#------------------------------------------------------------------------------ #$Date: 2011-09-28 14:24:46 +0000 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://cod.ibt.lt/cod/hkl/2/01/31/2013197.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013197_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Glidewell, Christopher' 'Low, John N.' 'Melguizo, Manuel' 'Quesada, Antonio' _publ_section_title ; Two polymorphs, with Z' = 1 and 2, of 2-amino-4-chloro-6-morpholinopyrimidine in P2~1~/c, and 2-amino-4-chloro-6-piperidinopyrimidine, which is isomorphous and almost isostructural with the Z' = 2 polymorph ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o4 _journal_page_last o8 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 120.677 _cell_angle_gamma 90.000 _cell_length_a 13.8139 _cell_length_b 8.4804 _cell_length_c 19.8379 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7709 _[local]_cod_data_source_file sk1595IIsup4.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 269 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 198.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 191.52 151.16 3.66 o 3 0 0 15063.85 14241.31 417.99 o 4 0 0 7766.33 7691.85 226.63 o 5 0 0 39564.38 39360.13 1042.84 o 6 0 0 143.69 182.63 7.66 o 7 0 0 4175.31 4418.22 128.63 o 8 0 0 1340.78 1342.66 53.53 o 9 0 0 548.32 451.05 16.12 o 10 0 0 473.71 453.20 25.76 o 11 0 0 166.63 103.08 15.47 o 12 0 0 616.84 587.90 36.15 o 13 0 0 33.85 41.27 15.47 o 14 0 0 204.18 175.52 25.81 o 15 0 0 5.05 15.51 25.81 o 1 1 0 553.80 534.53 8.48 o 2 1 0 2012.05 1925.13 33.46 o 3 1 0 479.44 490.93 8.68 o 4 1 0 1577.17 1502.79 25.90 o 5 1 0 326.41 351.34 8.19 o 6 1 0 2496.32 2762.47 53.72 o 7 1 0 1208.07 1321.90 30.12 o 8 1 0 26.52 11.57 2.58 o 9 1 0 157.89 166.33 6.24 o 10 1 0 263.95 268.25 11.91 o 11 1 0 307.10 255.90 12.38 o 12 1 0 254.05 310.87 20.73 o 13 1 0 1704.03 1763.62 67.56 o 14 1 0 68.84 51.57 15.47 o 15 1 0 41.05 33.57 14.61 o 0 2 0 1569.85 1520.80 35.66 o 1 2 0 18107.37 16592.78 260.64 o 2 2 0 8483.49 8311.57 121.62 o 3 2 0 297.16 306.89 7.19 o 4 2 0 235.95 270.91 5.16 o 5 2 0 151.73 145.40 4.67 o 6 2 0 1881.97 1922.28 36.55 o 7 2 0 608.21 591.41 11.46 o 8 2 0 80.88 70.91 4.47 o 9 2 0 454.16 445.77 13.07 o 10 2 0 147.34 145.44 8.95 o 11 2 