#------------------------------------------------------------------------------
#$Date: 2024-07-05 19:17:46 +0300 (Fri, 05 Jul 2024) $
#$Revision: 293053 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/58/7715805.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7715805
loop_
_publ_author_name
'Flichot, Hadrien'
'Sickinger, Annika'
'Brom, Jules'
'Lefeuvre, Bertrand'
'Dorcet, Vincent'
'Guizouarn, Thierry'
'Cador, Olivier'
'Le Guennic, Boris'
'Micouin, Laurent'
'Maury, Olivier'
'Benedetti, Erica'
'Pointillart, Fabrice'
_publ_section_title
;
 Magneto-structural correlation in lanthanide luminescent
 [2.2]paracyclophane-based single-molecule magnets.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8191
_journal_page_last               8201
_journal_paper_doi               10.1039/d4dt00536h
_journal_volume                  53
_journal_year                    2024
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C110 H73 Dy2 F36 Na O16 P4, C32 H12 B F24'
_chemical_formula_sum            'C142 H85 B Dy2 F60 Na O16 P4'
_chemical_formula_weight         3669.77
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   difmap
_audit_update_record
;
2023-09-26 deposited with the CCDC.	2024-04-22 downloaded from the CCDC.
;
_cell_angle_alpha                85.259(10)
_cell_angle_beta                 84.050(10)
_cell_angle_gamma                78.874(9)
_cell_formula_units_Z            2
_cell_length_a                   13.426(5)
_cell_length_b                   21.081(7)
_cell_length_c                   27.045(10)
_cell_measurement_reflns_used    9389
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      22.7791
_cell_measurement_theta_min      2.2761
_cell_measurement_wavelength     0.710730
_cell_volume                     7455(5)
_computing_cell_refinement       'APEX3 (Bruker, 2015)'
_computing_data_collection       'Bruker APEX3 (Bruker, 2015)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_molecular_graphics
;
   'SXGRAPH (L. Farrugia, 1999), Mercury (CSD, 2020)'
;
_computing_publication_material  'CRYSCALC (T. Roisnel, local program, 2020)'
_computing_structure_refinement  'SHELXL-2018_3 (Sheldrick, 2018)'
_computing_structure_solution    'SHELXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      150(2)
_diffrn_detector                 CMOS-PHOTON70
_diffrn_detector_area_resol_mean 10.4167
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.959
_diffrn_measurement_device_type  'D8 VENTURE Bruker AXS'
_diffrn_measurement_method       'rotation images'
_diffrn_orient_matrix_UB_11      0.0646354
_diffrn_orient_matrix_UB_12      0.0000842
_diffrn_orient_matrix_UB_13      -0.0219811
_diffrn_orient_matrix_UB_21      0.0364514
_diffrn_orient_matrix_UB_22      0.0040268
_diffrn_orient_matrix_UB_23      0.0296843
_diffrn_orient_matrix_UB_31      0.0173806
_diffrn_orient_matrix_UB_32      -0.0482757
_diffrn_orient_matrix_UB_33      0.0048372
_diffrn_radiation_monochromator  'multilayer monochromator'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'Incoatec microfocus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1560
_diffrn_reflns_av_unetI/netI     0.1539
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       35
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            161273
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.984
_diffrn_reflns_theta_min         1.862
_diffrn_source_current           1.00
_diffrn_source_power             50.0
_diffrn_source_voltage           50.00
_exptl_absorpt_coefficient_mu    1.177
_exptl_absorpt_correction_T_max  0.889
_exptl_absorpt_correction_T_min  0.683
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
  [Sheldrick, G.M. (2014). SADABS Bruker AXS Inc., Madison, Wisconsin, USA]
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.635
_exptl_crystal_description       prism
_exptl_crystal_F_000             3626
_exptl_crystal_size_max          0.230
_exptl_crystal_size_mid          0.140
_exptl_crystal_size_min          0.100
_refine_diff_density_max         4.064
_refine_diff_density_min         -3.852
_refine_diff_density_rms         0.265
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.079
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1982
_refine_ls_number_reflns         34446
_refine_ls_number_restraints     823
_refine_ls_restrained_S_all      1.070
_refine_ls_R_factor_all          0.3052
_refine_ls_R_factor_gt           0.2031
_refine_ls_shift/su_max          0.042
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0001P)²+703.0660P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.4421
_refine_ls_wR_factor_ref         0.5036
_reflns_number_gt                17227
_reflns_number_total             34446
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            d4dt00536h2.cif
_cod_data_source_block           HF01c
_cod_depositor_comments
'Adding full bibliography for 7715801--7715805.cif.'
_cod_database_code               7715805
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.22862(8) 0.21193(5) 0.89566(5) 0.0424(3) Uani 1 1 d . . . . .
Na1 Na 0.1450(8) 0.2323(5) 0.7601(4) 0.057(3) Uani 1 1 d . . . . .
O1 O 0.2797(10) 0.2457(8) 0.8101(7) 0.047(4) Uani 1 1 d . . . . .
O2 O 0.3899(12) 0.2424(9) 0.8939(7) 0.053(4) Uani 1 1 d . . . . .
O3 O 0.0890(11) 0.2184(8) 0.8465(7) 0.049(4) Uani 1 1 d . . . . .
O4 O 0.0733(11) 0.2244(8) 0.9502(6) 0.045(4) Uani 1 1 d . U . . .
O5 O 0.1731(11) 0.1124(7) 0.9098(7) 0.047(4) Uani 1 1 d . . . . .
O6 O 0.3521(11) 0.1300(7) 0.8633(6) 0.044(4) Uani 1 1 d . . . . .
O7 O 0.1916(11) 0.3184(7) 0.9071(6) 0.043(4) Uani 1 1 d . . . . .
O8 O 0.2785(11) 0.1868(7) 0.9726(6) 0.046(4) Uani 1 1 d . . . . .
P1 P 0.1313(4) 0.3795(3) 0.9303(3) 0.0413(14) Uani 1 1 d . . . . .
P2 P 0.3303(4) 0.1761(3) 1.0201(3) 0.0412(14) Uani 1 1 d . . . . .
F1 F 0.297(4) 0.255(2) 0.7144(16) 0.106(9) Uani 0.45(3) 1 d D . P A 1
F2 F 0.336(4) 0.346(2) 0.7292(17) 0.106(9) Uani 0.45(3) 1 d D . P A 1
F3 F 0.454(3) 0.267(3) 0.7073(15) 0.106(9) Uani 0.45(3) 1 d D . P A 1
C1 C 0.365(3) 0.281(2) 0.7363(16) 0.11(3) Uani 0.45(3) 1 d D . P A 1
F1B F 0.301(3) 0.214(2) 0.7152(13) 0.106(9) Uani 0.55(3) 1 d D . P A 2
F2B F 0.344(3) 0.308(2) 0.7115(14) 0.106(9) Uani 0.55(3) 1 d D . P A 2
F3B F 0.460(3) 0.222(2) 0.7110(13) 0.106(9) Uani 0.55(3) 1 d D . P A 2
C1B C 0.366(3) 0.2469(19) 0.7329(15) 0.11(3) Uani 0.55(3) 1 d D . P A 2
C2 C 0.367(2) 0.2493(15) 0.7898(12) 0.070(9) Uani 1 1 d D . . . .
C3 C 0.454(2) 0.2522(16) 0.8107(12) 0.072(9) Uani 1 1 d . . . . .
H3 H 0.514161 0.256870 0.789699 0.086 Uiso 1 1 calc R U . . .
C4 C 0.4578(16) 0.2484(11) 0.8621(11) 0.050(6) Uani 1 1 d . . . . .
C5 C 0.5589(19) 0.2535(8) 0.8782(8) 0.064(8) Uani 1 1 d D . . . .
F4 F 0.6344(18) 0.2701(14) 0.8444(9) 0.084(5) Uani 0.63(3) 1 d D . P B 1
F5 F 0.5514(19) 0.2976(14) 0.9137(10) 0.084(5) Uani 0.63(3) 1 d D . P B 1
F6 F 0.6064(18) 0.1973(10) 0.9016(12) 0.084(5) Uani 0.63(3) 1 d D . P B 1
F4B F 0.614(3) 0.2980(18) 0.8546(16) 0.084(5) Uani 0.37(3) 1 d D . P B 2
F5B F 0.564(3) 0.262(3) 0.9277(10) 0.084(5) Uani 0.37(3) 1 d D . P B 2
F6B F 0.626(3) 0.1960(13) 0.8717(19) 0.084(5) Uani 0.37(3) 1 d D . P B 2
F7 F -0.0396(18) 0.2325(11) 0.7732(8) 0.079(5) Uani 0.66(2) 1 d D . P A 1
F8 F -0.0147(16) 0.1339(10) 0.7998(9) 0.079(5) Uani 0.66(2) 1 d D . P A 1
F9 F -0.1550(13) 0.1956(13) 0.8202(9) 0.079(5) Uani 0.66(2) 1 d D . P A 1
F7B F -0.020(3) 0.209(2) 0.7676(9) 0.079(5) Uani 0.34(2) 1 d D . P A 2
F8B F -0.089(3) 0.1390(15) 0.8124(16) 0.079(5) Uani 0.34(2) 1 d D . P A 2
F9B F -0.144(2) 0.2390(18) 0.8211(17) 0.079(5) Uani 0.34(2) 1 d D . P A 2
C6 C -0.0518(14) 0.1951(9) 0.8170(10) 0.064(5) Uani 1 1 d D U . . .
C7 C 0.0008(18) 0.2067(13) 0.8588(11) 0.055(4) Uani 1 1 d . U . . .
C8 C -0.0539(17) 0.2042(12) 0.9074(10) 0.050(4) Uani 1 1 d . U . . .
H8 H -0.122431 0.197687 0.911258 0.060 Uiso 1 1 calc R U . . .
C9 C -0.0046(17) 0.2114(13) 0.9485(10) 0.052(4) Uani 1 1 d . U . . .
C10 C -0.0745(18) 0.2051(13) 0.9951(11) 0.054(5) Uani 1 1 d . U . . .
F10 F -0.0656(13) 0.1399(8) 1.0100(7) 0.078(5) Uani 1 1 d . . . . .
F11 F -0.1736(10) 0.2246(8) 0.9919(6) 0.065(4) Uani 1 1 d . . . . .
F12 F -0.0482(11) 0.2319(9) 1.0324(6) 0.071(5) Uani 1 1 d . . . . .
F13 F 0.1045(16) 0.0114(10) 0.9642(9) 0.099(7) Uani 1 1 d . . . . .
F14 F 0.0414(13) 0.0301(8) 0.8937(9) 0.103(8) Uani 1 1 d . . . . .
F15 F 0.1638(15) -0.0505(7) 0.9064(9) 0.093(6) Uani 1 1 d . . . . .
C11 C 0.1267(19) 0.0119(12) 0.9150(14) 0.066(9) Uani 1 1 d . . . . .
C12 C 0.2052(15) 0.0531(10) 0.9001(10) 0.043(6) Uani 1 1 d . . . . .
C13 C 0.2971(18) 0.0267(11) 0.8767(12) 0.061(8) Uani 1 1 d . . . . .
H13 H 0.314612 -0.018527 0.872488 0.073 Uiso 1 1 calc R U . . .
C14 C 0.3623(18) 0.0665(13) 0.8599(9) 0.053(7) Uani 1 1 d . . . . .
C15 C 0.465(2) 0.0413(14) 0.8324(14) 0.071(9) Uani 1 1 d . . . . .
F16 F 0.4817(17) -0.0228(8) 0.8308(10) 0.119(9) Uani 1 1 d . . . . .
F17 F 0.4683(15) 0.0626(11) 0.7845(8) 0.102(7) Uani 1 1 d . . . . .
F18 F 0.5447(13) 0.0572(10) 0.8483(9) 0.097(7) Uani 1 1 d . . . . .
C21 C 0.1550(16) 0.4488(11) 0.8919(10) 0.044(6) Uani 1 1 d . . . . .
C22 C 0.2289(18) 0.4416(13) 0.8522(11) 0.057(7) Uani 1 1 d . . . . .
H22 H 0.268906 0.400032 0.846788 0.069 Uiso 1 1 calc R U . . .
C23 C 0.245(2) 0.4934(15) 0.8207(11) 0.064(8) Uani 1 1 d . . . . .
H23 H 0.289948 0.487349 0.791095 0.077 Uiso 1 1 calc R U . . .
C24 C 0.196(2) 0.5543(15) 0.8327(13) 0.077(10) Uani 1 1 d . . . . .
H24 H 0.214814 0.590901 0.813693 0.092 Uiso 1 1 calc R U . . .
C25 C 0.121(2) 0.5640(14) 0.8714(14) 0.081(10) Uani 1 1 d . . . . .
H25 H 0.082309 0.606040 0.876817 0.097 Uiso 1 1 calc R U . . .
C26 C 0.102(2) 0.5123(11) 0.9015(11) 0.062(8) Uani 1 1 d . . . . .
H26 H 0.053509 0.518597 0.929544 0.074 Uiso 1 1 calc R U . . .
C27 C -0.001(2) 0.3800(10) 0.9308(10) 0.051(6) Uani 1 1 d . . . . .
C28 C -0.041(2) 0.3737(14) 0.8845(12) 0.062(8) Uani 1 1 d . . . . .
H28 H 0.004203 0.372692 0.854886 0.075 Uiso 1 1 calc R U . . .
C29 C -0.136(2) 0.3692(15) 0.8808(12) 0.067(8) Uani 1 1 d . . . . .
H29 H -0.157686 0.364621 0.849145 0.080 Uiso 1 1 calc R U . . .
C30 C -0.2054(17) 0.3710(13) 0.9221(13) 0.066(9) Uani 1 1 d . . . . .
H30 H -0.273030 0.365349 0.919256 0.080 Uiso 1 1 calc R U . . .
C31 C -0.175(2) 0.3813(12) 0.9678(11) 0.056(7) Uani 1 1 d . U . . .
H31 H -0.222965 0.384634 0.996456 0.067 Uiso 1 1 calc R U . . .
C32 C -0.0725(15) 0.3868(10) 0.9711(11) 0.045(6) Uani 1 1 d . . . . .
H32 H -0.052443 0.395395 1.002150 0.054 Uiso 1 1 calc R U . . .
C41 C 0.4616(17) 0.1351(10) 1.0104(10) 0.044(6) Uani 1 1 d . . . . .
C42 C 0.483(2) 0.0880(14) 0.9761(13) 0.073(9) Uani 1 1 d . . . . .
H42 H 0.430966 0.077540 0.958739 0.087 Uiso 1 1 calc R U . . .
C43 C 0.585(3) 0.0562(17) 0.9681(15) 0.092(12) Uani 1 1 d . . . . .
H43 H 0.601026 0.022403 0.945829 0.110 Uiso 1 1 calc R U . . .
C44 C 0.662(2) 0.0723(13) 0.9913(14) 0.073(9) Uani 1 1 d . . . . .
H44 H 0.730428 0.050554 0.984514 0.087 Uiso 1 1 calc R U . . .
C45 C 0.639(2) 0.1212(15) 1.0252(14) 0.075(9) Uani 1 1 d . . . . .
H45 H 0.690686 0.132481 1.042342 0.090 Uiso 1 1 calc R U . . .
C46 C 0.5377(17) 0.1528(12) 1.0330(13) 0.068(9) Uani 1 1 d . . . . .
H46 H 0.521232 0.187460 1.054521 0.081 Uiso 1 1 calc R U . . .
C47 C 0.2685(18) 0.1236(12) 1.0621(10) 0.051(6) Uani 1 1 d . . . . .
C48 C 0.311(2) 0.0940(12) 1.1059(10) 0.058(7) Uani 1 1 d . . . . .
