#------------------------------------------------------------------------------ #$Date: 2011-09-28 14:24:46 +0000 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://cod.ibt.lt/cod/hkl/2/01/32/2013236.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013236_Fobs loop_ _publ_author_name 'Van\N:S-bis[(N-salicylidene-DL-valinato-\k^3^O,N,O')cuprate(II)] ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m190 _journal_page_last m192 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.128 _cell_angle_beta 72.381 _cell_angle_gamma 69.917 _cell_length_a 8.4753 _cell_length_b 9.5364 _cell_length_c 10.1210 _exptl_crystal_F_000 386.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file av1132Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jm_02_04 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 168.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 520.44 0.52 0.57 o 2 0 0 1100.82 959.40 167.66 o 3 0 0 36.74 24.20 1.15 o 4 0 0 1985.40 2032.47 27.92 o 5 0 0 3381.00 3468.67 27.35 o 6 0 0 1475.28 1504.67 30.87 o 7 0 0 9.99 10.14 2.78 o 8 0 0 19.89 19.05 3.47 o 9 0 0 953.74 909.14 13.84 o -8 1 0 27.74 26.39 4.65 o -7 1 0 131.01 130.06 6.38 o -6 1 0 3221.58 3330.41 140.30 o -5 1 0 19.18 16.95 2.69 o -4 1 0 426.91 355.28 6.59 o -3 1 0 4.34 7.67 1.22 o -2 1 0 1535.66 1522.76 87.54 o -1 1 0 275.04 128.89 85.00 o 1 1 0 1467.57 0.56 0.45 o 2 1 0 101.04 102.16 9.96 o 3 1 0 3104.37 3267.20 27.53 o 4 1 0 35.37 37.90 1.84 o 5 1 0 3085.22 3149.21 16.64 o 6 1 0 320.71 332.91 3.95 o 7 1 0 5.13 3.86 2.01 o 8 1 0 201.92 187.86 5.54 o 9 1 0 539.88 499.07 8.02 o -8 2 0 133.96 122.48 8.07 o -7 2 0 781.12 785.80 12.98 o -6 2 0 523.73 539.67 9.73 o -5 2 0 239.08 259.57 7.44 o -4 2 0 1197.56 1263.50 33.31 o -3 2 0 1401.29 1497.10 20.86 o -2 2 0 148.52 148.57 2.94 o -1 2 0 42.84 65.90 1.94 o 0 2 0 238.57 261.23 2.30 o 1 2 0 2377.87 2828.65 48.69 o 2 2 0 3521.37 3736.50 16.70 o 3 2 0 899.44 960.86 5.77 o 4 2 0 1.19 2.57 0.75 o 5 2 0 435.21 431.80 4.01 o 6 2 0 2742.11 2795.99 11.13 o 7 2 0 200.02 195.95 4.78 o 8 2 0 136.61 126.71 4.96 o 9 2 0 218.26 212.96 10.05 o -8 3 0 231.19 222.90 9.68 o -7 3 0 62.96 73.00 7.32 o -6 3 0 552.92 562.36 10.97 o -5 3 0 224.09 233.64 7.32 o -4 3 0 4217.21 4638.44 123.84 o -3 3 0 25.57 23.74 2.29 o -2 3 0 216.95 234.83 13.07 o -1 3 0 957.97 1075.36 7.79 o 0 3 0 6866.78 