#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:28:50 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180785 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/16/2011697.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011697_Fobs loop_ _publ_author_name 'Parvez, Masood' 'Yadav, Veejendra K.' 'Senthil, Govindaraji' _publ_section_title ; Some Diels--Alder adducts of 6-vinyl-1-oxa-4-thiaspiro[4.5]dec-6-ene ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 82 _journal_page_last 85 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.944 _cell_angle_gamma 90.000 _cell_length_a 13.2577 _cell_length_b 7.3897 _cell_length_c 14.2874 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.8392 _cod_data_source_file da1148IIIasup3.hkl _cod_data_source_block IIIa #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound-IIIa ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4208.25 4152.96 52.80 o 3 0 0 640.77 599.52 20.14 o 4 0 0 9966.53 9772.92 121.12 o 5 0 0 4334.71 4698.35 73.60 o 6 0 0 383.58 329.92 26.57 o 7 0 0 583.31 620.06 31.09 o 8 0 0 1355.22 1311.60 47.61 o 9 0 0 148.58 80.37 16.56 o 10 0 0 99.03 114.18 15.13 o 11 0 0 229.30 225.40 21.15 o 12 0 0 192.04 219.35 19.08 o 13 0 0 0.92 -36.99 36.99 o 14 0 0 765.34 748.91 53.57 o 15 0 0 4.32 77.32 42.55 o 1 1 0 6421.42 6006.02 71.98 o 2 1 0 146.18 141.71 13.58 o 3 1 0 453.15 423.44 19.59 o 4 1 0 140.93 142.31 12.35 o 5 1 0 777.93 891.13 29.38 o 6 1 0 1191.08 1233.18 37.26 o 7 1 0 837.37 863.36 35.34 o 8 1 0 274.67 213.43 19.63 o 9 1 0 185.98 176.86 15.29 o 10 1 0 118.15 81.71 15.13 o 11 1 0 258.42 235.15 21.14 o 12 1 0 255.51 282.42 27.47 o 13 1 0 7.10 13.73 33.28 o 14 1 0 240.85 258.47 23.17 o 15 1 0 759.38 806.78 66.42 o 0 2 0 2.69 16.89 8.97 o 1 2 0 1.60 20.30 15.05 o 2 2 0 4427.91 4339.22 63.86 o 3 2 0 47.40 75.16 8.66 o 4 2 0 2884.44 2996.16 54.48 o 5 2 0 781.54 776.53 30.94 o 6 2 0 1703.73 1603.01 46.47 o 7 2 0 12.41 -21.26 21.26 o 8 2 0 2243.92 2213.30 61.34 o 9 2 0 771.13 753.58 45.00 o 10 2 0 69.06 58.25 31.14 o 11 2 0 17.18 25.26 29.93 o 12 2 0 284.99 270.63 23.42 o 13 2 0 7.48 31.96 34.68 o 14 2 0 173.62 130.54 21.88 o 1 3 0 164.90 169.07 14.16 o 2 3 0 4.48 6.46 16.45 o 3 3 0 1192.83 1292.70 37.03 o 4 3 0 1.42 -19.25 19.25 o 5 3 0 138.69 104.52 11.37 o 6 3 0 629.45 738.10 36.59 o 7 3 