H48 H 0.375124 0.101521 1.113503 0.070 Uiso 1 1 calc R U . . .
C49 C 0.260(2) 0.0548(13) 1.1371(11) 0.063(8) Uani 1 1 d . . . . .
H49 H 0.288943 0.034861 1.166369 0.076 Uiso 1 1 calc R U . . .
C50 C 0.165(2) 0.0433(17) 1.1268(14) 0.086(11) Uani 1 1 d . . . . .
H50 H 0.130520 0.015578 1.148760 0.103 Uiso 1 1 calc R U . . .
C51 C 0.122(3) 0.0729(17) 1.0842(14) 0.087(11) Uani 1 1 d . . . . .
H51 H 0.059282 0.064237 1.076324 0.105 Uiso 1 1 calc R U . . .
C52 C 0.171(2) 0.1146(14) 1.0533(13) 0.078(11) Uani 1 1 d . . . . .
H52 H 0.138487 0.137565 1.025818 0.094 Uiso 1 1 calc R U . . .
C33 C 0.1541(16) 0.3851(9) 0.9943(7) 0.047(6) Uani 1 1 d D . . . .
C34 C 0.1185(16) 0.3375(9) 1.0273(7) 0.049(6) Uani 1 1 d D . . . .
H34 H 0.091986 0.304284 1.014413 0.058 Uiso 1 1 calc R U . . .
C35 C 0.1215(19) 0.3382(9) 1.0785(8) 0.056(7) Uani 1 1 d D . . . .
C36 C 0.1476(17) 0.3929(9) 1.0963(8) 0.054(7) Uani 1 1 d D . . . .
H36 H 0.140642 0.398275 1.131139 0.065 Uiso 1 1 calc R U . . .
C37 C 0.1833(16) 0.4390(10) 1.0637(7) 0.048(6) Uani 1 1 d D . . . .
H37 H 0.199464 0.476210 1.076253 0.057 Uiso 1 1 calc R U . . .
C38 C 0.1958(15) 0.4321(9) 1.0132(7) 0.046(6) Uani 1 1 d D . . . .
C39 C 0.2860(17) 0.4594(11) 0.9858(11) 0.054(7) Uani 1 1 d D . . . .
H39A H 0.295744 0.497288 1.002804 0.064 Uiso 1 1 calc R U . . .
H39B H 0.270155 0.474372 0.951352 0.064 Uiso 1 1 calc R U . . .
C40 C 0.3856(17) 0.4088(11) 0.9841(11) 0.059(8) Uani 1 1 d D . . . .
H40A H 0.397111 0.392049 0.950423 0.071 Uiso 1 1 calc R U . . .
H40B H 0.441927 0.431856 0.987514 0.071 Uiso 1 1 calc R U . . .
C53 C 0.3384(15) 0.2502(9) 1.0457(7) 0.038(5) Uani 1 1 d D . . . .
C54 C 0.3711(15) 0.2943(9) 1.0095(7) 0.044(6) Uani 1 1 d D . . . .
H54 H 0.376790 0.284379 0.975578 0.052 Uiso 1 1 calc R U . . .
C55 C 0.3957(16) 0.3522(9) 1.0206(9) 0.054(7) Uani 1 1 d D . . . .
C56 C 0.398(2) 0.3627(11) 1.0701(9) 0.068(8) Uani 1 1 d D . . . .
C57 C 0.3612(17) 0.3203(11) 1.1068(9) 0.066(9) Uani 1 1 d D . . . .
H57 H 0.364391 0.326989 1.140831 0.080 Uiso 1 1 calc R U . . .
C58 C 0.3196(16) 0.2685(10) 1.0947(7) 0.055(7) Uani 1 1 d D . . . .
C59 C 0.2328(19) 0.2499(11) 1.1311(9) 0.053(6) Uani 1 1 d D . . . .
H59A H 0.235849 0.266050 1.164095 0.064 Uiso 1 1 calc R U . . .
H59B H 0.240498 0.202103 1.135026 0.064 Uiso 1 1 calc R U . . .
C60 C 0.1286(19) 0.2794(12) 1.1110(11) 0.059(7) Uani 1 1 d D . . . .
H60A H 0.107780 0.245969 1.092814 0.071 Uiso 1 1 calc R U . . .
H60B H 0.077867 0.288344 1.140077 0.071 Uiso 1 1 calc R U . . .
Dy2 Dy 0.09296(11) 0.22859(6) 0.61904(5) 0.0575(4) Uani 1 1 d . . . . .
O101 O 0.0246(14) 0.3371(7) 0.5886(6) 0.052(4) Uani 1 1 d . . . . .
O102 O 0.0776(12) 0.2978(7) 0.6881(6) 0.045(4) Uani 1 1 d . . . . .
O103 O 0.1287(16) 0.1616(8) 0.6941(7) 0.067(6) Uani 1 1 d . . . . .
O104 O 0.0555(17) 0.1241(8) 0.6089(9) 0.082(7) Uani 1 1 d . . . . .
O105 O 0.2523(13) 0.1572(8) 0.6044(9) 0.068(6) Uani 1 1 d . . . . .
O106 O 0.2205(16) 0.2871(8) 0.6048(7) 0.064(5) Uani 1 1 d . . . . .
O107 O 0.0881(14) 0.2238(9) 0.5374(7) 0.060(5) Uani 1 1 d . . . . .
O108 O -0.0698(14) 0.2372(8) 0.6394(7) 0.059(5) Uani 1 1 d . . . . .
P101 P 0.0714(7) 0.2216(4) 0.4825(3) 0.065(2) Uani 1 1 d . . . . .
P102 P -0.1871(6) 0.2399(3) 0.6389(3) 0.0579(18) Uani 1 1 d . . . . .
F101 F 0.030(4) 0.4376(12) 0.5242(10) 0.22(2) Uani 1 1 d . . . . .
F102 F -0.105(3) 0.4556(14) 0.5596(15) 0.191(19) Uani 1 1 d . . . . .
F103 F 0.0019(19) 0.5020(8) 0.5783(8) 0.106(8) Uani 1 1 d . . . . .
C101 C -0.004(3) 0.4477(15) 0.5649(15) 0.083(11) Uani 1 1 d . . . . .
C102 C 0.016(3) 0.3896(13) 0.6039(10) 0.070(9) Uani 1 1 d . . . . .
C103 C 0.0328(17) 0.4031(10) 0.6508(8) 0.038(5) Uani 1 1 d . . . . .
H103 H 0.026556 0.447353 0.657337 0.046 Uiso 1 1 calc R U . . .
C104 C 0.0577(18) 0.3575(12) 0.6888(10) 0.049(6) Uani 1 1 d . . . . .
C105 C 0.051(3) 0.3809(19) 0.7426(14) 0.087(12) Uani 1 1 d . . . . .
F104 F -0.0416(18) 0.3771(11) 0.7649(8) 0.104(7) Uani 1 1 d . . . . .
F105 F 0.1236(14) 0.3463(8) 0.7685(6) 0.076(5) Uani 1 1 d . . . . .
F106 F 0.0596(14) 0.4426(8) 0.7441(6) 0.073(5) Uani 1 1 d . . . . .
F107 F 0.213(2) 0.1185(11) 0.7774(10) 0.155(7) Uani 1 1 d D . . . .
F108 F 0.2983(19) 0.0389(11) 0.7396(10) 0.155(7) Uani 1 1 d D . . . .
F109 F 0.1522(19) 0.0332(11) 0.7750(10) 0.155(7) Uani 1 1 d D . . . .
C106 C 0.202(2) 0.0745(10) 0.7451(12) 0.105(8) Uani 1 1 d D U . . .
C107 C 0.144(3) 0.1017(15) 0.7019(15) 0.097(7) Uani 1 1 d . U . . .
C108 C 0.129(3) 0.0564(14) 0.6742(14) 0.093(7) Uani 1 1 d . U . . .
H108 H 0.153771 0.012375 0.684295 0.112 Uiso 1 1 calc R U . . .
C109 C 0.079(2) 0.0704(12) 0.6306(11) 0.094(7) Uani 1 1 d D U . . .
C110 C 0.0637(17) 0.0131(11) 0.6050(8) 0.101(8) Uani 1 1 d D U . . .
F110 F 0.064(4) -0.0420(12) 0.6350(12) 0.159(12) Uani 0.44(3) 1 d D . P C 1
F111 F -0.027(3) 0.0220(15) 0.584(2) 0.159(12) Uani 0.44(3) 1 d D . P C 1
F112 F 0.134(3) -0.0048(19) 0.5665(16) 0.159(12) Uani 0.44(3) 1 d D . P C 1
F210 F 0.151(2) -0.0300(15) 0.5934(17) 0.159(12) Uani 0.56(3) 1 d D . P C 2
F211 F 0.003(3) -0.0241(15) 0.6321(13) 0.159(12) Uani 0.56(3) 1 d D . P C 2
F212 F 0.022(4) 0.0277(12) 0.5609(12) 0.159(12) Uani 0.56(3) 1 d D . P C 2
F113 F 0.476(3) 0.0872(17) 0.6278(15) 0.145(11) Uani 0.58(3) 1 d D . P D 1
F114 F 0.364(3) 0.0460(14) 0.593(2) 0.145(11) Uani 0.58(3) 1 d D . P D 1
F115 F 0.472(3) 0.0967(18) 0.5466(14) 0.145(11) Uani 0.58(3) 1 d D . P D 1
F213 F 0.412(5) 0.068(2) 0.6377(13) 0.145(11) Uani 0.42(3) 1 d D . P D 2
F214 F 0.381(4) 0.057(2) 0.561(2) 0.145(11) Uani 0.42(3) 1 d D . P D 2
F215 F 0.510(2) 0.101(2) 0.575(2) 0.145(11) Uani 0.42(3) 1 d D . P D 2
C111 C 0.410(2) 0.0993(13) 0.5907(10) 0.105(7) Uani 1 1 d D U . . .
C112 C 0.339(2) 0.1632(13) 0.5954(17) 0.095(6) Uani 1 1 d D U . . .
C113 C 0.376(2) 0.2189(13) 0.5864(15) 0.089(6) Uani 1 1 d . U . . .
H113 H 0.447723 0.216952 0.579341 0.107 Uiso 1 1 calc R U . . .
C114 C 0.308(2) 0.2815(11) 0.5874(11) 0.099(5) Uani 1 1 d D U . . .
C115 C 0.3582(16) 0.3403(10) 0.5793(9) 0.112(5) Uani 1 1 d D U . . .
C121 C 0.138(4) 0.146(2) 0.4591(18) 0.108(8) Uani 1 1 d . U . . .
F116 F 0.391(2) 0.3514(11) 0.6181(9) 0.109(3) Uani 0.704(18) 1 d D U P E 1
F117 F 0.2856(15) 0.3905(8) 0.5672(12) 0.109(3) Uani 0.704(18) 1 d D U P E 1
F118 F 0.4223(18) 0.3344(11) 0.5412(10) 0.109(3) Uani 0.704(18) 1 d D U P E 1
F216 F 0.320(4) 0.3796(17) 0.6133(17) 0.109(3) Uani 0.296(18) 1 d D U P E 2
F217 F 0.4548(19) 0.3183(17) 0.586(2) 0.109(3) Uani 0.296(18) 1 d D U P E 2
F218 F 0.348(4) 0.366(2) 0.5356(13) 0.109(3) Uani 0.296(18) 1 d D U P E 2
C122 C 0.197(4) 0.105(2) 0.4878(19) 0.115(8) Uani 1 1 d . U . . .
H122 H 0.199392 0.113656 0.521547 0.138 Uiso 1 1 calc R U . . .
C123 C 0.259(4) 0.048(2) 0.4682(18) 0.119(8) Uani 1 1 d . U . . .
H123 H 0.305953 0.019782 0.487522 0.143 Uiso 1 1 calc R U . . .
C124 C 0.248(4) 0.038(2) 0.4218(19) 0.118(8) Uani 1 1 d . U . . .
H124 H 0.281870 -0.003069 0.410235 0.142 Uiso 1 1 calc R U . . .
C125 C 0.195(4) 0.077(2) 0.3903(19) 0.115(8) Uani 1 1 d . U . . .
H125 H 0.196759 0.066924 0.356548 0.139 Uiso 1 1 calc R U . . .
C126 C 0.135(3) 0.135(2) 0.4086(17) 0.111(8) Uani 1 1 d . U . . .
H126 H 0.094256 0.165019 0.387391 0.134 Uiso 1 1 calc R U . . .
C127 C 0.130(4) 0.284(2) 0.4464(15) 0.117(8) Uani 1 1 d . U . . .
C128 C 0.187(4) 0.315(2) 0.4662(15) 0.117(8) Uani 1 1 d . U . . .
H128 H 0.196403 0.306160 0.500484 0.140 Uiso 1 1 calc R U . . .
C129 C 0.237(4) 0.365(2) 0.4379(15) 0.121(8) Uani 1 1 d . U . . .
H129 H 0.281712 0.385819 0.452927 0.145 Uiso 1 1 calc R U . . .
C130 C 0.217(4) 0.380(2) 0.3893(16) 0.124(8) Uani 1 1 d . U . . .
H130 H 0.250588 0.410067 0.369115 0.149 Uiso 1 1 calc R U . . .
C131 C 0.149(4) 0.351(2) 0.3707(16) 0.128(8) Uani 1 1 d . U . . .
H131 H 0.124941 0.365997 0.339318 0.154 Uiso 1 1 calc R U . . .
C132 C 0.115(4) 0.298(2) 0.3987(16) 0.127(8) Uani 1 1 d . U . . .
H132 H 0.079827 0.271540 0.382700 0.153 Uiso 1 1 calc R U . . .
C141 C -0.223(2) 0.1713(16) 0.6735(12) 0.069(8) Uani 1 1 d . . . . .
C142 C -0.144(3) 0.1292(19) 0.7014(18) 0.113(16) Uani 1 1 d . . . . .
H142 H -0.079061 0.140426 0.702814 0.136 Uiso 1 1 calc R U . . .
C143 C -0.168(4) 0.072(2) 0.726(2) 0.17(3) Uani 1 1 d . . . . .
H143 H -0.119135 0.041505 0.743304 0.201 Uiso 1 1 calc R U . . .
C144 C -0.271(5) 0.061(2) 0.7234(18) 0.14(2) Uani 1 1 d . . . . .
H144 H -0.288924 0.022507 0.739962 0.163 Uiso 1 1 calc R U . . .
C145 C -0.338(5) 0.100(4) 0.6998(17) 0.16(3) Uani 1 1 d . . . . .
H145 H -0.405253 0.090909 0.700741 0.193 Uiso 1 1 calc R U . . .
C146 C -0.314(3) 0.155(2) 0.6730(13) 0.093(12) Uani 1 1 d . . . . .
H146 H -0.363800 0.181703 0.654016 0.112 Uiso 1 1 calc R U . . .
C147 C -0.2586(17) 0.3081(12) 0.6691(12) 0.117(8) Uani 1 1 d G U . . .
C148 C -0.2090(13) 0.3408(13) 0.6985(12) 0.119(8) Uani 1 1 d G U . . .
H148 H -0.137922 0.327409 0.701304 0.143 Uiso 1 1 calc R U . . .
C149 C -0.2633(18) 0.3931(13) 0.7240(11) 0.122(8) Uani 1 1 d G U . . .
H149 H -0.229387 0.415469 0.744112 0.146 Uiso 1 1 calc R U . . .
C150 C -0.3672(17) 0.4128(12) 0.7199(12) 0.124(8) Uani 1 1 d G U . . .
H150 H -0.404366 0.448507 0.737294 0.149 Uiso 1 1 calc R U . . .
