#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180794 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012585.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012585_Fobs loop_ _publ_author_name 'N\"ather, Christian' 'Je\&s, Inke' _publ_section_title ; catena-Poly[[bis(nicotinamide-\kN^1^)copper(I)]-\m-thiocyanato-\k^2^N:S] ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m190 _journal_page_last m192 _journal_volume 58 _journal_year 2002 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9304 _cell_length_b 21.3533 _cell_length_c 7.5895 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.8113 _cod_data_source_file ln1135Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CuSCN-Bis(Nicotinsaureamid) in Pnma (ij331)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 232.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4053.29 4026.37 65.80 o 4 0 0 8212.21 8470.32 125.55 o 6 0 0 10251.52 11108.98 354.39 o 8 0 0 2836.39 2928.17 67.90 o 10 0 0 4248.25 4101.83 79.71 o 2 1 0 2295.16 2155.24 19.03 o 4 1 0 175.28 144.34 10.84 o 6 1 0 1866.30 1962.72 12.40 o 8 1 0 635.17 676.48 25.68 o 10 1 0 344.10 401.09 13.64 o 0 2 0 9101.50 7599.81 227.31 o 2 2 0 13434.07 11266.29 161.02 o 4 2 0 9757.18 10087.59 105.39 o 6 2 0 4552.86 4360.20 97.40 o 8 2 0 2284.78 2371.08 57.98 o 10 2 0 1216.12 1188.17 38.62 o 2 3 0 3669.13 3567.08 55.53 o 4 3 0 2211.97 2269.77 38.28 o 6 3 0 3430.00 3569.87 37.56 o 8 3 0 1189.08 1261.56 17.40 o 10 3 0 856.76 871.74 21.75 o 0 4 0 9151.69 8082.63 115.67 o 2 4 0 54184.73 59570.93 729.56 o 4 4 0 12042.86 12531.39 234.28 o 6 4 0 8985.63 9251.14 101.55 o 8 4 0 4430.45 4379.86 35.75 o 10 4 0 242.02 245.71 11.78 o 2 5 0 29527.54 32796.04 284.50 o 4 5 0 566.76 620.49 22.84 o 6 5 0 79.78 64.53 11.08 o 8 5 0 250.72 216.61 11.39 o 10 5 0 730.44 738.64 19.12 o 0 6 0 30592.17 30271.71 716.19 o 2 6 0 3265.39 3007.75 40.82 o 4 6 0 18034.78 18744.75 265.04 o 6 6 0 8307.66 8436.82 101.84 o 8 6 0 590.76 566.15 13.71 o 10 6 0 1274.31 1190.97 36.71 o 2 7 0 962.93 1058.46 13.61 o 4 7 0 2031.34 1906.96 39.87 o 6 7 0 2480.96 2430.96 52.05 o 8 7 0 207.65 247.16 11.72 o 10 7 0 1334.71 1362.86 22.10 o 0 8 0 8623.40 8796.93 31.50 o 2 8 0 2822.94 2400.45 54.73 o 4 8 0 20466.84 21747.38 293.11 o 6 8 0 7545.06 7833.25 91.81 o 8 8 0 486.14 493.50 13.32 o 10 8 0 951.86 919.65 13.34 o 2 9 0 201.88 221.30 9.75 o 4 9 0 2795.18 2940.67 47.22 o 6 9 0 557.30 559.93 13.05 o 8 9 0 780.27 811.87 21.23 o 10 9 0 222.49 248.81 14.25 o 0 10 0 41444.33 48450.15 974.93 o 2 10 0 14847.73 15476.45 126.24 o 4 10 0 3421.51 3447.26 37.21 o 6 10 0 3828.97 3834.96 52.56 o 8 10 0 3105.15 3030.16 104.51 o 10 10 0 706.44 700.29 19.63 o 2 11 0 8.88 4.62 7.73 o 4 11 0 99.60 113.14 11.16 o 6 11 0 1868.55 1994.43 26.94 o 8 11 0 234.72 220.95 11.11 o 0 12 0 9927.72 10804.22 382.76 o 2 12 0 3849.18 3842.92 54.82 o 4 12 0 2843.93 2690.79 30.04 o 6 12 0 1914.61 1915.28 26.92 o 8 12 0 1021.12 1052.00 19.67 o 2 13 0 420.99 430.78 9.85 o 4 13 0 818.22 811.07 17.68 o 6 13 0 5387.61 5319.48 146.40 o 8 13 0 93.15 128.26 11.21 o 0 14 0 18445.53 19035.03 98.25 o 2 14 0 8171.28 8350.03 164.82 o 4 14 0 2527.15 2546.31 25.32 o 6 14 0 4092.29 4103.97 92.66 o 8 