#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:30:06 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180786 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/17/2011744.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011744_Fobs loop_ _publ_author_name 'Casta\~neda, Fernando' 'Terraza, Claudio A.' 'Garland, Maria Teresa' 'Bunton, Clifford A.' 'Baggio, Ricardo F.' _publ_section_title ; Methyl, ethyl, isopropyl and tert-butyl 3-oxo-2-(triphenylphosphoranylidene)butyrates, a common pattern for a preferred conformation ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 180 _journal_page_last 184 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.8152 _cell_length_b 16.2264 _cell_length_c 17.6696 _exptl_crystal_F_000 1648.00 _reflns_d_resolution_high 0.8402 _cod_data_source_file bk1566IIIsup3.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 288.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 79498.91 69629.18 410.36 o 4 0 0 2664.32 2741.46 62.00 o 6 0 0 317.59 279.28 28.98 o 8 0 0 584.39 547.32 36.45 o 10 0 0 1255.98 1286.58 53.19 o 12 0 0 356.29 307.86 48.70 o 14 0 0 1574.29 1634.70 71.62 o 16 0 0 506.88 506.16 59.66 o 2 1 0 2025.39 1852.12 36.40 o 4 1 0 2033.12 2157.89 50.63 o 6 1 0 7469.63 7411.27 124.81 o 8 1 0 3650.78 3514.02 71.45 o 10 1 0 4245.78 3805.28 79.42 o 12 1 0 1788.18 1891.39 70.03 o 14 1 0 294.59 323.39 51.69 o 16 1 0 3.15 125.99 47.80 o 0 2 0 33070.81 36976.46 270.79 o 2 2 0 412.31 363.99 22.41 o 4 2 0 27447.84 26906.09 322.37 o 6 2 0 3920.43 4110.74 72.37 o 8 2 0 1631.15 1417.31 45.43 o 10 2 0 0.39 -35.16 35.46 o 12 2 0 108.06 148.00 45.12 o 14 2 0 48.06 66.93 48.20 o 16 2 0 260.82 341.81 56.97 o 2 3 0 8870.32 10062.04 147.53 o 4 3 0 15597.82 16252.76 215.69 o 6 3 0 3052.98 3055.32 60.79 o 8 3 0 39.62 30.28 32.87 o 10 3 0 1624.62 1773.86 58.57 o 12 3 0 1257.36 1372.90 65.04 o 14 3 0 163.00 128.68 49.10 o 16 3 0 3.51 -50.29 50.39 o 0 4 0 3379.26 3472.21 72.00 o 2 4 0 3195.67 2829.89 57.83 o 4 4 0 813.97 659.25 32.57 o 6 4 0 38.06 60.95 30.28 o 8 4 0 718.34 625.02 40.44 o 10 4 0 168.15 162.94 41.63 o 12 4 0 157.82 222.79 49.50 o 14 4 0 20.77 -0.10 47.31 o 16 4 0 0.89 -15.14 52.98 o 2 5 0 13763.09 14836.73 211.35 o 4 5 0 928.28 875.51 36.06 o 6 5 0 2676.64 2709.50 