0 339.82 302.79 21.35 o 8 3 0 122.63 101.22 14.00 o 9 3 0 163.07 166.91 16.11 o 10 3 0 677.56 646.79 45.34 o 11 3 0 442.00 418.43 31.76 o 12 3 0 136.69 144.41 18.65 o 13 3 0 80.68 47.88 39.24 o 14 3 0 466.92 539.40 37.73 o 0 4 0 1266.68 1283.64 41.71 o 1 4 0 338.76 316.52 28.53 o 2 4 0 2287.23 2157.37 55.11 o 3 4 0 182.59 224.37 17.31 o 4 4 0 45.03 27.44 22.50 o 5 4 0 241.25 209.46 20.68 o 6 4 0 1172.07 1138.30 48.76 o 7 4 0 7.91 29.73 26.60 o 8 4 0 973.85 845.22 48.85 o 9 4 0 35.71 22.41 30.60 o 10 4 0 257.79 271.41 22.75 o 11 4 0 27.91 16.69 34.45 o 12 4 0 59.07 27.02 39.28 o 13 4 0 512.91 546.44 51.92 o 1 5 0 115.43 117.56 13.84 o 2 5 0 386.71 396.00 34.90 o 3 5 0 68.29 62.30 13.29 o 4 5 0 4.23 5.68 23.79 o 5 5 0 63.11 77.37 13.96 o 6 5 0 143.63 144.38 16.12 o 7 5 0 7.69 -23.95 29.89 o 8 5 0 9.62 10.40 33.41 o 9 5 0 379.03 374.74 31.72 o 10 5 0 22.56 22.19 33.54 o 11 5 0 19.26 -6.97 33.85 o 12 5 0 39.52 50.59 40.69 o 0 6 0 2319.80 2249.02 71.96 o 1 6 0 314.57 303.88 25.89 o 2 6 0 62.26 36.41 31.69 o 3 6 0 12.27 -22.59 31.16 o 4 6 0 792.51 794.11 50.15 o 5 6 0 24.85 37.33 14.84 o 6 6 0 759.15 697.54 49.32 o 7 6 0 29.38 21.06 32.76 o 8 6 0 92.46 121.26 18.36 o 9 6 0 17.35 67.88 34.85 o 10 6 0 38.93 13.13 36.50 o 11 6 0 55.17 65.55 19.88 o 1 7 0 837.88 761.00 52.13 o 2 7 0 7.68 -9.08 35.05 o 3 7 0 882.13 824.76 55.86 o 4 7 0 68.11 89.25 18.50 o 5 7 0 42.11 33.25 36.10 o 6 7 0 19.07 39.40 37.33 o 7 7 0 0.99 -7.74 36.17 o 8 7 0 0.30 -8.03 35.65 o 9 7 0 52.62 42.20 39.40 o 0 8 0 11.94 36.24 34.07 o 1 8 0 4.22 8.59 36.97 o 2 8 0 241.52 258.92 22.59 o 3 8 0 0.38 -27.64 37.55 o 4 8 0 19.39 8.32 40.46 o 5 8 0 19.27 26.15 37.61 o 6 8 0 41.23 8.57 40.84 o -15 1 1 4.33 30.40 36.70 o -14 1 1 34.87 19.28 37.10 o -13 1 1 82.26 75.12 18.39 o -12 1 1 29.48 -24.82 34.76 o -11 1 1 322.02 300.50 26.93 o -10 1 1 864.66 925.92 45.45 o -9 1 1 20.98 26.24 24.35 o -8 1 1 229.91 263.97 26.38 o -7 1 1 384.83 411.05 27.98 o -6 1 1 16.77 21.14 17.61 o -5 1 1 193.24 250.06 20.16 o -4 1 1 527.38 572.23 22.81 o -3 1 1 3406.39 3252.45 49.90 o -2 1 1 303.04 352.58 15.42 o -1 1 1 4604.87 4591.62 57.65 o 0 1 1 4194.88 3979.25 35.91 o 1 1 1 29.37 13.85 10.82 o 2 1 1 5245.88 5051.34 67.13 o 3 1 1 1814.42 1841.07 36.48 o 4 1 1 716.40 776.56 26.62 o 5 1 1 342.49 292.62 22.17 o 6 1 1 2588.15 2681.64 57.82 