7480.36 43.61 o 1 3 0 1607.74 1704.14 33.57 o 2 3 0 113.49 82.99 1.83 o 3 3 0 410.84 468.74 3.06 o 4 3 0 537.57 625.49 16.77 o 5 3 0 5997.10 6421.73 26.38 o 6 3 0 35.84 31.64 2.22 o 7 3 0 343.18 344.22 4.39 o 8 3 0 341.97 314.91 9.19 o 9 3 0 829.08 806.31 13.53 o -7 4 0 165.32 179.68 8.59 o -6 4 0 890.75 923.67 13.90 o -5 4 0 114.05 109.47 6.06 o -4 4 0 2291.00 2477.24 16.91 o -3 4 0 193.54 206.33 6.23 o -2 4 0 26.75 33.17 1.73 o -1 4 0 9312.06 10866.74 182.15 o 0 4 0 3817.75 4476.61 44.65 o 1 4 0 1172.44 1229.66 12.44 o 2 4 0 71.39 110.16 3.30 o 3 4 0 549.41 540.23 4.00 o 4 4 0 326.24 365.96 3.22 o 5 4 0 2626.88 2754.40 10.83 o 6 4 0 14.06 15.00 2.56 o 7 4 0 1046.17 1086.71 8.99 o 8 4 0 411.17 408.86 6.91 o 9 4 0 214.89 209.89 8.76 o -6 5 0 88.04 85.86 6.98 o -5 5 0 5.21 5.66 3.27 o -4 5 0 65.32 78.71 5.83 o -3 5 0 191.08 166.26 23.61 o -2 5 0 819.18 731.12 122.15 o -1 5 0 489.03 437.68 70.57 o 0 5 0 44.81 52.05 2.64 o 1 5 0 247.55 220.56 4.39 o 2 5 0 2417.36 2530.41 65.67 o 3 5 0 93.93 102.35 1.96 o 4 5 0 747.41 792.01 16.62 o 5 5 0 50.78 47.56 2.91 o 6 5 0 29.25 26.31 2.83 o 7 5 0 1018.93 1056.03 9.15 o 8 5 0 331.55 321.29 6.54 o 9 5 0 3.46 4.15 2.60 o -6 6 0 0.36 2.90 4.25 o -5 6 0 11.00 11.20 3.45 o -4 6 0 2098.77 2284.81 19.10 o -3 6 0 1466.91 1541.22 14.50 o -2 6 0 718.50 632.30 88.82 o -1 6 0 7.68 12.28 2.14 o 0 6 0 104.42 98.34 11.33 o 1 6 0 2452.05 2539.01 167.95 o 2 6 0 1347.93 1413.87 54.99 o 3 6 0 710.65 757.49 15.25 o 4 6 0 24.67 25.31 1.58 o 5 6 0 988.33 1037.73 22.08 o 6 6 0 10.25 15.87 2.65 o 7 6 0 882.93 950.21 12.92 o 8 6 0 113.75 105.53 7.41 o 9 6 0 26.27 26.28 5.63 o -5 7 0 500.96 503.00 12.18 o -4 7 0 779.65 822.16 12.92 o -3 7 0 320.90 328.43 8.84 o -2 7 0 6.02 6.80 2.89 o -1 7 0 618.97 624.23 60.62 o 0 7 0 14.53 11.30 2.63 o 1 7 0 1773.91 1810.14 123.77 o 2 7 0 32.12 29.00 2.04 o 3 7 0 113.96 107.63 3.69 o 4 7 0 650.78 641.59 10.08 o 5 7 0 395.55 409.53 9.25 o 6 7 0 631.38 616.12 11.00 o 7 7 0 3.01 3.22 2.81 o 8 7 0 4.08 5.48 3.73 o -4 8 0 418.32 437.07 11.06 o -3 8 0 141.82 144.73 8.41 o -2 8 0 961.90 1041.09 13.58 o -1 8 0 57.13 45.53 6.16 o 0 8 0 278.74 256.75 25.67 o 1 8 0 94.84 88.33 5.37 o 2 8 0 1267.44 1209.46 12.81 o 3 8 0 1327.32 1364.67 14.33 o 4 8 0 561.50 565.95 10.17 o 5 8 0 8.77 6.72 3.22 o 6 8 0 452.99 448.58 10.34 o 7 8 0 1667.74 1699.97 18.38 o 8 8 0 0.27 1.95 