2 C60 143.57(7) . . ?
C57 Fe2 C60 68.62(7) . . ?
C59 Fe2 C60 40.63(7) . . ?
C58 Fe2 C60 68.29(7) . . ?
C52 Fe2 C53 40.61(7) . . ?
C57 Fe2 C53 109.66(7) . . ?
C59 Fe2 C53 135.19(7) . . ?
C58 Fe2 C53 107.75(7) . . ?
C60 Fe2 C53 175.70(7) . . ?
C52 Fe2 C51 40.98(6) . . ?
C57 Fe2 C51 142.48(7) . . ?
C59 Fe2 C51 140.57(8) . . ?
C58 Fe2 C51 175.35(7) . . ?
C60 Fe2 C51 115.41(7) . . ?
C53 Fe2 C51 68.46(7) . . ?
C52 Fe2 C54 68.40(7) . . ?
C57 Fe2 C54 135.55(7) . . ?
C59 Fe2 C54 108.03(8) . . ?
C58 Fe2 C54 106.95(7) . . ?
C60 Fe2 C54 138.12(8) . . ?
C53 Fe2 C54 40.45(7) . . ?
C51 Fe2 C54 68.44(7) . . ?
C52 Fe2 C56 114.92(7) . . ?
C57 Fe2 C56 40.95(7) . . ?
C59 Fe2 C56 68.52(7) . . ?
C58 Fe2 C56 68.54(7) . . ?
C60 Fe2 C56 40.77(7) . . ?
C53 Fe2 C56 140.17(7) . . ?
C51 Fe2 C56 116.07(7) . . ?
C54 Fe2 C56 175.49(7) . . ?
C52 Fe2 C55 68.51(7) . . ?
C57 Fe2 C55 175.76(7) . . ?
C59 Fe2 C55 110.42(8) . . ?
C58 Fe2 C55 135.92(7) . . ?
C60 Fe2 C55 113.38(7) . . ?
C53 Fe2 C55 68.07(7) . . ?
C51 Fe2 C55 40.70(7) . . ?
C54 Fe2 C55 40.47(7) . . ?
C56 Fe2 C55 142.91(7) . . ?
C5 C1 C2 107.24(15) . . ?
C5 C1 Fe1 68.90(9) . . ?
C2 C1 Fe1 69.57(9) . . ?
C5 C1 Sb1 128.25(13) . . ?
C2 C1 Sb1 123.59(12) . . ?
Fe1 C1 Sb1 118.22(8) . . ?
C3 C2 C1 108.21(16) . . ?
C3 C2 Fe1 70.10(10) . . ?
C1 C2 Fe1 69.40(9) . . ?
C3 C2 H2 125.9 . . ?
C1 C2 H2 125.9 . . ?
Fe1 C2 H2 126.2 . . ?
C4 C3 C2 108.20(16) . . ?
C4 C3 Fe1 69.31(10) . . ?
C2 C3 Fe1 69.39(10) . . ?
C4 C3 H3 125.9 . . ?
C2 C3 H3 125.9 . . ?
Fe1 C3 H3 127.0 . . ?
C3 C4 C5 108.24(16) . . ?
C3 C4 Fe1 70.22(10) . . ?
C5 C4 Fe1 69.04(10) . . ?
C3 C4 H4 125.9 . . ?
C5 C4 H4 125.9 . . ?
Fe1 C4 H4 126.4 . . ?
C4 C5 C1 108.11(16) . . ?
C4 C5 Fe1 70.08(10) . . ?
C1 C5 Fe1 69.96(9) . . ?
C4 C5 H5 125.9 . . ?
C1 C5 H5 125.9 . . ?
Fe1 C5 H5 125.6 . . ?
C10 C6 C7 107.03(15) . . ?
C10 C6 Fe1 69.38(9) . . ?
C7 C6 Fe1 69.38(9) . . ?
C10 C6 Sb2 121.84(12) . . ?
C7 C6 Sb2 130.59(13) . . ?
Fe1 C6 Sb2 119.79(8) . . ?
C8 C7 C6 108.19(16) . . ?
C8 C7 Fe1 70.26(10) . . ?
C6 C7 Fe1 69.46(9) . . ?
C8 C7 H7 125.9 . . ?
C6 C7 H7 125.9 . . ?
Fe1 C7 H7 126.0 . . ?
C7 C8 C9 108.36(15) . . ?
C7 C8 Fe1 69.24(10) . . ?