o 7 1 1 26.07 -32.36 32.36 o 8 1 1 627.64 671.90 37.81 o 9 1 1 7.56 -32.88 32.88 o 10 1 1 11.22 -19.25 29.43 o 11 1 1 236.93 260.41 24.84 o 12 1 1 395.20 477.66 45.36 o 13 1 1 0.22 -14.98 37.08 o 14 1 1 93.72 93.62 20.25 o -15 2 1 46.50 39.13 42.65 o -14 2 1 95.24 40.98 41.35 o -13 2 1 20.56 30.87 33.30 o -12 2 1 35.89 29.60 32.58 o -11 2 1 335.78 322.64 27.82 o -10 2 1 29.90 55.22 14.24 o -9 2 1 356.54 352.40 33.01 o -8 2 1 46.57 43.58 23.91 o -7 2 1 99.28 38.44 23.06 o -6 2 1 556.60 666.00 30.07 o -5 2 1 27.46 28.64 17.56 o -4 2 1 402.60 392.02 22.21 o -3 2 1 446.83 513.92 22.68 o -2 2 1 9.31 -9.33 15.47 o -1 2 1 16.34 23.91 15.29 o 0 2 1 99.39 110.15 12.10 o 1 2 1 2861.49 2828.58 47.61 o 2 2 1 84.54 89.88 8.59 o 3 2 1 880.70 932.02 28.96 o 4 2 1 26.80 5.08 17.81 o 5 2 1 321.30 344.01 24.48 o 6 2 1 163.67 173.27 14.13 o 7 2 1 0.11 -0.74 20.39 o 8 2 1 22.59 -15.45 24.80 o 9 2 1 115.93 109.88 15.38 o 10 2 1 270.17 259.83 21.41 o 11 2 1 204.87 188.99 19.03 o 12 2 1 9.57 14.20 33.28 o 13 2 1 12.94 46.79 33.48 o 14 2 1 54.57 44.52 39.98 o -14 3 1 51.23 -5.03 42.80 o -13 3 1 1.99 -34.61 34.61 o -12 3 1 1.28 -8.17 34.68 o -11 3 1 403.64 430.63 29.31 o -10 3 1 201.36 216.03 20.14 o -9 3 1 17.64 3.07 26.80 o -8 3 1 201.12 178.86 17.74 o -7 3 1 486.17 527.99 33.52 o -6 3 1 58.20 24.71 21.08 o -5 3 1 0.13 12.35 17.45 o -4 3 1 954.62 955.01 34.43 o -3 3 1 757.53 794.65 30.62 o -2 3 1 1170.37 1173.54 34.21 o -1 3 1 197.12 200.09 14.87 o 0 3 1 1384.71 1412.51 25.86 o 1 3 1 78.88 66.28 9.33 o 2 3 1 29.51 39.19 8.84 o 3 3 1 58.46 76.96 9.84 o 4 3 1 164.37 151.62 12.98 o 5 3 1 780.15 774.08 35.94 o 6 3 1 146.59 169.22 14.94 o 7 3 1 5.43 20.68 22.44 o 8 3 1 4.44 21.01 25.97 o 9 3 1 159.32 156.74 16.43 o 10 3 1 1.12 -10.01 30.38 o 11 3 1 18.18 -12.51 32.43 o 12 3 1 220.65 236.99 20.39 o 13 3 1 34.65 37.33 37.22 o -13 4 1 16.03 22.14 38.51 o -12 4 1 85.02 111.58 17.81 o -11 4 1 84.40 23.10 35.50 o -10 4 1 1.10 -9.59 30.67 o -9 4 1 76.47 91.30 15.54 o -8 4 1 1.16 -30.72 30.72 o -7 4 1 75.87 67.71 13.42 o -6 4 1 38.62 21.79 24.06 o -5 4 1 574.75 589.79 35.79 o -4 4 1 105.69 118.45 12.44 o -3 4 1 512.14 568.43 33.65 o -2 4 1 191.79 179.51 14.51 o -1 4 1 412.67 424.11 29.36 o 0 4 1 1752.07 1676.20 33.31 o 1 4 1 2138.10 2187.29 54.51 o 2 4 1 1006.09 1124.90 40.44 o 3 4 1 452.31 532.28 