61.08 o 8 5 0 1.17 22.61 34.16 o 10 5 0 484.41 513.04 47.81 o 12 5 0 601.78 593.52 56.17 o 14 5 0 172.41 179.57 51.29 o 16 5 0 85.79 55.47 54.38 o 0 6 0 11467.86 11672.66 192.48 o 2 6 0 6961.35 6227.62 104.45 o 4 6 0 1762.81 1620.18 44.53 o 6 6 0 1642.86 1821.09 52.40 o 8 6 0 2791.10 2689.73 68.05 o 10 6 0 583.42 522.41 49.60 o 12 6 0 557.17 588.33 52.69 o 14 6 0 518.34 567.31 61.85 o 16 6 0 169.96 167.02 56.97 o 2 7 0 1101.70 1283.86 43.53 o 4 7 0 1725.33 1945.09 52.50 o 6 7 0 302.06 287.34 35.06 o 8 7 0 1.95 -30.38 37.65 o 10 7 0 330.12 349.59 50.40 o 12 7 0 84.77 70.31 46.41 o 14 7 0 36.57 110.95 52.59 o 16 7 0 16.11 33.36 52.98 o 0 8 0 797.29 860.02 41.74 o 2 8 0 8283.05 8351.53 139.95 o 4 8 0 3271.42 3429.12 75.73 o 6 8 0 134.56 126.98 35.95 o 8 8 0 912.14 941.97 51.40 o 10 8 0 1902.08 1862.51 70.03 o 12 8 0 46.79 118.82 50.79 o 14 8 0 77.91 30.08 52.98 o 16 8 0 136.15 90.13 57.86 o 2 9 0 1406.07 1158.15 49.71 o 4 9 0 2590.21 2878.51 68.55 o 6 9 0 1027.50 1107.44 53.19 o 8 9 0 58.38 56.17 44.22 o 10 9 0 231.72 283.15 50.89 o 12 9 0 536.45 597.49 61.45 o 14 9 0 29.17 -17.03 56.57 o 0 10 0 92.47 79.78 38.14 o 2 10 0 1377.60 1484.75 54.99 o 4 10 0 93.13 96.21 39.44 o 6 10 0 11.04 -2.59 41.63 o 8 10 0 144.16 89.14 49.50 o 10 10 0 791.77 913.95 63.65 o 12 10 0 313.58 349.58 61.85 o 14 10 0 34.90 62.05 56.57 o 2 11 0 434.94 329.18 46.51 o 4 11 0 23.06 62.74 42.92 o 6 11 0 98.21 72.21 46.01 o 8 11 0 94.51 52.98 48.20 o 10 11 0 157.61 179.07 47.81 o 12 11 0 51.35 71.11 54.78 o 14 11 0 10.24 -27.89 60.45 o 0 12 0 140.68 147.60 46.91 o 2 12 0 281.91 278.17 50.40 o 4 12 0 766.90 637.36 56.67 o 6 12 0 88.26 -6.27 51.29 o 8 12 0 402.56 282.36 51.79 o 10 12 0 1.31 25.99 46.41 o 12 12 0 71.92 85.85 55.67 o 2 13 0 317.86 312.84 56.97 o 4 13 0 173.43 170.71 53.48 o 6 13 0 24.56 -38.24 46.91 o 8 13 0 179.37 254.86 53.88 o 10 13 0 118.07 38.74 54.38 o 12 13 0 38.75 138.14 58.26 o 0 14 0 1810.53 1746.73 77.40 o 2 14 0 2322.41 2256.68 82.78 o 4 14 0 495.42 453.67 58.36 o 6 14 0 79.20 16.53 50.79 o 8 14 0 28.16 113.84 53.88 o 10 14 0 201.45 278.27 59.16 o 12 14 0 140.56 129.17 62.65 o 2 15 0 391.02 414.92 64.04 o 4 15 0 469.66 450.18 58.76 o 6 15 0 571.38 605.56 62.75 o 8 15 0 244.99 236.14 57.47 o 10 15 0 19.16 -17.03 56.57 