0 1076.62 1141.61 38.26 o 12 2 0 138.00 118.76 12.40 o 13 2 0 52.57 63.93 12.40 o 14 2 0 0.18 -1.49 12.40 o 15 2 0 524.62 490.09 29.68 o 1 3 0 240.64 243.73 4.29 o 2 3 0 2172.61 2132.63 32.39 o 3 3 0 7.60 1.33 2.66 o 4 3 0 119.32 129.28 3.32 o 5 3 0 691.59 668.32 11.65 o 6 3 0 5.29 9.53 2.28 o 7 3 0 218.35 195.36 5.37 o 8 3 0 269.75 269.85 7.37 o 9 3 0 1752.88 1668.17 37.83 o 10 3 0 279.73 251.75 18.05 o 11 3 0 178.26 145.26 10.97 o 12 3 0 72.86 56.83 10.97 o 13 3 0 21.12 15.51 15.51 o 14 3 0 1218.15 1169.86 99.32 o 0 4 0 608.57 521.48 16.79 o 1 4 0 1813.32 1741.35 26.13 o 2 4 0 47.02 55.52 2.14 o 3 4 0 238.54 235.20 4.29 o 4 4 0 837.52 837.42 16.82 o 5 4 0 771.78 792.18 13.55 o 6 4 0 1036.16 1019.42 17.56 o 7 4 0 192.65 203.77 7.39 o 8 4 0 36.24 41.79 4.70 o 9 4 0 203.08 231.24 16.31 o 10 4 0 540.62 503.01 20.63 o 11 4 0 615.73 600.45 25.66 o 12 4 0 175.45 186.25 14.64 o 13 4 0 73.85 81.28 15.49 o 14 4 0 2.68 7.40 15.51 o 1 5 0 23.05 15.16 2.36 o 2 5 0 1465.29 1530.29 33.24 o 3 5 0 96.92 112.95 3.51 o 4 5 0 295.52 248.47 7.01 o 5 5 0 5.80 7.89 2.38 o 6 5 0 9.04 24.35 4.06 o 7 5 0 884.63 968.55 21.15 o 8 5 0 478.42 492.17 19.13 o 9 5 0 386.87 349.72 17.20 o 10 5 0 0.07 -3.88 4.91 o 11 5 0 210.12 211.58 18.19 o 12 5 0 23.30 14.82 23.31 o 13 5 0 1.83 -15.56 15.56 o 0 6 0 71.36 68.04 3.02 o 1 6 0 446.72 462.48 9.30 o 2 6 0 45.34 53.41 2.43 o 3 6 0 18.24 24.31 2.71 o 4 6 0 8.20 7.15 2.76 o 5 6 0 3.49 8.72 2.73 o 6 6 0 320.53 330.73 8.74 o 7 6 0 207.17 189.18 11.71 o 8 6 0 265.44 250.57 9.65 o 9 6 0 188.73 177.05 11.05 o 10 6 0 5.32 -9.36 18.19 o 12 6 0 18.02 15.56 20.77 o 1 7 0 1.14 0.00 2.63 o 2 7 0 502.31 477.33 15.87 o 3 7 0 929.81 970.95 17.90 o 4 7 0 31.58 38.80 3.78 o 5 7 0 1135.08 1174.91 29.41 o 6 7 0 1268.37 1223.01 31.83 o 7 7 0 2.78 5.25 6.07 o 8 7 0 27.89 26.95 9.58 o 9 7 0 276.71 270.43 26.04 o 10 7 0 306.78 389.77 31.21 o 11 7 0 4.91 5.17 20.77 o 0 8 0 2372.17 2473.65 82.23 o 1 8 0 1616.24 1660.63 35.25 o 2 8 0 319.81 302.90 28.58 o 3 8 0 185.66 181.19 6.29 o 4 8 0 84.52 92.35 6.34 o 5 8 0 14.43 26.71 6.17 o 6 8 0 2453.55 2578.37 172.05 o 7 8 0 0.53 14.71 8.72 o 8 8 0 130.10 139.63 14.87 o 9 8 0 44.17 55.45 17.89 o 10 8 0 104.57 83.10 15.60 o 1 9 0 711.14 744.02 27.19 o 2 9 0 316.96 302.22 18.77 o 3 9 0 376.69 369.84 14.13 o 4 