31.18 o 4 4 1 939.41 904.40 41.26 o 5 4 1 15.20 8.03 23.37 o 6 4 1 27.77 31.40 18.03 o 7 4 1 235.78 237.84 22.92 o 8 4 1 550.40 562.86 42.27 o 9 4 1 54.04 45.60 29.29 o 10 4 1 29.07 34.19 33.30 o 11 4 1 79.33 21.14 37.62 o 12 4 1 496.74 414.76 36.48 o 13 4 1 3.00 -40.55 40.55 o -12 5 1 279.85 290.77 26.22 o -11 5 1 199.11 212.16 20.68 o -10 5 1 3.98 -34.03 34.03 o -9 5 1 3.63 -22.39 32.21 o -8 5 1 645.42 575.19 48.90 o -7 5 1 228.48 261.17 25.29 o -6 5 1 1.28 43.14 24.59 o -5 5 1 271.00 272.65 23.70 o -4 5 1 13.27 -1.45 25.68 o -3 5 1 1511.33 1573.59 53.88 o -2 5 1 307.69 327.83 31.43 o -1 5 1 412.10 397.34 24.30 o 0 5 1 754.72 749.82 30.23 o 1 5 1 260.65 200.89 17.74 o 2 5 1 657.43 692.93 38.30 o 3 5 1 1275.67 1327.64 48.85 o 4 5 1 44.30 49.99 13.89 o 5 5 1 99.77 95.82 15.25 o 6 5 1 642.22 619.33 44.07 o 7 5 1 6.39 1.47 31.49 o 8 5 1 194.55 185.33 18.85 o 9 5 1 1.00 17.63 32.59 o 10 5 1 28.60 60.29 33.38 o 11 5 1 103.36 95.26 19.52 o 12 5 1 0.22 34.17 20.94 o -11 6 1 23.08 18.41 37.04 o -10 6 1 1.30 26.46 35.37 o -9 6 1 53.64 52.68 36.95 o -8 6 1 105.24 108.99 17.89 o -7 6 1 5.16 37.24 31.76 o -6 6 1 281.37 337.29 28.74 o -5 6 1 1.08 1.43 29.16 o -4 6 1 31.68 5.28 30.96 o -3 6 1 0.48 23.75 28.93 o -2 6 1 279.56 260.19 24.42 o -1 6 1 162.71 175.94 17.18 o 0 6 1 141.66 127.88 17.35 o 1 6 1 319.29 335.62 27.44 o 2 6 1 6.92 26.93 28.80 o 3 6 1 1749.69 1724.67 66.55 o 4 6 1 504.50 448.35 44.11 o 5 6 1 149.45 136.30 17.50 o 6 6 1 177.80 190.65 18.88 o 7 6 1 187.43 234.72 21.95 o 8 6 1 106.28 121.72 18.50 o 9 6 1 243.13 224.89 22.46 o 10 6 1 154.76 202.96 21.26 o -9 7 1 62.97 104.05 19.74 o -8 7 1 129.56 149.61 20.70 o -7 7 1 3.21 56.49 35.35 o -6 7 1 186.80 172.00 20.79 o -5 7 1 268.89 312.45 30.51 o -4 7 1 411.65 442.59 33.92 o -3 7 1 503.88 517.43 46.56 o -2 7 1 3.68 41.24 31.12 o -1 7 1 32.60 41.35 34.46 o 0 7 1 160.99 164.76 13.53 o 1 7 1 166.85 187.90 19.41 o 2 7 1 55.49 42.74 35.99 o 3 7 1 31.41 44.62 36.75 o 4 7 1 111.19 97.33 19.27 o 5 7 1 26.24 10.35 35.30 o 6 7 1 14.25 32.83 35.05 o 7 7 1 1.17 -36.93 36.93 o 8 7 1 83.50 108.21 20.25 o -6 8 1 61.36 96.77 19.48 o -5 8 1 2.15 -38.59 38.59 o -4 8 1 33.86 44.52 25.64 o -3 8 1 9.66 3.85 37.53 o -2 8 1 97.25 110.57 20.76 o -1 8 1 5.64 -21.41 35.45 o 0 8 1 8.99 27.07 25.57 o 1 8 1 37.90 44.72 19.43 o 2 8 1 179.39 212.91 