o 0 16 0 448.59 458.85 63.15 o 2 16 0 12.98 -49.00 57.37 o 4 16 0 415.05 464.62 64.44 o 6 16 0 981.25 884.97 75.10 o 8 16 0 767.55 781.76 75.00 o 2 17 0 898.24 787.35 73.71 o 4 17 0 255.11 296.99 61.85 o 6 17 0 58.07 121.31 57.86 o 8 17 0 48.86 114.33 59.56 o 0 18 0 223.82 294.80 66.23 o 2 18 0 0.09 30.67 57.37 o 4 18 0 44.85 -18.82 63.94 o 6 18 0 94.77 226.78 61.35 o 2 19 0 16.90 -53.98 63.54 o 1 1 1 24.09 25.89 13.54 o 2 1 1 464.14 540.84 21.22 o 3 1 1 4004.09 4051.73 74.62 o 4 1 1 17244.01 16223.38 236.49 o 5 1 1 1461.02 1464.21 38.06 o 6 1 1 118.62 127.98 26.29 o 7 1 1 11.67 -21.11 28.88 o 8 1 1 263.30 306.96 33.37 o 9 1 1 0.03 22.01 33.76 o 10 1 1 221.72 157.06 38.54 o 11 1 1 552.62 465.93 46.51 o 12 1 1 345.88 426.68 51.69 o 13 1 1 132.37 81.67 48.60 o 14 1 1 18.97 -47.01 47.80 o 15 1 1 32.56 -34.06 46.41 o 16 1 1 0.02 -18.82 50.00 o 17 1 1 3.25 36.35 54.28 o 0 2 1 26152.92 29119.98 243.11 o 1 2 1 4503.95 4951.30 83.29 o 2 2 1 17497.71 18143.62 213.65 o 3 2 1 3331.43 3561.95 68.81 o 4 2 1 86.01 81.87 26.69 o 5 2 1 676.47 637.31 31.68 o 6 2 1 177.45 224.59 28.48 o 7 2 1 381.01 414.94 33.37 o 8 2 1 1555.36 1568.92 48.42 o 9 2 1 257.55 297.30 37.75 o 10 2 1 11.61 -10.06 35.46 o 11 2 1 1.31 -15.14 40.34 o 12 2 1 113.48 154.87 45.61 o 13 2 1 321.50 341.82 51.29 o 14 2 1 383.04 492.51 57.87 o 15 2 1 259.47 208.35 55.67 o 16 2 1 216.13 211.74 54.38 o 17 2 1 32.78 80.27 54.78 o 1 3 1 3917.98 3889.62 71.14 o 2 3 1 83226.02 91140.29 608.75 o 3 3 1 4860.17 4865.71 88.38 o 4 3 1 7300.10 6956.15 107.48 o 5 3 1 2273.83 2489.82 53.21 o 6 3 1 572.94 521.83 32.47 o 7 3 1 434.81 468.72 34.26 o 8 3 1 2335.11 2572.11 64.96 o 9 3 1 971.85 949.07 47.91 o 10 3 1 2005.23 1971.40 61.27 o 11 3 1 1604.20 1646.42 63.75 o 12 3 1 146.21 134.25 47.81 o 13 3 1 2.51 74.20 43.82 o 14 3 1 4.23 40.43 47.31 o 15 3 1 257.50 235.54 55.28 o 16 3 1 270.17 213.43 57.87 o 17 3 1 15.13 37.05 55.67 o 0 4 1 15971.87 17115.05 241.64 o 1 4 1 217.41 220.32 29.38 o 2 4 1 10382.60 10970.31 165.99 o 3 4 1 1407.74 1173.79 35.77 o 4 4 1 632.76 596.96 32.97 o 5 4 1 7.49 61.15 26.69 o 6 4 1 4807.60 4834.81 84.44 o 7 4 1 222.99 204.08 34.16 o 8 4 1 4840.02 4754.70 89.90 o 9 4 1 636.56 609.97 45.62 o 10 4 1 1585.67 1492.03 57.68 o 11 4 1 653.17 753.09 53.59 o 