14 0 1879.53 1905.25 13.02 o 2 15 0 14.22 19.15 9.98 o 4 15 0 639.40 655.63 21.24 o 6 15 0 13.30 -10.26 14.53 o 8 15 0 95.95 66.38 11.74 o 0 16 0 3873.19 3815.48 77.04 o 2 16 0 2916.92 2974.83 39.21 o 4 16 0 1740.38 1766.77 36.28 o 6 16 0 978.75 989.60 17.28 o 8 16 0 896.27 862.93 26.09 o 2 17 0 0.13 32.93 11.48 o 4 17 0 1158.18 1121.29 14.92 o 6 17 0 129.07 171.68 11.90 o 8 17 0 128.24 52.66 15.70 o 0 18 0 3420.52 3367.31 219.69 o 2 18 0 872.56 859.10 16.82 o 4 18 0 6399.83 6468.81 46.04 o 6 18 0 3023.93 3053.54 35.01 o 8 18 0 59.65 58.22 72.46 o 2 19 0 742.04 709.72 14.29 o 4 19 0 92.28 83.00 10.42 o 6 19 0 26.48 23.17 12.93 o 0 20 0 2963.01 3033.84 50.38 o 2 20 0 1437.82 1508.83 19.41 o 4 20 0 1222.86 1180.71 15.78 o 6 20 0 1106.02 1146.67 30.49 o 2 21 0 136.20 133.09 11.25 o 4 21 0 408.87 381.38 13.28 o 6 21 0 32.49 28.87 15.50 o 0 22 0 310.71 305.15 15.59 o 2 22 0 2001.73 2032.17 52.11 o 4 22 0 741.98 757.93 16.61 o 2 23 0 227.83 207.22 15.17 o 4 23 0 0.39 6.80 13.99 o 0 24 0 2877.60 2913.93 140.11 o 2 24 0 517.07 551.18 12.36 o 4 24 0 446.65 439.52 26.31 o 2 25 0 14.10 17.53 13.99 o 0 26 0 1847.63 1754.85 27.29 o 1 0 1 7447.52 5974.59 85.80 o 2 0 1 6837.79 6356.15 494.18 o 3 0 1 163.61 124.42 12.59 o 4 0 1 237.75 193.14 10.76 o 5 0 1 6.86 9.90 9.98 o 6 0 1 374.67 434.52 10.57 o 7 0 1 481.28 494.42 14.48 o 8 0 1 28.09 11.91 14.61 o 9 0 1 471.60 482.97 11.41 o 10 0 1 90.02 111.53 24.03 o 0 1 1 11929.19 10150.82 183.65 o 1 1 1 2990.96 2859.04 46.87 o 2 1 1 9068.07 7653.71 49.07 o 3 1 1 7.98 8.19 8.71 o 4 1 1 5316.15 5256.41 34.55 o 5 1 1 10.39 20.59 8.79 o 6 1 1 2984.98 3040.25 24.21 o 7 1 1 205.41 219.56 8.65 o 8 1 1 1134.19 1126.57 14.93 o 9 1 1 728.79 710.85 8.27 o 10 1 1 568.87 546.84 11.02 o 1 2 1 285.26 296.66 11.57 o 2 2 1 743.18 670.45 14.07 o 3 2 1 3559.37 3809.92 49.39 o 4 2 1 901.10 902.78 13.36 o 5 2 1 102.25 105.96 8.84 o 6 2 1 1530.16 1601.89 16.17 o 7 2 1 0.23 -8.13 8.13 o 8 2 1 440.64 456.20 11.02 o 9 2 1 642.65 608.71 8.86 o 10 2 1 309.13 305.21 8.07 o 0 3 1 2980.30 2663.42 89.34 o 1 3 1 4547.91 4574.75 133.38 o 2 3 1 2055.81 1837.18 19.33 o 3 3 1 558.46 443.49 8.33 o 4 3 1 7145.15 7335.31 33.72 o 5 3 1 2610.13 2761.45 29.38 o 6 3 1 2623.39 2586.31 33.82 o 7 3 1 21.43 6.73 8.15 o 8 3 1 584.24 582.47 8.27 o 9 3 1 727.20 719.20 8.47 o 10 3 1 395.86 367.35 8.80 o 1 4 1 15231.92 13998.83 207.98 o 2 4 1 87.88 65.91 7.72 o 3 4 1 284.35 292.01 7.89 o 4 4 1 7.07 -0.72 12.24 o 5 4 1 66.69 60.71 8.70 o 6 4 1 118.24 124.80 7.48 o 7 4 1 118.12 133.44 10.67 o 8 4 1 94.27 98.50 7.90 o 9 4 1 196.55 208.47 8.92 o 10 4 1 97.69 121.29 12.69 o 0 5 1 41517.47 43021.71 345.19 o 1 5 1 3754.69 4051.63 41.23 o 2 5 1 14137.45 14462.42 96.16 o 3 5 1 979.08 909.36 9.82 o 4 5 1 1566.32 1449.90 20.83 o 5 5 1 506.38 450.44 8.29 o 6 5 1 2515.45 2455.10 31.84 o 7 5 1 359.62 406.24 12.62 o 8 5 1 2180.38 2156.13 23.70 o 9 5 1 4.65 -1.38 9.40 o 10 5 1 343.03 360.85 10.30 o 1 6 1 609.11 590.54 9.56 o 2 6 1 64.00 86.96 6.90 o 3 6 1 979.22 1141.82 10.40 o 4 6 1 95.19 82.12 5.98 o 5 6 1 396.39 422.89 7.47 o 6 6 1 373.07 370.17 6.65 o 7 6 1 383.50 373.41 8.89 o 8 6 1 77.49 103.50 11.44 o 9 6 1 3.31 3.79 7.29 o 10 6 1 171.18 184.39 10.48 o 0 7 