#------------------------------------------------------------------------------ #$Date: 2011-09-28 14:24:46 +0000 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://cod.ibt.lt/cod/hkl/2/01/33/2013337.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013337_Fobs loop_ _publ_author_name 'Centore, Roberto' 'Tuzi, Angela' 'Liguori, Dario' _publ_section_title ; Bis[N,N'-diisopropyl-N-(trimethylsilyl)benzamidinium] di-\m-chloro-bis[tetrachlorozirconate(IV)] dichloromethane disolvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m241 _journal_page_last m242 _journal_volume 59 _journal_year 2003 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.6100 _cell_length_b 17.3500 _cell_length_c 16.8320 _exptl_crystal_F_000 2560.00 _reflns_d_resolution_high 0.7576 _[local]_cod_data_source_file na1614Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zr in P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 595.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45677.71 54876.36 90.74 o 4 0 0 125775.37 121372.95 190.44 o 6 0 0 99197.89 91780.03 208.86 o 8 0 0 2207.79 2437.49 66.49 o 10 0 0 46448.55 44206.45 198.29 o 12 0 0 3206.21 2377.59 89.31 o 14 0 0 28521.20 28011.56 203.99 o 16 0 0 32659.65 32794.80 242.26 o 18 0 0 35423.16 35914.91 275.71 o 20 0 0 9464.26 8959.85 185.04 o 22 0 0 321.74 347.49 72.97 o 24 0 0 56.07 70.77 80.04 o 2 1 0 370.95 526.88 21.21 o 4 1 0 5191.42 5484.87 50.92 o 6 1 0 18.05 76.00 25.25 o 8 1 0 2687.62 3010.25 68.57 o 10 1 0 1267.88 1280.33 70.47 o 12 1 0 18578.08 19446.15 157.29 o 14 1 0 2300.49 2345.03 103.04 o 16 1 0 54.55 -59.24 106.72 o 18 1 0 159.42 107.02 65.96 o 20 1 0 1075.23 1175.70 88.48 o 22 1 0 161.25 137.26 130.67 o 24 1 0 112.27 194.13 85.33 o 0 2 0 28212.29 38054.94 87.53 o 2 2 0 355127.25 343925.38 275.06 o 4 2 0 3709.80 3361.78 48.19 o 6 2 0 1328.32 1203.39 53.30 o 8 2 0 578.55 501.63 43.91 o 10 2 0 4497.67 3904.35 85.15 o 12 2 0 15225.64 14272.70 143.44 o 14 2 0 71.63 43.02 87.17 o 16 2 0 13933.21 13951.89 176.00 o 18 2 0 14380.84 14639.50 194.84 o 20 2 0 2143.89 2063.50 136.31 o 22 2 0 26.42 -32.27 71.19 o 24 2 0 444.64 521.36 88.06 o 2 3 0 722.97 879.01 33.99 o 4 3 0 17141.68 21409.11 99.17 o 6 3 0 1228.12 1555.87 57.10 o 8 3 0 5824.62 5973.25 84.73 o 10 3 0 8.42 32.21 63.46 o 12 3 0 5169.85 5345.18 107.55 o 14 3 0 286.40 348.44 49.44 o 16 3 0 880.70 881.09 67.03 o 18 3 0 1136.32 1214.38 103.87 o 20 3 0 385.58 365.67 67.15 o 22 3 0 99.22 125.32 70.59 o 24 3 0 134.12 197.40 87.17 o 0 4 0 3025.81 2910.36 