9 0 1267.98 1347.63 64.21 o 5 9 0 69.84 66.87 8.75 o 6 9 0 96.75 85.35 7.80 o 7 9 0 279.28 304.03 16.16 o 8 9 0 0.81 20.99 12.56 o 0 10 0 798.09 905.01 63.94 o 1 10 0 0.42 21.47 21.47 o 2 10 0 71.14 71.98 8.74 o 3 10 0 10.79 12.29 9.37 o 4 10 0 15.00 23.89 23.31 o 5 10 0 194.70 210.70 21.10 o 6 10 0 38.51 26.45 20.59 o -15 1 1 588.48 578.64 30.92 o -14 1 1 493.35 467.41 35.82 o -13 1 1 976.01 916.16 34.63 o -12 1 1 428.00 423.75 18.28 o -11 1 1 148.87 104.90 8.60 o -10 1 1 162.87 149.71 6.84 o -9 1 1 0.04 1.96 3.03 o -8 1 1 750.75 727.60 17.55 o -7 1 1 28.49 61.70 5.92 o -6 1 1 2142.16 2394.18 44.29 o -5 1 1 10.25 16.93 2.13 o -4 1 1 758.71 742.47 13.85 o -3 1 1 2776.81 2738.58 42.61 o -2 1 1 637.70 636.72 9.45 o 1 1 1 3135.78 3026.66 46.63 o 2 1 1 4229.45 4248.87 63.20 o 3 1 1 10066.49 9813.61 192.41 o 4 1 1 717.38 632.01 12.39 o 5 1 1 2062.36 2094.88 39.06 o 6 1 1 758.46 838.76 18.64 o 7 1 1 2873.22 3081.99 63.30 o 8 1 1 138.75 117.65 5.72 o 9 1 1 185.64 190.37 8.12 o 10 1 1 555.70 555.24 21.84 o 11 1 1 22.01 15.42 7.28 o 12 1 1 275.84 243.10 15.56 o 13 1 1 26.99 18.05 10.94 o 14 1 1 779.63 795.47 38.22 o -15 2 1 21.24 6.64 12.39 o -14 2 1 382.32 338.52 21.94 o -13 2 1 57.55 64.61 18.05 o -12 2 1 16.23 15.51 7.31 o -11 2 1 439.55 442.43 19.01 o -10 2 1 846.47 829.86 21.24 o -9 2 1 48.31 35.94 7.89 o -8 2 1 278.02 252.11 6.49 o -7 2 1 373.28 383.82 7.64 o -6 2 1 2138.70 2228.46 36.03 o -5 2 1 531.68 525.64 9.89 o -4 2 1 1122.63 1105.41 17.60 o -3 2 1 5034.39 4902.17 67.33 o -2 2 1 30.34 33.04 3.21 o 0 2 1 2837.92 2727.13 91.10 o 2 2 1 3837.40 3719.63 50.71 o 3 2 1 114.29 130.70 3.48 o 4 2 1 2250.47 2574.80 43.80 o 5 2 1 1435.20 1509.23 25.85 o 6 2 1 7703.60 7904.93 153.80 o 7 2 1 897.07 910.07 18.11 o 8 2 1 70.02 66.97 3.78 o 9 2 1 424.95 384.53 14.28 o 10 2 1 401.46 391.00 25.17 o 11 2 1 585.63 656.43 27.19 o 12 2 1 82.84 89.41 15.53 o 13 2 1 280.60 283.94 18.26 o 14 2 1 113.63 127.83 20.43 o -15 3 1 656.27 668.10 36.61 o -14 3 1 1.88 8.62 9.25 o -13 3 1 25.30 -2.59 12.93 o -12 3 1 585.96 581.71 25.62 o -11 3 1 638.42 585.88 34.67 o -10 3 1 1906.31 1859.20 51.61 o -9 3 1 553.75 520.62 13.48 o -8 3 1 184.00 186.85 6.00 o -7 3 1 507.05 519.16 11.32 o -6 3 1 264.91 278.53 6.44 o -5 3 1 98.13 117.79 3.76 o -4 3 1 1016.29 1039.56 16.95 o -3 