C151 C -0.4168(13) 0.3801(14) 0.6904(12) 0.127(8) Uani 1 1 d G U . . .
H151 H -0.487881 0.393485 0.687667 0.153 Uiso 1 1 calc R U . . .
C152 C -0.3625(17) 0.3278(13) 0.6650(11) 0.124(8) Uani 1 1 d G U . . .
H152 H -0.396418 0.305425 0.644858 0.149 Uiso 1 1 calc R U . . .
C133 C -0.067(2) 0.2440(18) 0.4690(14) 0.183(11) Uani 1 1 d DG U . . .
C134 C -0.111(3) 0.3025(18) 0.4895(13) 0.188(11) Uani 1 1 d DG U . . .
H134 H -0.075520 0.319724 0.512436 0.225 Uiso 1 1 calc R U . . .
C135 C -0.205(3) 0.3358(16) 0.4763(13) 0.188(12) Uani 1 1 d DG U . . .
C136 C -0.256(2) 0.3106(18) 0.4427(13) 0.190(12) Uani 1 1 d DG U . . .
H136 H -0.320602 0.333290 0.433747 0.229 Uiso 1 1 calc R U . . .
C137 C -0.213(3) 0.2521(18) 0.4223(12) 0.187(11) Uani 1 1 d DG U . . .
H137 H -0.248010 0.234856 0.399287 0.224 Uiso 1 1 calc R U . . .
C138 C -0.119(3) 0.2188(15) 0.4354(13) 0.188(11) Uani 1 1 d DG U . . .
C139 C -0.121(4) 0.1457(19) 0.4399(15) 0.193(12) Uani 1 1 d D U . . .
H13A H -0.158730 0.136218 0.412846 0.231 Uiso 1 1 calc R U . . .
H13B H -0.049566 0.122042 0.434033 0.231 Uiso 1 1 calc R U . . .
C140 C -0.166(4) 0.119(2) 0.4886(15) 0.194(13) Uani 1 1 d D U . . .
H14A H -0.200659 0.084527 0.479203 0.233 Uiso 1 1 calc R U . . .
H14B H -0.107272 0.095892 0.506100 0.233 Uiso 1 1 calc R U . . .
C153 C -0.226(3) 0.2374(17) 0.5797(12) 0.156(9) Uani 1 1 d DG U . . .
C154 C -0.189(2) 0.1755(16) 0.5637(12) 0.159(9) Uani 1 1 d DG U . . .
H154 H -0.131813 0.149156 0.577352 0.191 Uiso 1 1 calc R U . . .
C155 C -0.237(2) 0.1522(14) 0.5278(13) 0.162(9) Uani 1 1 d DG U . . .
C156 C -0.322(2) 0.1907(17) 0.5079(12) 0.161(9) Uani 1 1 d DG U . . .
H156 H -0.354583 0.174757 0.483354 0.193 Uiso 1 1 calc R U . . .
C157 C -0.358(2) 0.2527(16) 0.5238(13) 0.155(9) Uani 1 1 d DG U . . .
H157 H -0.415666 0.279011 0.510214 0.186 Uiso 1 1 calc R U . . .
C158 C -0.310(2) 0.2760(13) 0.5597(13) 0.159(9) Uani 1 1 d DG U . . .
C159 C -0.323(3) 0.3502(18) 0.5588(15) 0.164(10) Uani 1 1 d D U . . .
H15A H -0.293654 0.362210 0.587983 0.196 Uiso 1 1 calc R U . . .
H15B H -0.396698 0.369413 0.561303 0.196 Uiso 1 1 calc R U . . .
C160 C -0.270(3) 0.3779(19) 0.5104(16) 0.168(11) Uani 1 1 d D U . . .
H16A H -0.324758 0.404055 0.491350 0.202 Uiso 1 1 calc R U . . .
H16B H -0.229509 0.408321 0.520411 0.202 Uiso 1 1 calc R U . . .
B1 B 0.467(2) 0.6637(17) 0.7239(15) 0.067(10) Uani 1 1 d . . . . .
C301 C 0.432(2) 0.6179(13) 0.6863(12) 0.061(8) Uani 1 1 d . . . . .
C302 C 0.502(2) 0.5921(14) 0.6476(12) 0.065(8) Uani 1 1 d . . . . .
H302 H 0.567040 0.604817 0.641973 0.078 Uiso 1 1 calc R U . . .
C303 C 0.476(3) 0.5446(15) 0.6151(13) 0.070(9) Uani 1 1 d . . . . .
C304 C 0.385(3) 0.5221(19) 0.6193(17) 0.099(14) Uani 1 1 d . . . . .
H304 H 0.366908 0.491395 0.599583 0.119 Uiso 1 1 calc R U . . .
C305 C 0.324(4) 0.554(3) 0.658(3) 0.160(10) Uani 1 1 d D U . . .
C306 C 0.340(3) 0.5931(15) 0.6906(13) 0.080(10) Uani 1 1 d . . . . .
H306 H 0.290042 0.604974 0.717227 0.096 Uiso 1 1 calc R U . . .
C307 C 0.548(6) 0.524(2) 0.574(2) 0.15(3) Uani 1 1 d . . . . .
F301 F 0.535(2) 0.4714(14) 0.5539(10) 0.160(13) Uani 1 1 d . . . . .
F302 F 0.649(3) 0.5060(10) 0.5885(10) 0.121(9) Uani 1 1 d . . . . .
F303 F 0.558(3) 0.5701(14) 0.5369(10) 0.154(12) Uani 1 1 d . . . . .
C308 C 0.234(3) 0.5217(12) 0.6676(10) 0.164(9) Uani 1 1 d D U . . .
F304 F 0.190(2) 0.5109(14) 0.6258(11) 0.179(10) Uani 1 1 d D U . . .
F305 F 0.152(2) 0.5563(13) 0.6949(12) 0.170(10) Uani 1 1 d D U . . .
F306 F 0.243(2) 0.4615(12) 0.6930(11) 0.163(9) Uani 1 1 d D U . . .
C311 C 0.520(3) 0.7230(16) 0.6982(14) 0.090(6) Uani 1 1 d . U . . .
C312 C 0.562(3) 0.7589(16) 0.7261(14) 0.089(5) Uani 1 1 d . U . . .
H312 H 0.557718 0.748617 0.761023 0.107 Uiso 1 1 calc R U . . .
C313 C 0.612(3) 0.8114(17) 0.7078(15) 0.098(5) Uani 1 1 d . U . . .
C314 C 0.602(3) 0.8288(18) 0.6554(15) 0.099(6) Uani 1 1 d . U . . .
H314 H 0.628147 0.864865 0.639870 0.119 Uiso 1 1 calc R U . . .
C315 C 0.554(3) 0.7941(19) 0.6281(15) 0.099(5) Uani 1 1 d . U . . .
C316 C 0.511(3) 0.7435(17) 0.6460(14) 0.092(6) Uani 1 1 d . U . . .
H316 H 0.475962 0.722311 0.625553 0.110 Uiso 1 1 calc R U . . .
C317 C 0.654(4) 0.847(2) 0.7383(19) 0.114(6) Uani 1 1 d . U . . .
F311 F 0.620(2) 0.8455(10) 0.7863(10) 0.124(7) Uani 1 1 d . U . . .
F312 F 0.642(2) 0.9079(12) 0.7250(10) 0.140(8) Uani 1 1 d . U . . .
F313 F 0.750(3) 0.8221(13) 0.7409(11) 0.146(8) Uani 1 1 d . U . . .
C318 C 0.542(4) 0.809(2) 0.5712(18) 0.111(6) Uani 1 1 d . U . . .
F314 F 0.540(2) 0.7670(14) 0.5453(9) 0.123(7) Uani 1 1 d . U . . .
F315 F 0.462(2) 0.8584(14) 0.5656(9) 0.138(8) Uani 1 1 d . U . . .
F316 F 0.616(2) 0.8414(14) 0.5538(9) 0.135(7) Uani 1 1 d . U . . .
C321 C 0.365(2) 0.7015(17) 0.7563(13) 0.079(10) Uani 1 1 d . . . . .
C322 C 0.3599(19) 0.7091(14) 0.8070(12) 0.062(8) Uani 1 1 d . . . . .
H322 H 0.416851 0.690991 0.824988 0.075 Uiso 1 1 calc R U . . .
C323 C 0.270(3) 0.744(2) 0.8324(15) 0.105(14) Uani 1 1 d . . . . .
C324 C 0.189(3) 0.775(2) 0.8077(15) 0.121(18) Uani 1 1 d D . . . .
H324 H 0.142196 0.810026 0.821773 0.145 Uiso 1 1 calc R U . F 1
C325 C 0.178(4) 0.754(5) 0.7602(17) 0.274(9) Uani 0.61(3) 1 d D U P G 1
C425 C 0.186(9) 0.772(11) 0.755(2) 0.274(9) Uani 0.39(3) 1 d D . P G 2
C326 C 0.274(3) 0.731(2) 0.7347(15) 0.122(17) Uani 1 1 d D . . . .
H326 H 0.278510 0.735174 0.699307 0.146 Uiso 1 1 calc R U . G 1
C327 C 0.270(3) 0.745(3) 0.8857(17) 0.117(18) Uani 1 1 d . . . . .
F321 F 0.3607(17) 0.7452(17) 0.9024(10) 0.150(12) Uani 1 1 d . . . . .
F322 F 0.234(3) 0.6996(13) 0.9150(11) 0.175(15) Uani 1 1 d . . . . .
F323 F 0.2167(17) 0.8029(11) 0.9028(9) 0.103(7) Uani 1 1 d . . . . .
C328 C 0.094(4) 0.792(3) 0.7304(14) 0.276(7) Uani 0.61(3) 1 d D U P G 1
C428 C 0.096(5) 0.811(4) 0.730(2) 0.276(7) Uani 0.39(3) 1 d D . P G 2
F324 F 0.023(4) 0.811(4) 0.7649(14) 0.277(5) Uani 0.61(3) 1 d D U P G 1
F325 F 0.066(5) 0.753(3) 0.7025(18) 0.277(5) Uani 0.61(3) 1 d D U P G 1
F326 F 0.120(4) 0.840(3) 0.7033(18) 0.277(5) Uani 0.61(3) 1 d D U P G 1
F424 F 0.017(7) 0.785(5) 0.745(3) 0.277(5) Uani 0.39(3) 1 d D U P G 2
F425 F 0.116(7) 0.808(6) 0.683(2) 0.277(5) Uani 0.39(3) 1 d D U P G 2
F426 F 0.075(7) 0.872(4) 0.741(3) 0.277(5) Uani 0.39(3) 1 d D U P G 2
C331 C 0.540(2) 0.6127(12) 0.7593(11) 0.055(7) Uani 1 1 d . . . . .
C332 C 0.647(2) 0.6065(13) 0.7522(11) 0.065(8) Uani 1 1 d . . . . .
H332 H 0.675144 0.635365 0.728401 0.078 Uiso 1 1 calc R U . . .
C333 C 0.712(3) 0.5605(13) 0.7781(11) 0.066(8) Uani 1 1 d . . . . .
C334 C 0.674(2) 0.5216(13) 0.8181(11) 0.060(7) Uani 1 1 d . . . . .
H334 H 0.717005 0.492099 0.838533 0.072 Uiso 1 1 calc R U . . .
C335 C 0.571(2) 0.5292(13) 0.8255(12) 0.062(7) Uani 1 1 d . . . . .
C336 C 0.507(2) 0.5719(13) 0.7967(11) 0.058(7) Uani 1 1 d . . . . .
H336 H 0.435218 0.573406 0.803035 0.070 Uiso 1 1 calc R U . . .
C337 C 0.825(2) 0.5574(14) 0.7689(12) 0.064(8) Uani 1 1 d . . . . .
F331 F 0.8548(14) 0.5347(10) 0.7240(7) 0.087(6) Uani 1 1 d . . . . .
F332 F 0.8508(13) 0.6127(8) 0.7693(8) 0.084(6) Uani 1 1 d . . . . .
F333 F 0.8765(13) 0.5156(9) 0.8018(7) 0.074(5) Uani 1 1 d . . . . .
C338 C 0.516(3) 0.4861(16) 0.8667(17) 0.092(12) Uani 1 1 d . . . . .
F334 F 0.5841(15) 0.4677(10) 0.9031(9) 0.100(7) Uani 1 1 d . . . . .
F335 F 0.498(2) 0.4363(11) 0.8498(10) 0.132(10) Uani 1 1 d . . . . .
F336 F 0.4383(16) 0.5174(11) 0.8891(8) 0.098(7) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O8 Dy1 O7 92.8(6) . . ?
O8 Dy1 O6 91.7(6) . . ?
O7 Dy1 O6 144.0(5) . . ?
O8 Dy1 O5 82.3(6) . . ?
O7 Dy1 O5 146.0(5) . . ?
O6 Dy1 O5 70.0(5) . . ?
O8 Dy1 O2 74.2(6) . . ?
O7 Dy1 O2 75.8(6) . . ?
O6 Dy1 O2 71.2(6) . . ?
O5 Dy1 O2 133.5(6) . . ?
O8 Dy1 O3 143.6(6) . . ?
O7 Dy1 O3 92.5(6) . . ?
O6 Dy1 O3 104.6(6) . . ?
O5 Dy1 O3 73.4(5) . . ?
O2 Dy1 O3 141.8(6) . . ?
O8 Dy1 O4 74.8(5) . . ?
O7 Dy1 O4 76.2(5) . . ?
O6 Dy1 O4 139.1(5) . . ?
O5 Dy1 O4 70.0(5) . . ?
O2 Dy1 O4 136.6(6) . . ?
O3 Dy1 O4 71.6(6) . . ?
O8 Dy1 O1 145.6(5) . . ?
O7 Dy1 O1 84.7(6) . . ?
O6 Dy1 O1 71.9(6) . . ?
O5 Dy1 O1 117.6(6) . . ?
O2 Dy1 O1 71.9(5) . . ?
O3 Dy1 O1 70.9(5) . . ?
O4 Dy1 O1 136.7(5) . . ?
O8 Dy1 Na1 172.8(4) . . ?
O7 Dy1 Na1 94.3(4) . . ?
O6 Dy1 Na1 83.1(4) . . ?
O5 Dy1 Na1 91.2(5) . . ?
O2 Dy1 Na1 108.6(5) . . ?
O3 Dy1 Na1 35.1(4) . . ?
O4 Dy1 Na1 106.0(4) . . ?
O1 Dy1 Na1 36.7(4) . . ?
F1B Na1 F7B 144.5(14) . . ?
F1B Na1 O3 133.9(11) . . ?
F7B Na1 O3 71.0(8) . . ?
F1 Na1 O3 135.1(12) . . ?
F1B Na1 F105 100.1(13) . . ?
F7B Na1 F105 105.7(12) . . ?
F1 Na1 F105 79.2(14) . . ?
O3 Na1 F105 89.2(7) . . ?
F1B Na1 F107 75.1(13) . . ?
F7B Na1 F107 89.5(12) . . ?
F1 Na1 F107 95.0(14) . . ?
O3 Na1 F107 78.9(8) . . ?
F105 Na1 F107 156.6(8) . . ?
F1B Na1 O1 68.8(10) . . ?
F7B Na1 O1 141.7(9) . . ?
F1 Na1 O1 64.4(11) . . ?
O3 Na1 O1 70.7(6) . . ?
F105 Na1 O1 74.4(6) . . ?
F107 Na1 O1 82.6(7) . . ?
F1B Na1 O102 88.2(11) . . ?
F7B Na1 O102 80.3(9) . . ?
F1 Na1 O102 78.4(12) . . ?
O3 Na1 O102 135.7(7) . . ?
