#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:16:52 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180775 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010608.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010608_Fobs loop_ _publ_author_name 'Hoch, Constantin' 'R\"ohr, Caroline' _publ_section_title ; Rubidium stannate(IV), Rb~4~SnO~4~ ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 136 _journal_page_last 137 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.720 _cell_angle_beta 79.480 _cell_angle_gamma 66.640 _cell_length_a 6.7730 _cell_length_b 6.7760 _cell_length_c 10.1220 _exptl_crystal_F_000 460.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file br1266Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Rb4SnO4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 277.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 72894.66 81177.66 578.27 o 3 0 0 172.95 183.84 23.97 o 4 0 0 33486.45 37110.39 508.68 o 5 0 0 943.84 1001.51 44.72 o 6 0 0 8284.74 9183.66 239.85 o 7 0 0 956.93 1059.25 69.59 o -6 1 0 1159.21 1166.63 68.35 o -5 1 0 2396.02 2369.54 75.29 o -4 1 0 1561.11 1472.27 52.25 o -3 1 0 2764.88 2612.82 73.11 o -2 1 0 461.54 18.89 172.65 o -1 1 0 3126.06 2815.33 81.22 o 2 1 0 550.68 629.34 18.59 o 3 1 0 1625.22 1874.35 52.63 o 4 1 0 5277.99 5692.90 133.74 o 5 1 0 783.19 895.11 39.75 o 6 1 0 3795.25 4268.42 140.23 o 7 1 0 853.75 898.59 63.94 o -6 2 0 440.46 602.89 108.04 o -5 2 0 69.98 86.90 366.85 o -4 2 0 1419.87 1123.62 88.99 o -3 2 0 150.06 116.53 48.40 o -2 2 0 2146.41 1914.19 61.02 o -1 2 0 35.37 -123.89 82.60 o 0 2 0 457.00 435.01 14.05 o 1 2 0 23.36 0.00 58.78 o 2 2 0 2034.15 2548.60 73.45 o 3 2 0 146.19 200.73 22.33 o 4 2 0 1041.38 1174.93 32.69 o 5 2 0 247.72 275.61 35.62 o 6 2 0 1302.78 1429.63 53.57 o 7 2 0 77.07 44.96 53.58 o -5 3 0 6448.82 4713.47 147.95 o -4 3 0 725.11 645.87 71.96 o -3 3 0 8979.20 8479.40 245.39 o -2 3 0 3518.85 3665.04 118.02 o -1 3 0 7435.08 8421.72 236.33 o 0 3 0 6013.20 7057.94 265.49 o 1 3 0 1902.44 2297.56 66.94 o 2 3 0 9740.94 11979.65 231.65 o 3 3 0 99.78 8.49 81.05 o 4 3 0 5050.48 5841.46 144.46 o 5 3 0 1422.52 1460.49 44.62 o 6 3 0 3835.39 4245.30 115.06 o 7 3 0 1277.88 1247.93 62.60 o -4 4 0 76.44 58.44 73.70 o -3 4 0 1074.23 1041.87 67.80 o -2 4 0 847.15 964.22 52.39 o -1 4 0 2565.94 2840.62 72.70 o 0 4 0 596.89 667.91 25.90 o 1 4 0 10105.29 10874.99 265.53 o 2 4 0 1307.53 1394.62 41.96 o 3 4 0 10303.33 11248.67 271.36 o 4 4 0 844.36 847.24 38.26 o 5 4 0 5605.39 5590.97 170.36 o 6 4 0 216.31 23.96 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