1 24.01 14.06 11.49 o 1 7 1 26.48 18.37 7.81 o 2 7 1 5256.58 5230.75 55.87 o 3 7 1 8536.61 9032.00 116.29 o 4 7 1 3587.48 3517.52 35.01 o 5 7 1 1947.77 1942.02 23.59 o 6 7 1 1115.15 1135.48 12.13 o 7 7 1 175.61 180.57 7.21 o 8 7 1 637.42 672.85 9.70 o 9 7 1 119.62 130.41 10.89 o 10 7 1 403.66 392.92 11.12 o 1 8 1 1126.30 1167.79 15.36 o 2 8 1 318.44 331.93 6.87 o 3 8 1 264.47 307.63 11.04 o 4 8 1 15.75 27.45 6.54 o 5 8 1 218.11 233.34 6.95 o 6 8 1 985.51 977.74 15.54 o 7 8 1 290.39 312.64 7.65 o 8 8 1 271.30 253.69 7.07 o 9 8 1 120.54 106.58 7.83 o 10 8 1 123.76 138.24 9.95 o 0 9 1 16710.13 17412.88 226.40 o 1 9 1 302.00 258.78 7.72 o 2 9 1 4348.52 4392.57 49.81 o 3 9 1 650.72 716.08 7.13 o 4 9 1 4263.00 4363.38 42.44 o 5 9 1 2127.21 2113.69 15.01 o 6 9 1 3303.14 3290.70 43.11 o 7 9 1 195.82 189.12 7.13 o 8 9 1 698.24 705.07 11.47 o 9 9 1 318.30 320.36 7.58 o 10 9 1 360.97 339.37 9.08 o 1 10 1 1238.10 1315.91 17.63 o 2 10 1 921.14 846.72 14.40 o 3 10 1 443.56 515.78 8.63 o 4 10 1 362.15 378.31 7.15 o 5 10 1 27.76 27.41 6.72 o 6 10 1 284.80 326.07 12.24 o 7 10 1 422.27 430.38 8.91 o 8 10 1 36.10 33.06 7.43 o 9 10 1 0.36 -2.74 9.77 o 10 10 1 76.39 76.66 11.07 o 0 11 1 4828.59 4864.15 59.55 o 1 11 1 1974.73 1932.79 26.34 o 2 11 1 1713.93 1630.96 16.47 o 3 11 1 686.01 639.96 10.29 o 4 11 1 2117.65 2056.65 25.29 o 5 11 1 359.23 362.64 7.39 o 6 11 1 1000.95 1012.48 15.65 o 7 11 1 206.33 214.19 9.71 o 8 11 1 412.36 392.83 9.72 o 9 11 1 525.75 529.87 8.56 o 1 12 1 714.00 777.19 14.30 o 2 12 1 134.26 122.93 7.43 o 3 12 1 666.06 648.50 9.91 o 4 12 1 814.43 754.17 9.39 o 5 12 1 6.62 -2.04 8.08 o 6 12 1 331.45 345.68 9.74 o 7 12 1 0.47 -6.38 8.51 o 8 12 1 150.35 150.00 8.02 o 9 12 1 81.29 94.41 9.88 o 0 13 1 661.83 607.14 13.19 o 1 13 1 1280.80 1257.91 19.55 o 2 13 1 2866.98 2832.19 28.68 o 3 13 1 1041.33 1064.36 11.15 o 4 13 1 3441.94 3378.94 51.84 o 5 13 1 519.08 489.95 8.01 o 6 13 1 1473.09 1466.91 13.28 o 7 13 1 363.76 393.09 10.57 o 8 13 1 478.62 493.92 16.78 o 9 13 1 325.54 362.71 12.90 o 1 14 1 225.91 225.62 8.84 o 2 14 1 341.38 324.63 7.02 o 3 14 1 234.59 236.28 6.52 o 4 14 1 303.70 272.17 12.23 o 5 14 1 21.47 10.02 7.96 o 6 14 1 175.97 176.41 9.08 o 7 14 1 294.90 253.77 8.13 o 8 14 1 16.37 19.27 8.31 o 9 14 1 1.34 23.52 8.54 o 0 15 1 4307.95 4167.66 68.64 o 1 15 1 556.26 523.48 8.21 o 2 15 1 2898.91 2947.99 24.74 o 3 15 1 5.10 3.17 7.01 o 4 15 1 398.93 387.15 8.40 o 5 15 1 568.42 604.97 9.19 o 6 15 1 587.46 551.15 16.38 o 7 15 1 83.08 99.09 8.98 o 8 15 1 730.57 737.66 12.04 o 1 16 1 372.17 383.94 7.09 o 2 16 1 59.67 68.80 7.76 o 3 16 1 254.41 303.26 8.51 o 4 16 1 94.97 107.78 7.50 o 5 16 1 39.27 39.30 9.03 o 6 16 1 217.61 203.65 7.60 o 7 16 1 22.85 11.78 8.40 o 8 16 1 26.01 15.72 9.90 o 0 17 1 846.50 805.07 20.39 o 1 17 1 331.35 320.28 10.30 o 2 17 1 1095.66 1157.92 9.35 o 3 17 1 631.94 630.43 9.65 o 4 17 1 841.61 812.53 16.64 o 5 17 1 1078.31 1077.88 23.42 o 6 17 1 460.79 452.94 11.10 o 7 17 1 2.66 14.43 12.21 o 8 17 1 199.84 150.22 8.67 o 1 18 1 4.92 4.99 7.71 o 2 18 1 501.78 494.67 6.46 o 3 18 1 487.67 459.83 7.74 o 4 18 1 155.79 169.83 7.33 o 5 18 1 31.74 39.30 7.40 o 6 18 1 24.70 17.22 9.73 o 7 18 1 115.67 134.01 11.29 o 0 