3.73 o -2 9 0 506.69 508.60 10.83 o -1 9 0 120.26 147.37 6.40 o 0 9 0 169.64 161.90 6.92 o 1 9 0 1534.87 1460.73 14.13 o 2 9 0 2.93 5.11 3.27 o 3 9 0 733.19 723.29 11.57 o 4 9 0 241.22 229.19 7.98 o 5 9 0 27.76 24.81 4.71 o 6 9 0 635.51 682.11 13.01 o 7 9 0 1456.04 1443.21 17.43 o 1 10 0 968.97 927.23 12.61 o 2 10 0 331.49 328.66 8.84 o 3 10 0 593.99 559.92 10.85 o 4 10 0 23.42 22.14 4.31 o 5 10 0 18.69 16.20 4.97 o 6 10 0 1207.79 1320.85 17.00 o 3 11 0 479.93 481.69 10.80 o -5 -10 1 2.78 3.39 3.10 o -4 -10 1 102.80 104.04 6.92 o -3 -10 1 124.07 112.48 7.09 o -2 -10 1 35.14 33.89 4.74 o -1 -10 1 1262.56 1206.33 14.47 o 0 -10 1 57.33 58.55 5.14 o -7 -9 1 846.99 804.84 14.79 o -6 -9 1 91.64 85.98 6.69 o -5 -9 1 129.80 118.80 7.04 o -4 -9 1 9.42 7.50 3.45 o -3 -9 1 1237.16 1169.06 14.70 o -2 -9 1 688.01 653.45 11.14 o -1 -9 1 230.57 226.23 7.98 o 0 -9 1 1.27 2.23 1.85 o 1 -9 1 20.63 24.18 3.66 o 2 -9 1 2063.32 2136.03 19.33 o -7 -8 1 815.41 862.79 14.56 o -6 -8 1 1.24 2.73 3.02 o -5 -8 1 1.55 1.78 2.15 o -4 -8 1 454.25 439.45 9.30 o -3 -8 1 89.74 92.87 6.09 o -2 -8 1 625.48 578.99 10.02 o -1 -8 1 28.66 26.54 2.44 o 0 -8 1 272.26 249.68 23.71 o 1 -8 1 16.99 8.96 2.13 o 2 -8 1 821.51 815.51 110.76 o 3 -8 1 26.85 29.84 5.80 o 4 -8 1 73.25 72.54 7.04 o -8 -7 1 605.22 611.52 12.78 o -7 -7 1 236.33 253.88 8.64 o -6 -7 1 33.36 39.20 4.68 o -5 -7 1 181.65 189.36 6.83 o -4 -7 1 652.63 640.67 10.48 o -3 -7 1 285.63 282.97 7.27 o -2 -7 1 2666.29 2823.49 196.68 o -1 -7 1 507.21 503.15 36.00 o 0 -7 1 2.23 3.27 1.70 o 1 -7 1 351.71 348.00 39.34 o 2 -7 1 38.89 31.70 3.10 o 3 -7 1 214.94 193.58 23.26 o 4 -7 1 1166.71 1158.06 14.76 o 5 -7 1 291.87 280.94 9.85 o -8 -6 1 87.98 91.66 7.41 o -7 -6 1 1021.51 1047.61 13.81 o -6 -6 1 546.53 552.91 10.34 o -5 -6 1 412.31 402.64 8.76 o -4 -6 1 4.37 4.88 2.90 o -3 -6 1 122.88 115.51 5.70 o -2 -6 1 7735.39 7415.79 24.98 o -1 -6 1 518.23 515.34 45.37 o 0 -6 1 424.60 396.54 40.43 o 1 -6 1 26.39 26.19 3.37 o 2 -6 1 1381.21 1288.37 206.23 o 3 -6 1 739.24 679.57 94.98 o 4 -6 1 1507.30 1622.21 16.20 o 5 -6 1 16.79 17.06 4.22 o 6 -6 1 20.28 20.99 5.23 o -9 -5 1 74.40 76.27 6.98 o -8 -5 1 1228.78 1262.47 15.62 o -7 -5 1 159.72 158.66 6.58 o -6 -5 1 1252.44 1318.01 14.04 o -5 -5 1 85.98 94.38 3.39 o -4 -5 1 1010.97 1063.58 8.30 o -3 -5 1 307.55 288.58 6.85 o -2 -5 1 6283.29 6468.93 