12 4 1 229.95 244.61 48.20 o 13 4 1 35.83 5.98 46.91 o 14 4 1 78.50 69.42 49.50 o 15 4 1 49.60 75.69 49.10 o 16 4 1 206.51 245.40 58.26 o 17 4 1 111.89 170.51 56.97 o 1 5 1 532.39 545.86 31.18 o 2 5 1 1133.05 1043.57 34.37 o 3 5 1 12.91 -16.63 26.29 o 4 5 1 7547.84 8001.89 134.78 o 5 5 1 1354.12 1520.52 44.03 o 6 5 1 2597.92 2780.90 64.97 o 7 5 1 10.58 -4.48 32.47 o 8 5 1 103.03 56.77 34.66 o 9 5 1 97.01 86.65 39.04 o 10 5 1 554.57 554.88 48.70 o 11 5 1 286.76 274.49 47.31 o 12 5 1 61.27 126.29 46.01 o 13 5 1 12.99 -6.67 43.82 o 14 5 1 23.90 67.33 50.39 o 15 5 1 63.05 35.95 50.00 o 16 5 1 32.58 37.35 52.19 o 0 6 1 13.78 16.43 27.59 o 1 6 1 289.16 304.68 29.38 o 2 6 1 9857.19 9945.85 158.33 o 3 6 1 666.33 696.66 36.06 o 4 6 1 10741.48 10701.01 159.00 o 5 6 1 105.01 53.28 31.57 o 6 6 1 93.00 124.49 31.57 o 7 6 1 1905.97 1903.61 54.69 o 8 6 1 0.06 -23.01 36.35 o 9 6 1 108.89 66.53 40.73 o 10 6 1 2399.84 2435.20 71.93 o 11 6 1 694.24 650.70 53.59 o 12 6 1 185.68 215.62 48.70 o 13 6 1 87.28 53.68 47.81 o 14 6 1 2.58 -47.21 47.31 o 15 6 1 0.01 -49.10 52.59 o 16 6 1 5.21 94.51 52.19 o 1 7 1 8.95 12.65 29.78 o 2 7 1 648.89 769.86 38.25 o 3 7 1 973.05 952.30 41.34 o 4 7 1 2149.70 2329.13 60.98 o 5 7 1 367.25 457.66 37.75 o 6 7 1 5.83 20.82 30.67 o 7 7 1 93.19 87.05 35.95 o 8 7 1 16.11 58.76 39.84 o 9 7 1 307.15 375.58 44.72 o 10 7 1 3.26 -40.83 45.12 o 11 7 1 11.01 -2.59 48.20 o 12 7 1 2.99 78.88 45.12 o 13 7 1 2.21 -47.21 48.20 o 14 7 1 40.66 60.65 50.79 o 15 7 1 0.25 66.13 53.88 o 16 7 1 24.58 -15.14 56.07 o 0 8 1 465.68 497.71 37.75 o 1 8 1 1991.33 2033.37 53.80 o 2 8 1 40.95 -9.96 34.16 o 3 8 1 201.15 212.44 36.35 o 4 8 1 569.72 530.69 41.24 o 5 8 1 359.98 369.51 38.15 o 6 8 1 4.50 14.04 34.16 o 7 8 1 166.51 153.88 39.04 o 8 8 1 45.00 53.18 39.84 o 9 8 1 70.81 0.10 44.22 o 10 8 1 199.99 185.95 48.60 o 11 8 1 54.04 39.24 49.50 o 12 8 1 482.91 546.50 60.06 o 13 8 1 374.49 274.19 59.16 o 14 8 1 55.66 -26.19 51.29 o 15 8 1 14.23 -29.48 52.59 o 16 8 1 4.59 28.78 53.88 o 1 9 1 1.83 17.63 33.76 o 2 9 1 36.81 69.62 34.16 o 3 9 1 154.85 211.74 35.95 o 4 9 1 130.62 148.90 36.85 o 5 9 1 232.26 203.48 40.34 o 6 9 1 322.30 256.86 43.42 o 7 9 1 168.72 177.38 43.82 o 8 9 1 66.89 35.85 42.93 o 9 9 1 100.89 99.50 47.31 o 10 9 1 121.36 