F105 Na1 O102 66.6(6) . . ?
F107 Na1 O102 134.9(8) . . ?
O1 Na1 O102 130.1(7) . . ?
F1 Na1 F7 154.7(12) . . ?
O3 Na1 F7 68.2(7) . . ?
F105 Na1 F7 93.3(8) . . ?
F107 Na1 F7 100.7(9) . . ?
O1 Na1 F7 137.2(8) . . ?
O102 Na1 F7 76.5(7) . . ?
F1B Na1 O103 74.3(11) . . ?
F7B Na1 O103 70.2(11) . . ?
F1 Na1 O103 88.4(13) . . ?
O3 Na1 O103 126.3(8) . . ?
F105 Na1 O103 136.4(7) . . ?
F107 Na1 O103 65.2(7) . . ?
O1 Na1 O103 136.0(8) . . ?
O102 Na1 O103 70.0(6) . . ?
F7 Na1 O103 80.3(9) . . ?
F1B Na1 C1B 24.5(8) . . ?
F7B Na1 C1B 168.9(12) . . ?
O3 Na1 C1B 117.8(9) . . ?
F105 Na1 C1B 81.9(9) . . ?
F107 Na1 C1B 85.9(10) . . ?
O1 Na1 C1B 47.5(9) . . ?
O102 Na1 C1B 95.8(9) . . ?
O103 Na1 C1B 98.8(10) . . ?
F1B Na1 C6 156.1(12) . . ?
F7B Na1 C6 24.6(7) . . ?
F1 Na1 C6 176.9(14) . . ?
O3 Na1 C6 46.6(7) . . ?
F105 Na1 C6 103.8(7) . . ?
F107 Na1 C6 82.6(8) . . ?
O1 Na1 C6 117.2(8) . . ?
O102 Na1 C6 101.8(7) . . ?
F7 Na1 C6 25.4(5) . . ?
O103 Na1 C6 88.7(8) . . ?
C1B Na1 C6 162.3(10) . . ?
C2 O1 Dy1 129.4(17) . . ?
C2 O1 Na1 120.3(19) . . ?
Dy1 O1 Na1 106.8(6) . . ?
C4 O2 Dy1 135.1(18) . . ?
C7 O3 Dy1 129.9(17) . . ?
C7 O3 Na1 119.3(17) . . ?
Dy1 O3 Na1 109.9(7) . . ?
C9 O4 Dy1 134.2(19) . . ?
C12 O5 Dy1 138.4(14) . . ?
C14 O6 Dy1 136.5(15) . . ?
P1 O7 Dy1 154.9(10) . . ?
P2 O8 Dy1 168.3(10) . . ?
O7 P1 C27 109.4(10) . . ?
O7 P1 C21 109.2(11) . . ?
C27 P1 C21 106.0(10) . . ?
O7 P1 C33 113.8(9) . . ?
C27 P1 C33 105.9(11) . . ?
C21 P1 C33 112.2(10) . . ?
O8 P2 C47 108.6(11) . . ?
O8 P2 C53 112.6(9) . . ?
C47 P2 C53 113.7(11) . . ?
O8 P2 C41 112.0(11) . . ?
C47 P2 C41 105.7(11) . . ?
C53 P2 C41 104.1(10) . . ?
C1 F1 Na1 121(3) . . ?
F3 C1 F2 105(2) . . ?
F3 C1 F1 105(2) . . ?
F2 C1 F1 105(2) . . ?
F3 C1 C2 115(3) . . ?
F2 C1 C2 119(4) . . ?
F1 C1 C2 106(3) . . ?
C1B F1B Na1 111(2) . . ?
F3B C1B F1B 105(2) . . ?
F3B C1B F2B 105(2) . . ?
F1B C1B F2B 105(2) . . ?
F3B C1B C2 112(3) . . ?
F1B C1B C2 119(3) . . ?
F2B C1B C2 110(3) . . ?
F3B C1B Na1 147.7(18) . . ?
F1B C1B Na1 44.5(18) . . ?
F2B C1B Na1 95.3(15) . . ?
C2 C1B Na1 83.1(18) . . ?
O1 C2 C3 130(3) . . ?
O1 C2 C1 113(3) . . ?
C3 C2 C1 112(3) . . ?
O1 C2 C1B 109(3) . . ?
C3 C2 C1B 121(3) . . ?
C2 C3 C4 121(2) . . ?
C2 C3 H3 119.3 . . ?
C4 C3 H3 119.3 . . ?
O2 C4 C3 128(2) . . ?
O2 C4 C5 118(2) . . ?
C3 C4 C5 114(2) . . ?
F4 C5 F6 102.9(16) . . ?
F4 C5 F5 102.7(16) . . ?
F6 C5 F5 102.6(16) . . ?
F5B C5 F4B 102.0(16) . . ?
F5B C5 F6B 101.9(16) . . ?
F4B C5 F6B 101.8(16) . . ?
F4 C5 C4 121(2) . . ?
F6 C5 C4 113(2) . . ?
F5 C5 C4 113(2) . . ?
F5B C5 C4 118(2) . . ?
F4B C5 C4 121(3) . . ?
F6B C5 C4 110(2) . . ?
C6 F7 Na1 104.7(14) . . ?
C6 F7B Na1 111(3) . . ?
F9 C6 F7 100.8(17) . . ?
F7B C6 F8B 99.9(17) . . ?
F9 C6 F8 100.1(17) . . ?
F7 C6 F8 99.7(16) . . ?
F7B C6 F9B 99.4(17) . . ?
F8B C6 F9B 99.2(17) . . ?
F9 C6 C7 123(2) . . ?
F7 C6 C7 118(2) . . ?
F7B C6 C7 124(3) . . ?
F8B C6 C7 125(3) . . ?
F8 C6 C7 112(2) . . ?
F9B C6 C7 104(3) . . ?
F9 C6 Na1 150.6(16) . . ?
F7 C6 Na1 49.9(11) . . ?
F7B C6 Na1 45(2) . . ?
F8B C6 Na1 126.0(19) . . ?
F8 C6 Na1 85.2(10) . . ?
F9B C6 Na1 122.1(17) . . ?
C7 C6 Na1 79.9(13) . . ?
O3 C7 C8 129(2) . . ?
O3 C7 C6 114(2) . . ?
C8 C7 C6 117(2) . . ?
C9 C8 C7 119(2) . . ?
C9 C8 H8 120.7 . . ?
C7 C8 H8 120.7 . . ?
O4 C9 C8 130(3) . . ?
O4 C9 C10 121(3) . . ?
C8 C9 C10 110(2) . . ?
F12 C10 F11 109(2) . . ?
F12 C10 F10 105(2) . . ?
F11 C10 F10 104(2) . . ?
F12 C10 C9 112(2) . . ?
F11 C10 C9 118(2) . . ?
F10 C10 C9 108(2) . . ?
F14 C11 F13 108(3) . . ?
F14 C11 F15 109(3) . . ?
F13 C11 F15 104(2) . . ?
F14 C11 C12 115(2) . . ?
F13 C11 C12 109(3) . . ?
F15 C11 C12 111(2) . . ?
O5 C12 C13 127.6(19) . . ?
O5 C12 C11 112(2) . . ?
C13 C12 C11 120(2) . . ?
C14 C13 C12 118(2) . . ?
C14 C13 H13 120.9 . . ?
C12 C13 H13 120.9 . . ?
O6 C14 C13 129(2) . . ?
O6 C14 C15 109(2) . . ?
C13 C14 C15 121(2) . . ?
F18 C15 F16 108(2) . . ?
F18 C15 F17 104(3) . . ?
F16 C15 F17 104(3) . . ?
F18 C15 C14 117(3) . . ?
F16 C15 C14 112(3) . . ?
F17 C15 C14 112(2) . . ?
C22 C21 C26 118(2) . . ?
C22 C21 P1 119.8(19) . . ?
C26 C21 P1 122(2) . . ?
C23 C22 C21 121(2) . . ?
C23 C22 H22 119.5 . . ?
C21 C22 H22 119.5 . . ?
C22 C23 C24 119(3) . . ?
C22 C23 H23 120.7 . . ?
C24 C23 H23 120.7 . . ?
C23 C24 C25 122(3) . . ?
C23 C24 H24 119.0 . . ?
C25 C24 H24 119.0 . . ?
C26 C25 C24 119(3) . . ?
C26 C25 H25 120.7 . . ?
C24 C25 H25 120.7 . . ?
C25 C26 C21 121(3) . . ?
C25 C26 H26 119.5 . . ?
C21 C26 H26 119.5 . . ?
C32 C27 C28 115(3) . . ?
C32 C27 P1 127(2) . . ?
C28 C27 P1 118(2) . . ?
C29 C28 C27 123(3) . . ?
C29 C28 H28 118.3 . . ?
C27 C28 H28 118.3 . . ?
C28 C29 C30 121(3) . . ?
C28 C29 H29 119.4 . . ?
C30 C29 H29 119.4 . . ?
C29 C30 C31 119(2) . . ?
C29 C30 H30 120.4 . . ?
C31 C30 H30 120.4 . . ?
C30 C31 C32 119(3) . . ?
C30 C31 H31 120.5 . . ?
C32 C31 H31 120.5 . . ?
C27 C32 C31 122(3) . . ?
C27 C32 H32 119.0 . . ?
C31 C32 H32 119.0 . . ?
C46 C41 C42 121(2) . . ?
C46 C41 P2 122(2) . . ?
C42 C41 P2 116.9(19) . . ?
C41 C42 C43 117(3) . . ?
C41 C42 H42 121.4 . . ?
C43 C42 H42 121.4 . . ?
C44 C43 C42 122(3) . . ?
C44 C43 H43 118.8 . . ?
C42 C43 H43 118.8 . . ?
C43 C44 C45 119(3) . . ?
C43 C44 H44 120.3 . . ?
C45 C44 H44 120.3 . . ?
C46 C45 C44 118(3) . . ?
C46 C45 H45 120.9 . . ?
C44 C45 H45 120.9 . . ?
C41 C46 C45 122(3) . . ?
C41 C46 H46 119.2 . . ?
C45 C46 H46 119.2 . . ?
C52 C47 C48 119(3) . . ?
C52 C47 P2 119(2) . . ?
C48 C47 P2 122(2) . . ?
C49 C48 C47 120(3) . . ?
C49 C48 H48 120.1 . . ?
C47 C48 H48 120.1 . . ?
C48 C49 C50 121(3) . . ?
C48 C49 H49 119.4 . . ?
C50 C49 H49 119.4 . . ?
C51 C50 C49 119(3) . . ?
C51 C50 H50 120.4 . . ?
C49 C50 H50 120.4 . . ?
C52 C51 C50 120(3) . . ?
C52 C51 H51 119.8 . . ?
C50 C51 H51 119.8 . . ?
C51 C52 C47 120(3) . . ?
C51 C52 H52 119.8 . . ?
C47 C52 H52 119.8 . . ?
C38 C33 C34 119.2(17) . . ?
C38 C33 P1 127.1(14) . . ?
C34 C33 P1 113.6(14) . . ?
C35 C34 C33 121.2(17) . . ?
C35 C34 H34 119.4 . . ?
C33 C34 H34 119.4 . . ?
C34 C35 C36 117.2(16) . . ?
C34 C35 C60 121.9(19) . . ?
C36 C35 C60 118.3(19) . . ?
C37 C36 C35 120.5(18) . . ?
C37 C36 H36 119.8 . . ?
C35 C36 H36 119.8 . . ?
C38 C37 C36 121.1(17) . . ?
C38 C37 H37 119.5 . . ?
C36 C37 H37 119.5 . . ?
C37 C38 C33 119.0(16) . . ?
C37 C38 C39 114.4(17) . . ?
C33 C38 C39 122.7(18) . . ?
C38 C39 C40 112.2(18) . . ?
C38 C39 H39A 109.2 . . ?
C40 C39 H39A 109.2 . . ?
C38 C39 H39B 109.2 . . ?
C40 C39 H39B 109.2 . . ?
H39A C39 H39B 107.9 . . ?
C55 C40 C39 120(2) . . ?
C55 C40 H40A 107.4 . . ?
C39 C40 H40A 107.4 . . ?
C55 C40 H40B 107.4 . . ?
C39 C40 H40B 107.4 . . ?
H40A C40 H40B 107.0 . . ?
C54 C53 C58 117.7(16) . . ?
C54 C53 P2 111.9(13) . . ?
C58 C53 P2 130.4(13) . . ?
C55 C54 C53 123.1(17) . . ?
C55 C54 H54 118.5 . . ?
C53 C54 H54 118.5 . . ?
C56 C55 C54 117.9(17) . . ?
C56 C55 C40 118.3(19) . . ?
C54 C55 C40 120.7(19) . . ?
C55 C56 C57 119.1(18) . . ?
C58 C57 C56 121.7(18) . . ?
C58 C57 H57 119.1 . . ?
C56 C57 H57 119.1 . . ?
C57 C58 C53 117.6(16) . . ?
C57 C58 C59 116.4(18) . . ?
C53 C58 C59 123.4(18) . . ?
C58 C59 C60 109.9(19) . . ?
C58 C59 H59A 109.7 . . ?
C60 C59 H59A 109.7 . . ?
C58 C59 H59B 109.7 . . ?
C60 C59 H59B 109.7 . . ?
H59A C59 H59B 108.2 . . ?
C35 C60 C59 118(2) . . ?
C35 C60 H60A 107.7 . . ?
C59 C60 H60A 107.7 . . ?
C35 C60 H60B 107.7 . . ?
C59 C60 H60B 107.7 . . ?
H60A C60 H60B 107.1 . . ?
O108 Dy2 O107 97.0(7) . . ?
O108 Dy2 O106 142.9(7) . . ?
O107 Dy2 O106 90.5(7) . . ?
O108 Dy2 O105 146.5(6) . . ?
O107 Dy2 O105 82.9(7) . . ?
O106 Dy2 O105 70.4(6) . . ?
O108 Dy2 O104 74.5(7) . . ?
O107 Dy2 O104 74.6(7) . . ?
O106 Dy2 O104 142.0(7) . . ?
O105 Dy2 O104 73.2(7) . . ?
O108 Dy2 O101 76.8(6) . . ?
O107 Dy2 O101 74.4(6) . . ?
O106 Dy2 O101 70.4(7) . . ?
O105 Dy2 O101 134.1(6) . . ?
O104 Dy2 O101 134.2(6) . . ?
O108 Dy2 O103 90.5(7) . . ?
O107 Dy2 O103 142.3(6) . . ?
O106 Dy2 O103 105.4(7) . . ?
O105 Dy2 O103 71.2(7) . . ?
O104 Dy2 O103 72.0(7) . . ?
O101 Dy2 O103 143.0(6) . . ?
O108 Dy2 O102 81.5(6) . . ?
O107 Dy2 O102 146.6(6) . . ?
O106 Dy2 O102 72.7(6) . . ?
O105 Dy2 O102 116.4(6) . . ?
O104 Dy2 O102 135.3(7) . . ?
O101 Dy2 O102 72.8(5) . . ?
O103 Dy2 O102 71.1(6) . . ?
O108 Dy2 Na1 91.2(5) . . ?
O107 Dy2 Na1 171.7(5) . . ?
O106 Dy2 Na1 83.3(5) . . ?
O105 Dy2 Na1 89.8(6) . . ?
O104 Dy2 Na1 107.1(6) . . ?
O101 Dy2 Na1 108.4(4) . . ?
O103 Dy2 Na1 36.3(5) . . ?
O102 Dy2 Na1 35.7(4) . . ?
C102 O101 Dy2 134.8(18) . . ?
C104 O102 Dy2 130.3(16) . . ?
