#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:45:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180802 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/33/2013316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013316_Fobs loop_ _publ_author_name 'Thinagar, S.' 'Velmurugan, D.' 'Shanmuga Sundara Raj, S.' 'Fun, Hoong-Kun' 'Gupta, S. C.' 'Merazig, H.' 'Bouacida, S.' _publ_section_title ; 3,3'-[o-Phenylenebis(methyleneoxy)]bis(6-chloroflavone) and 3,3'-propylenedioxybis[6-chloro-2-(2-furyl)-4H-1-benzopyran-4-one] ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o181 _journal_page_last o183 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.393 _cell_angle_gamma 90.000 _cell_length_a 13.2360 _cell_length_b 10.7990 _cell_length_c 21.7750 _exptl_crystal_F_000 1336.00 _reflns_d_resolution_high 0.7021 _cod_data_source_file na1583Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' velalg6 in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 352.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 917.35 1076.55 27.84 o 4 0 0 119181.29 115351.73 549.57 o 6 0 0 8478.33 9034.56 193.18 o 8 0 0 18786.51 20582.29 345.92 o 10 0 0 20.91 7.14 35.45 o 12 0 0 259.48 288.23 26.65 o 14 0 0 47.44 -22.24 64.71 o 16 0 0 1.29 -13.44 79.58 o 18 0 0 40.66 0.00 68.40 o 1 1 0 131.81 142.39 5.83 o 3 1 0 11431.25 11310.06 155.59 o 5 1 0 10060.15 10659.02 192.83 o 7 1 0 12188.68 12559.69 250.28 o 9 1 0 1317.33 1435.56 47.46 o 11 1 0 238.01 218.64 22.60 o 13 1 0 277.29 356.51 29.62 o 15 1 0 9.35 -24.62 65.07 o 17 1 0 19.67 -31.76 31.76 o 0 2 0 4424.98 4079.70 81.60 o 2 2 0 124135.88 119213.75 499.02 o 4 2 0 5505.73 5439.72 134.90 o 6 2 0 5733.46 6127.64 167.37 o 8 2 0 1155.11 1072.50 30.10 o 10 2 0 65.14 68.99 17.84 o 12 2 0 562.77 539.70 33.90 o 14 2 0 29.18 -34.02 70.78 o 16 2 0 7.84 -54.72 69.71 o 18 2 0 3.96 -32.71 76.73 o 1 3 0 77414.68 72076.04 427.17 o 3 3 0 700.66 882.06 24.74 o 5 3 0 6767.38 6973.42 179.98 o 7 3 0 2271.30 2509.84 71.25 o 9 3 0 1163.66 1322.55 40.56 o 11 3 0 234.61 195.33 25.69 o 13 3 0 209.63 150.95 28.31 o 15 3 0 5.57 12.73 77.68 o 17 3 0 2.83 -8.92 32.83 o 0 4 0 2491.26 2401.00 66.50 o 2 4 0 44.32 44.37 10.94 o 4 4 0 9679.71 9680.96 210.08 o 6 4 0 158.09 220.90 17.61 o 8 4 0 598.86 634.03 29.74 o 10 4 0 315.72 323.44 26.29 o 12 4 0 