109.06 48.20 o 11 9 1 32.26 86.75 46.41 o 12 9 1 58.51 100.39 50.00 o 13 9 1 320.11 248.10 57.47 o 14 9 1 32.80 38.04 57.37 o 15 9 1 39.51 16.83 56.57 o 0 10 1 1245.83 1238.78 51.50 o 1 10 1 1355.58 1527.09 54.99 o 2 10 1 728.38 719.04 46.52 o 3 10 1 1092.62 1088.63 49.21 o 4 10 1 206.28 256.86 42.13 o 5 10 1 731.63 654.59 49.60 o 6 10 1 287.59 317.02 44.32 o 7 10 1 58.00 111.94 42.03 o 8 10 1 337.90 385.94 50.40 o 9 10 1 5.04 16.13 47.31 o 10 10 1 29.29 87.34 46.91 o 11 10 1 8.13 61.35 50.39 o 12 10 1 32.67 95.41 52.59 o 13 10 1 42.35 127.28 54.78 o 14 10 1 123.74 93.72 56.07 o 15 10 1 24.76 5.18 53.88 o 1 11 1 1.57 11.55 39.44 o 2 11 1 15.09 25.00 39.44 o 3 11 1 16.51 76.89 41.23 o 4 11 1 42.07 84.06 43.42 o 5 11 1 115.36 119.81 42.53 o 6 11 1 104.30 51.69 45.12 o 7 11 1 3.35 -44.02 45.12 o 8 11 1 2.88 -19.02 46.91 o 9 11 1 50.71 -27.59 49.10 o 10 11 1 32.64 140.53 50.00 o 11 11 1 86.14 73.20 52.98 o 12 11 1 466.68 379.47 61.85 o 13 11 1 571.99 648.69 66.63 o 14 11 1 197.82 259.25 62.25 o 0 12 1 4783.42 5028.04 102.55 o 1 12 1 2460.32 2464.04 73.62 o 2 12 1 2991.29 3002.21 80.40 o 3 12 1 1188.63 1333.66 63.25 o 4 12 1 1630.65 1501.08 67.34 o 5 12 1 146.19 152.88 48.60 o 6 12 1 240.61 300.08 50.89 o 7 12 1 17.23 -12.45 45.61 o 8 12 1 4.05 43.62 46.41 o 9 12 1 0.21 -7.37 47.80 o 10 12 1 34.07 103.48 47.81 o 11 12 1 220.53 223.09 58.76 o 12 12 1 192.40 291.42 57.86 o 13 12 1 49.14 165.23 58.76 o 1 13 1 90.98 104.87 52.98 o 2 13 1 488.70 538.63 58.76 o 3 13 1 70.97 156.96 51.69 o 4 13 1 214.56 252.77 53.08 o 5 13 1 36.62 69.12 47.31 o 6 13 1 32.41 28.09 46.91 o 7 13 1 40.89 -8.27 47.31 o 8 13 1 18.76 11.05 50.00 o 9 13 1 37.38 17.23 49.50 o 10 13 1 57.84 10.06 50.79 o 11 13 1 16.53 16.53 58.26 o 12 13 1 95.12 173.09 59.16 o 0 14 1 2017.28 2142.75 79.69 o 1 14 1 527.61 612.04 62.25 o 2 14 1 0.50 44.82 51.69 o 3 14 1 15.35 27.99 52.59 o 4 14 1 145.01 170.41 50.40 o 5 14 1 98.25 29.08 49.50 o 6 14 1 236.53 215.53 52.19 o 7 14 1 438.29 391.82 58.36 o 8 14 1 125.46 221.00 53.88 o 9 14 1 44.95 83.26 50.39 o 10 14 1 8.63 51.59 52.98 o 11 14 1 29.06 93.02 57.37 o 12 14 1 41.93 99.20 60.45 o 1 15 1 394.15 382.16 60.56 o 2 15 1 343.40 359.25 59.16 o 3 15 1 310.13 434.44 59.16 o 4 15 1 34.40 63.34 53.48 o 5 15 1 0.02 