19 1 3188.02 3171.88 70.74 o 1 19 1 8.08 16.84 8.57 o 2 19 1 505.48 497.93 7.80 o 3 19 1 473.06 508.44 9.50 o 4 19 1 901.34 892.17 9.45 o 5 19 1 126.62 160.57 8.58 o 6 19 1 916.46 903.95 19.85 o 7 19 1 72.01 75.75 11.73 o 1 20 1 127.52 124.38 10.24 o 2 20 1 124.09 124.10 7.56 o 3 20 1 58.24 65.95 7.53 o 4 20 1 70.17 58.62 7.87 o 5 20 1 52.40 59.83 8.32 o 6 20 1 2.08 0.80 9.52 o 7 20 1 8.02 -6.77 36.34 o 0 21 1 650.25 623.95 34.11 o 1 21 1 141.61 148.19 7.92 o 2 21 1 429.21 435.01 7.68 o 3 21 1 498.53 486.55 7.22 o 4 21 1 379.91 389.12 10.31 o 5 21 1 602.03 594.34 10.14 o 6 21 1 108.71 95.92 8.86 o 1 22 1 319.96 310.80 7.69 o 2 22 1 48.66 38.62 7.44 o 3 22 1 144.22 141.21 8.44 o 4 22 1 2.07 2.98 7.81 o 5 22 1 5.96 13.25 11.52 o 0 23 1 5.71 -4.26 14.57 o 1 23 1 204.18 204.36 8.47 o 2 23 1 899.02 910.95 16.31 o 3 23 1 63.85 76.43 8.58 o 4 23 1 594.29 555.34 13.11 o 5 23 1 15.87 4.37 12.50 o 1 24 1 1.03 4.72 8.15 o 2 24 1 17.50 9.55 8.88 o 3 24 1 1.47 2.75 8.99 o 4 24 1 7.48 3.70 10.43 o 0 25 1 510.57 470.90 14.89 o 1 25 1 207.64 216.85 9.39 o 2 25 1 257.24 260.99 9.39 o 3 25 1 183.30 153.00 22.72 o 1 26 1 108.46 115.92 50.61 o 0 0 2 1856.95 2038.25 38.65 o 1 0 2 205.36 135.68 15.91 o 2 0 2 547.82 511.19 12.87 o 3 0 2 282.59 341.16 12.80 o 4 0 2 540.16 618.70 12.46 o 5 0 2 3530.93 3603.94 22.65 o 6 0 2 230.70 230.37 11.24 o 7 0 2 699.64 655.97 14.46 o 8 0 2 8.05 12.97 12.20 o 9 0 2 350.16 370.81 12.75 o 10 0 2 168.26 169.56 16.10 o 1 1 2 148.30 158.98 11.37 o 2 1 2 96.59 107.28 9.72 o 3 1 2 268.74 270.33 8.44 o 4 1 2 453.26 557.65 13.85 o 5 1 2 19.54 23.12 7.39 o 6 1 2 1726.25 1721.48 28.07 o 7 1 2 22.96 58.86 8.87 o 8 1 2 0.31 -8.33 8.33 o 9 1 2 120.79 125.08 8.86 o 10 1 2 55.79 51.70 12.48 o 0 2 2 9346.12 7986.26 208.59 o 1 2 2 7557.68 7251.43 224.25 o 2 2 2 15.59 11.70 8.79 o 3 2 2 11971.71 12757.21 212.02 o 4 2 2 220.37 256.91 17.65 o 5 2 2 3345.07 3352.21 33.73 o 6 2 2 161.15 153.08 7.49 o 7 2 2 631.62 658.44 10.01 o 8 2 2 117.75 106.93 7.73 o 9 2 2 1121.62 1083.12 15.51 o 10 2 2 34.06 56.88 10.60 o 1 3 2 55.42 42.89 10.49 o 2 3 2 4.43 1.28 8.50 o 3 3 2 79.19 80.15 7.61 o 4 3 2 1097.80 1167.54 7.63 o 5 3 2 4.94 -3.97 7.56 o 6 3 2 20.04 35.94 7.67 o 7 3 2 105.00 125.85 9.30 o 8 3 2 75.25 41.62 9.58 o 9 3 2 319.96 287.38 7.51 o 10 3 2 117.11 127.02 8.85 o 0 4 2 3996.33 3702.18 50.52 o 1 4 2 1764.36 1544.48 18.09 o 2 4 2 28.85 27.71 7.93 o 3 4 2 1623.45 1388.94 21.10 o 4 4 2 1106.86 1114.64 12.37 o 5 4 2 299.35 257.72 8.06 o 6 4 2 357.38 352.45 7.16 o 7 4 2 1238.78 1237.63 13.78 o 8 4 2 0.23 14.78 8.69 o 9 4 2 398.43 393.25 9.09 o 10 4 2 15.68 29.04 9.49 o 1 5 2 3072.21 3112.45 31.41 o 2 5 2 395.19 374.89 7.53 o 3 5 2 414.83 406.99 7.38 o 4 5 2 169.14 161.52 8.50 o 5 5 2 4.84 14.40 7.12 o 6 5 2 129.49 121.66 8.03 o 7 5 2 962.98 958.21 13.04 o 8 5 2 6.78 51.97 8.51 o 9 5 2 194.23 186.33 8.98 o 10 5 2 79.60 70.52 10.15 o 0 6 2 1247.95 1374.38 18.20 o 1 6 2 4196.85 4190.76 37.61 o 2 6 2 212.89 289.34 6.76 o 3 6 2 3283.23 3220.65 44.71 o 4 6 2 1698.00 1873.24 29.21 o 5 6 2 1900.06 1801.07 32.57 o 6 6 2 641.49 643.15 7.06 o 7 6 2 1413.40 1358.13 17.00 o 8 6 2 86.19 84.92 7.25 o 9 6 2 552.22 558.37 10.25 o 10 6 2 18.67 9.05 10.31 