51.16 o 2 4 0 5113.63 4684.83 56.27 o 4 4 0 29101.88 30239.95 125.62 o 6 4 0 41132.54 43188.34 166.08 o 8 4 0 495.40 518.27 42.43 o 10 4 0 9.81 44.57 66.19 o 12 4 0 4147.29 4837.78 105.35 o 14 4 0 28.74 -10.64 88.66 o 16 4 0 0.33 12.36 101.19 o 18 4 0 857.27 932.37 92.99 o 20 4 0 403.03 510.54 68.16 o 22 4 0 0.65 -131.08 131.08 o 24 4 0 542.70 576.91 88.48 o 2 5 0 1.14 116.17 25.85 o 4 5 0 4399.63 4230.39 68.99 o 6 5 0 303.96 128.23 29.41 o 8 5 0 18480.06 17986.66 133.04 o 10 5 0 13018.03 12645.58 130.73 o 12 5 0 435.09 516.96 52.35 o 14 5 0 445.28 701.10 68.51 o 16 5 0 6.97 89.07 102.32 o 18 5 0 1608.88 1329.06 111.53 o 20 5 0 878.75 762.01 70.95 o 22 5 0 167.52 207.50 72.73 o 24 5 0 554.61 643.88 90.91 o 0 6 0 28370.93 35800.88 156.81 o 2 6 0 1624.47 1698.83 60.67 o 4 6 0 3062.11 3321.31 70.24 o 6 6 0 3039.59 2928.72 75.23 o 8 6 0 14232.90 15573.77 132.69 o 10 6 0 16340.52 17485.86 152.47 o 12 6 0 4703.43 5019.73 117.42 o 14 6 0 2574.86 2331.84 111.71 o 16 6 0 817.07 752.62 60.19 o 18 6 0 0.21 56.75 115.87 o 20 6 0 652.56 693.91 72.97 o 22 6 0 34.35 -101.01 137.44 o 24 6 0 135.80 -158.77 158.77 o 2 7 0 9999.12 12032.25 104.82 o 4 7 0 13554.58 16465.97 121.40 o 6 7 0 107845.10 111070.86 303.58 o 8 7 0 82076.98 82967.38 284.39 o 10 7 0 53255.14 53110.44 253.31 o 12 7 0 17890.27 18490.31 177.67 o 14 7 0 5147.89 4916.69 132.33 o 16 7 0 0.00 67.92 109.45 o 18 7 0 469.91 537.93 68.81 o 20 7 0 2606.67 2880.11 151.64 o 22 7 0 1266.48 1515.52 134.23 o 24 7 0 1728.08 1932.71 152.89 o 0 8 0 72326.68 83082.29 268.64 o 2 8 0 19484.90 20084.27 136.01 o 4 8 0 782.70 745.01 60.55 o 6 8 0 59225.33 64813.98 250.93 o 8 8 0 140.91 -86.16 86.81 o 10 8 0 13886.02 14705.40 160.91 o 12 8 0 10524.85 10418.80 155.92 o 14 8 0 7062.27 6698.84 146.23 o 16 8 0 2994.20 2674.58 131.62 o 18 8 0 4338.94 4594.28 153.25 o 20 8 0 92.76 -24.07 136.31 o 22 8 0 14.29 -147.36 147.36 o 24 8 0 780.17 879.13 97.57 o 2 9 0 156.37 -26.32 68.99 o 4 9 0 25295.50 28185.90 173.03 o 6 9 0 18715.16 18603.03 156.63 o 8 9 0 27223.46 27071.71 191.16 o 10 9 0 17617.13 16326.69 170.66 o 12 9 0 5176.14 4926.14 132.86 o 14 9 0 336.05 93.53 59.96 o 16 9 0 556.02 680.84 67.20 o 18 9 0 1892.73 1955.23 142.73 o 20 9 0 67.06 -5.59 75.11 o 22 9 0 684.44 638.53 90.74 o 0 10 0 19.38 34.46 42.78 o 2 10 0 15018.72 15336.21 143.14 o 4 10 0 6745.03 7095.29 114.92 o 6 10 0 1300.93 1692.24 95.13 o 8 10 0 5608.99 5527.83 121.46 o 10 10 0 821.75 1186.15 103.21 o 12 10 0 16979.44 16989.40 187.95 o 14 10 0 812.01 567.17 60.91 o 16 