C9 C8 Fe1 69.66(10) . . ?
C7 C8 H8 125.8 . . ?
C9 C8 H8 125.8 . . ?
Fe1 C8 H8 126.9 . . ?
C8 C9 C10 108.15(16) . . ?
C8 C9 Fe1 69.94(10) . . ?
C10 C9 Fe1 69.30(9) . . ?
C8 C9 H9 125.9 . . ?
C10 C9 H9 125.9 . . ?
Fe1 C9 H9 126.4 . . ?
C9 C10 C6 108.27(15) . . ?
C9 C10 Fe1 70.09(10) . . ?
C6 C10 Fe1 69.51(9) . . ?
C9 C10 H10 125.9 . . ?
C6 C10 H10 125.9 . . ?
Fe1 C10 H10 126.1 . . ?
C16 C11 C12 119.27(16) . . ?
C16 C11 Sb1 117.01(13) . . ?
C12 C11 Sb1 123.61(13) . . ?
C11 C12 C13 119.72(18) . . ?
C11 C12 H12 120.1 . . ?
C13 C12 H12 120.1 . . ?
C14 C13 C12 120.60(19) . . ?
C14 C13 H13 119.7 . . ?
C12 C13 H13 119.7 . . ?
C13 C14 C15 120.08(18) . . ?
C13 C14 H14 120.0 . . ?
C15 C14 H14 120.0 . . ?
C16 C15 C14 119.38(18) . . ?
C16 C15 H15 120.3 . . ?
C14 C15 H15 120.3 . . ?
C15 C16 C11 120.93(17) . . ?
C15 C16 H16 119.5 . . ?
C11 C16 H16 119.5 . . ?
C18 C17 C22 119.49(16) . . ?
C18 C17 Sb1 119.40(13) . . ?
C22 C17 Sb1 121.10(13) . . ?
C17 C18 C19 120.32(18) . . ?
C17 C18 H18 119.8 . . ?
C19 C18 H18 119.8 . . ?
C20 C19 C18 119.93(19) . . ?
C20 C19 H19 120.0 . . ?
C18 C19 H19 120.0 . . ?
C19 C20 C21 120.31(19) . . ?
C19 C20 H20 119.8 . . ?
C21 C20 H20 119.8 . . ?
C20 C21 C22 120.16(19) . . ?
C20 C21 H21 119.9 . . ?
C22 C21 H21 119.9 . . ?
C17 C22 C21 119.79(18) . . ?
C17 C22 H22 120.1 . . ?
C21 C22 H22 120.1 . . ?
C24 C23 C28 119.75(16) . . ?
C24 C23 Sb2 118.71(13) . . ?
C28 C23 Sb2 121.45(13) . . ?
C23 C24 C25 119.94(19) . . ?
C23 C24 H24 120.0 . . ?
C25 C24 H24 120.0 . . ?
C26 C25 C24 119.78(19) . . ?
C26 C25 H25 120.1 . . ?
C24 C25 H25 120.1 . . ?
C27 C26 C25 120.60(18) . . ?
C27 C26 H26 119.7 . . ?
C25 C26 H26 119.7 . . ?
C26 C27 C28 120.3(2) . . ?
C26 C27 H27 119.9 . . ?
C28 C27 H27 119.9 . . ?
C23 C28 C27 119.63(19) . . ?
C23 C28 H28 120.2 . . ?
C27 C28 H28 120.2 . . ?
C34 C29 C30 119.41(17) . . ?
C34 C29 Sb2 118.90(13) . . ?
C30 C29 Sb2 121.67(13) . . ?
C31 C30 C29 120.00(18) . . ?
C31 C30 H30 120.0 . . ?
C29 C30 H30 120.0 . . ?
C32 C31 C30 120.01(19) . . ?
C32 C31 H31 120.0 . . ?
C30 C31 H31 120.0 . . ?
C33 C32 C31 120.60(19) . . ?
C33 C32 H32 119.7 . . ?
C31 C32 H32 119.7 . . ?
C32 C33 C34 119.5(2) . . ?
C32 C33 H33 120.3 . . ?
C34 C33 H33 120.3 . . ?
C29 C34 C33 120.52(19) . . ?
C29 C34 H34 119.7 . . ?
C33 C34 H34 119.7 . . ?
C55 C51 C52 107.49(15) . . ?
C55 C51 Fe2 69.83(9) . . ?
C52 C51 Fe2 69.24(9) . . ?