148.00 200.56 26.53 o 14 4 0 24.52 -12.01 24.15 o 16 4 0 2.82 35.69 25.58 o 18 4 0 0.77 -85.05 94.69 o 1 5 0 29.09 -8.33 36.04 o 3 5 0 18792.85 18996.97 303.10 o 5 5 0 84.38 94.81 15.82 o 7 5 0 894.13 874.20 33.78 o 9 5 0 13.70 12.37 18.68 o 11 5 0 601.16 628.92 37.95 o 13 5 0 2.38 34.50 52.70 o 15 5 0 44.30 0.00 74.94 o 17 5 0 23.63 18.91 38.18 o 0 6 0 1003.26 1157.32 34.85 o 2 6 0 126.14 139.53 15.58 o 4 6 0 2.45 11.54 45.44 o 6 6 0 22.37 1.90 17.61 o 8 6 0 30.63 92.19 19.63 o 10 6 0 88.01 96.00 24.27 o 12 6 0 82.37 75.06 26.77 o 14 6 0 0.98 -87.67 87.67 o 16 6 0 0.70 31.76 80.89 o 1 7 0 478.53 443.35 23.55 o 3 7 0 1954.62 1837.86 54.60 o 5 7 0 2033.61 2034.14 59.12 o 7 7 0 9.37 -19.51 19.51 o 9 7 0 25.30 4.04 19.27 o 11 7 0 90.09 78.87 26.29 o 13 7 0 19.71 -51.75 73.16 o 15 7 0 60.33 44.01 33.78 o 0 8 0 55.64 28.31 18.32 o 2 8 0 1521.83 1386.07 44.37 o 4 8 0 1341.63 1418.19 44.85 o 6 8 0 980.93 956.88 41.87 o 8 8 0 37.79 45.08 22.36 o 10 8 0 24.55 -70.18 70.18 o 12 8 0 35.95 27.48 27.84 o 14 8 0 0.77 15.11 106.11 o 16 8 0 6.42 -68.64 87.55 o 1 9 0 616.73 486.89 31.29 o 3 9 0 0.77 21.53 21.77 o 5 9 0 320.31 300.72 29.50 o 7 9 0 129.17 72.80 27.12 o 9 9 0 122.50 108.73 31.52 o 11 9 0 6.02 -51.75 65.90 o 13 9 0 4.14 30.21 93.14 o 15 9 0 8.10 -67.80 126.93 o 0 10 0 513.91 557.07 34.26 o 2 10 0 3.92 18.68 57.57 o 4 10 0 0.25 29.38 51.03 o 6 10 0 6.23 32.12 71.85 o 8 10 0 148.08 101.23 31.40 o 10 10 0 5.89 -22.60 28.91 o 12 10 0 60.44 45.68 132.04 o 14 10 0 6.17 -67.80 112.41 o 1 11 0 3.71 10.59 69.35 o 3 11 0 50.82 43.54 68.88 o 5 11 0 17.53 4.88 25.69 o 7 11 0 54.60 30.33 30.81 o 9 11 0 0.98 -30.45 30.45 o 11 11 0 2.96 0.00 36.16 o 13 11 0 0.02 5.71 40.92 o 0 12 0 70.42 47.58 75.18 o 2 12 0 31.60 37.83 23.32 o 4 12 0 12.52 17.84 24.27 o 6 12 0 34.77 -53.17 93.97 o 8 12 0 16.02 44.13 84.46 o 1 13 0 35.52 1.90 31.88 o 3 13 0 90.48 41.04 85.53 o 5 13 0 12.69 56.50 30.10 o 7 13 0 38.81 -93.50 107.89 o 9 13 0 76.36 -125.86 125.86 o 0 14 0 7.39 -95.28 95.28 o 2 14 0 50.73 30.81 94.93 o 4 14 0 0.10 -95.16 95.16 o 6 14 0 5.68 0.00 89.57 o 1 15 0 9.54 33.31 94.33 o 3 15 0 12.58 -84.82 125.86 o -17 1 1 0.47 -30.21 70.78 o -15 1 1 0.05 17.61 21.77 o -13 1 1 0.94 0.00 69.11 o -11 1 1 9.42 -8.09 47.70 o -9 1 1 324.61 396.00 24.39 o -7 1 1 3454.55 3954.68 101.23 o -5 1 1 5170.62 