105.05 o -1 -5 1 848.09 947.09 27.17 o 0 -5 1 411.93 457.30 48.11 o 1 -5 1 1145.28 1081.36 157.01 o 2 -5 1 562.74 481.13 88.98 o 3 -5 1 2160.36 2017.46 311.73 o 4 -5 1 151.60 158.46 6.63 o 5 -5 1 142.46 137.90 7.47 o 6 -5 1 7.80 10.65 4.82 o -9 -4 1 385.44 373.86 10.63 o -8 -4 1 1230.23 1240.86 10.38 o -7 -4 1 59.03 52.97 3.99 o -6 -4 1 259.95 268.30 5.22 o -5 -4 1 813.89 812.71 6.52 o -4 -4 1 12.38 27.11 1.45 o -3 -4 1 454.86 423.14 4.77 o -2 -4 1 115.07 89.17 2.88 o -1 -4 1 143.17 154.67 11.36 o 0 -4 1 118.19 95.82 2.64 o 1 -4 1 6443.97 7652.35 92.78 o 2 -4 1 108.96 113.64 5.57 o 3 -4 1 1386.36 1527.04 12.69 o 4 -4 1 820.88 856.16 10.83 o 5 -4 1 14.23 15.16 4.14 o 6 -4 1 258.53 271.06 8.79 o 7 -4 1 38.54 36.04 6.63 o -9 -3 1 137.46 118.74 7.27 o -8 -3 1 173.61 162.28 7.44 o -7 -3 1 525.73 494.41 12.46 o -6 -3 1 2716.56 2896.18 31.39 o -5 -3 1 1333.82 1439.06 24.85 o -4 -3 1 85.25 88.72 4.73 o -3 -3 1 1813.48 2081.46 19.02 o -2 -3 1 3683.95 3735.88 22.45 o -1 -3 1 925.34 998.03 38.39 o 0 -3 1 1400.38 1355.88 29.95 o 1 -3 1 25.37 37.68 3.62 o 2 -3 1 524.93 602.28 5.03 o 3 -3 1 3769.19 3985.57 13.86 o 4 -3 1 1852.14 1972.56 88.10 o 5 -3 1 1522.49 1624.01 14.56 o 6 -3 1 62.85 58.70 4.91 o 7 -3 1 767.94 801.45 13.58 o 8 -3 1 41.38 42.44 6.66 o -9 -2 1 161.30 172.33 8.84 o -8 -2 1 331.43 330.08 6.39 o -7 -2 1 236.58 237.79 5.22 o -6 -2 1 2714.14 2752.44 8.08 o -5 -2 1 2.78 3.50 1.45 o -4 -2 1 5.35 18.75 2.10 o -3 -2 1 3258.63 3656.69 29.45 o -2 -2 1 10064.15 11368.86 277.68 o -1 -2 1 2823.74 3097.12 62.96 o 0 -2 1 349.30 255.38 4.28 o 1 -2 1 2734.67 3168.63 11.57 o 2 -2 1 13.05 12.81 2.73 o 3 -2 1 6629.75 7046.13 275.68 o 4 -2 1 16.12 20.66 1.85 o 5 -2 1 847.24 835.45 26.07 o 6 -2 1 393.72 397.09 9.16 o 7 -2 1 2450.36 2539.13 19.87 o 8 -2 1 354.19 355.51 10.08 o -9 -1 1 556.77 521.95 11.43 o -8 -1 1 416.20 412.98 7.10 o -7 -1 1 114.04 112.80 4.53 o -6 -1 1 381.67 369.62 4.54 o -5 -1 1 4.76 7.07 1.43 o -4 -1 1 1699.89 1898.40 12.34 o -3 -1 1 7773.76 8349.28 33.56 o -2 -1 1 1.26 3.26 0.90 o -1 -1 1 1087.97 761.87 458.69 o 0 -1 1 3225.22 3117.23 1652.17 o 1 -1 1 207.44 221.03 2.26 o 2 -1 1 812.78 854.28 58.38 o 3 -1 1 551.43 585.07 42.97 o 4 -1 1 117.13 128.62 2.50 o 5 -1 1 860.15 847.43 9.20 o 6 -1 1 997.75 990.42 56.56 o 7 -1 1 20.91 20.89 2.99 o 8 -1 1 617.36 619.42 11.43 o 9 -1 1 30.41 26.62 4.74 