C55 C51 Sb3 127.33(13) . . ?
C52 C51 Sb3 125.04(12) . . ?
Fe2 C51 Sb3 129.45(8) . . ?
C53 C52 C51 107.86(15) . . ?
C53 C52 Fe2 69.96(10) . . ?
C51 C52 Fe2 69.78(9) . . ?
C53 C52 H52 126.1 . . ?
C51 C52 H52 126.1 . . ?
Fe2 C52 H52 125.8 . . ?
C54 C53 C52 108.34(15) . . ?
C54 C53 Fe2 69.80(10) . . ?
C52 C53 Fe2 69.43(10) . . ?
C54 C53 H53 125.8 . . ?
C52 C53 H53 125.8 . . ?
Fe2 C53 H53 126.5 . . ?
C53 C54 C55 108.15(15) . . ?
C53 C54 Fe2 69.76(10) . . ?
C55 C54 Fe2 69.93(10) . . ?
C53 C54 H54 125.9 . . ?
C55 C54 H54 125.9 . . ?
Fe2 C54 H54 126.0 . . ?
C54 C55 C51 108.15(16) . . ?
C54 C55 Fe2 69.60(10) . . ?
C51 C55 Fe2 69.47(9) . . ?
C54 C55 H55 125.9 . . ?
C51 C55 H55 125.9 . . ?
Fe2 C55 H55 126.6 . . ?
C60 C56 C57 107.33(15) . . ?
C60 C56 Fe2 69.39(10) . . ?
C57 C56 Fe2 69.08(9) . . ?
C60 C56 Sb4 127.68(12) . . ?
C57 C56 Sb4 124.84(13) . . ?
Fe2 C56 Sb4 123.33(8) . . ?
C58 C57 C56 108.03(16) . . ?
C58 C57 Fe2 69.84(10) . . ?
C56 C57 Fe2 69.97(9) . . ?
C58 C57 H57 126.0 . . ?
C56 C57 H57 126.0 . . ?
Fe2 C57 H57 125.8 . . ?
C59 C58 C57 108.26(16) . . ?
C59 C58 Fe2 69.72(10) . . ?
C57 C58 Fe2 69.50(10) . . ?
C59 C58 H58 125.9 . . ?
C57 C58 H58 125.9 . . ?
Fe2 C58 H58 126.5 . . ?
C58 C59 C60 108.22(16) . . ?
C58 C59 Fe2 69.80(10) . . ?
C60 C59 Fe2 69.77(10) . . ?
C58 C59 H59 125.9 . . ?
C60 C59 H59 125.9 . . ?
Fe2 C59 H59 126.1 . . ?
C59 C60 C56 108.15(16) . . ?
C59 C60 Fe2 69.60(10) . . ?
C56 C60 Fe2 69.84(10) . . ?
C59 C60 H60 125.9 . . ?
C56 C60 H60 125.9 . . ?
Fe2 C60 H60 126.2 . . ?
C66 C61 C62 119.52(16) . . ?
C66 C61 Sb3 120.13(12) . . ?
C62 C61 Sb3 120.34(13) . . ?
C63 C62 C61 120.23(18) . . ?
C63 C62 H62 119.9 . . ?
C61 C62 H62 119.9 . . ?
C64 C63 C62 119.71(18) . . ?
C64 C63 H63 120.1 . . ?
C62 C63 H63 120.1 . . ?
C63 C64 C65 120.69(17) . . ?
C63 C64 H64 119.7 . . ?
C65 C64 H64 119.7 . . ?
C64 C65 C66 119.71(18) . . ?
C64 C65 H65 120.1 . . ?
C66 C65 H65 120.1 . . ?
C61 C66 C65 120.11(17) . . ?
C61 C66 H66 119.9 . . ?
C65 C66 H66 119.9 . . ?
C72 C67 C68 119.04(18) . . ?
C72 C67 Sb3 122.67(14) . . ?
C68 C67 Sb3 118.23(14) . . ?
C67 C68 C69 120.7(2) . . ?
C67 C68 H68 119.6 . . ?
C69 C68 H68 119.6 . . ?
C70 C69 C68 119.6(2) . . ?
C70 C69 H69 120.2 . . ?
C68 C69 H69 120.2 . . ?
C71 C70 C69 120.0(2) . . ?
C71 C70 H70 120.0 . . ?
C69 C70 H70 120.0 . . ?
C70 C71 C72 120.6(2) . . ?