5198.72 136.80 o -3 1 1 55.12 30.93 7.73 o -1 1 1 505.98 540.30 16.06 o 1 1 1 92.04 76.73 5.35 o 3 1 1 48430.96 49269.63 326.53 o 5 1 1 1814.62 2110.27 63.52 o 7 1 1 0.91 1.19 10.94 o 9 1 1 568.03 606.20 28.55 o 11 1 1 225.12 207.82 24.39 o 13 1 1 0.35 -17.37 22.13 o 15 1 1 33.53 12.37 75.06 o 17 1 1 50.32 54.01 31.88 o -18 2 1 8.83 -104.68 104.68 o -16 2 1 48.91 35.09 32.47 o -14 2 1 190.99 210.43 26.17 o -12 2 1 8.13 -10.47 19.98 o -10 2 1 524.63 566.35 29.38 o -8 2 1 1669.61 1794.68 48.41 o -6 2 1 597.13 548.39 20.46 o -4 2 1 463.31 474.40 16.30 o -2 2 1 819.72 833.40 23.55 o 0 2 1 47519.32 42987.39 187.20 o 2 2 1 41657.66 40835.09 295.84 o 4 2 1 2275.71 2684.00 68.40 o 6 2 1 1.86 20.94 9.52 o 8 2 1 1074.00 1191.70 34.14 o 10 2 1 1007.33 1060.97 38.07 o 12 2 1 93.45 128.83 23.55 o 14 2 1 5.05 0.00 23.55 o 16 2 1 2.05 13.68 59.72 o 18 2 1 3.87 49.13 85.17 o -17 3 1 24.91 0.00 76.25 o -15 3 1 0.95 -25.58 67.57 o -13 3 1 15.14 -52.82 64.24 o -11 3 1 1152.64 1256.41 45.20 o -9 3 1 168.92 178.43 21.17 o -7 3 1 534.75 434.54 21.77 o -5 3 1 3233.19 3570.81 89.81 o -3 3 1 20526.46 20311.31 260.87 o -1 3 1 3810.72 3874.27 105.04 o 1 3 1 1882.72 1723.67 50.68 o 3 3 1 13178.23 12836.62 208.05 o 5 3 1 235.44 271.69 15.82 o 7 3 1 379.93 386.13 20.46 o 9 3 1 42.00 -34.85 48.77 o 11 3 1 182.92 204.48 24.74 o 13 3 1 1.78 -24.86 24.86 o 15 3 1 20.17 -12.85 68.99 o 17 3 1 91.90 104.68 34.02 o -18 4 1 1.80 31.17 37.23 o -16 4 1 4.19 29.38 27.36 o -14 4 1 76.75 79.11 25.46 o -12 4 1 522.69 529.59 35.81 o -10 4 1 629.30 575.27 32.59 o -8 4 1 57.45 47.23 19.03 o -6 4 1 1612.94 1602.21 50.79 o -4 4 1 60.05 90.17 12.97 o -2 4 1 207.40 251.71 14.87 o 0 4 1 2045.85 2251.61 61.08 o 2 4 1 774.16 962.59 25.10 o 4 4 1 4652.16 4649.86 103.61 o 6 4 1 189.73 115.62 16.89 o 8 4 1 693.82 809.97 33.31 o 10 4 1 53.68 -8.09 55.79 o 12 4 1 1.09 -9.87 21.89 o 14 4 1 0.05 -3.45 23.79 o 16 4 1 83.58 94.69 36.28 o 18 4 1 7.40 51.15 88.62 o -17 5 1 17.02 -85.77 85.77 o -13 5 1 216.54 225.18 30.10 o -11 5 1 32.07 43.54 22.60 o -9 5 1 1542.86 1753.76 58.29 o -7 5 1 30.72 32.71 50.32 o -5 5 1 6052.97 6476.42 137.75 o -3 5 1 12.80 -42.94 42.94 o -1 5 1 181.61 550.76 20.22 o 1 5 1 149.57 157.14 15.58 o 3 5 1 2912.58 2979.24 89.22 o 5 5 1 56.23 80.30 14.87 o 7 5 1 0.14 26.29 52.46 o 9 5 1 211.91 257.78 25.58 o 