o -8 0 1 73.06 70.87 6.15 o -7 0 1 26.55 30.70 5.40 o -6 0 1 1888.60 1958.20 43.08 o -5 0 1 36.86 46.01 2.21 o -4 0 1 111.52 71.23 5.48 o -3 0 1 2.76 6.50 0.78 o -2 0 1 1810.40 1463.13 192.69 o -1 0 1 378.52 0.73 0.60 o 1 0 1 231.18 63.24 35.54 o 2 0 1 1406.32 1361.02 101.20 o 3 0 1 28.28 22.81 2.15 o 4 0 1 355.18 434.04 9.50 o 5 0 1 1084.37 1089.70 24.41 o 6 0 1 13.15 14.30 2.43 o 7 0 1 8.50 7.90 1.90 o 8 0 1 900.97 863.11 20.45 o 9 0 1 825.45 812.88 14.85 o -8 1 1 191.92 164.66 8.10 o -7 1 1 605.36 614.94 10.77 o -6 1 1 4289.75 4518.80 22.66 o -5 1 1 1568.48 1530.06 115.79 o -4 1 1 32.51 53.68 1.97 o -3 1 1 1255.62 1594.84 88.62 o -2 1 1 775.75 818.70 37.61 o -1 1 1 8044.17 4587.93 2424.15 o 0 1 1 1145.64 0.64 0.58 o 1 1 1 77.56 37.88 11.84 o 2 1 1 277.75 331.87 3.53 o 3 1 1 8682.49 9341.07 146.04 o 4 1 1 2376.62 2609.20 57.91 o 5 1 1 2458.30 2521.63 43.58 o 6 1 1 39.85 36.09 2.85 o 7 1 1 404.05 375.41 6.13 o 8 1 1 822.22 820.80 15.66 o 9 1 1 28.52 24.42 3.30 o -8 2 1 10.89 11.03 4.82 o -7 2 1 391.40 415.30 10.11 o -6 2 1 543.44 555.52 10.48 o -5 2 1 528.44 581.91 9.51 o -4 2 1 1515.82 1629.03 65.19 o -3 2 1 2047.73 2237.43 21.08 o -2 2 1 1454.45 1601.56 13.15 o -1 2 1 1939.14 2201.78 27.01 o 0 2 1 1460.13 1671.60 16.98 o 1 2 1 200.74 242.66 5.28 o 2 2 1 489.22 494.62 3.61 o 3 2 1 248.65 239.30 2.02 o 4 2 1 977.95 1081.57 11.66 o 5 2 1 1836.41 1945.40 8.26 o 6 2 1 564.40 583.47 5.87 o 7 2 1 95.30 98.08 3.74 o 8 2 1 119.26 107.54 6.89 o 9 2 1 62.73 59.76 6.09 o -7 3 1 54.69 60.76 6.92 o -6 3 1 180.26 174.97 8.18 o -5 3 1 1313.25 1378.49 13.87 o -4 3 1 3255.94 3325.58 37.39 o -3 3 1 215.05 212.49 19.31 o -2 3 1 34.48 26.91 2.54 o -1 3 1 1822.03 1976.66 14.15 o 0 3 1 549.69 615.94 6.04 o 1 3 1 8928.14 10123.49 108.95 o 2 3 1 374.16 454.94 5.05 o 3 3 1 283.04 327.65 5.12 o 4 3 1 1556.94 1695.26 39.50 o 5 3 1 4175.78 4289.19 17.92 o 6 3 1 1821.96 1902.97 20.31 o 7 3 1 1414.05 1424.95 13.81 o 8 3 1 96.39 93.24 6.58 o 9 3 1 22.61 12.92 3.68 o -7 4 1 137.51 142.46 8.96 o -6 4 1 502.33 519.05 11.34 o -5 4 1 702.17 713.06 11.03 o -4 4 1 95.70 102.95 5.80 o -3 4 1 12.92 11.87 1.53 o -2 4 1 577.94 569.19 34.88 o -1 4 1 6246.83 6950.92 59.52 o 0 4 1 1472.78 1660.34 27.35 o 1 4 1 1489.58 1536.67 36.68 o 2 4 1 1316.77 1595.64 33.63 o 3 4 1 2642.43 3035.54 44.28 o 4 4 1 4804.78 5298.53 84.62 o 5 4 1 1400.11 