C70 C71 H71 119.7 . . ?
C72 C71 H71 119.7 . . ?
C67 C72 C71 120.1(2) . . ?
C67 C72 H72 120.0 . . ?
C71 C72 H72 120.0 . . ?
C78 C73 C74 119.59(16) . . ?
C78 C73 Sb4 122.63(13) . . ?
C74 C73 Sb4 117.63(13) . . ?
C75 C74 C73 120.11(18) . . ?
C75 C74 H74 119.9 . . ?
C73 C74 H74 119.9 . . ?
C76 C75 C74 120.12(18) . . ?
C76 C75 H75 119.9 . . ?
C74 C75 H75 119.9 . . ?
C77 C76 C75 120.09(17) . . ?
C77 C76 H76 120.0 . . ?
C75 C76 H76 120.0 . . ?
C76 C77 C78 120.34(18) . . ?
C76 C77 H77 119.8 . . ?
C78 C77 H77 119.8 . . ?
C73 C78 C77 119.75(17) . . ?
C73 C78 H78 120.1 . . ?
C77 C78 H78 120.1 . . ?
C80 C79 C84 119.52(17) . . ?
C80 C79 Sb4 116.81(13) . . ?
C84 C79 Sb4 123.55(13) . . ?
C81 C80 C79 120.43(18) . . ?
C81 C80 H80 119.8 . . ?
C79 C80 H80 119.8 . . ?
C82 C81 C80 119.7(2) . . ?
C82 C81 H81 120.1 . . ?
C80 C81 H81 120.1 . . ?
C81 C82 C83 120.29(19) . . ?
C81 C82 H82 119.9 . . ?
C83 C82 H82 119.9 . . ?
C82 C83 C84 120.3(2) . . ?
C82 C83 H83 119.8 . . ?
C84 C83 H83 119.8 . . ?
C83 C84 C79 119.65(19) . . ?
C83 C84 H84 120.2 . . ?
C79 C84 H84 120.2 . . ?
F3B Sb5 F4B 94.5(7) . . ?
F3B Sb5 F1A 130.8(5) . . ?
F4B Sb5 F1A 132.3(5) . . ?
F3B Sb5 F4A 134.6(5) . . ?
F4B Sb5 F4A 40.1(5) . . ?
F1A Sb5 F4A 93.03(10) . . ?
F3B Sb5 F5 98.7(4) . . ?
F4B Sb5 F5 95.8(4) . . ?
F1A Sb5 F5 91.71(7) . . ?
F4A Sb5 F5 89.96(6) . . ?
F3B Sb5 F6 81.6(4) . . ?
F4B Sb5 F6 83.9(4) . . ?
F1A Sb5 F6 88.39(7) . . ?
F4A Sb5 F6 89.65(6) . . ?
F5 Sb5 F6 179.59(6) . . ?
F3B Sb5 F2A 42.9(5) . . ?
F4B Sb5 F2A 137.3(5) . . ?
F1A Sb5 F2A 89.74(8) . . ?
F4A Sb5 F2A 177.10(9) . . ?
F5 Sb5 F2A 89.11(6) . . ?
F6 Sb5 F2A 91.29(6) . . ?
F3B Sb5 F3A 46.6(5) . . ?
F4B Sb5 F3A 50.0(5) . . ?
F1A Sb5 F3A 177.37(8) . . ?
F4A Sb5 F3A 89.41(9) . . ?
F5 Sb5 F3A 89.27(7) . . ?
F6 Sb5 F3A 90.65(7) . . ?
F2A Sb5 F3A 87.83(8) . . ?
F3B Sb5 F2B 93.7(6) . . ?
F4B Sb5 F2B 171.7(6) . . ?
F1A Sb5 F2B 39.6(4) . . ?
F4A Sb5 F2B 131.6(4) . . ?
F5 Sb5 F2B 83.8(4) . . ?
F6 Sb5 F2B 96.5(4) . . ?
F2A Sb5 F2B 51.0(4) . . ?
F3A Sb5 F2B 138.2(4) . . ?
F3B Sb5 F1B 178.9(6) . . ?
F4B Sb5 F1B 86.6(6) . . ?
F1A Sb5 F1B 48.1(3) . . ?
F4A Sb5 F1B 46.5(3) . . ?
F5 Sb5 F1B 81.1(3) . . ?
F6 Sb5 F1B 98.6(3) . . ?
F2A Sb5 F1B 135.9(3) . . ?