o 1 7 2 364.51 352.78 6.92 o 2 7 2 3804.00 4136.48 42.43 o 3 7 2 206.11 173.38 6.40 o 4 7 2 127.12 150.35 8.17 o 5 7 2 6.49 8.18 7.05 o 6 7 2 126.29 125.61 8.94 o 7 7 2 140.43 138.23 7.21 o 8 7 2 51.68 34.64 7.91 o 9 7 2 207.22 186.67 7.81 o 10 7 2 211.44 209.69 10.06 o 0 8 2 450.39 420.59 11.50 o 1 8 2 4774.09 4710.81 45.00 o 2 8 2 342.15 380.14 8.16 o 3 8 2 3933.72 3873.10 29.06 o 4 8 2 60.55 54.57 6.99 o 5 8 2 1551.70 1559.15 17.82 o 6 8 2 192.98 188.10 8.22 o 7 8 2 240.14 259.40 7.40 o 8 8 2 9.53 10.87 8.55 o 9 8 2 737.90 710.58 14.66 o 10 8 2 2.22 -12.02 12.02 o 1 9 2 0.99 32.73 7.56 o 2 9 2 2.48 -6.35 6.35 o 3 9 2 932.56 1006.89 14.87 o 4 9 2 90.46 116.95 7.21 o 5 9 2 1.51 0.34 6.94 o 6 9 2 32.55 45.30 8.05 o 7 9 2 26.00 13.11 6.14 o 8 9 2 16.07 4.87 6.85 o 9 9 2 240.83 235.92 8.00 o 10 9 2 83.05 61.41 13.67 o 0 10 2 36.05 7.11 9.96 o 1 10 2 752.39 666.77 9.08 o 2 10 2 244.14 281.81 8.49 o 3 10 2 276.91 259.09 7.75 o 4 10 2 556.44 548.71 7.00 o 5 10 2 2738.10 2808.72 20.96 o 6 10 2 211.14 221.31 7.55 o 7 10 2 613.43 618.91 14.92 o 8 10 2 0.60 12.51 7.90 o 9 10 2 337.42 326.50 10.08 o 1 11 2 94.06 115.48 8.33 o 2 11 2 354.39 389.55 8.62 o 3 11 2 42.16 43.98 7.47 o 4 11 2 33.48 23.63 7.31 o 5 11 2 22.50 14.33 8.43 o 6 11 2 105.26 127.00 7.53 o 7 11 2 0.94 -8.13 8.13 o 8 11 2 59.13 63.25 8.56 o 9 11 2 0.56 -2.06 10.12 o 0 12 2 5536.24 6006.24 189.95 o 1 12 2 2921.62 2836.67 32.19 o 2 12 2 285.09 316.29 7.09 o 3 12 2 5030.30 5082.91 76.53 o 4 12 2 21.40 25.12 7.90 o 5 12 2 1853.88 1893.45 21.52 o 6 12 2 95.56 103.04 7.62 o 7 12 2 401.20 427.56 7.53 o 8 12 2 1.40 8.43 8.40 o 9 12 2 492.46 512.44 7.82 o 1 13 2 328.56 375.21 7.17 o 2 13 2 2.94 5.05 7.05 o 3 13 2 12.09 1.48 6.64 o 4 13 2 2.06 6.71 8.40 o 5 13 2 10.12 7.76 6.84 o 6 13 2 233.94 237.66 7.55 o 7 13 2 2.19 -0.17 7.67 o 8 13 2 0.44 20.78 8.26 o 9 13 2 64.49 60.18 8.29 o 0 14 2 1201.60 1234.92 44.77 o 1 14 2 693.59 677.51 8.35 o 2 14 2 41.30 49.26 7.28 o 3 14 2 940.31 920.02 10.90 o 4 14 2 13.94 13.88 7.75 o 5 14 2 17.35 30.83 7.98 o 6 14 2 6.31 -8.28 8.88 o 7 14 2 848.17 872.57 11.14 o 8 14 2 24.41 11.10 11.05 o 9 14 2 150.14 152.90 72.56 o 1 15 2 50.17 40.96 6.91 o 2 15 2 354.77 360.46 7.51 o 3 15 2 39.20 64.57 8.09 o 4 15 2 3.92 11.56 7.87 o 5 15 2 2.02 15.53 10.30 o 6 15 2 274.99 291.71 9.66 o 7 15 2 241.43 222.19 8.50 o 8 15 2 7.56 -3.01 9.13 o 0 16 2 0.03 12.94 17.54 o 1 16 2 1959.94 1919.06 38.28 o 2 16 2 105.30 134.91 8.14 o 3 16 2 1687.56 1681.49 25.74 o 4 16 2 1.33 2.38 7.85 o 5 16 2 1184.66 1199.13 24.56 o 6 16 2 78.31 77.88 8.36 o 7 16 2 465.34 456.95 13.16 o 8 16 2 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13.18 o 1 22 2 208.05 224.30 10.93 o 2 22 2 14.70 8.91 8.78 o 3 22 2 1267.56 1175.87 22.26 o 4 22 2 1.30 14.37 9.41 o 5 22 2 297.75 307.57 10.36 o 1 23 2 430.70 423.87 8.46 o 2 23 2 12.83 7.88 8.55 o 3 23 2 4.50 -2.74 9.54 o 4 23 2 18.16 35.82 8.86 o 0 24 2 55.26 34.07 13.04 o 1 24 2 307.62 315.51 12.38 o 2 24 2 16.61 2.44 9.03 o 3 24 2 169.50 169.99 8.29 o 1 25 2 0.94 -1.23 10.95 o 2 25 2 52.80 33.98 14.23 o 1 0 3 1024.51 1038.76 49.94 o 2 0 3 571.80 592.46 12.33 o 3 0 3 979.62 1044.77 13.55 o 4 0 3 426.11 447.65 13.78 o 5 0 3 31.66 32.66 