1499.73 23.70 o 6 4 1 855.89 922.45 7.78 o 7 4 1 278.55 290.23 5.97 o 8 4 1 1679.81 1697.87 15.88 o 9 4 1 170.66 148.72 8.76 o -6 5 1 135.34 135.57 7.87 o -5 5 1 503.54 505.44 10.65 o -4 5 1 412.85 409.27 8.73 o -3 5 1 275.53 292.13 7.58 o -2 5 1 1164.84 1046.35 58.12 o -1 5 1 2895.37 3352.96 115.28 o 0 5 1 630.02 683.05 6.76 o 1 5 1 1187.82 1249.92 35.56 o 2 5 1 330.37 294.15 7.04 o 3 5 1 114.62 118.62 1.61 o 4 5 1 1455.35 1443.49 21.55 o 5 5 1 26.47 26.09 1.82 o 6 5 1 0.97 2.29 1.64 o 7 5 1 122.20 131.65 4.46 o 8 5 1 96.47 95.08 4.72 o 9 5 1 239.62 225.08 8.62 o -6 6 1 81.94 83.59 7.09 o -5 6 1 720.34 745.03 13.01 o -4 6 1 1190.92 1251.42 14.56 o -3 6 1 1274.17 1437.41 14.42 o -2 6 1 685.97 744.62 10.42 o -1 6 1 120.83 105.17 10.54 o 0 6 1 10.11 7.15 1.89 o 1 6 1 2633.51 2693.18 143.71 o 2 6 1 453.42 511.59 22.01 o 3 6 1 277.71 301.74 4.26 o 4 6 1 1525.88 1608.60 10.79 o 5 6 1 446.92 447.56 5.84 o 6 6 1 1080.96 1151.52 8.56 o 7 6 1 56.99 67.83 4.02 o 8 6 1 76.62 76.86 4.61 o 9 6 1 15.09 13.38 3.12 o -5 7 1 1425.34 1456.74 17.83 o -4 7 1 12.00 11.80 4.82 o -3 7 1 664.29 724.61 11.57 o -2 7 1 147.65 152.95 6.46 o -1 7 1 912.62 990.98 11.52 o 0 7 1 2164.97 2320.78 185.19 o 1 7 1 997.58 1069.25 72.32 o 2 7 1 1070.07 1035.17 41.75 o 3 7 1 1296.68 1378.21 22.71 o 4 7 1 3698.44 3925.51 70.66 o 5 7 1 60.15 60.75 3.26 o 6 7 1 1940.90 2073.10 24.47 o 7 7 1 2.37 2.96 1.94 o 8 7 1 16.45 19.13 4.71 o 9 7 1 284.45 275.31 10.60 o -4 8 1 172.91 166.01 8.27 o -3 8 1 497.39 500.13 10.45 o -2 8 1 822.13 855.30 11.97 o -1 8 1 49.89 42.39 4.08 o 0 8 1 754.54 758.03 45.92 o 1 8 1 1.74 2.93 2.04 o 2 8 1 235.80 228.13 4.37 o 3 8 1 328.63 328.85 5.11 o 4 8 1 3264.95 3396.69 20.33 o 5 8 1 261.63 258.08 7.75 o 6 8 1 363.36 380.18 9.76 o 7 8 1 233.49 220.06 8.36 o 8 8 1 17.34 15.16 4.22 o -3 9 1 1495.24 1594.61 17.86 o -2 9 1 35.52 38.22 4.36 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o 6 0 10 403.94 469.58 48.70 o -2 1 10 68.21 68.81 6.58 o -1 1 10 109.36 108.46 8.07 o 0 1 10 867.32 947.39 14.01 o 1 1 10 285.21 317.84 10.14 o 2 1 10 1.81 1.58 2.70 o 3 1 10 9.39 12.29 3.70 o -2 2 10 427.65 465.47 12.26 o -1 2 10 233.01 239.27 9.51 o 0 2 10 560.34 577.78 11.92 o 1 2 10 6.62 9.51 4.02 o 2 2 10 23.10 21.80 4.71 o 3 2 10 95.92 100.05 6.60 o -2 3 10 3.85 4.74 4.11 o -1 3 10 2.47 5.46 3.65 o 0 3 10 390.10 385.44 10.60 