C104 O102 Na1 119.9(16) . . ?
Dy2 O102 Na1 108.7(6) . . ?
C107 O103 Dy2 131(2) . . ?
C107 O103 Na1 121(2) . . ?
Dy2 O103 Na1 108.4(7) . . ?
C109 O104 Dy2 133(2) . . ?
C112 O105 Dy2 135.7(18) . . ?
C114 O106 Dy2 140.1(17) . . ?
P101 O107 Dy2 173.4(13) . . ?
P102 O108 Dy2 164.5(13) . . ?
O107 P101 C121 110.2(18) . . ?
O107 P101 C127 108.5(16) . . ?
C121 P101 C127 106(2) . . ?
O107 P101 C133 113.8(14) . . ?
C121 P101 C133 114.4(19) . . ?
C127 P101 C133 104(2) . . ?
O108 P102 C153 113.8(15) . . ?
O108 P102 C141 110.0(13) . . ?
C153 P102 C141 105.1(17) . . ?
O108 P102 C147 111.2(11) . . ?
C153 P102 C147 110.8(15) . . ?
C141 P102 C147 105.5(16) . . ?
F101 C101 F103 115(4) . . ?
F101 C101 F102 101(4) . . ?
F103 C101 F102 101(3) . . ?
F101 C101 C102 116(3) . . ?
F103 C101 C102 117(3) . . ?
F102 C101 C102 104(3) . . ?
O101 C102 C103 126(2) . . ?
O101 C102 C101 116(3) . . ?
C103 C102 C101 117(3) . . ?
C104 C103 C102 125(2) . . ?
C104 C103 H103 117.5 . . ?
C102 C103 H103 117.5 . . ?
O102 C104 C103 129(2) . . ?
O102 C104 C105 112(3) . . ?
C103 C104 C105 118(2) . . ?
F105 C105 F106 106(3) . . ?
F105 C105 F104 111(3) . . ?
F106 C105 F104 105(2) . . ?
F105 C105 C104 111(2) . . ?
F106 C105 C104 114(3) . . ?
F104 C105 C104 108(3) . . ?
C105 F105 Na1 113(2) . . ?
C106 F107 Na1 120(2) . . ?
F107 C106 F108 102.0(19) . . ?
F107 C106 F109 102.1(19) . . ?
F108 C106 F109 101.6(19) . . ?
F107 C106 C107 115(2) . . ?
F108 C106 C107 122(3) . . ?
F109 C106 C107 111(3) . . ?
O103 C107 C108 130(3) . . ?
O103 C107 C106 117(3) . . ?
C108 C107 C106 112(3) . . ?
C107 C108 C109 123(3) . . ?
C107 C108 H108 118.6 . . ?
C109 C108 H108 118.6 . . ?
O104 C109 C108 127(3) . . ?
O104 C109 C110 117(2) . . ?
C108 C109 C110 116.0(19) . . ?
F110 C110 F112 104.3(16) . . ?
F212 C110 F211 104.5(16) . . ?
F110 C110 F111 103.8(16) . . ?
F112 C110 F111 103.9(16) . . ?
F212 C110 F210 103.9(16) . . ?
F211 C110 F210 103.6(16) . . ?
F212 C110 C109 114.9(14) . . ?
F110 C110 C109 114.8(14) . . ?
F112 C110 C109 114.6(14) . . ?
F211 C110 C109 114.6(14) . . ?
F111 C110 C109 114.1(14) . . ?
F210 C110 C109 114.0(14) . . ?
F215 C111 F214 106.0(16) . . ?
F215 C111 F213 105.8(16) . . ?
F214 C111 F213 105.6(16) . . ?
F113 C111 F114 105.7(16) . . ?
F113 C111 F115 105.4(16) . . ?
F114 C111 F115 105.5(16) . . ?
F215 C111 C112 117(3) . . ?
F214 C111 C112 115(3) . . ?
F213 C111 C112 107(3) . . ?
F113 C111 C112 112(3) . . ?
F114 C111 C112 115(3) . . ?
F115 C111 C112 113(3) . . ?
O105 C112 C113 128(3) . . ?
O105 C112 C111 112(2) . . ?
C113 C112 C111 119(3) . . ?
C112 C113 C114 120(3) . . ?
C112 C113 H113 119.9 . . ?
C114 C113 H113 119.9 . . ?
O106 C114 C113 122(2) . . ?
O106 C114 C115 120.0(19) . . ?
C113 C114 C115 115.8(19) . . ?
F116 C115 F118 115.8(17) . . ?
F218 C115 F216 113.1(18) . . ?
F218 C115 F217 110.8(18) . . ?
F216 C115 F217 108.7(18) . . ?
F116 C115 F117 108.1(16) . . ?
F118 C115 F117 105.2(16) . . ?
F116 C115 C114 110.8(14) . . ?
F218 C115 C114 110.2(15) . . ?
F118 C115 C114 109.8(14) . . ?
F216 C115 C114 108.5(15) . . ?
F217 C115 C114 105.3(14) . . ?
F117 C115 C114 106.5(13) . . ?
C122 C121 C126 121(4) . . ?
C122 C121 P101 119(4) . . ?
C126 C121 P101 119(4) . . ?
C121 C122 C123 120(5) . . ?
C121 C122 H122 120.0 . . ?
C123 C122 H122 120.0 . . ?
C124 C123 C122 117(5) . . ?
C124 C123 H123 121.7 . . ?
C122 C123 H123 121.7 . . ?
C125 C124 C123 127(5) . . ?
C125 C124 H124 116.6 . . ?
C123 C124 H124 116.6 . . ?
C124 C125 C126 117(5) . . ?
C124 C125 H125 121.3 . . ?
C126 C125 H125 121.3 . . ?
C121 C126 C125 118(5) . . ?
C121 C126 H126 121.2 . . ?
C125 C126 H126 121.2 . . ?
C128 C127 C132 119(4) . . ?
C128 C127 P101 121(3) . . ?
C132 C127 P101 120(3) . . ?
C127 C128 C129 123(4) . . ?
C127 C128 H128 118.7 . . ?
C129 C128 H128 118.7 . . ?
C130 C129 C128 118(4) . . ?
C130 C129 H129 121.1 . . ?
C128 C129 H129 121.1 . . ?
C131 C130 C129 118(4) . . ?
C131 C130 H130 120.8 . . ?
C129 C130 H130 120.8 . . ?
C130 C131 C132 119(4) . . ?
C130 C131 H131 120.4 . . ?
C132 C131 H131 120.4 . . ?
C127 C132 C131 122(4) . . ?
C127 C132 H132 119.0 . . ?
C131 C132 H132 119.0 . . ?
C146 C141 C142 120(3) . . ?
C146 C141 P102 123(3) . . ?
C142 C141 P102 117(2) . . ?
C143 C142 C141 118(4) . . ?
C143 C142 H142 121.1 . . ?
C141 C142 H142 121.1 . . ?
C142 C143 C144 117(5) . . ?
C142 C143 H143 121.7 . . ?
C144 C143 H143 121.7 . . ?
C145 C144 C143 124(5) . . ?
C145 C144 H144 118.2 . . ?
C143 C144 H144 118.2 . . ?
C144 C145 C146 121(5) . . ?
C144 C145 H145 119.7 . . ?
C146 C145 H145 119.7 . . ?
C141 C146 C145 122(4) . . ?
C141 C146 H146 119.2 . . ?
C145 C146 H146 119.2 . . ?
C148 C147 C152 120.0 . . ?
C148 C147 P102 118.5(14) . . ?
C152 C147 P102 121.5(14) . . ?
C149 C148 C147 120.0 . . ?
C149 C148 H148 120.0 . . ?
C147 C148 H148 120.0 . . ?
C148 C149 C150 120.0 . . ?
C148 C149 H149 120.0 . . ?
C150 C149 H149 120.0 . . ?
C151 C150 C149 120.0 . . ?
C151 C150 H150 120.0 . . ?
C149 C150 H150 120.0 . . ?
C152 C151 C150 120.0 . . ?
C152 C151 H151 120.0 . . ?
C150 C151 H151 120.0 . . ?
C151 C152 C147 120.0 . . ?
C151 C152 H152 120.0 . . ?
C147 C152 H152 120.0 . . ?
C134 C133 C138 120.0 . . ?
C134 C133 P101 109.1(18) . . ?
C138 C133 P101 129.3(19) . . ?
C135 C134 C133 120.0 . . ?
C135 C134 H134 120.0 . . ?
C133 C134 H134 120.0 . . ?
C134 C135 C136 120.0 . . ?
C134 C135 C160 120(2) . . ?
C136 C135 C160 114(2) . . ?
C137 C136 C135 120.0 . . ?
C137 C136 H136 120.0 . . ?
C135 C136 H136 120.0 . . ?
C138 C137 C136 120.0 . . ?
C138 C137 H137 120.0 . . ?
C136 C137 H137 120.0 . . ?
C137 C138 C133 120.0 . . ?
C137 C138 C139 109(2) . . ?
C133 C138 C139 119(2) . . ?
C140 C139 C138 117(3) . . ?
C140 C139 H13A 108.1 . . ?
C138 C139 H13A 108.1 . . ?
C140 C139 H13B 108.1 . . ?
C138 C139 H13B 108.1 . . ?
H13A C139 H13B 107.3 . . ?
C155 C140 C139 130(3) . . ?
C155 C140 H14A 104.8 . . ?
C139 C140 H14A 104.8 . . ?
C155 C140 H14B 104.8 . . ?
C139 C140 H14B 104.8 . . ?
H14A C140 H14B 105.8 . . ?
C154 C153 C158 120.0 . . ?
C154 C153 P102 108.0(19) . . ?
C158 C153 P102 126.8(19) . . ?
C153 C154 C155 120.0 . . ?
C153 C154 H154 120.0 . . ?
C155 C154 H154 120.0 . . ?
C156 C155 C154 120.0 . . ?
C156 C155 C140 111(2) . . ?
C154 C155 C140 114(2) . . ?
C155 C156 C157 120.0 . . ?
C155 C156 H156 120.0 . . ?
C157 C156 H156 120.0 . . ?
C156 C157 C158 120.0 . . ?
C156 C157 H157 120.0 . . ?
C158 C157 H157 120.0 . . ?
C157 C158 C153 120.0 . . ?
C157 C158 C159 115(2) . . ?
C153 C158 C159 120(2) . . ?
C158 C159 C160 111(3) . . ?
C158 C159 H15A 109.4 . . ?
C160 C159 H15A 109.4 . . ?
C158 C159 H15B 109.4 . . ?
C160 C159 H15B 109.4 . . ?
H15A C159 H15B 108.0 . . ?
C135 C160 C159 121(3) . . ?
C135 C160 H16A 107.1 . . ?
C159 C160 H16A 107.1 . . ?
C135 C160 H16B 107.1 . . ?
C159 C160 H16B 107.1 . . ?
H16A C160 H16B 106.8 . . ?
C301 B1 C311 117(3) . . ?
C301 B1 C331 104(2) . . ?
C311 B1 C331 113(2) . . ?
C301 B1 C321 109(2) . . ?
C311 B1 C321 103(3) . . ?
C331 B1 C321 112(3) . . ?
C302 C301 C306 113(3) . . ?
C302 C301 B1 119(2) . . ?
C306 C301 B1 128(3) . . ?
C301 C302 C303 120(3) . . ?
C301 C302 H302 120.0 . . ?
C303 C302 H302 120.0 . . ?
C304 C303 C307 117(4) . . ?
C304 C303 C302 126(4) . . ?
C307 C303 C302 117(3) . . ?
C303 C304 C305 106(4) . . ?
C303 C304 H304 126.9 . . ?
C305 C304 H304 126.9 . . ?
C306 C305 C304 134(4) . . ?
C306 C305 C308 119(5) . . ?
C304 C305 C308 106(4) . . ?
C305 C306 C301 121(4) . . ?
C305 C306 H306 119.6 . . ?
C301 C306 H306 119.6 . . ?
F301 C307 F303 108(4) . . ?
F301 C307 F302 103(5) . . ?
F303 C307 F302 102(5) . . ?
F301 C307 C303 115(5) . . ?
F303 C307 C303 115(5) . . ?
F302 C307 C303 112(4) . . ?
F305 C308 F304 102(2) . . ?
F305 C308 F306 101(2) . . ?
F304 C308 F306 102(2) . . ?
F305 C308 C305 115(4) . . ?
F304 C308 C305 116(4) . . ?
F306 C308 C305 119(3) . . ?
C312 C311 C316 119(3) . . ?
C312 C311 B1 121(3) . . ?
C316 C311 B1 120(3) . . ?
C311 C312 C313 126(4) . . ?
C311 C312 H312 117.1 . . ?
C313 C312 H312 117.1 . . ?
C317 C313 C312 124(4) . . ?
C317 C313 C314 124(4) . . ?
C312 C313 C314 112(3) . . ?
C315 C314 C313 121(4) . . ?
C315 C314 H314 119.5 . . ?
C313 C314 H314 119.5 . . ?
C316 C315 C314 125(4) . . ?
C316 C315 C318 111(4) . . ?
C314 C315 C318 124(4) . . ?
C315 C316 C311 117(3) . . ?
C315 C316 H316 121.7 . . ?
C311 C316 H316 121.7 . . ?
F312 C317 F313 111(4) . . ?
F312 C317 F311 104(4) . . ?
F313 C317 F311 101(4) . . ?
F312 C317 C313 114(4) . . ?
F313 C317 C313 109(4) . . ?
F311 C317 C313 117(4) . . ?
F314 C318 F316 110(5) . . ?
F314 C318 F315 112(4) . . ?
F316 C318 F315 97(4) . . ?
F314 C318 C315 121(4) . . ?
F316 C318 C315 105(4) . . ?
F315 C318 C315 109(4) . . ?
C322 C321 C326 113(3) . . ?
C322 C321 B1 124(3) . . ?
C326 C321 B1 123(3) . . ?
C321 C322 C323 121(3) . . ?
C321 C322 H322 119.7 . . ?
C323 C322 H322 119.7 . . ?
C324 C323 C322 122(4) . . ?
C324 C323 C327 122(4) . . ?
C322 C323 C327 116(3) . . ?
C323 C324 C325 118(3) . . ?
C323 C324 C425 123(3) . . ?
C323 C324 H324 120.9 . . ?
C325 C324 H324 120.8 . . ?
C324 C325 C326 111(4) . . ?
C324 C325 C328 119(5) . . ?
C326 C325 C328 118(5) . . ?
C324 C425 C326 111(4) . . ?
C324 C425 C428 119(3) . . ?
C326 C425 C428 130(4) . . ?
C321 C326 C325 127(4) . . ?
C321 C326 C425 130(4) . . ?
C321 C326 H326 116.5 . . ?
C325 C326 H326 116.5 . . ?
F322 C327 F321 104(5) . . ?
F322 C327 F323 105(3) . . ?
F321 C327 F323 99(4) . . ?
F322 C327 C323 120(5) . . ?
F321 C327 C323 116(3) . . ?
F323 C327 C323 111(5) . . ?
F325 C328 F326 110(2) . . ?
F325 C328 F324 111(2) . . ?
F326 C328 F324 111(2) . . ?
F325 C328 C325 109(5) . . ?
F326 C328 C325 114(7) . . ?
F324 C328 C325 102(4) . . ?
F425 C428 F424 109(2) . . ?
F425 C428 F426 109(2) . . ?
F424 C428 F426 109(2) . . ?
F425 C428 C425 108(5) . . ?
F424 C428 C425 108(10) . . ?
F426 C428 C425 114(10) . . ?
C336 C331 C332 114(3) . . ?
C336 C331 B1 125(2) . . ?
C332 C331 B1 121(3) . . ?