3 1 4660.20 4615.70 73.56 o -2 3 1 152.18 219.41 4.52 o -1 3 1 740.82 684.56 11.79 o 0 3 1 1102.09 1105.05 18.44 o 1 3 1 3865.07 3995.63 57.61 o 2 3 1 1586.53 1648.11 29.17 o 3 3 1 2526.09 2607.96 43.74 o 4 3 1 850.52 843.13 13.73 o 5 3 1 1827.42 1910.54 36.76 o 6 3 1 229.17 219.47 5.81 o 7 3 1 2304.86 2297.54 42.85 o 8 3 1 5703.78 5981.71 125.16 o 9 3 1 297.07 264.56 10.83 o 10 3 1 17.88 44.57 10.36 o 11 3 1 398.44 392.37 21.90 o 12 3 1 32.75 30.98 10.95 o 13 3 1 542.84 584.84 48.33 o 14 3 1 917.47 818.90 43.92 o -14 4 1 609.01 650.25 46.35 o -13 4 1 115.66 85.46 14.62 o -12 4 1 1.10 -6.21 8.61 o -11 4 1 13.53 -1.03 6.91 o -10 4 1 2.51 -5.85 6.64 o -9 4 1 1583.29 1598.27 52.03 o -8 4 1 1801.65 1802.48 42.48 o -7 4 1 423.43 440.49 12.06 o -6 4 1 0.46 -0.44 2.25 o -5 4 1 1547.57 1471.86 23.09 o -4 4 1 1303.45 1467.63 26.29 o -3 4 1 1962.13 2079.88 36.34 o -2 4 1 922.28 853.15 13.05 o -1 4 1 3.32 2.63 2.63 o 0 4 1 473.62 420.51 7.52 o 1 4 1 13.48 10.23 2.15 o 2 4 1 2601.23 2767.25 49.73 o 3 4 1 791.60 694.76 12.05 o 4 4 1 753.59 862.58 13.65 o 5 4 1 96.92 80.63 2.90 o 6 4 1 33.40 37.71 2.89 o 7 4 1 34.82 24.14 4.69 o 8 4 1 18.71 24.25 6.00 o 9 4 1 139.49 133.57 10.15 o 10 4 1 0.07 -6.21 8.82 o 11 4 1 79.19 86.02 10.97 o 12 4 1 1040.36 1059.57 87.34 o 13 4 1 14.96 20.73 10.34 o -13 5 1 287.63 274.63 31.11 o -12 5 1 280.62 289.27 28.48 o -11 5 1 3.88 -4.16 8.64 o -10 5 1 543.98 535.36 23.69 o -9 5 1 2232.27 2319.11 75.85 o -8 5 1 1458.05 1461.25 36.97 o -7 5 1 14.62 16.50 2.71 o -6 5 1 20.78 21.46 3.79 o -5 5 1 20.54 22.71 2.29 o -4 5 1 2438.84 2385.25 41.40 o -3 5 1 40.94 31.46 2.15 o -2 5 1 739.84 743.19 12.68 o -1 5 1 1660.96 1601.64 31.91 o 0 5 1 218.23 185.95 4.29 o 1 5 1 345.66 319.35 5.35 o 2 5 1 1186.06 1253.87 22.40 o 3 5 1 1999.67 2046.38 37.47 o 4 5 1 766.64 753.29 14.24 o 5 5 1 1507.91 1480.99 27.20 o 6 5 1 1878.13 1905.72 36.47 o 7 5 1 1865.74 1899.09 50.18 o 8 5 1 3148.60 3338.26 83.63 o 9 5 1 396.54 377.47 21.12 o 10 5 1 32.39 38.37 10.36 o 11 5 1 271.26 292.48 16.24 o 12 5 1 13.83 12.97 11.00 o 13 5 1 322.99 300.30 31.07 o -13 6 1 27.51 25.94 25.94 o -12 6 1 77.36 119.33 20.77 o -11 6 1 3.02 5.17 15.56 o -10 6 1 417.82 445.44 20.03 o -9 6 1 226.78 221.08 46.21 o -8 6 1 21.17 27.24 5.67 o -7 6 1 429.77 445.86 11.82 o -6 6 1 