11 5 1 179.92 209.84 27.48 o 13 5 1 10.87 34.62 66.26 o 15 5 1 6.16 27.48 51.39 o 17 5 1 124.28 154.40 37.23 o -16 6 1 23.93 31.64 80.77 o -14 6 1 104.90 194.37 29.98 o -12 6 1 236.19 212.34 28.55 o -10 6 1 57.25 100.04 22.24 o -8 6 1 59.51 112.53 22.48 o -6 6 1 15.96 -6.66 39.61 o -4 6 1 7903.76 7759.12 222.21 o -2 6 1 0.00 -5.23 41.99 o 0 6 1 540.48 600.28 19.39 o 2 6 1 230.30 293.23 19.39 o 4 6 1 5345.16 5499.79 133.35 o 6 6 1 783.99 764.05 32.24 o 8 6 1 198.88 146.55 21.53 o 10 6 1 30.55 -28.07 66.85 o 12 6 1 4.88 0.00 77.68 o 14 6 1 1.27 0.00 72.56 o 16 6 1 72.97 0.00 110.03 o -15 7 1 20.70 -77.08 85.77 o -13 7 1 138.39 158.81 31.17 o -11 7 1 2.79 -11.06 75.66 o -9 7 1 2.23 -56.15 60.67 o -7 7 1 0.10 16.18 36.04 o -5 7 1 21.36 -61.26 61.26 o -3 7 1 105.84 119.19 19.75 o -1 7 1 86.95 87.91 17.72 o 1 7 1 385.51 451.44 22.96 o 3 7 1 48.72 19.15 50.68 o 5 7 1 1637.95 1498.01 43.66 o 7 7 1 100.26 146.55 24.50 o 9 7 1 6.02 34.85 20.34 o 11 7 1 5.87 4.76 24.62 o 13 7 1 51.13 49.96 27.36 o 15 7 1 4.14 24.27 31.88 o -16 8 1 22.04 2.85 42.71 o -14 8 1 26.10 10.82 29.50 o -12 8 1 0.04 -93.38 93.38 o -10 8 1 41.50 11.06 61.86 o -8 8 1 28.58 14.99 21.65 o -6 8 1 233.22 166.66 25.46 o -4 8 1 53.66 -30.57 70.78 o -2 8 1 54.57 97.66 22.01 o 0 8 1 42.31 -35.97 43.67 o 2 8 1 376.86 329.51 27.48 o 4 8 1 2.35 -68.28 68.28 o 6 8 1 282.19 269.79 30.93 o 8 8 1 1.73 0.00 66.50 o 10 8 1 47.12 -33.43 79.46 o 12 8 1 41.26 25.69 27.84 o 14 8 1 95.00 -30.33 88.62 o 16 8 1 40.38 -37.23 43.18 o -15 9 1 92.09 0.00 109.91 o -13 9 1 6.47 -90.64 90.64 o -11 9 1 1.63 -89.57 89.57 o -9 9 1 128.96 227.21 31.40 o -7 9 1 4.93 -10.11 64.71 o -5 9 1 62.68 -45.20 70.66 o -3 9 1 2202.24 2314.88 63.88 o -1 9 1 187.92 182.24 25.46 o 1 9 1 458.74 471.78 32.24 o 3 9 1 268.33 8.45 18.91 o 5 9 1 1889.70 1985.85 62.93 o 7 9 1 353.54 333.91 30.33 o 9 9 1 33.07 45.56 71.97 o 11 9 1 11.88 -77.68 77.68 o 13 9 1 9.98 -15.11 72.56 o 15 9 1 32.52 17.01 103.37 o -14 10 1 3.95 -22.60 40.68 o -12 10 1 0.61 43.54 29.38 o -10 10 1 0.72 -78.27 78.27 o -8 10 1 0.07 35.45 67.80 o -6 10 1 0.79 3.09 24.74 o -4 10 1 47.59 58.88 24.98 o -2 10 1 321.23 387.20 29.86 o 0 10 1 283.03 219.59 149.65 o 2 10 1 314.26 267.17 32.00 o 4 10 1 368.17 346.87 31.17 o 6 10 1 650.06 625.35 41.63 o 8 10 1 280.09 256.83 34.74 o 10 10 1 47.50 34.02 