12.42 o 6 0 3 18.53 18.36 9.78 o 7 0 3 279.69 259.47 11.01 o 8 0 3 78.54 62.77 13.98 o 9 0 3 1384.97 1416.22 20.24 o 10 0 3 78.25 101.78 15.62 o 0 1 3 24903.08 27750.00 430.46 o 1 1 3 5545.57 5335.66 39.65 o 2 1 3 4151.40 4086.27 33.97 o 3 1 3 2762.94 2663.90 17.59 o 4 1 3 5689.50 5916.21 60.67 o 5 1 3 3714.06 3817.78 48.41 o 6 1 3 3199.68 3262.71 42.93 o 7 1 3 1514.32 1441.29 13.00 o 8 1 3 826.08 808.28 13.60 o 9 1 3 285.62 271.08 8.61 o 10 1 3 761.01 750.08 19.15 o 1 2 3 767.52 793.44 9.91 o 2 2 3 40.71 24.07 8.04 o 3 2 3 488.17 487.10 11.62 o 4 2 3 730.00 664.80 9.21 o 5 2 3 421.66 396.10 6.90 o 6 2 3 1014.77 965.55 14.15 o 7 2 3 55.47 47.32 7.56 o 8 2 3 567.95 550.46 8.26 o 9 2 3 4.29 7.98 10.03 o 10 2 3 473.52 503.39 9.60 o 0 3 3 3298.47 3054.84 24.05 o 1 3 3 7271.42 7347.48 47.66 o 2 3 3 6231.13 6397.36 40.33 o 3 3 3 8499.21 8996.00 68.68 o 4 3 3 2091.33 2000.36 27.78 o 5 3 3 1284.64 1171.34 8.27 o 6 3 3 1954.89 1943.99 21.57 o 7 3 3 1327.87 1299.06 19.82 o 8 3 3 1250.97 1308.08 18.25 o 9 3 3 498.13 484.61 8.98 o 10 3 3 230.48 207.70 9.47 o 1 4 3 355.15 356.54 9.55 o 2 4 3 265.41 204.06 8.26 o 3 4 3 129.80 113.83 7.35 o 4 4 3 8.07 1.14 8.47 o 5 4 3 196.87 207.01 6.90 o 6 4 3 550.50 599.81 9.74 o 7 4 3 310.22 302.15 7.59 o 8 4 3 25.56 33.26 8.66 o 9 4 3 257.69 257.76 8.86 o 10 4 3 197.95 206.43 8.96 o 0 5 3 9456.33 9701.29 635.28 o 1 5 3 2125.14 1946.85 19.84 o 2 5 3 12622.58 13433.37 117.00 o 3 5 3 2512.74 2432.91 24.26 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246.93 7.72 o 9 8 3 47.42 52.28 9.07 o 0 9 3 11266.79 11789.55 142.65 o 1 9 3 4569.77 4568.76 33.46 o 2 9 3 3648.83 3614.46 39.85 o 3 9 3 292.42 243.92 7.38 o 4 9 3 5154.23 5303.31 72.60 o 5 9 3 1376.93 1318.69 15.19 o 6 9 3 2624.89 2642.11 27.76 o 7 9 3 870.52 903.14 15.14 o 8 9 3 629.53 637.53 8.52 o 9 9 3 339.87 318.05 11.26 o 1 10 3 245.24 258.52 8.58 o 2 10 3 5.27 4.99 8.21 o 3 10 3 75.82 49.41 8.25 o 4 10 3 215.30 224.48 6.75 o 5 10 3 32.58 64.52 7.53 o 6 10 3 2.15 -1.03 6.96 o 7 10 3 338.53 329.04 7.28 o 8 10 3 104.63 120.33 9.82 o 9 10 3 742.23 740.94 13.73 o 0 11 3 1847.09 1813.49 21.57 o 1 11 3 2494.19 2451.81 31.67 o 2 11 3 2906.70 2917.15 35.85 o 3 11 3 3349.86 3359.58 38.20 o 4 11 3 1260.28 1262.88 19.65 o 5 11 3 1371.15 1372.45 16.14 o 6 11 3 1140.08 1244.28 11.51 o 7 11 3 1444.92 1431.22 19.88 o 8 11 3 610.48 631.20 12.51 o 9 11 3 181.69 202.90 8.40 o 1 12 3 133.98 131.31 7.89 o 2 12 3 182.15 209.03 7.83 o 3 12 3 37.57 50.49 7.57 o 4 12 3 67.39 86.29 9.63 o 5 12 3 265.20 262.65 7.96 o 6 12 3 921.85 971.71 11.48 o 7 12 3 4.75 3.11 10.66 o 8 12 3 108.51 110.54 8.32 o 9 12 3 3.97 -1.17 10.42 o 0 13 3 3470.45 3415.60 95.51 o 1 13 3 1859.13 1865.79 17.76 o 2 13 3 2667.00 2766.31 27.65 o 3 13 3 2363.98 2322.98 18.81 o 4 13 3 1256.97 1248.61 18.63 o 5 13 3 358.30 369.91 8.11 o 6 13 3 1115.99 1122.09 13.26 o 7 13 3 593.61 559.25 9.27 o 8 13 3 601.99 580.61 10.61 o 1 14 3 376.27 372.77 7.23 o 2 14 3 7.24 -0.14 8.50 o 3 14 3 247.81 259.13 7.92 o 4 14 3 22.43 22.97 7.72 o 5 14 3 66.89 52.11 9.51 o 6 14 3 311.43 287.16 9.70 o 7 14 3 29.10 24.61 9.15 o 8 14 3 2.66 -5.53 8.70 o 0 15 3 4329.35 4287.74 110.11 o 1 15 3 906.45 944.38 13.60 o 2 15 3 1487.29 