21.43 o 3 8 1 10.99 -24.64 38.22 o 4 8 1 80.22 78.88 20.41 o 5 8 1 102.70 128.49 20.41 o 6 8 1 57.11 59.09 42.82 o -15 0 2 326.11 343.12 34.46 o -14 0 2 350.11 506.98 45.89 o -13 0 2 47.85 77.83 17.07 o -12 0 2 2.43 -28.71 31.50 o -11 0 2 241.56 241.05 19.16 o -10 0 2 126.59 136.44 14.02 o -9 0 2 954.95 1009.25 43.65 o -8 0 2 2690.12 2508.61 62.47 o -7 0 2 2136.61 2223.92 52.97 o -6 0 2 853.65 794.12 30.36 o -5 0 2 741.75 797.97 27.42 o -4 0 2 689.81 806.29 25.26 o -3 0 2 3069.75 3292.62 49.15 o -2 0 2 10243.34 10156.08 116.78 o -1 0 2 352.97 350.95 11.88 o 0 0 2 5988.01 6003.85 51.97 o 1 0 2 2920.29 2901.34 41.47 o 2 0 2 26437.39 22900.26 252.91 o 3 0 2 17177.82 16349.91 189.25 o 4 0 2 6313.50 6680.31 93.01 o 5 0 2 617.58 623.14 27.84 o 6 0 2 135.93 105.77 11.11 o 7 0 2 660.25 668.70 34.21 o 8 0 2 1728.33 1867.65 58.02 o 9 0 2 8.54 -28.60 28.60 o 10 0 2 10.46 10.11 29.56 o 11 0 2 4.03 22.86 30.25 o 12 0 2 42.71 51.79 16.98 o 13 0 2 117.10 110.84 20.36 o 14 0 2 70.58 46.83 40.66 o -15 1 2 96.41 82.75 42.02 o -14 1 2 114.05 111.67 20.79 o -13 1 2 705.18 721.96 52.55 o -12 1 2 111.33 117.27 16.20 o -11 1 2 0.85 -27.22 29.85 o -10 1 2 322.85 346.14 34.10 o -9 1 2 67.68 75.28 12.58 o -8 1 2 226.38 204.86 18.94 o -7 1 2 1776.59 1889.90 49.97 o -6 1 2 120.61 135.04 12.24 o -5 1 2 1649.45 1711.38 39.06 o -4 1 2 870.02 858.59 27.20 o -3 1 2 398.16 426.45 19.77 o -2 1 2 1319.60 1226.68 26.33 o -1 1 2 2939.40 2939.42 42.84 o 0 1 2 5097.62 5079.09 46.04 o 1 1 2 24501.90 21512.77 237.57 o 2 1 2 3757.71 3913.64 57.56 o 3 1 2 1499.48 1519.86 35.19 o 4 1 2 1898.83 1899.03 41.58 o 5 1 2 4422.11 4395.73 74.58 o 6 1 2 1143.76 1136.28 39.31 o 7 1 2 1033.02 968.37 40.62 o 8 1 2 119.13 83.22 14.35 o 9 1 2 1224.07 819.65 56.11 o 10 1 2 149.59 -58.03 58.03 o 11 1 2 277.93 291.61 28.94 o 12 1 2 401.12 408.22 35.70 o 13 1 2 227.96 228.52 23.84 o 14 1 2 61.89 67.30 43.76 o -15 2 2 150.01 150.64 23.46 o -14 2 2 798.93 816.55 59.03 o -13 2 2 319.38 363.01 32.01 o -12 2 2 19.41 25.04 31.76 o -11 2 2 1696.60 1582.73 63.10 o -10 2 2 745.73 716.68 43.44 o -9 2 2 142.21 127.38 13.73 o -8 2 2 1010.69 1049.69 42.98 o -7 2 2 214.11 156.13 13.84 o -6 2 2 1545.32 1559.32 43.44 o -5 2 2 933.24 920.22 32.21 o -4 2 2 350.93 356.00 21.74 o -3 2 2 1219.13 1335.92 32.94 o -2 2 2 1718.76 1739.91 36.57 o -1 2 2 