C333 C332 C331 123(3) . . ?
C333 C332 H332 118.4 . . ?
C331 C332 H332 118.4 . . ?
C332 C333 C334 120(3) . . ?
C332 C333 C337 120(3) . . ?
C334 C333 C337 119(3) . . ?
C335 C334 C333 116(3) . . ?
C335 C334 H334 122.0 . . ?
C333 C334 H334 122.0 . . ?
C334 C335 C336 123(3) . . ?
C334 C335 C338 122(3) . . ?
C336 C335 C338 115(3) . . ?
C335 C336 C331 123(3) . . ?
C335 C336 H336 118.4 . . ?
C331 C336 H336 118.4 . . ?
F332 C337 F331 108(3) . . ?
F332 C337 F333 109(2) . . ?
F331 C337 F333 107(2) . . ?
F332 C337 C333 113(2) . . ?
F331 C337 C333 108(2) . . ?
F333 C337 C333 112(3) . . ?
F336 C338 F335 112(4) . . ?
F336 C338 F334 105(3) . . ?
F335 C338 F334 109(3) . . ?
F336 C338 C335 113(3) . . ?
F335 C338 C335 112(3) . . ?
F334 C338 C335 105(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O8 2.242(16) . ?
Dy1 O7 2.244(15) . ?
Dy1 O6 2.311(15) . ?
Dy1 O5 2.348(15) . ?
Dy1 O2 2.370(16) . ?
Dy1 O3 2.385(16) . ?
Dy1 O4 2.411(15) . ?
Dy1 O1 2.432(17) . ?
Dy1 Na1 3.910(10) . ?
Na1 F1B 2.30(4) . ?
Na1 F7B 2.35(4) . ?
Na1 F1 2.39(5) . ?
Na1 O3 2.39(2) . ?
Na1 F105 2.392(19) . ?
Na1 F107 2.42(3) . ?
Na1 O1 2.438(18) . ?
Na1 O102 2.441(17) . ?
Na1 F7 2.47(3) . ?
Na1 O103 2.47(2) . ?
Na1 C1B 3.06(4) . ?
Na1 C6 3.118(19) . ?
O1 C2 1.25(3) . ?
O2 C4 1.20(3) . ?
O3 C7 1.26(3) . ?
O4 C9 1.14(3) . ?
O5 C12 1.28(3) . ?
O6 C14 1.33(3) . ?
O7 P1 1.529(16) . ?
O8 P2 1.505(17) . ?
P1 C27 1.78(3) . ?
P1 C21 1.78(2) . ?
P1 C33 1.81(2) . ?
P2 C47 1.78(3) . ?
P2 C53 1.784(18) . ?
P2 C41 1.81(2) . ?
F1 C1 1.35(2) . ?
F2 C1 1.35(2) . ?
F3 C1 1.35(2) . ?
C1 C2 1.54(5) . ?
F1B C1B 1.36(2) . ?
F2B C1B 1.36(2) . ?
F3B C1B 1.35(2) . ?
C1B C2 1.54(5) . ?
C2 C3 1.37(4) . ?
C3 C4 1.39(4) . ?
C3 H3 0.9500 . ?
C4 C5 1.49(4) . ?
C5 F4 1.371(17) . ?
C5 F6 1.371(17) . ?
C5 F5 1.374(18) . ?
C5 F5B 1.377(18) . ?
C5 F4B 1.379(18) . ?
C5 F6B 1.379(18) . ?
F7 C6 1.382(18) . ?
F8 C6 1.390(18) . ?
F9 C6 1.377(18) . ?
F7B C6 1.385(18) . ?
F8B C6 1.387(19) . ?
F9B C6 1.392(18) . ?
C6 C7 1.45(4) . ?
C7 C8 1.44(4) . ?
C8 C9 1.38(4) . ?
C8 H8 0.9500 . ?
C9 C10 1.50(4) . ?
C10 F12 1.31(3) . ?
C10 F11 1.32(3) . ?
C10 F10 1.39(3) . ?
F13 C11 1.33(4) . ?
F14 C11 1.31(3) . ?
F15 C11 1.34(3) . ?
C11 C12 1.50(3) . ?
C12 C13 1.36(3) . ?
C13 C14 1.35(4) . ?
C13 H13 0.9500 . ?
C14 C15 1.52(3) . ?
C15 F18 1.31(4) . ?
C15 F16 1.33(3) . ?
C15 F17 1.33(4) . ?
C21 C22 1.38(4) . ?
C21 C26 1.42(3) . ?
C22 C23 1.37(4) . ?
C22 H22 0.9500 . ?
C23 C24 1.37(4) . ?
C23 H23 0.9500 . ?
C24 C25 1.38(4) . ?
C24 H24 0.9500 . ?
C25 C26 1.35(4) . ?
C25 H25 0.9500 . ?
C26 H26 0.9500 . ?
C27 C32 1.37(3) . ?
C27 C28 1.44(4) . ?
C28 C29 1.32(4) . ?
C28 H28 0.9500 . ?
C29 C30 1.37(4) . ?
C29 H29 0.9500 . ?
C30 C31 1.38(4) . ?
C30 H30 0.9500 . ?
C31 C32 1.42(3) . ?
C31 H31 0.9500 . ?
C32 H32 0.9500 . ?
C41 C46 1.37(3) . ?
C41 C42 1.38(4) . ?
C42 C43 1.41(4) . ?
C42 H42 0.9500 . ?
C43 C44 1.37(5) . ?
C43 H43 0.9500 . ?
C44 C45 1.40(4) . ?
C44 H44 0.9500 . ?
C45 C46 1.40(3) . ?
C45 H45 0.9500 . ?
C46 H46 0.9500 . ?
C47 C52 1.40(4) . ?
C47 C48 1.41(4) . ?
C48 C49 1.36(4) . ?
C48 H48 0.9500 . ?
C49 C50 1.40(4) . ?
C49 H49 0.9500 . ?
C50 C51 1.39(4) . ?
C50 H50 0.9500 . ?
C51 C52 1.37(4) . ?
C51 H51 0.9500 . ?
C52 H52 0.9500 . ?
C33 C38 1.381(16) . ?
C33 C34 1.408(16) . ?
C34 C35 1.391(17) . ?
C34 H34 0.9500 . ?
C35 C36 1.402(17) . ?
C35 C60 1.45(3) . ?
C36 C37 1.381(17) . ?
C36 H36 0.9500 . ?
C37 C38 1.374(16) . ?
C37 H37 0.9500 . ?
C38 C39 1.54(3) . ?
C39 C40 1.54(3) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 C55 1.48(3) . ?
C40 H40A 0.9900 . ?
C40 H40B 0.9900 . ?
C53 C54 1.390(16) . ?
C53 C58 1.395(16) . ?
C54 C55 1.388(16) . ?
C54 H54 0.9500 . ?
C55 C56 1.379(17) . ?
C56 C57 1.397(17) . ?
C57 C58 1.394(17) . ?
C57 H57 0.9500 . ?
C58 C59 1.54(3) . ?
C59 C60 1.55(3) . ?
C59 H59A 0.9900 . ?
C59 H59B 0.9900 . ?
C60 H60A 0.9900 . ?
C60 H60B 0.9900 . ?
Dy2 O108 2.174(19) . ?
Dy2 O107 2.227(18) . ?
Dy2 O106 2.280(19) . ?
Dy2 O105 2.383(17) . ?
Dy2 O104 2.40(2) . ?
Dy2 O101 2.405(16) . ?
Dy2 O103 2.411(17) . ?
Dy2 O102 2.432(16) . ?
O101 C102 1.19(3) . ?
O102 C104 1.24(3) . ?
O103 C107 1.24(3) . ?
O104 C109 1.23(3) . ?
O105 C112 1.19(3) . ?
O106 C114 1.21(3) . ?
O107 P101 1.530(19) . ?
O108 P102 1.566(18) . ?
P101 C121 1.80(4) . ?
P101 C127 1.83(4) . ?
P101 C133 1.90(3) . ?
P102 C153 1.74(3) . ?
P102 C141 1.77(3) . ?
P102 C147 1.776(17) . ?
F101 C101 1.17(4) . ?
F102 C101 1.35(5) . ?
F103 C101 1.25(4) . ?
C101 C102 1.55(4) . ?
C102 C103 1.37(3) . ?
C103 C104 1.37(3) . ?
C103 H103 0.9500 . ?
C104 C105 1.56(4) . ?
C105 F105 1.33(3) . ?
C105 F106 1.33(4) . ?
C105 F104 1.34(4) . ?
F107 C106 1.36(2) . ?
F108 C106 1.36(2) . ?
F109 C106 1.36(2) . ?
C106 C107 1.49(5) . ?
C107 C108 1.32(5) . ?
C108 C109 1.40(4) . ?
C108 H108 0.9500 . ?
C109 C110 1.500(19) . ?
C110 F212 1.36(2) . ?
C110 F110 1.36(2) . ?
C110 F112 1.36(2) . ?
C110 F211 1.36(2) . ?
C110 F111 1.37(2) . ?
C110 F210 1.37(2) . ?
F113 C111 1.38(2) . ?
F114 C111 1.38(2) . ?
F115 C111 1.38(2) . ?
F213 C111 1.38(2) . ?
F214 C111 1.38(2) . ?
F215 C111 1.37(2) . ?
C111 C112 1.503(19) . ?
C112 C113 1.36(4) . ?
C113 C114 1.46(4) . ?
C113 H113 0.9500 . ?
C114 C115 1.513(18) . ?
C115 F116 1.237(16) . ?
C115 F218 1.264(17) . ?
C115 F118 1.270(16) . ?
C115 F216 1.289(17) . ?
C115 F217 1.315(17) . ?
C115 F117 1.338(16) . ?
C121 C122 1.32(6) . ?
C121 C126 1.41(6) . ?
C122 C123 1.42(5) . ?
C122 H122 0.9500 . ?
C123 C124 1.32(6) . ?
C123 H123 0.9500 . ?
C124 C125 1.30(6) . ?
C124 H124 0.9500 . ?
C125 C126 1.43(5) . ?
C125 H125 0.9500 . ?
C126 H126 0.9500 . ?
C127 C128 1.27(5) . ?
C127 C132 1.33(5) . ?
C128 C129 1.47(5) . ?
C128 H128 0.9500 . ?
C129 C130 1.37(5) . ?
C129 H129 0.9500 . ?
C130 C131 1.34(6) . ?
C130 H130 0.9500 . ?
C131 C132 1.43(5) . ?
C131 H131 0.9500 . ?
C132 H132 0.9500 . ?
C141 C146 1.34(4) . ?
C141 C142 1.48(5) . ?
C142 C143 1.41(5) . ?
C142 H142 0.9500 . ?
C143 C144 1.45(7) . ?
C143 H143 0.9500 . ?
C144 C145 1.29(7) . ?
C144 H144 0.9500 . ?
C145 C146 1.40(6) . ?
C145 H145 0.9500 . ?
C146 H146 0.9500 . ?
C147 C148 1.3900 . ?
C147 C152 1.3900 . ?
C148 C149 1.3900 . ?
C148 H148 0.9500 . ?
C149 C150 1.3900 . ?
C149 H149 0.9500 . ?
C150 C151 1.3900 . ?
C150 H150 0.9500 . ?
C151 C152 1.3900 . ?
C151 H151 0.9500 . ?
C152 H152 0.9500 . ?
C133 C134 1.3900 . ?
C133 C138 1.3900 . ?
C134 C135 1.3900 . ?
C134 H134 0.9500 . ?
C135 C136 1.3900 . ?
C135 C160 1.44(3) . ?
C136 C137 1.3900 . ?
C136 H136 0.9500 . ?
C137 C138 1.3900 . ?
C137 H137 0.9500 . ?
C138 C139 1.54(3) . ?
C139 C140 1.51(3) . ?
C139 H13A 0.9900 . ?
C139 H13B 0.9900 . ?
C140 C155 1.48(3) . ?
C140 H14A 0.9900 . ?
C140 H14B 0.9900 . ?
C153 C154 1.3900 . ?
C153 C158 1.3900 . ?
C154 C155 1.3900 . ?
C154 H154 0.9500 . ?
C155 C156 1.3900 . ?
C156 C157 1.3900 . ?
C156 H156 0.9500 . ?
C157 C158 1.3900 . ?
C157 H157 0.9500 . ?
C158 C159 1.54(3) . ?
C159 C160 1.55(3) . ?
C159 H15A 0.9900 . ?
C159 H15B 0.9900 . ?
C160 H16A 0.9900 . ?
C160 H16B 0.9900 . ?
B1 C301 1.62(4) . ?
B1 C311 1.63(5) . ?
B1 C331 1.63(4) . ?
B1 C321 1.65(5) . ?
C301 C302 1.41(4) . ?
C301 C306 1.41(4) . ?
C302 C303 1.50(4) . ?
C302 H302 0.9500 . ?
C303 C304 1.39(4) . ?
C303 C307 1.44(7) . ?
C304 C305 1.39(7) . ?
C304 H304 0.9500 . ?
C305 C306 1.32(7) . ?
C305 C308 1.49(2) . ?
C306 H306 0.9500 . ?
C307 F301 1.32(4) . ?
C307 F303 1.36(5) . ?
C307 F302 1.41(7) . ?
C308 F305 1.38(2) . ?
C308 F304 1.38(2) . ?
C308 F306 1.38(2) . ?
C311 C312 1.34(4) . ?
C311 C316 1.45(5) . ?
C312 C313 1.43(5) . ?
C312 H312 0.9500 . ?
C313 C317 1.39(5) . ?
C313 C314 1.45(5) . ?
C314 C315 1.36(5) . ?
C314 H314 0.9500 . ?
C315 C316 1.34(5) . ?
C315 C318 1.56(5) . ?
C316 H316 0.9500 . ?
C317 F312 1.28(4) . ?
C317 F313 1.30(5) . ?
C317 F311 1.33(5) . ?
C318 F314 1.17(5) . ?
C318 F316 1.35(5) . ?
C318 F315 1.36(5) . ?
C321 C322 1.39(4) . ?
C321 C326 1.41(5) . ?
C322 C323 1.43(4) . ?
C322 H322 0.9500 . ?
C323 C324 1.36(5) . ?
C323 C327 1.44(6) . ?
C324 C325 1.43(4) . ?
C324 C425 1.43(4) . ?
C324 H324 0.9500 . ?
C325 C326 1.43(4) . ?
C325 C328 1.51(2) . ?
C425 C326 1.43(4) . ?
C425 C428 1.51(2) . ?
C326 H326 0.9500 . ?
C327 F322 1.31(6) . ?
C327 F321 1.35(4) . ?
C327 F323 1.39(5) . ?
C328 F325 1.29(2) . ?
C328 F326 1.29(2) . ?
C328 F324 1.29(2) . ?
C428 F425 1.30(2) . ?
C428 F424 1.30(2) . ?
C428 F426 1.30(2) . ?
C331 C336 1.37(4) . ?
C331 C332 1.41(4) . ?
C332 C333 1.37(4) . ?
C332 H332 0.9500 . ?
C333 C334 1.42(4) . ?
C333 C337 1.50(4) . ?
C334 C335 1.36(4) . ?
C334 H334 0.9500 . ?
C335 C336 1.37(3) . ?
C335 C338 1.59(5) . ?
C336 H336 0.9500 . ?
C337 F332 1.28(3) . ?
C337 F331 1.33(3) . ?
C337 F333 1.34(3) . ?
C338 F336 1.25(4) . ?
C338 F335 1.25(4) . ?
C338 F334 1.39(5) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy1 O7 P1 C27 -46(3) . . . . ?
Dy1 O7 P1 C21 -161(2) . . . . ?