102.17 92.11 5.28 o -5 6 1 1833.61 1827.37 55.02 o -4 6 1 0.20 3.35 2.75 o -3 6 1 12.23 13.02 2.31 o -2 6 1 5.93 5.67 2.11 o -1 6 1 1537.98 1557.85 82.45 o 0 6 1 1375.92 1469.76 31.65 o 1 6 1 118.29 127.46 4.46 o 2 6 1 270.54 263.62 7.08 o 3 6 1 46.49 48.75 2.29 o 4 6 1 569.69 595.28 13.67 o 5 6 1 867.48 809.17 29.02 o 6 6 1 837.55 859.16 19.12 o 7 6 1 128.94 135.97 6.28 o 8 6 1 755.92 704.35 32.98 o 9 6 1 69.48 62.32 15.60 o 10 6 1 6.22 7.30 15.60 o 11 6 1 375.27 415.16 36.33 o 12 6 1 681.02 752.06 62.28 o -12 7 1 0.09 -10.39 20.77 o -11 7 1 35.13 62.32 20.77 o -8 7 1 26.61 15.06 6.69 o -7 7 1 233.02 203.85 11.01 o -6 7 1 102.90 108.68 6.23 o -5 7 1 13.32 5.98 2.85 o -4 7 1 1.67 3.41 2.38 o -3 7 1 14.36 11.33 2.10 o -2 7 1 95.98 70.84 9.86 o -1 7 1 379.84 360.28 49.99 o 0 7 1 1062.23 1061.23 21.77 o 1 7 1 211.45 199.73 5.01 o 2 7 1 209.27 216.75 7.29 o 3 7 1 20.05 18.43 2.12 o 4 7 1 146.28 144.67 5.47 o 5 7 1 1585.23 1556.18 37.14 o 6 7 1 2.61 3.28 6.70 o 7 7 1 140.49 116.50 12.35 o 8 7 1 515.15 483.71 36.47 o 9 7 1 0.61 -5.22 15.60 o 10 7 1 30.53 31.16 15.60 o 11 7 1 24.16 46.72 15.56 o -10 8 1 190.05 186.97 20.77 o -9 8 1 58.75 59.48 12.62 o -8 8 1 27.62 31.56 16.11 o -7 8 1 6.16 10.71 16.02 o -6 8 1 128.60 135.41 11.24 o -5 8 1 9.85 19.98 4.60 o -4 8 1 35.33 35.66 7.54 o -3 8 1 195.88 185.77 6.46 o -2 8 1 438.16 443.49 9.88 o -1 8 1 111.23 106.75 3.47 o 0 8 1 539.29 405.69 116.16 o 1 8 1 822.38 825.85 19.54 o 2 8 1 120.87 106.38 5.74 o 3 8 1 27.34 22.05 6.83 o 4 8 1 1.23 2.15 4.09 o 5 8 1 704.40 678.39 23.42 o 6 8 1 256.76 230.32 14.95 o 7 8 1 133.50 133.27 12.59 o 8 8 1 1.00 3.16 8.70 o 9 8 1 51.96 45.85 12.67 o 10 8 1 2.20 10.39 20.77 o -9 9 1 629.38 628.99 50.76 o -8 9 1 388.83 384.23 36.38 o -7 9 1 0.02 -4.28 4.87 o -6 9 1 29.00 19.15 10.20 o -5 9 1 270.57 264.75 11.53 o -4 9 1 723.24 768.99 27.95 o -3 9 1 318.70 340.23 14.14 o -2 9 1 26.55 32.30 4.54 o -1 9 1 496.14 493.48 18.67 o 0 9 1 434.29 463.75 18.27 o 1 9 1 339.85 348.28 12.98 o 2 9 1 90.90 102.21 7.98 o 3 9 1 60.50 61.52 10.19 o 4 9 1 82.62 92.13 7.08 o 5 9 1 52.31 45.17 10.60 o 6 9 1 0.09 8.87 6.15 o 7 9 1 2.04 -1.80 10.71 o 8 9 1 95.35 99.09 25.11 o -6 10 1 0.02 0.00 15.56 o -5 10 1 502.16 463.26 34.32 o -4 10 1 680.70 733.93 37.22 o -3 10 1 0.27 3.51 9.37 o -2 10 1 