o 1 3 10 475.94 451.71 11.08 o 2 3 10 1191.49 1152.52 14.21 o 3 3 10 2.40 2.38 3.27 o 4 3 10 0.71 2.12 1.74 o 5 3 10 23.41 23.66 4.71 o 6 3 10 683.30 739.91 12.00 o 7 3 10 12.46 10.08 4.57 o -1 4 10 2.85 2.35 3.70 o 0 4 10 1048.70 1071.71 15.36 o 1 4 10 2.10 2.46 1.53 o 2 4 10 892.75 932.08 24.68 o 3 4 10 11.65 11.89 2.39 o 4 4 10 375.28 372.48 9.75 o 5 4 10 424.18 417.54 9.02 o 6 4 10 135.89 143.35 7.21 o 7 4 10 467.73 455.53 10.68 o -1 5 10 239.20 263.76 10.74 o 0 5 10 577.75 585.96 13.21 o 1 5 10 9.45 8.98 2.60 o 2 5 10 419.53 413.99 15.87 o 3 5 10 150.91 156.29 5.42 o 4 5 10 0.51 2.85 2.04 o 5 5 10 468.79 458.89 16.80 o 6 5 10 94.75 94.97 6.83 o 7 5 10 16.58 13.12 5.31 o 0 6 10 156.03 165.09 10.02 o 1 6 10 6.88 5.43 2.44 o 2 6 10 606.28 605.00 9.17 o 3 6 10 1.70 2.61 1.82 o 4 6 10 179.51 163.00 6.72 o 5 6 10 698.84 685.79 22.51 o 6 6 10 421.75 421.57 14.37 o 7 6 10 212.47 211.30 9.73 o 1 7 10 389.45 406.77 8.00 o 2 7 10 822.48 839.00 10.17 o 3 7 10 428.74 413.54 8.08 o 4 7 10 129.08 120.19 6.89 o 5 7 10 690.97 675.98 26.75 o 6 7 10 109.66 104.14 5.27 o 3 8 10 15.80 18.00 3.52 o 4 8 10 27.22 30.97 3.86 o 5 8 10 345.13 329.96 7.77 o 0 -1 11 61.50 66.48 7.29 o 1 -1 11 23.09 61.03 21.78 o 2 -1 11 85.54 120.38 4.25 o 3 -1 11 688.93 770.92 46.72 o 4 -1 11 154.73 232.85 50.02 o 0 0 11 579.47 653.90 19.53 o 1 0 11 42.82 72.90 18.59 o 2 0 11 11.14 41.22 17.34 o 3 0 11 300.94 352.84 7.21 o 4 0 11 104.24 153.83 28.77 o 5 0 11 3.55 25.47 2.01 o -1 1 11 30.86 36.53 6.43 o 0 1 11 673.86 769.20 13.99 o 1 1 11 188.22 185.97 8.10 o 2 1 11 4.65 6.46 3.65 o -1 2 11 718.66 816.82 15.22 o 0 2 11 183.85 200.56 9.39 o 1 2 11 27.58 22.51 5.17 o 2 2 11 12.30 14.44 4.34 o 3 2 11 738.41 774.37 12.20 o 0 3 11 344.65 380.09 11.92 o 1 3 11 87.79 88.71 7.87 o 2 3 11 82.63 80.12 7.41 o 3 3 11 178.87 166.73 8.04 o 4 3 11 47.53 40.84 5.92 o 0 4 11 510.54 523.71 13.64 o 1 4 11 250.19 255.49 10.37 o 2 4 11 131.33 124.31 8.84 o 3 4 11 57.71 55.02 6.89 o 4 4 11 0.18 1.69 2.61 o 5 4 11 916.38 912.04 12.75 o 6 4 11 29.32 20.33 3.91 o 1 5 11 465.76 479.02 12.75 o 2 5 11 76.82 77.95 6.23 o 3 5 11 380.72 398.91 16.10 o 4 5 11 469.04 472.27 15.87 o 5 5 11 528.05 550.42 10.04 o 6 5 11 154.45 157.65 7.98 o 2 6 11 419.79 460.42 8.95 o 3 6 11 5.73 4.85 2.80 o 4 6 11 138.54 138.43 5.82 o 5 6 11 597.97 603.53 10.65 o 3 3 12 1.39 2.04 2.96 o