Dy1 O7 P1 C33 73(2) . . . . ?
Dy1 O8 P2 C47 -169(5) . . . . ?
Dy1 O8 P2 C53 64(5) . . . . ?
Dy1 O8 P2 C41 -53(5) . . . . ?
Na1 F1 C1 F3 159(3) . . . . ?
Na1 F1 C1 F2 -90(4) . . . . ?
Na1 F1 C1 C2 37(3) . . . . ?
Na1 F1B C1B F3B 167(2) . . . . ?
Na1 F1B C1B F2B -82(3) . . . . ?
Na1 F1B C1B C2 41(3) . . . . ?
Dy1 O1 C2 C3 -19(5) . . . . ?
Na1 O1 C2 C3 -175(3) . . . . ?
Dy1 O1 C2 C1 -173(2) . . . . ?
Na1 O1 C2 C1 31(4) . . . . ?
Dy1 O1 C2 C1B 158.1(19) . . . . ?
Na1 O1 C2 C1B 2(3) . . . . ?
F3 C1 C2 O1 -158(3) . . . . ?
F2 C1 C2 O1 75(4) . . . . ?
F1 C1 C2 O1 -43(3) . . . . ?
F3 C1 C2 C3 43(4) . . . . ?
F2 C1 C2 C3 -83(3) . . . . ?
F1 C1 C2 C3 159(3) . . . . ?
F3B C1B C2 O1 -152(2) . . . . ?
F1B C1B C2 O1 -29(3) . . . . ?
F2B C1B C2 O1 91(3) . . . . ?
Na1 C1B C2 O1 -2(2) . . . . ?
F3B C1B C2 C3 25(4) . . . . ?
F1B C1B C2 C3 148(3) . . . . ?
F2B C1B C2 C3 -91(3) . . . . ?
Na1 C1B C2 C3 176(3) . . . . ?
O1 C2 C3 C4 3(6) . . . . ?
C1 C2 C3 C4 157(3) . . . . ?
C1B C2 C3 C4 -174(3) . . . . ?
Dy1 O2 C4 C3 15(4) . . . . ?
Dy1 O2 C4 C5 -165.5(14) . . . . ?
C2 C3 C4 O2 0(5) . . . . ?
C2 C3 C4 C5 -179(3) . . . . ?
O2 C4 C5 F4 -170(2) . . . . ?
C3 C4 C5 F4 9(3) . . . . ?
O2 C4 C5 F6 68(3) . . . . ?
C3 C4 C5 F6 -113(3) . . . . ?
O2 C4 C5 F5 -48(3) . . . . ?
C3 C4 C5 F5 131(3) . . . . ?
O2 C4 C5 F5B -11(4) . . . . ?
C3 C4 C5 F5B 168(3) . . . . ?
O2 C4 C5 F4B -137(3) . . . . ?
C3 C4 C5 F4B 42(4) . . . . ?
O2 C4 C5 F6B 105(3) . . . . ?
C3 C4 C5 F6B -76(3) . . . . ?
Na1 F7 C6 F9 -177.5(16) . . . . ?
Na1 F7 C6 F8 -75(2) . . . . ?
Na1 F7 C6 C7 46(2) . . . . ?
Na1 F7B C6 F8B -132(3) . . . . ?
Na1 F7B C6 F9B 127(3) . . . . ?
Na1 F7B C6 C7 12(3) . . . . ?
Dy1 O3 C7 C8 20(4) . . . . ?
Na1 O3 C7 C8 -172(2) . . . . ?
Dy1 O3 C7 C6 -160.7(14) . . . . ?
Na1 O3 C7 C6 7(3) . . . . ?
F9 C6 C7 O3 -165.3(18) . . . . ?
F7 C6 C7 O3 -39(3) . . . . ?
F7B C6 C7 O3 -14(4) . . . . ?
F8B C6 C7 O3 122(3) . . . . ?
F8 C6 C7 O3 76(2) . . . . ?
F9B C6 C7 O3 -126(3) . . . . ?
Na1 C6 C7 O3 -5.0(19) . . . . ?
F9 C6 C7 C8 14(3) . . . . ?
F7 C6 C7 C8 141(2) . . . . ?
F7B C6 C7 C8 166(3) . . . . ?
F8B C6 C7 C8 -59(3) . . . . ?
F8 C6 C7 C8 -105(2) . . . . ?
F9B C6 C7 C8 54(3) . . . . ?
Na1 C6 C7 C8 174(2) . . . . ?
O3 C7 C8 C9 -4(4) . . . . ?
C6 C7 C8 C9 177(2) . . . . ?
Dy1 O4 C9 C8 -26(4) . . . . ?
Dy1 O4 C9 C10 159.5(17) . . . . ?
C7 C8 C9 O4 7(5) . . . . ?
C7 C8 C9 C10 -178(2) . . . . ?
O4 C9 C10 F12 17(4) . . . . ?
C8 C9 C10 F12 -159(2) . . . . ?
O4 C9 C10 F11 144(3) . . . . ?
C8 C9 C10 F11 -31(3) . . . . ?
O4 C9 C10 F10 -99(3) . . . . ?
C8 C9 C10 F10 85(3) . . . . ?
Dy1 O5 C12 C13 4(4) . . . . ?
Dy1 O5 C12 C11 -174(2) . . . . ?
F14 C11 C12 O5 59(4) . . . . ?
F13 C11 C12 O5 -63(3) . . . . ?
F15 C11 C12 O5 -177(2) . . . . ?
F14 C11 C12 C13 -118(3) . . . . ?
F13 C11 C12 C13 120(3) . . . . ?
F15 C11 C12 C13 5(4) . . . . ?
O5 C12 C13 C14 -3(5) . . . . ?
C11 C12 C13 C14 174(3) . . . . ?
Dy1 O6 C14 C13 -1(4) . . . . ?
Dy1 O6 C14 C15 178.8(18) . . . . ?
C12 C13 C14 O6 2(5) . . . . ?
C12 C13 C14 C15 -178(3) . . . . ?
O6 C14 C15 F18 51(3) . . . . ?
C13 C14 C15 F18 -129(3) . . . . ?
O6 C14 C15 F16 176(3) . . . . ?
C13 C14 C15 F16 -4(4) . . . . ?
O6 C14 C15 F17 -69(3) . . . . ?
C13 C14 C15 F17 111(3) . . . . ?
O7 P1 C21 C22 -8(2) . . . . ?
C27 P1 C21 C22 -126(2) . . . . ?
C33 P1 C21 C22 119(2) . . . . ?
O7 P1 C21 C26 174(2) . . . . ?
C27 P1 C21 C26 56(2) . . . . ?
C33 P1 C21 C26 -59(2) . . . . ?
C26 C21 C22 C23 -5(4) . . . . ?
P1 C21 C22 C23 177(2) . . . . ?
C21 C22 C23 C24 8(4) . . . . ?
C22 C23 C24 C25 -9(5) . . . . ?
C23 C24 C25 C26 7(6) . . . . ?
C24 C25 C26 C21 -4(5) . . . . ?
C22 C21 C26 C25 3(4) . . . . ?
P1 C21 C26 C25 -179(3) . . . . ?
O7 P1 C27 C32 126.3(19) . . . . ?
C21 P1 C27 C32 -116(2) . . . . ?
C33 P1 C27 C32 3(2) . . . . ?
O7 P1 C27 C28 -55(2) . . . . ?
C21 P1 C27 C28 63(2) . . . . ?
C33 P1 C27 C28 -177.9(18) . . . . ?
C32 C27 C28 C29 -6(4) . . . . ?
P1 C27 C28 C29 176(2) . . . . ?
C27 C28 C29 C30 1(5) . . . . ?
C28 C29 C30 C31 4(4) . . . . ?
C29 C30 C31 C32 -3(4) . . . . ?
C28 C27 C32 C31 6(3) . . . . ?
P1 C27 C32 C31 -175.0(18) . . . . ?
C30 C31 C32 C27 -2(4) . . . . ?
O8 P2 C41 C46 139(2) . . . . ?
C47 P2 C41 C46 -103(2) . . . . ?
C53 P2 C41 C46 17(3) . . . . ?
O8 P2 C41 C42 -37(2) . . . . ?
C47 P2 C41 C42 81(2) . . . . ?
C53 P2 C41 C42 -159(2) . . . . ?
C46 C41 C42 C43 4(5) . . . . ?
P2 C41 C42 C43 180(3) . . . . ?
C41 C42 C43 C44 -3(5) . . . . ?
C42 C43 C44 C45 1(6) . . . . ?
C43 C44 C45 C46 -2(5) . . . . ?
C42 C41 C46 C45 -5(5) . . . . ?
P2 C41 C46 C45 -180(2) . . . . ?
C44 C45 C46 C41 3(5) . . . . ?
O8 P2 C47 C52 -17(3) . . . . ?
C53 P2 C47 C52 109(3) . . . . ?
C41 P2 C47 C52 -138(2) . . . . ?
O8 P2 C47 C48 167(2) . . . . ?
C53 P2 C47 C48 -67(2) . . . . ?
C41 P2 C47 C48 47(2) . . . . ?
C52 C47 C48 C49 4(4) . . . . ?
P2 C47 C48 C49 179(2) . . . . ?
C47 C48 C49 C50 0(5) . . . . ?
C48 C49 C50 C51 0(5) . . . . ?
C49 C50 C51 C52 -2(6) . . . . ?
C50 C51 C52 C47 5(6) . . . . ?
C48 C47 C52 C51 -6(5) . . . . ?
P2 C47 C52 C51 178(3) . . . . ?
O7 P1 C33 C38 118(2) . . . . ?
C27 P1 C33 C38 -122(2) . . . . ?
C21 P1 C33 C38 -7(2) . . . . ?
O7 P1 C33 C34 -66.5(18) . . . . ?
C27 P1 C33 C34 53.7(18) . . . . ?
C21 P1 C33 C34 168.9(16) . . . . ?
C38 C33 C34 C35 2(3) . . . . ?
P1 C33 C34 C35 -174.2(17) . . . . ?
C33 C34 C35 C36 9(3) . . . . ?
C33 C34 C35 C60 -153(2) . . . . ?
C34 C35 C36 C37 -9(3) . . . . ?
C60 C35 C36 C37 153(2) . . . . ?
C35 C36 C37 C38 -1(3) . . . . ?
C36 C37 C38 C33 12(3) . . . . ?
C36 C37 C38 C39 -146(2) . . . . ?
C34 C33 C38 C37 -13(3) . . . . ?
P1 C33 C38 C37 163.0(17) . . . . ?
C34 C33 C38 C39 144(2) . . . . ?
P1 C33 C38 C39 -40(3) . . . . ?
C37 C38 C39 C40 89(3) . . . . ?
C33 C38 C39 C40 -69(3) . . . . ?
C38 C39 C40 C55 -21(3) . . . . ?
O8 P2 C53 C54 -45.7(18) . . . . ?
C47 P2 C53 C54 -169.7(15) . . . . ?
C41 P2 C53 C54 75.8(18) . . . . ?
O8 P2 C53 C58 136(2) . . . . ?
C47 P2 C53 C58 12(2) . . . . ?
C41 P2 C53 C58 -103(2) . . . . ?
C58 C53 C54 C55 7(3) . . . . ?
P2 C53 C54 C55 -171.8(17) . . . . ?
C53 C54 C55 C56 7(3) . . . . ?
C53 C54 C55 C40 -153(2) . . . . ?
C39 C40 C55 C56 -67(3) . . . . ?
C39 C40 C55 C54 93(3) . . . . ?
C54 C55 C56 C57 -10(4) . . . . ?
C40 C55 C56 C57 151(2) . . . . ?
C55 C56 C57 C58 -2(4) . . . . ?
C56 C57 C58 C53 16(3) . . . . ?
C56 C57 C58 C59 -147(2) . . . . ?
C54 C53 C58 C57 -18(3) . . . . ?
P2 C53 C58 C57 160.6(18) . . . . ?
C54 C53 C58 C59 143(2) . . . . ?
P2 C53 C58 C59 -38(3) . . . . ?
C57 C58 C59 C60 99(2) . . . . ?
C53 C58 C59 C60 -62(3) . . . . ?
C34 C35 C60 C59 104(3) . . . . ?
C36 C35 C60 C59 -58(3) . . . . ?
C58 C59 C60 C35 -27(3) . . . . ?
Dy2 O108 P102 C153 -8(5) . . . . ?
Dy2 O108 P102 C141 110(4) . . . . ?
Dy2 O108 P102 C147 -133(4) . . . . ?
Dy2 O101 C102 C103 -10(6) . . . . ?
Dy2 O101 C102 C101 163(2) . . . . ?
F101 C101 C102 O101 -30(6) . . . . ?
F103 C101 C102 O101 -170(4) . . . . ?
F102 C101 C102 O101 80(4) . . . . ?
F101 C101 C102 C103 144(5) . . . . ?
F103 C101 C102 C103 4(6) . . . . ?
F102 C101 C102 C103 -107(4) . . . . ?
O101 C102 C103 C104 -3(5) . . . . ?
C101 C102 C103 C104 -176(3) . . . . ?
Dy2 O102 C104 C103 4(4) . . . . ?
Na1 O102 C104 C103 170(2) . . . . ?
Dy2 O102 C104 C105 177.4(18) . . . . ?
Na1 O102 C104 C105 -16(3) . . . . ?
C102 C103 C104 O102 6(5) . . . . ?
C102 C103 C104 C105 -167(3) . . . . ?
O102 C104 C105 F105 41(4) . . . . ?
C103 C104 C105 F105 -145(3) . . . . ?
O102 C104 C105 F106 161(2) . . . . ?
C103 C104 C105 F106 -24(4) . . . . ?
O102 C104 C105 F104 -82(3) . . . . ?
C103 C104 C105 F104 93(3) . . . . ?
F106 C105 F105 Na1 -169.8(18) . . . . ?
F104 C105 F105 Na1 76(3) . . . . ?
C104 C105 F105 Na1 -45(4) . . . . ?
Na1 F107 C106 F108 132(2) . . . . ?
Na1 F107 C106 F109 -123(2) . . . . ?
Na1 F107 C106 C107 -3(3) . . . . ?
Dy2 O103 C107 C108 -13(7) . . . . ?
Na1 O103 C107 C108 172(4) . . . . ?
Dy2 O103 C107 C106 157(2) . . . . ?
Na1 O103 C107 C106 -18(5) . . . . ?
F107 C106 C107 O103 14(5) . . . . ?
F108 C106 C107 O103 -111(3) . . . . ?
F109 C106 C107 O103 129(3) . . . . ?
F107 C106 C107 C108 -175(3) . . . . ?
F108 C106 C107 C108 61(4) . . . . ?
F109 C106 C107 C108 -59(4) . . . . ?
O103 C107 C108 C109 -8(8) . . . . ?
C106 C107 C108 C109 -178(3) . . . . ?
Dy2 O104 C109 C108 9(6) . . . . ?
Dy2 O104 C109 C110 -164.4(16) . . . . ?
C107 C108 C109 O104 10(7) . . . . ?
C107 C108 C109 C110 -177(4) . . . . ?
O104 C109 C110 F212 -2(3) . . . . ?
C108 C109 C110 F212 -175(4) . . . . ?
O104 C109 C110 F110 -163(3) . . . . ?
C108 C109 C110 F110 23(4) . . . . ?
O104 C109 C110 F112 76(3) . . . . ?
C108 C109 C110 F112 -97(4) . . . . ?
O104 C109 C110 F211 -123(3) . . . . ?
C108 C109 C110 F211 64(4) . . . . ?
O104 C109 C110 F111 -43(3) . . . . ?
C108 C109 C110 F111 143(4) . . . . ?