30.38 52.98 o 6 15 1 127.32 163.73 54.78 o 7 15 1 45.70 126.58 54.38 o 8 15 1 6.20 -31.97 53.88 o 9 15 1 4.73 16.83 57.37 o 10 15 1 0.03 -6.57 51.69 o 11 15 1 10.62 10.26 60.05 o 0 16 1 122.61 87.05 58.26 o 1 16 1 29.74 -29.18 56.57 o 2 16 1 190.86 186.04 58.26 o 3 16 1 67.98 -35.95 56.57 o 4 16 1 23.33 36.65 57.37 o 5 16 1 0.17 49.40 54.28 o 6 16 1 0.99 32.17 53.88 o 7 16 1 17.51 110.25 53.88 o 8 16 1 3.82 -37.35 59.56 o 9 16 1 3.72 -8.27 56.97 o 1 17 1 96.21 156.86 58.26 o 2 17 1 50.28 102.68 62.25 o 3 17 1 0.03 -22.81 58.66 o 4 17 1 329.95 445.99 61.85 o 5 17 1 2.41 24.20 56.07 o 6 17 1 112.48 8.17 59.16 o 7 17 1 2.14 -40.04 55.67 o 8 17 1 70.71 80.07 59.56 o 0 18 1 338.96 368.51 65.73 o 1 18 1 4.53 113.74 59.56 o 2 18 1 513.90 476.18 68.42 o 3 18 1 176.04 204.17 64.84 o 4 18 1 485.80 532.05 70.12 o 5 18 1 149.19 304.96 61.35 o 6 18 1 232.23 272.79 65.73 o 1 19 1 0.03 -48.90 60.85 o 2 19 1 12.75 14.44 58.26 o 0 0 2 20355.14 21394.88 187.94 o 1 0 2 62620.28 56740.73 355.89 o 2 0 2 33897.37 32810.13 286.59 o 3 0 2 3336.49 3373.00 65.12 o 4 0 2 444.44 385.28 26.79 o 5 0 2 173.84 196.71 26.29 o 6 0 2 10458.23 10277.58 165.51 o 7 0 2 621.37 677.92 36.06 o 8 0 2 38.39 56.87 28.09 o 9 0 2 58.14 6.08 32.87 o 10 0 2 235.20 242.32 38.15 o 11 0 2 924.37 968.56 52.69 o 12 0 2 119.71 122.40 45.12 o 13 0 2 600.38 445.11 52.69 o 14 0 2 23.08 -39.94 45.61 o 15 0 2 317.50 325.48 57.47 o 16 0 2 216.32 165.93 55.18 o 17 0 2 98.21 110.55 53.48 o 1 1 2 1385.29 1350.60 30.80 o 2 1 2 140.20 140.34 20.22 o 3 1 2 32301.64 33881.10 335.31 o 4 1 2 5824.81 5522.40 85.91 o 5 1 2 2574.01 2696.81 55.11 o 6 1 2 1543.04 1474.69 41.84 o 7 1 2 3845.78 3982.73 78.74 o 8 1 2 206.27 166.03 31.57 o 9 1 2 903.89 886.01 43.93 o 10 1 2 26.93 84.65 35.95 o 11 1 2 837.46 785.88 50.10 o 12 1 2 37.87 133.06 42.53 o 13 1 2 1062.12 1134.70 63.65 o 14 1 2 76.30 106.57 46.91 o 15 1 2 41.55 58.96 47.81 o 16 1 2 3.11 47.71 51.69 o 17 1 2 49.00 5.78 55.67 o 0 2 2 2031.64 2331.65 47.46 o 1 2 2 2985.89 3225.45 60.45 o 2 2 2 764.69 815.94 28.19 o 3 2 2 2834.35 2732.23 54.93 o 4 2 2 29.73 61.05 25.40 o 5 2 2 2109.75 2042.75 48.63 o 6 2 2 5208.89 5314.11 88.24 o 7 2 2 874.81 913.92 39.15 o 8 2 2 471.74 471.51 35.16 o 9 2 2 12.81 3.39 32.87 o 10 2 2 128.50 55.08 35.95 