529.47 469.98 21.61 o 0 2 2 3301.00 3400.66 38.20 o 1 2 2 1227.00 1254.19 31.27 o 2 2 2 3066.11 3053.42 52.88 o 3 2 2 592.74 596.18 25.33 o 4 2 2 167.53 196.51 14.82 o 5 2 2 1184.41 1223.95 40.29 o 6 2 2 8.10 8.68 20.54 o 7 2 2 700.97 744.39 38.21 o 8 2 2 120.77 110.89 13.91 o 9 2 2 1.50 4.30 25.69 o 10 2 2 131.62 140.66 16.69 o 11 2 2 519.03 491.48 44.51 o 12 2 2 23.12 9.17 35.92 o 13 2 2 2.63 -10.37 35.57 o 14 2 2 80.78 91.61 20.65 o -14 3 2 194.13 207.13 21.72 o -13 3 2 2.69 12.86 35.97 o -12 3 2 51.79 17.52 34.43 o -11 3 2 32.13 29.11 30.80 o -10 3 2 1.25 24.44 28.15 o -9 3 2 124.34 102.96 15.63 o -8 3 2 72.96 79.24 13.49 o -7 3 2 100.15 87.69 12.31 o -6 3 2 755.02 858.10 36.95 o -5 3 2 2096.90 2155.30 53.73 o -4 3 2 549.34 541.18 28.69 o -3 3 2 16.61 -19.07 19.07 o -2 3 2 2481.69 2932.24 56.64 o -1 3 2 3257.95 3604.04 62.97 o 0 3 2 221.08 216.95 10.84 o 1 3 2 875.99 881.25 30.85 o 2 3 2 2.27 12.00 17.47 o 3 3 2 1631.01 1569.16 43.96 o 4 3 2 333.89 288.97 26.37 o 5 3 2 311.44 293.13 19.05 o 6 3 2 333.72 339.02 30.51 o 7 3 2 669.48 724.49 40.24 o 8 3 2 389.62 319.64 25.15 o 9 3 2 651.00 679.51 45.78 o 10 3 2 3.28 38.08 21.57 o 11 3 2 430.54 449.09 32.63 o 12 3 2 20.57 -10.51 36.84 o 13 3 2 170.76 145.19 22.08 o -13 4 2 65.61 81.93 19.08 o -12 4 2 92.86 92.06 18.58 o -11 4 2 8.98 51.62 29.85 o -10 4 2 898.87 845.98 52.91 o -9 4 2 575.14 575.84 43.89 o -8 4 2 273.71 275.94 24.97 o -7 4 2 367.86 343.99 33.43 o -6 4 2 180.44 180.13 16.38 o -5 4 2 1898.65 1940.30 56.22 o -4 4 2 74.13 13.91 23.79 o -3 4 2 21.46 -2.60 20.76 o -2 4 2 1763.25 1983.03 52.66 o -1 4 2 290.43 304.59 27.35 o 0 4 2 219.77 246.15 14.89 o 1 4 2 0.16 -4.78 20.88 o 2 4 2 0.02 1.42 21.34 o 3 4 2 36.41 42.02 22.28 o 4 4 2 136.88 142.29 13.40 o 5 4 2 98.21 78.77 13.11 o 6 4 2 285.09 274.10 23.62 o 7 4 2 206.02 238.26 19.47 o 8 4 2 6.09 -17.69 28.51 o 9 4 2 2.61 15.09 29.31 o 10 4 2 14.15 47.92 30.62 o 11 4 2 49.47 82.46 17.43 o 12 4 2 62.48 3.23 40.17 o -12 5 2 23.60 -11.91 37.44 o -11 5 2 203.16 211.13 21.12 o -10 5 2 52.09 -35.72 35.72 o -9 5 2 42.33 66.26 15.92 o -8 5 2 7.71 -32.61 32.61 o -7 5 2 720.72 707.98 44.78 o -6 5 2 6.60 31.69 27.84 o -5 5 2 285.53 273.70 24.13 o -4 5 2 1.03 -26.58 26.58 o -3 5 2 767.24 688.84 40.82 o -2 5 2 236.91 225.60 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