1491.03 10.05 o 3 15 3 892.88 919.50 8.53 o 4 15 3 1196.21 1229.46 10.55 o 5 15 3 1570.57 1514.38 34.00 o 6 15 3 900.46 884.11 20.96 o 7 15 3 998.74 1012.76 20.22 o 8 15 3 335.84 303.87 9.09 o 1 16 3 168.77 161.27 7.63 o 2 16 3 38.69 31.44 7.58 o 3 16 3 56.80 38.33 7.00 o 4 16 3 354.57 360.04 9.81 o 5 16 3 23.83 28.02 7.68 o 6 16 3 29.07 33.78 9.21 o 7 16 3 0.35 1.43 10.64 o 0 17 3 1449.29 1591.90 33.61 o 1 17 3 986.81 1013.91 9.61 o 2 17 3 699.64 686.36 9.11 o 3 17 3 1466.20 1466.11 19.73 o 4 17 3 541.58 553.77 9.34 o 5 17 3 766.06 748.34 14.00 o 6 17 3 450.82 448.20 9.27 o 7 17 3 199.30 204.68 10.08 o 1 18 3 91.95 90.40 7.55 o 2 18 3 0.05 39.55 7.59 o 3 18 3 337.22 317.14 8.43 o 4 18 3 122.43 114.74 7.37 o 5 18 3 66.09 67.04 8.37 o 6 18 3 7.33 42.91 11.91 o 7 18 3 1.00 0.12 10.08 o 0 19 3 1572.10 1570.11 45.22 o 1 19 3 1196.25 1198.37 14.20 o 2 19 3 824.60 837.47 17.04 o 3 19 3 152.44 161.32 8.02 o 4 19 3 1163.40 1155.07 15.09 o 5 19 3 203.69 229.83 9.06 o 6 19 3 625.20 590.25 9.68 o 1 20 3 5.61 -6.59 6.91 o 2 20 3 80.68 62.78 7.35 o 3 20 3 50.52 44.95 8.49 o 4 20 3 5.11 6.13 10.47 o 5 20 3 24.99 15.31 9.97 o 6 20 3 111.38 143.17 15.09 o 0 21 3 321.32 314.48 12.63 o 1 21 3 702.34 713.62 10.19 o 2 21 3 288.81 299.55 8.23 o 3 21 3 521.07 529.94 8.50 o 4 21 3 301.81 300.98 13.30 o 5 21 3 284.79 304.48 10.34 o 1 22 3 66.52 56.68 8.68 o 2 22 3 27.22 21.03 9.00 o 3 22 3 34.16 49.57 10.05 o 4 22 3 93.85 109.22 9.37 o 0 23 3 278.69 307.27 16.86 o 1 23 3 547.66 548.34 12.08 o 2 23 3 647.51 660.12 10.99 o 3 23 3 220.48 227.32 8.64 o 1 24 3 0.13 13.38 9.32 o 2 24 3 11.45 10.67 8.85 o 0 0 4 15348.01 16736.70 176.68 o 1 0 4 1057.69 918.95 15.65 o 2 0 4 7373.62 7831.98 66.02 o 3 0 4 771.65 728.15 12.63 o 4 0 4 4310.92 4446.38 33.46 o 5 0 4 3292.08 3327.30 25.80 o 6 0 4 2348.38 2347.59 29.24 o 7 0 4 707.91 689.13 15.35 o 8 0 4 996.82 976.18 24.97 o 9 0 4 6.02 2.39 9.95 o 1 1 4 532.04 591.37 9.49 o 2 1 4 188.58 191.92 9.08 o 3 1 4 328.50 303.02 8.56 o 4 1 4 60.21 61.46 7.47 o 5 1 4 73.60 65.34 7.24 o 6 1 4 3.49 9.80 8.54 o 7 1 4 69.82 56.08 8.62 o 8 1 4 160.99 169.63 7.64 o 9 1 4 174.22 176.85 8.98 o 0 2 4 23.55 -3.04 13.07 o 1 2 4 394.97 311.88 9.70 o 2 2 4 3414.14 3528.79 37.38 o 3 2 4 1891.86 1983.94 17.58 o 4 2 4 2455.20 2512.64 30.63 o 5 2 4 249.53 231.32 8.09 o 6 2 4 974.74 1031.01 9.52 o 7 2 4 124.94 109.37 9.12 o 8 2 4 717.93 698.37 7.56 o 9 2 4 36.56 46.75 8.62 o 1 3 4 1177.19 1367.14 17.59 o 2 3 4 124.81 160.99 10.00 o 3 3 4 1216.50 1327.37 13.40 o 4 3 4 788.58 782.41 10.06 o 5 3 4 778.67 776.03 13.48 o 6 3 4 122.00 118.39 8.14 o 7 3 4 0.72 28.69 10.57 o 8 3 4 421.44 402.97 7.25 o 9 3 4 219.88 220.76 9.61 o 0 4 4 4093.67 3836.15 123.23 o 1 4 4 2690.32 2651.34 44.70 o 2 4 4 8493.32 9095.18 64.65 o 3 4 4 598.98 533.70 9.59 o 4 4 4 3284.05 3417.17 30.05 o 5 4 4 290.13 309.35 8.70 o 6 4 4 1772.10 1856.40 14.31 o 7 4 4 958.00 1033.90 9.96 o 8 4 4 1606.46 1569.90 20.56 o 9 4 4 23.57 19.77 10.64 o 1 5 4 222.54 263.98 11.00 o 2 5 4 509.92 562.81 9.58 o 3 5 4 71.02 74.43 8.31 o 4 5 4 63.10 67.20 8.32 o 5 5 4 28.20 17.53 9.41 o 6 5 4 2.02 5.56 9.07 o 7 5 4 463.61 460.76 14.31 o 8 5 4 1.03 -2.72 8.24 o 9 5 4 349.53 338.90 11.43 o 0 6 4 