F3A Sb5 F1B 134.4(3) . . ?
F2B Sb5 F1B 85.2(5) . . ?
F2B F1A F1B 134.8(7) . . ?
F2B F1A Sb5 72.3(6) . . ?
F1B F1A Sb5 70.0(4) . . ?
F3B F2A F2B 127.9(7) . . ?
F3B F2A Sb5 63.0(6) . . ?
F2B F2A Sb5 65.3(4) . . ?
F3B F3A F4B 120.5(7) . . ?
F3B F3A Sb5 61.1(5) . . ?
F4B F3A Sb5 62.8(5) . . ?
F4B F4A F1B 139.4(7) . . ?
F4B F4A Sb5 68.7(6) . . ?
F1B F4A Sb5 70.8(4) . . ?
F4A F1B F1A 121.6(6) . . ?
F4A F1B Sb5 62.6(4) . . ?
F1A F1B Sb5 61.9(4) . . ?
F1A F2B F2A 129.9(9) . . ?
F1A F2B Sb5 68.1(5) . . ?
F2A F2B Sb5 63.7(4) . . ?
F2A F3B F3A 140.9(10) . . ?
F2A F3B Sb5 74.1(6) . . ?
F3A F3B Sb5 72.2(6) . . ?
F4A F4B F3A 136.6(10) . . ?
F4A F4B Sb5 71.2(6) . . ?
F3A F4B Sb5 67.2(5) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Sb2 2.6350(2) . ?
Au1 Sb4 2.63508(17) . ?
Au1 Sb1 2.63574(18) . ?
Au1 Sb3 2.63606(19) . ?
Sb1 C1 2.1059(17) . ?
Sb1 C17 2.1318(17) . ?
Sb1 C11 2.1337(16) . ?
Sb2 C6 2.0951(16) . ?
Sb2 C29 2.1264(17) . ?
Sb2 C23 2.1274(16) . ?
Sb3 C51 2.1003(16) . ?
Sb3 C67 2.1313(17) . ?
Sb3 C61 2.1323(16) . ?
Sb4 C56 2.1083(17) . ?
Sb4 C79 2.1233(17) . ?
Sb4 C73 2.1341(16) . ?
Fe1 C5 2.0327(17) . ?
Fe1 C10 2.0430(16) . ?
Fe1 C7 2.0437(17) . ?
Fe1 C6 2.0447(16) . ?
Fe1 C4 2.0465(17) . ?
Fe1 C1 2.0469(16) . ?
Fe1 C2 2.0492(17) . ?
Fe1 C9 2.0534(17) . ?
Fe1 C8 2.0572(17) . ?
Fe1 C3 2.0586(17) . ?
Fe2 C52 2.0444(17) . ?
Fe2 C57 2.0444(17) . ?
Fe2 C59 2.0480(18) . ?
Fe2 C58 2.0490(18) . ?
Fe2 C60 2.0503(17) . ?
Fe2 C53 2.0515(17) . ?
Fe2 C51 2.0516(16) . ?
Fe2 C54 2.0520(17) . ?
Fe2 C56 2.0563(17) . ?
Fe2 C55 2.0564(17) . ?
C1 C5 1.434(2) . ?
C1 C2 1.436(2) . ?
C2 C3 1.422(2) . ?
C2 H2 0.9500 . ?
C3 C4 1.420(3) . ?
C3 H3 0.9500 . ?
C4 C5 1.425(3) . ?
C4 H4 0.9500 . ?
C5 H5 0.9500 . ?
C6 C10 1.435(2) . ?
C6 C7 1.437(2) . ?
C7 C8 1.419(3) . ?
C7 H7 0.9500 . ?
C8 C9 1.419(3) . ?
C8 H8 0.9500 . ?
C9 C10 1.422(2) . ?
C9 H9 0.9500 . ?
C10 H10 0.9500 . ?
C11 C16 1.389(2) . ?
C11 C12 1.390(2) . ?
C12 C13 1.395(3) . ?
C12 H12 0.9500 . ?
C13 C14 1.375(3) . ?
C13 H13 0.9500 . ?
C14 C15 1.390(3) . ?
C14 H14 0.9500 . ?
C15 C16 1.389(3) . ?
C15 H15 0.9500 . ?
C16 H16 0.9500 . ?
C17 C18 1.392(2) . ?
C17 C22 1.394(3) . ?
C18 C19 1.395(3) . ?