31.40 o 12 10 1 139.68 76.37 117.29 o 14 10 1 64.43 -33.90 79.58 o -13 11 1 18.13 -85.53 95.28 o -11 11 1 11.65 28.91 33.19 o -9 11 1 1.20 -75.06 75.06 o -7 11 1 34.17 21.41 26.53 o -5 11 1 7.01 -81.48 81.48 o -3 11 1 29.37 -10.94 74.70 o -1 11 1 154.88 104.32 27.60 o 1 11 1 56.21 13.56 24.98 o 3 11 1 138.34 123.12 27.84 o 5 11 1 78.15 49.37 25.81 o 7 11 1 93.61 0.00 96.71 o 9 11 1 66.86 72.56 32.24 o 11 11 1 47.75 22.24 37.23 o 13 11 1 16.05 -127.04 127.04 o -10 12 1 23.35 31.64 112.06 o -8 12 1 14.15 71.49 29.86 o -6 12 1 12.01 26.65 27.24 o -4 12 1 19.05 35.81 27.84 o -2 12 1 17.80 10.35 26.29 o 0 12 1 22.59 -24.44 41.37 o 2 12 1 46.01 -12.01 71.37 o 4 12 1 59.08 62.69 96.35 o 6 12 1 0.91 -26.65 84.22 o 8 12 1 98.69 14.75 96.59 o 10 12 1 4.49 31.76 97.78 o -9 13 1 12.02 0.00 107.06 o -7 13 1 21.77 46.75 97.31 o -5 13 1 0.11 44.01 31.40 o -3 13 1 15.03 0.00 31.05 o -1 13 1 0.34 13.44 81.60 o 1 13 1 8.38 40.21 83.74 o 5 13 1 0.01 -44.01 76.25 o 7 13 1 4.69 15.58 77.92 o 9 13 1 9.73 33.07 84.34 o -6 14 1 0.88 32.71 83.51 o -4 14 1 21.88 -7.97 37.47 o -2 14 1 2.13 0.00 75.54 o 0 14 1 83.19 50.49 25.92 o 2 14 1 15.04 30.81 78.63 o 4 14 1 36.03 34.38 37.95 o 6 14 1 0.75 -16.42 96.95 o -3 15 1 3.27 -91.48 91.48 o -1 15 1 9.97 19.51 37.47 o 1 15 1 1.35 -100.16 100.16 o -18 0 2 125.46 107.65 36.52 o -16 0 2 259.31 230.77 34.97 o -14 0 2 75.68 100.04 25.34 o -12 0 2 1239.74 1386.19 47.94 o -10 0 2 1693.65 1834.53 55.91 o -8 0 2 1166.58 1383.69 42.35 o -6 0 2 7393.99 8253.02 186.76 o -4 0 2 6415.33 6568.85 135.25 o -2 0 2 7.61 7.97 5.71 o 2 0 2 24801.65 23408.92 189.02 o 4 0 2 7862.78 8144.77 151.79 o 6 0 2 2616.50 2239.70 71.85 o 8 0 2 8644.75 8908.47 232.20 o 10 0 2 2485.45 2402.78 72.09 o 12 0 2 43.26 16.77 23.20 o 14 0 2 214.25 183.79 25.10 o 16 0 2 1.01 13.56 75.42 o 18 0 2 28.83 8.09 35.33 o -15 1 2 57.55 45.80 28.79 o -13 1 2 159.36 180.69 24.50 o -11 1 2 453.62 400.88 27.24 o -9 1 2 0.90 13.68 13.09 o -7 1 2 0.21 -1.19 10.71 o -5 1 2 2853.70 3418.31 79.94 o -3 1 2 2056.80 2137.63 50.56 o -1 1 2 739.77 587.52 17.96 o 1 1 2 19737.87 18487.72 155.24 o 3 1 2 33532.58 31959.09 270.62 o 5 1 2 5904.46 6183.55 152.03 o 7 1 2 3706.35 4201.99 107.18 o 9 1 2 977.78 1050.14 35.33 o 11 1 2 22.05 55.79 18.91 o 13 1 2 33.41 46.51 22.60 o 15 1 2 20.12 -61.98 75.42 o 17 1 2 1.31 