163.92 157.16 15.97 o -1 10 1 5.25 2.84 8.08 o 0 10 1 74.61 64.12 16.02 o 1 10 1 45.22 32.32 16.16 o 2 10 1 8.41 21.70 21.70 o 3 10 1 85.82 81.57 21.74 o 4 10 1 2.53 3.17 8.74 o 5 10 1 42.30 42.97 12.62 o 6 10 1 114.00 133.13 15.79 o -16 0 2 30.35 25.81 25.81 o -15 0 2 166.29 170.48 20.68 o -14 0 2 635.92 589.20 41.41 o -13 0 2 1173.25 1297.63 57.01 o -12 0 2 253.81 253.35 20.68 o -11 0 2 210.24 191.35 15.51 o -10 0 2 1265.29 1324.67 42.19 o -9 0 2 313.21 330.19 13.34 o -8 0 2 3108.32 3284.34 95.87 o -7 0 2 218.59 191.98 10.36 o -6 0 2 8559.43 9362.74 265.06 o -5 0 2 1409.63 1301.45 38.49 o -4 0 2 2179.70 1916.57 42.73 o -3 0 2 4174.22 3914.66 85.70 o 1 0 2 6545.28 6319.03 160.98 o 2 0 2 3343.86 3307.56 107.59 o 3 0 2 30.59 30.51 3.59 o 4 0 2 473.35 474.68 15.96 o 5 0 2 3639.08 4203.18 113.59 o 6 0 2 4613.29 4875.65 142.62 o 7 0 2 5603.66 5878.11 188.54 o 8 0 2 521.92 582.07 24.60 o 9 0 2 802.62 717.35 35.92 o 10 0 2 657.43 564.41 35.96 o 11 0 2 624.94 693.57 36.01 o 12 0 2 657.91 689.33 41.22 o 13 0 2 800.43 824.03 51.57 o 14 0 2 51.10 41.22 15.47 o -16 1 2 146.44 138.35 19.84 o -15 1 2 486.54 548.63 30.92 o -14 1 2 795.57 828.32 34.63 o -13 1 2 2048.38 2087.65 67.12 o -12 1 2 283.78 282.94 18.17 o -11 1 2 302.28 278.09 12.76 o -10 1 2 129.13 126.60 14.28 o -9 1 2 1534.97 1441.92 29.22 o -8 1 2 176.16 193.25 6.22 o -7 1 2 699.60 822.89 15.24 o -6 1 2 707.78 694.11 12.86 o -5 1 2 665.36 732.71 11.02 o -4 1 2 1276.65 1242.71 18.95 o -3 1 2 1406.53 1342.13 19.90 o -2 1 2 272.33 295.12 3.54 o -1 1 2 77.57 60.64 2.63 o 0 1 2 3109.10 2974.87 44.20 o 1 1 2 12316.70 11692.72 188.29 o 2 1 2 13.34 10.18 3.61 o 3 1 2 1609.57 1481.20 27.30 o 4 1 2 2697.46 2821.27 50.80 o 5 1 2 536.24 559.86 10.46 o 6 1 2 4552.12 4861.48 90.61 o 7 1 2 334.11 335.67 8.15 o 8 1 2 1643.75 1608.76 38.09 o 9 1 2 89.92 93.52 7.53 o 10 1 2 18.22 8.56 12.83 o 11 1 2 443.63 512.31 48.66 o 12 1 2 0.74 6.18 8.57 o 13 1 2 766.27 763.28 51.66 o 14 1 2 1.04 13.27 12.39 o -15 2 2 165.42 168.65 16.16 o -14 2 2 22.43 -1.48 12.41 o -13 2 2 103.87 90.84 25.88 o -12 2 2 1084.20 994.18 34.67 o -11 2 2 164.12 151.08 9.71 o -10 2 2 103.62 101.15 5.65 o -9 2 2 123.85 143.16 5.03 o -8 2 2 622.30 634.05 12.89 o -7 2 2 857.18 840.80 13.82 o -6 2 2 187.85 201.05 4.76 o -5 2 2 500.12 608.81 12.17 