o 11 2 2 516.53 436.35 49.60 o 12 2 2 63.04 39.24 43.82 o 13 2 2 71.78 52.98 46.41 o 14 2 2 100.82 116.13 48.60 o 15 2 2 60.46 24.90 51.29 o 16 2 2 31.01 -8.86 52.59 o 17 2 2 137.87 160.45 57.86 o 1 3 2 22406.84 22895.13 264.35 o 2 3 2 3069.58 2667.83 54.24 o 3 3 2 27.95 32.67 25.00 o 4 3 2 54.82 40.54 25.89 o 5 3 2 134.07 145.01 27.59 o 6 3 2 4799.33 4764.99 85.04 o 7 3 2 2.36 -1.20 29.38 o 8 3 2 157.06 157.36 33.27 o 9 3 2 506.67 570.22 43.43 o 10 3 2 43.87 69.02 38.54 o 11 3 2 174.05 211.74 44.72 o 12 3 2 61.83 57.57 44.72 o 13 3 2 859.84 899.31 60.56 o 14 3 2 42.08 20.82 50.39 o 15 3 2 3.91 -4.28 50.79 o 16 3 2 17.58 -49.10 51.69 o 17 3 2 10.13 33.56 56.97 o 0 4 2 9520.48 10399.08 158.98 o 1 4 2 8933.39 9556.74 155.13 o 2 4 2 6974.99 6961.20 107.39 o 3 4 2 19699.31 19908.85 289.70 o 4 4 2 32.58 30.08 25.00 o 5 4 2 868.47 769.01 34.76 o 6 4 2 380.87 360.16 33.37 o 7 4 2 3316.29 3415.85 72.25 o 8 4 2 58.83 39.34 34.66 o 9 4 2 149.75 81.87 38.15 o 10 4 2 95.27 95.41 39.84 o 11 4 2 0.01 -31.07 41.23 o 12 4 2 63.98 -10.96 44.22 o 13 4 2 8.20 129.27 49.50 o 14 4 2 263.69 266.22 50.00 o 15 4 2 0.08 28.09 48.20 o 16 4 2 43.11 31.37 53.48 o 17 4 2 10.70 24.60 52.19 o 1 5 2 1334.90 1588.52 43.24 o 2 5 2 378.05 400.90 29.38 o 3 5 2 2525.72 2663.38 54.11 o 4 5 2 12898.44 13446.88 220.33 o 5 5 2 1031.16 1109.60 40.04 o 6 5 2 1389.10 1293.95 43.63 o 7 5 2 38.61 54.88 30.67 o 8 5 2 355.22 365.93 37.75 o 9 5 2 1.51 31.57 37.25 o 10 5 2 929.94 1024.84 54.48 o 11 5 2 24.16 58.46 42.92 o 12 5 2 5.80 -24.00 44.72 o 13 5 2 0.43 10.26 46.91 o 14 5 2 0.91 23.70 46.41 o 15 5 2 327.96 428.76 57.87 o 16 5 2 0.05 68.72 52.59 o 0 6 2 55.55 94.81 27.59 o 1 6 2 658.50 567.08 32.47 o 2 6 2 447.29 484.37 31.57 o 3 6 2 8804.05 8924.37 142.39 o 4 6 2 1352.53 1502.68 47.12 o 5 6 2 6266.26 6099.62 103.60 o 6 6 2 123.61 150.79 34.16 o 7 6 2 2193.77 2249.89 58.28 o 8 6 2 481.05 568.02 43.92 o 9 6 2 3367.60 3256.59 78.71 o 10 6 2 560.92 563.54 49.10 o 11 6 2 0.43 -20.82 46.01 o 12 6 2 142.27 128.98 49.10 o 13 6 2 31.56 15.54 46.91 o 14 6 2 7.27 37.15 50.00 o 15 6 2 146.57 131.96 54.38 o 16 6 2 11.76 -13.84 51.69 o 1 7 2 248.45 232.96 31.97 o 2 7 2 983.96 1104.02 41.84 o 3 7 2 2581.54 3204.83 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