10.82 29.03 o -18 2 2 9.82 -21.77 35.81 o -16 2 2 63.00 41.04 62.69 o -14 2 2 155.33 94.09 27.72 o -12 2 2 17.62 44.73 19.27 o -10 2 2 83.05 97.19 19.39 o -8 2 2 3137.64 3554.63 106.23 o -6 2 2 124.47 158.92 14.39 o -4 2 2 6779.61 7005.89 152.50 o -2 2 2 6.51 8.80 21.29 o 0 2 2 18958.74 17711.12 125.50 o 2 2 2 9210.92 9334.92 145.36 o 4 2 2 3851.42 3819.67 82.32 o 6 2 2 8.20 -34.38 34.38 o 8 2 2 2469.88 2671.27 77.92 o 10 2 2 306.47 322.49 23.91 o 12 2 2 12.15 -37.00 65.43 o 14 2 2 0.08 -34.26 59.36 o 16 2 2 0.01 -27.48 80.30 o 18 2 2 15.64 24.62 35.81 o -17 3 2 65.37 62.33 33.43 o -15 3 2 0.21 -25.58 67.69 o -13 3 2 93.76 127.16 23.79 o -11 3 2 651.30 799.02 37.35 o -9 3 2 14.13 -27.95 49.37 o -7 3 2 3.45 0.00 35.69 o -5 3 2 10156.35 11092.14 222.09 o -3 3 2 281.47 254.68 14.63 o -1 3 2 5849.28 5708.44 125.50 o 1 3 2 1220.85 1180.52 36.04 o 3 3 2 29205.24 29445.68 314.76 o 5 3 2 884.50 908.58 28.67 o 7 3 2 66.40 -22.13 41.52 o 9 3 2 2.58 -17.01 17.01 o 11 3 2 982.14 1064.18 43.06 o 13 3 2 21.07 -21.29 62.09 o 15 3 2 31.19 27.60 26.05 o 17 3 2 6.82 -26.88 32.47 o -18 4 2 0.04 -68.16 86.84 o -16 4 2 0.80 -4.16 28.55 o -14 4 2 11.48 84.46 22.36 o -12 4 2 703.15 648.66 38.42 o -10 4 2 358.03 316.78 27.36 o -8 4 2 857.73 831.14 32.95 o -6 4 2 1030.13 974.72 30.21 o -4 4 2 86.58 120.03 12.97 o -2 4 2 13505.45 13830.02 228.75 o 0 4 2 851.20 856.55 16.83 o 2 4 2 8291.35 8023.68 175.34 o 4 4 2 1792.14 1797.78 47.34 o 6 4 2 1134.83 1164.69 33.19 o 8 4 2 131.83 108.01 19.03 o 10 4 2 5.70 -49.25 56.86 o 12 4 2 385.66 374.59 30.81 o 14 4 2 134.84 0.00 72.68 o 16 4 2 124.40 145.84 34.50 o 18 4 2 3.33 45.56 33.19 o -17 5 2 0.46 -32.47 94.69 o -15 5 2 38.73 27.48 28.07 o -13 5 2 54.03 -11.54 73.87 o -11 5 2 280.90 321.66 26.17 o -9 5 2 968.78 1039.67 41.04 o -7 5 2 6.93 -46.15 57.81 o -5 5 2 193.68 182.72 16.42 o -3 5 2 1247.98 1104.74 32.95 o -1 5 2 4541.60 4341.88 100.16 o 1 5 2 3958.27 3768.63 92.90 o 3 5 2 1835.42 1777.08 50.20 o 5 5 2 3743.13 3818.12 108.25 o 7 5 2 510.37 586.57 29.62 o 9 5 2 545.10 603.58 32.59 o 13 5 2 60.30 84.46 26.41 o 15 5 2 7.72 41.40 71.61 o 17 5 2 16.75 40.80 38.54 o -16 6 2 0.48 -47.58 91.24 o -14 6 2 34.01 -26.53 83.74 o -12 6 2 52.79 28.79 24.74 o -10 6 2 473.41 462.98 32.83 o -8 6 2 3.69 -7.85 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