O104 C109 C110 F210 118(3) . . . . ?
C108 C109 C110 F210 -56(4) . . . . ?
Dy2 O105 C112 C113 -6(8) . . . . ?
Dy2 O105 C112 C111 178.7(19) . . . . ?
F215 C111 C112 O105 173(4) . . . . ?
F214 C111 C112 O105 48(5) . . . . ?
F213 C111 C112 O105 -69(5) . . . . ?
F113 C111 C112 O105 -115(4) . . . . ?
F114 C111 C112 O105 6(5) . . . . ?
F115 C111 C112 O105 127(4) . . . . ?
F215 C111 C112 C113 -3(6) . . . . ?
F214 C111 C112 C113 -128(5) . . . . ?
F213 C111 C112 C113 115(5) . . . . ?
F113 C111 C112 C113 69(5) . . . . ?
F114 C111 C112 C113 -170(4) . . . . ?
F115 C111 C112 C113 -49(5) . . . . ?
O105 C112 C113 C114 1(7) . . . . ?
C111 C112 C113 C114 176(3) . . . . ?
Dy2 O106 C114 C113 -27(5) . . . . ?
Dy2 O106 C114 C115 170.8(16) . . . . ?
C112 C113 C114 O106 14(6) . . . . ?
C112 C113 C114 C115 177(3) . . . . ?
O106 C114 C115 F116 83(3) . . . . ?
C113 C114 C115 F116 -80(3) . . . . ?
O106 C114 C115 F218 -93(4) . . . . ?
C113 C114 C115 F218 104(4) . . . . ?
O106 C114 C115 F118 -147(3) . . . . ?
C113 C114 C115 F118 49(3) . . . . ?
O106 C114 C115 F216 32(4) . . . . ?
C113 C114 C115 F216 -132(4) . . . . ?
O106 C114 C115 F217 148(4) . . . . ?
C113 C114 C115 F217 -16(4) . . . . ?
O106 C114 C115 F117 -34(3) . . . . ?
C113 C114 C115 F117 163(3) . . . . ?
O107 P101 C121 C122 -6(5) . . . . ?
C127 P101 C121 C122 111(4) . . . . ?
C133 P101 C121 C122 -136(4) . . . . ?
O107 P101 C121 C126 -178(3) . . . . ?
C127 P101 C121 C126 -61(4) . . . . ?
C133 P101 C121 C126 52(4) . . . . ?
C126 C121 C122 C123 -1(7) . . . . ?
P101 C121 C122 C123 -173(3) . . . . ?
C121 C122 C123 C124 -4(7) . . . . ?
C122 C123 C124 C125 8(8) . . . . ?
C123 C124 C125 C126 -7(8) . . . . ?
C122 C121 C126 C125 3(7) . . . . ?
P101 C121 C126 C125 175(3) . . . . ?
C124 C125 C126 C121 1(7) . . . . ?
O107 P101 C127 C128 9(6) . . . . ?
C121 P101 C127 C128 -109(5) . . . . ?
C133 P101 C127 C128 130(5) . . . . ?
O107 P101 C127 C132 -171(4) . . . . ?
C121 P101 C127 C132 71(5) . . . . ?
C133 P101 C127 C132 -50(5) . . . . ?
C132 C127 C128 C129 -1(9) . . . . ?
P101 C127 C128 C129 179(4) . . . . ?
C127 C128 C129 C130 4(9) . . . . ?
C128 C129 C130 C131 3(8) . . . . ?
C129 C130 C131 C132 -11(9) . . . . ?
C128 C127 C132 C131 -7(9) . . . . ?
P101 C127 C132 C131 173(4) . . . . ?
C130 C131 C132 C127 14(9) . . . . ?
O108 P102 C141 C146 -169(3) . . . . ?
C153 P102 C141 C146 -46(4) . . . . ?
C147 P102 C141 C146 71(3) . . . . ?
O108 P102 C141 C142 7(3) . . . . ?
C153 P102 C141 C142 130(3) . . . . ?
C147 P102 C141 C142 -112(3) . . . . ?
C146 C141 C142 C143 1(7) . . . . ?
P102 C141 C142 C143 -175(4) . . . . ?
C141 C142 C143 C144 -3(8) . . . . ?
C142 C143 C144 C145 1(9) . . . . ?
C143 C144 C145 C146 3(10) . . . . ?
C142 C141 C146 C145 2(6) . . . . ?
P102 C141 C146 C145 178(4) . . . . ?
C144 C145 C146 C141 -4(9) . . . . ?
O108 P102 C147 C148 -15(2) . . . . ?
C153 P102 C147 C148 -142(2) . . . . ?
C141 P102 C147 C148 105(2) . . . . ?
O108 P102 C147 C152 167.4(17) . . . . ?
C153 P102 C147 C152 40(3) . . . . ?
C141 P102 C147 C152 -73(2) . . . . ?
C152 C147 C148 C149 0.0 . . . . ?
P102 C147 C148 C149 -178(3) . . . . ?
C147 C148 C149 C150 0.0 . . . . ?
C148 C149 C150 C151 0.0 . . . . ?
C149 C150 C151 C152 0.0 . . . . ?
C150 C151 C152 C147 0.0 . . . . ?
C148 C147 C152 C151 0.0 . . . . ?
P102 C147 C152 C151 178(3) . . . . ?
O107 P101 C133 C134 51(2) . . . . ?
C121 P101 C133 C134 179(2) . . . . ?
C127 P101 C133 C134 -67(2) . . . . ?
O107 P101 C133 C138 -143(2) . . . . ?
C121 P101 C133 C138 -16(3) . . . . ?
C127 P101 C133 C138 99(3) . . . . ?
C138 C133 C134 C135 0.0 . . . . ?
P101 C133 C134 C135 167(3) . . . . ?
C133 C134 C135 C136 0.0 . . . . ?
C133 C134 C135 C160 153(3) . . . . ?
C134 C135 C136 C137 0.0 . . . . ?
C160 C135 C136 C137 -154(3) . . . . ?
C135 C136 C137 C138 0.0 . . . . ?
C136 C137 C138 C133 0.0 . . . . ?
C136 C137 C138 C139 142(3) . . . . ?
C134 C133 C138 C137 0.0 . . . . ?
P101 C133 C138 C137 -164(3) . . . . ?
C134 C133 C138 C139 -138(3) . . . . ?
P101 C133 C138 C139 58(4) . . . . ?
C137 C138 C139 C140 -83(4) . . . . ?
C133 C138 C139 C140 59(5) . . . . ?
C138 C139 C140 C155 21(7) . . . . ?
O108 P102 C153 C154 70.4(18) . . . . ?
C141 P102 C153 C154 -50(2) . . . . ?
C147 P102 C153 C154 -163.5(17) . . . . ?
O108 P102 C153 C158 -135(2) . . . . ?
C141 P102 C153 C158 104(2) . . . . ?
C147 P102 C153 C158 -9(3) . . . . ?
C158 C153 C154 C155 0.0 . . . . ?
P102 C153 C154 C155 156(3) . . . . ?
C153 C154 C155 C156 0.0 . . . . ?
C153 C154 C155 C140 136(3) . . . . ?
C139 C140 C155 C156 51(5) . . . . ?
C139 C140 C155 C154 -88(5) . . . . ?
C154 C155 C156 C157 0.0 . . . . ?
C140 C155 C156 C157 -137(3) . . . . ?
C155 C156 C157 C158 0.0 . . . . ?
C156 C157 C158 C153 0.0 . . . . ?
C156 C157 C158 C159 155(3) . . . . ?
C154 C153 C158 C157 0.0 . . . . ?
P102 C153 C158 C157 -151(3) . . . . ?
C154 C153 C158 C159 -154(3) . . . . ?
P102 C153 C158 C159 55(3) . . . . ?
C157 C158 C159 C160 -66(4) . . . . ?
C153 C158 C159 C160 89(4) . . . . ?
C134 C135 C160 C159 -70(5) . . . . ?
C136 C135 C160 C159 84(4) . . . . ?
C158 C159 C160 C135 -9(5) . . . . ?
C311 B1 C301 C302 50(4) . . . . ?
C331 B1 C301 C302 -75(3) . . . . ?
C321 B1 C301 C302 166(3) . . . . ?
C311 B1 C301 C306 -138(3) . . . . ?
C331 B1 C301 C306 97(3) . . . . ?
C321 B1 C301 C306 -22(4) . . . . ?
C306 C301 C302 C303 1(4) . . . . ?
B1 C301 C302 C303 174(3) . . . . ?
C301 C302 C303 C304 0(5) . . . . ?
C301 C302 C303 C307 176(3) . . . . ?
C307 C303 C304 C305 -174(4) . . . . ?
C302 C303 C304 C305 1(5) . . . . ?
C303 C304 C305 C306 -6(9) . . . . ?
C303 C304 C305 C308 -171(3) . . . . ?
C304 C305 C306 C301 8(10) . . . . ?
C308 C305 C306 C301 172(3) . . . . ?
C302 C301 C306 C305 -5(5) . . . . ?
B1 C301 C306 C305 -177(4) . . . . ?
C304 C303 C307 F301 -19(6) . . . . ?
C302 C303 C307 F301 164(4) . . . . ?
C304 C303 C307 F303 107(4) . . . . ?
C302 C303 C307 F303 -69(6) . . . . ?
C304 C303 C307 F302 -137(3) . . . . ?
C302 C303 C307 F302 47(4) . . . . ?
C306 C305 C308 F305 29(6) . . . . ?
C304 C305 C308 F305 -163(3) . . . . ?
C306 C305 C308 F304 147(4) . . . . ?
C304 C305 C308 F304 -45(5) . . . . ?
C306 C305 C308 F306 -92(5) . . . . ?
C304 C305 C308 F306 76(5) . . . . ?
C301 B1 C311 C312 -173(3) . . . . ?
C331 B1 C311 C312 -53(5) . . . . ?
C321 B1 C311 C312 68(4) . . . . ?
C301 B1 C311 C316 16(5) . . . . ?
C331 B1 C311 C316 136(4) . . . . ?
C321 B1 C311 C316 -103(4) . . . . ?
C316 C311 C312 C313 -10(7) . . . . ?
B1 C311 C312 C313 179(4) . . . . ?
C311 C312 C313 C317 -180(5) . . . . ?
C311 C312 C313 C314 8(6) . . . . ?
C317 C313 C314 C315 -176(5) . . . . ?
C312 C313 C314 C315 -4(6) . . . . ?
C313 C314 C315 C316 2(8) . . . . ?
C313 C314 C315 C318 -179(4) . . . . ?
C314 C315 C316 C311 -3(7) . . . . ?
C318 C315 C316 C311 178(4) . . . . ?
C312 C311 C316 C315 7(6) . . . . ?
B1 C311 C316 C315 178(4) . . . . ?
C312 C313 C317 F312 -142(5) . . . . ?
C314 C313 C317 F312 29(8) . . . . ?
C312 C313 C317 F313 93(6) . . . . ?
C314 C313 C317 F313 -96(5) . . . . ?
C312 C313 C317 F311 -20(7) . . . . ?
C314 C313 C317 F311 151(4) . . . . ?
C316 C315 C318 F314 -32(7) . . . . ?
C314 C315 C318 F314 148(5) . . . . ?
C316 C315 C318 F316 -158(4) . . . . ?
C314 C315 C318 F316 23(7) . . . . ?
C316 C315 C318 F315 99(5) . . . . ?
C314 C315 C318 F315 -80(6) . . . . ?
C301 B1 C321 C322 137(3) . . . . ?
C311 B1 C321 C322 -98(4) . . . . ?
C331 B1 C321 C322 23(4) . . . . ?
C301 B1 C321 C326 -44(5) . . . . ?
C311 B1 C321 C326 80(4) . . . . ?
C331 B1 C321 C326 -158(4) . . . . ?
C326 C321 C322 C323 0(5) . . . . ?
B1 C321 C322 C323 178(3) . . . . ?
C321 C322 C323 C324 -5(7) . . . . ?
C321 C322 C323 C327 175(4) . . . . ?
C322 C323 C324 C325 23(9) . . . . ?
C327 C323 C324 C325 -157(7) . . . . ?
C322 C323 C324 C425 4(16) . . . . ?
C327 C323 C324 C425 -177(14) . . . . ?
C323 C324 C325 C326 -32(11) . . . . ?
C323 C324 C325 C328 -175(7) . . . . ?
C323 C324 C425 C326 3(24) . . . . ?
C323 C324 C425 C428 -177(12) . . . . ?
C322 C321 C326 C325 -13(9) . . . . ?
B1 C321 C326 C325 168(7) . . . . ?
C322 C321 C326 C425 8(16) . . . . ?
B1 C321 C326 C425 -170(15) . . . . ?
C324 C325 C326 C321 29(12) . . . . ?
C328 C325 C326 C321 172(7) . . . . ?
C324 C425 C326 C321 -9(27) . . . . ?
C428 C425 C326 C321 170(15) . . . . ?
C324 C323 C327 F322 89(7) . . . . ?
C322 C323 C327 F322 -91(5) . . . . ?
C324 C323 C327 F321 -145(5) . . . . ?
C322 C323 C327 F321 34(7) . . . . ?
C324 C323 C327 F323 -34(7) . . . . ?
C322 C323 C327 F323 146(3) . . . . ?
C324 C325 C328 F325 -151(8) . . . . ?
C326 C325 C328 F325 69(10) . . . . ?
C324 C325 C328 F326 86(8) . . . . ?
C326 C325 C328 F326 -54(10) . . . . ?
C324 C325 C328 F324 -34(10) . . . . ?
C326 C325 C328 F324 -173(8) . . . . ?
C324 C425 C428 F425 172(16) . . . . ?
C326 C425 C428 F425 -7(28) . . . . ?
C324 C425 C428 F424 -70(21) . . . . ?
C326 C425 C428 F424 111(23) . . . . ?
C324 C425 C428 F426 50(23) . . . . ?
C326 C425 C428 F426 -129(21) . . . . ?
C301 B1 C331 C336 -75(4) . . . . ?
C311 B1 C331 C336 158(3) . . . . ?
C321 B1 C331 C336 42(4) . . . . ?
C301 B1 C331 C332 104(3) . . . . ?
C311 B1 C331 C332 -24(4) . . . . ?
C321 B1 C331 C332 -139(3) . . . . ?
C336 C331 C332 C333 4(4) . . . . ?
B1 C331 C332 C333 -174(3) . . . . ?
C331 C332 C333 C334 -8(5) . . . . ?
C331 C332 C333 C337 -179(3) . . . . ?
C332 C333 C334 C335 6(4) . . . . ?
C337 C333 C334 C335 177(3) . . . . ?
C333 C334 C335 C336 -1(5) . . . . ?
C333 C334 C335 C338 176(3) . . . . ?
C334 C335 C336 C331 -3(5) . . . . ?
C338 C335 C336 C331 -180(3) . . . . ?
C332 C331 C336 C335 1(4) . . . . ?
B1 C331 C336 C335 179(3) . . . . ?
C332 C333 C337 F332 48(4) . . . . ?
C334 C333 C337 F332 -124(3) . . . . ?
C332 C333 C337 F331 -71(3) . . . . ?
C334 C333 C337 F331 117(3) . . . . ?
C332 C333 C337 F333 172(3) . . . . ?
C334 C333 C337 F333 0(4) . . . . ?
C334 C335 C338 F336 140(4) . . . . ?
C336 C335 C338 F336 -43(5) . . . . ?
C334 C335 C338 F335 -92(5) . . . . ?
C336 C335 C338 F335 85(4) . . . . ?
C334 C335 C338 F334 27(4) . . . . ?
C336 C335 C338 F334 -156(3) . . . . ?