3674.79 3750.04 261.16 o 1 6 4 2767.87 2952.67 27.30 o 2 6 4 3832.03 3847.99 33.62 o 3 6 4 66.66 54.34 8.21 o 4 6 4 1860.61 1842.61 21.78 o 5 6 4 486.84 498.07 8.43 o 6 6 4 1031.39 1105.64 15.24 o 7 6 4 285.61 278.23 8.54 o 8 6 4 978.96 1008.81 19.56 o 9 6 4 143.32 138.73 8.77 o 1 7 4 54.39 58.41 8.86 o 2 7 4 1.07 1.83 9.11 o 3 7 4 47.61 50.59 8.06 o 4 7 4 111.76 94.11 7.63 o 5 7 4 1068.61 1087.28 14.25 o 6 7 4 593.22 603.55 8.91 o 7 7 4 348.73 354.65 8.37 o 8 7 4 360.57 352.18 8.00 o 9 7 4 0.31 -0.13 9.00 o 0 8 4 876.77 843.32 18.34 o 1 8 4 1591.72 1569.88 17.88 o 2 8 4 4179.83 4285.00 53.20 o 3 8 4 602.94 647.20 10.86 o 4 8 4 2032.35 2079.41 29.22 o 5 8 4 4.55 -2.13 8.41 o 6 8 4 1063.26 1026.99 13.40 o 7 8 4 175.84 153.35 8.63 o 8 8 4 776.32 837.41 14.61 o 9 8 4 148.70 137.21 9.38 o 1 9 4 127.69 120.99 8.16 o 2 9 4 188.12 204.24 8.53 o 3 9 4 160.80 140.73 7.80 o 4 9 4 152.63 138.21 9.47 o 5 9 4 42.45 46.57 8.77 o 6 9 4 142.58 140.03 8.74 o 7 9 4 36.94 34.55 8.03 o 8 9 4 232.94 223.87 9.30 o 9 9 4 258.15 255.65 11.08 o 0 10 4 6548.34 6676.30 115.35 o 1 10 4 715.87 712.96 12.17 o 2 10 4 4086.50 4217.98 65.86 o 3 10 4 670.55 666.17 10.50 o 4 10 4 1608.92 1625.13 25.57 o 5 10 4 426.06 438.63 8.74 o 6 10 4 988.58 1015.28 13.04 o 7 10 4 970.64 942.41 13.86 o 8 10 4 827.45 778.73 11.01 o 9 10 4 21.64 -72.68 72.68 o 1 11 4 98.92 117.53 7.54 o 2 11 4 18.50 12.51 7.23 o 3 11 4 242.57 235.47 9.21 o 4 11 4 166.81 145.25 8.97 o 5 11 4 97.24 89.59 8.28 o 6 11 4 24.59 8.67 9.15 o 7 11 4 7.91 4.53 8.90 o 8 11 4 143.63 159.24 9.53 o 0 12 4 846.46 809.96 14.84 o 1 12 4 111.52 117.80 7.00 o 2 12 4 1033.86 1079.55 10.62 o 3 12 4 336.31 323.98 8.43 o 4 12 4 1436.82 1392.62 10.57 o 5 12 4 725.77 680.08 10.38 o 6 12 4 502.87 537.34 11.37 o 7 12 4 5.35 3.09 8.75 o 8 12 4 350.91 356.59 8.80 o 1 13 4 218.85 216.49 9.01 o 2 13 4 45.82 59.44 8.59 o 3 13 4 285.77 280.85 8.24 o 4 13 4 7.30 0.74 7.43 o 5 13 4 131.37 142.07 8.47 o 6 13 4 174.25 145.48 8.10 o 7 13 4 0.08 -6.20 9.05 o 8 13 4 43.76 54.49 9.75 o 0 14 4 635.91 627.38 13.81 o 1 14 4 511.05 479.34 8.61 o 2 14 4 4078.95 4181.83 46.34 o 3 14 4 204.26 192.00 7.49 o 4 14 4 1632.05 1664.08 24.43 o 5 14 4 443.09 413.11 12.31 o 6 14 4 1029.01 1005.84 18.01 o 7 14 4 171.56 171.67 10.20 o 8 14 4 763.17 744.81 40.56 o 1 15 4 2.31 -4.53 7.31 o 2 15 4 262.64 246.18 8.66 o 3 15 4 34.10 26.68 7.98 o 4 15 4 17.83 -8.31 8.31 o 5 15 4 0.12 2.72 8.42 o 6 15 4 26.28 24.29 10.18 o 7 15 4 27.38 28.26 10.39 o 0 16 4 167.83 167.97 10.89 o 1 16 4 43.21 42.44 7.94 o 2 16 4 1305.77 1295.88 14.64 o 3 16 4 458.80 432.52 9.10 o 4 16 4 602.02 613.88 8.43 o 5 16 4 4.83 -8.29 10.37 o 6 16 4 265.53 268.60 9.62 o 7 16 4 279.00 235.70 9.39 o 1 17 4 234.78 272.41 12.35 o 2 17 4 13.21 -9.09 9.09 o 3 17 4 17.93 22.26 7.48 o 4 17 4 177.61 156.68 8.86 o 5 17 4 266.74 264.75 9.66 o 6 17 4 34.39 21.43 9.09 o 0 18 4 1587.16 1640.79 35.72 o 1 18 4 655.54 678.90 10.06 o 2 18 4 493.92 500.47 8.83 o 3 18 4 0.62 7.61 8.69 o 4 18 4 1408.39 1415.82 10.54 o 5 18 4 17.71 27.69 7.81 o 6 18 4 679.83 675.88 10.14 o 1 19 4 3.42 11.83 7.60 o 2 19 4 24.82 17.52 8.55 o 3 19 4 5.19 -3.51 9.20 o 4 19 4 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