o -4 2 2 6.80 5.28 1.87 o -3 2 2 6.54 5.35 2.39 o -2 2 2 5340.82 4919.30 320.33 o -1 2 2 2205.47 2125.39 39.79 o 0 2 2 1032.19 934.70 39.26 o 1 2 2 84.99 94.32 2.16 o 2 2 2 3.98 4.25 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23 834.46 863.02 33.85 o -12 3 23 269.31 236.17 16.89 o -11 3 23 292.00 278.70 17.58 o -10 3 23 54.66 60.65 9.78 o -9 3 23 211.86 216.15 14.00 o -8 3 23 89.99 107.97 10.75 o -7 3 23 5.24 2.09 10.77 o -6 3 23 247.11 252.47 18.13 o -5 3 23 22.91 34.00 10.76 o -4 3 23 20.71 36.54 10.74 o -3 3 23 43.64 47.59 12.59 o -12 4 23 0.01 -4.83 8.04 o -11 4 23 0.12 6.72 7.60 o -10 4 23 492.40 473.65 21.99 o -9 4 23 93.15 91.32 18.98 o -8 4 23 332.06 334.44 24.11 o -7 4 23 40.34 45.88 7.60 o -6 4 23 321.78 334.40 17.64 o -5 4 23 65.31 60.45 10.77 o -14 0 24 250.79 282.62 31.44 o -13 0 24 436.68 548.22 47.02 o -12 0 24 6.53 0.00 14.79 o -11 0 24 1513.10 1603.78 75.80 o -10 0 24 63.13 94.46 14.79 o -9 0 24 334.36 333.13 52.33 o -8 0 24 462.10 449.06 41.89 o -7 0 24 3.22 5.24 14.82 o -6 0 24 54.44 58.03 14.82 o -5 0 24 279.11 282.59 28.74 o -4 0 24 2050.08 2136.71 105.26 o -3 0 24 4.44 0.00 46.86 o -13 1 24 11.26 3.49 9.05 o -12 1 24 663.30 717.77 47.20 o -11 1 24 33.85 47.79 9.05 o -10 1 24 7.82 21.45 13.71 o -9 1 24 2.36 0.01 9.07 o -8 1 24 114.70 117.06 10.98 o -7 1 24 611.41 632.97 40.81 o -6 1 24 0.41 -7.64 9.58 o -5 1 24 13.76 19.19 12.07 o -4 1 24 195.32 204.18 23.52 o -13 2 24 152.04 172.19 14.48 o -12 2 24 0.07 -9.78 9.78 o -11 2 24 0.42 -10.44 10.75 o -10 2 24 105.38 105.17 12.06 o -9 2 24 221.85 213.80 13.85 o -8 2 24 32.33 29.34 10.77 o -7 2 24 71.20 65.81 10.79 o -6 2 24 4.48 9.72 8.82 o -5 2 24 104.55 114.61 26.00 o -4 2 24 0.23 -5.61 13.83 o -12 3 24 306.29 346.62 23.98 o -11 3 24 8.06 19.44 11.92 o -10 3 24 3.18 -2.60 10.72 o -9 3 24 6.76 -8.88 10.73 o -8 3 24 5.43 6.80 10.76 o -7 3 24 187.66 186.27 15.24 o -6 3 24 469.51 464.44 23.07 o -5 3 24 29.57 21.76 10.23 o -12 1 25 92.20 119.93 25.92 o -11 1 25 474.30 534.43 27.92 o -10 1 25 0.53 5.23 9.05 o -9 1 25 60.45 48.87 12.08 o -8 1 25 0.06 8.23 12.90 o -7 1 25 204.10 223.53 26.30 o -6 1 25 640.02 639.11 30.27 o -11 2 25 26.68 8.57 16.81 o -10 2 25 890.83 1056.24 39.98 o -9 2 25 573.09 566.14 38.12 o -8 2 25 9.68 12.92 16.73 o -7 2 25 354.03 376.92 20.88 o