C18 H18 0.9500 . ?
C19 C20 1.378(3) . ?
C19 H19 0.9500 . ?
C20 C21 1.385(3) . ?
C20 H20 0.9500 . ?
C21 C22 1.396(3) . ?
C21 H21 0.9500 . ?
C22 H22 0.9500 . ?
C23 C24 1.392(3) . ?
C23 C28 1.393(3) . ?
C24 C25 1.395(3) . ?
C24 H24 0.9500 . ?
C25 C26 1.380(3) . ?
C25 H25 0.9500 . ?
C26 C27 1.374(3) . ?
C26 H26 0.9500 . ?
C27 C28 1.394(3) . ?
C27 H27 0.9500 . ?
C28 H28 0.9500 . ?
C29 C34 1.390(3) . ?
C29 C30 1.394(2) . ?
C30 C31 1.388(3) . ?
C30 H30 0.9500 . ?
C31 C32 1.384(3) . ?
C31 H31 0.9500 . ?
C32 C33 1.382(3) . ?
C32 H32 0.9500 . ?
C33 C34 1.392(3) . ?
C33 H33 0.9500 . ?
C34 H34 0.9500 . ?
C51 C55 1.429(2) . ?
C51 C52 1.434(2) . ?
C52 C53 1.421(2) . ?
C52 H52 0.9500 . ?
C53 C54 1.418(3) . ?
C53 H53 0.9500 . ?
C54 C55 1.421(2) . ?
C54 H54 0.9500 . ?
C55 H55 0.9500 . ?
C56 C60 1.430(2) . ?
C56 C57 1.435(2) . ?
C57 C58 1.422(3) . ?
C57 H57 0.9500 . ?
C58 C59 1.417(3) . ?
C58 H58 0.9500 . ?
C59 C60 1.423(2) . ?
C59 H59 0.9500 . ?
C60 H60 0.9500 . ?
C61 C66 1.391(2) . ?
C61 C62 1.394(2) . ?
C62 C63 1.392(3) . ?
C62 H62 0.9500 . ?
C63 C64 1.382(3) . ?
C63 H63 0.9500 . ?
C64 C65 1.383(3) . ?
C64 H64 0.9500 . ?
C65 C66 1.394(2) . ?
C65 H65 0.9500 . ?
C66 H66 0.9500 . ?
C67 C72 1.378(3) . ?
C67 C68 1.388(3) . ?
C68 C69 1.392(3) . ?
C68 H68 0.9500 . ?
C69 C70 1.374(3) . ?
C69 H69 0.9500 . ?
C70 C71 1.373(3) . ?
C70 H70 0.9500 . ?
C71 C72 1.392(3) . ?
C71 H71 0.9500 . ?
C72 H72 0.9500 . ?
C73 C78 1.395(2) . ?
C73 C74 1.395(3) . ?
C74 C75 1.390(3) . ?
C74 H74 0.9500 . ?
C75 C76 1.386(3) . ?
C75 H75 0.9500 . ?
C76 C77 1.381(3) . ?
C76 H76 0.9500 . ?
C77 C78 1.396(3) . ?
C77 H77 0.9500 . ?
C78 H78 0.9500 . ?
C79 C80 1.393(3) . ?
C79 C84 1.394(2) . ?
C80 C81 1.388(3) . ?
C80 H80 0.9500 . ?
C81 C82 1.379(3) . ?
C81 H81 0.9500 . ?
C82 C83 1.386(3) . ?
C82 H82 0.9500 . ?
C83 C84 1.389(3) . ?
C83 H83 0.9500 . ?
C84 H84 0.9500 . ?
Sb5 F3B 1.740(13) . ?
Sb5 F4B 1.825(13) . ?
Sb5 F1A 1.8527(15) . ?
Sb5 F4A 1.8554(15) . ?
Sb5 F5 1.8698(12) . ?
Sb5 F6 1.8715(12) . ?
Sb5 F2A 1.8774(13) . ?
Sb5 F3A 1.8924(16) . ?
Sb5 F2B 1.902(12) . ?
Sb5 F1B 1.974(10) . ?
F1A F2B 1.274(13) . ?
F1A F1B 1.565(11) . ?
F2A F3B 1.330(14) . ?
F2A F2B 1.626(14) . ?
F3A F3B 1.444(15) . ?
F3A F4B 1.572(15) . ?
F4A F4B 1.263(14) . ?
F4A F1B 1.517(11) . ?