10 0 4265.47 3947.19 149.44 o 18 10 0 676.65 705.14 72.91 o 20 10 0 4.55 46.29 75.76 o 22 10 0 154.31 66.91 89.37 o 2 11 0 11040.32 12083.35 139.16 o 4 11 0 88.29 58.95 46.17 o 6 11 0 1348.55 1449.62 97.09 o 8 11 0 104.73 25.02 93.65 o 10 11 0 14.88 -1.31 98.04 o 12 11 0 647.81 554.39 59.96 o 14 11 0 1294.72 1335.42 106.30 o 16 11 0 2403.44 2056.49 138.21 o 18 11 0 26.08 -17.95 127.40 o 20 11 0 74.61 122.23 138.75 o 22 11 0 3.80 98.70 155.50 o 0 12 0 645.74 1030.23 89.78 o 2 12 0 3.65 -90.14 90.14 o 4 12 0 124.97 -12.42 92.58 o 6 12 0 591.69 762.31 64.47 o 8 12 0 19.58 49.02 53.48 o 10 12 0 318.73 457.72 57.64 o 12 12 0 483.05 544.17 60.61 o 14 12 0 862.58 743.77 66.67 o 16 12 0 321.20 360.92 69.58 o 18 12 0 63.41 137.50 134.47 o 20 12 0 186.12 316.89 88.00 o 22 12 0 5.78 -142.97 163.70 o 2 13 0 1285.40 1059.82 91.45 o 4 13 0 6819.69 6895.93 139.82 o 6 13 0 756.89 635.62 57.58 o 8 13 0 1727.92 1596.33 115.28 o 10 13 0 3108.07 2965.56 127.34 o 12 13 0 173.80 186.58 62.63 o 14 13 0 1062.57 943.78 86.34 o 16 13 0 501.66 370.31 72.79 o 18 13 0 284.79 89.25 141.60 o 20 13 0 1247.43 1264.17 101.25 o 0 14 0 8621.31 9255.82 162.40 o 2 14 0 1547.29 1576.31 119.38 o 4 14 0 9185.21 9240.55 164.18 o 6 14 0 2479.85 2250.73 126.74 o 8 14 0 43.11 -115.10 115.10 o 10 14 0 25.78 0.00 114.86 o 12 14 0 923.29 879.36 75.88 o 14 14 0 6292.81 6199.70 173.92 o 16 14 0 690.66 798.49 78.44 o 18 14 0 651.89 738.42 82.24 o 20 14 0 307.55 419.39 96.20 o 2 15 0 10428.17 10731.83 179.81 o 4 15 0 10185.90 11166.84 180.76 o 6 15 0 13043.24 13444.20 190.56 o 8 15 0 14442.25 14094.02 199.71 o 10 15 0 2177.76 2332.26 138.81 o 12 15 0 7033.76 7326.44 178.02 o 14 15 0 1354.09 1195.24 107.19 o 16 15 0 342.85 185.04 80.75 o 18 15 0 239.51 256.22 90.74 o 0 16 0 13.14 -46.17 126.21 o 2 16 0 5458.17 6028.16 162.93 o 4 16 0 2924.05 2716.29 155.03 o 6 16 0 327.19 -140.17 140.17 o 8 16 0 47.57 -132.63 132.63 o 10 16 0 4.74 -129.12 129.12 o 12 16 0 768.76 798.37 79.45 o 14 16 0 1623.90 1570.66 136.67 o 16 16 0 649.33 517.49 92.40 o 18 16 0 53.09 -160.85 160.85 o 2 17 0 1542.87 1494.07 126.45 o 4 17 0 7079.85 7392.75 176.66 o 6 17 0 11186.03 11370.72 198.46 o 8 17 0 2107.60 1924.99 143.62 o 10 17 0 4285.33 4033.05 163.88 o 12 17 0 1549.96 1372.32 120.33 o 14 17 0 964.49 780.37 86.22 o 16 17 0 50.31 21.81 158.30 o 0 18 0 45.72 39.57 139.58 o 2 18 0 981.85 1318.54 124.25 o 4 18 0 221.41 0.00 137.56 o 6 18 0 781.00 515.12 76.53 o 8 18 0 81.53 125.44 129.60 o 10 18 0 3.99 -139.40 139.40 o 12 18 0 19.47 -146.53 146.53 o 14 18 0 8.66 -2.38 157.70 o 2 19 0 99.92 -148.37 148.37 o 4 19 0 1303.44 1408.33 127.16 o 6 19 0 9.55 -139.10 139.10 o 8 19 0 118.38 147.13 138.45 o 10 19 0 250.82 244.34 79.74 o 12 19 0 57.10 40.23 153.01 o 14 19 0 32.63 -166.56 166.56 o 0 20 0 1156.02 1242.66 93.11 o 2 20 0 42.42 -154.97 154.97 o 4 20 0 1283.21 1256.51 99.95 o 6 20 0 315.76 322.48 79.33 o 8 20 0 145.25 100.42 82.12 o 10 20 0 341.47 337.63 90.14 o 12 20 0 36.99 -35.12 160.91 o 2 21 0 179.27 266.38 91.63 o 4 21 0 1.25 -76.89 159.31 o 6 21 0 320.22 117.89 164.65 o 8 21 0 89.49 55.91 92.81 o 10 21 0 154.18 125.08 94.48 o 0 22 0 2127.20 2212.76 177.13 o 2 22 0 2618.29 2597.09 208.63 o 4 22 0 1101.01 982.52 104.40 o 6 22 0 1063.03 1353.36 125.85 o 1 1 1 85082.56 91111.60 115.93 o 2 1 1 5259.41 6871.63 41.53 o 3 1 1 41687.85 43006.70 106.72 o 4 1 1 43282.32 46062.58 125.32 o 5 1 1 5966.30 6887.20 65.30 o 6 1 1 450.43 373.40 28.17 o 7 1 1 8024.98 7182.04 81.29 o 8 1 1 29818.38 27675.12 143.14 o 9 1 1 687.05 704.43 57.58 o 10 1 1 39359.39 39291.72 190.09 o 11 1 1 5244.85 6212.30 104.76 o 12 1 1 1166.80 1127.51 83.19 o 13 1 1 1981.85 2114.36 98.22 o 14 1 1 653.64 483.62 52.23 o 15 1 1 9839.69 10183.43 150.93 o 16 1 1 2085.27 1658.55 127.10 o 17 1 1 17460.82 17907.69 202.98 o 18 1 1 761.72 -142.25 142.25 o 19 1 1 10024.92 10113.62 183.49 o 20 1 1 632.20 130.84 140.17 o 21 1 1 1207.66 1120.37 96.32 o 22 1 1 257.35 235.36 72.49 o 23 1 1 14.05 6.42 136.13 o 24 1 1 363.67 311.60 88.66 o 25 1 1 194.21 9.80 164.00 o 0 2 1 2071.61 2746.42 38.33 o 1 2 1 455.75 580.84 25.25 o 2 2 1 13807.49 14473.00 63.82 o 3 2 1 41803.45 44250.61 116.76 o 4 2 1 891.72 929.75 39.34 o 5 2 1 473.70 513.04 45.04 o 6 2 1 37.06 32.27 26.68 o 7 2 1 30335.29 29356.67 139.70 o 8 2 1 1258.02 1219.49 62.45 o 9 2 1 13916.92 13411.28 115.93 o 10 2 1 12766.58 13767.33 125.56 o 11 2 1 7137.84 7258.70 108.44 o 12 2 1 2888.40 2706.07 94.95 o 13 2 1 452.07 324.44 46.35 o 14 2 1 87.17 -89.01 89.01 o 15 2 1 1049.80 1152.16 102.80 o 16 2 1 5590.39 5698.85 140.53 o 17 2 1 65.38 -116.35 116.35 o 18 2 1 852.87 883.46 77.84 o 19 2 1 410.45 302.39 67.15 o 20 2 1 14.84 -90.74 120.98 o 21 2 1 250.21 254.74 69.17 o 22 2 1 15.71 -131.68 131.68 o 23 2 1 101.92 164.59 74.51 o 24 2 1 3.66 32.32 148.19 o 25 2 1 436.99 722.61 93.35 o 1 3 1 14403.31 14963.58 70.95 o 2 3 1 85593.82 88301.55 166.08 o 3 3 1 81.69 0.36 35.18 o 4 3 1 13947.65 14278.34 85.98 o 5 3 1 15712.33 17506.84 101.37 o 6 3 1 4419.37 4548.70 69.52 o 7 3 1 151.50 190.09 29.18 o 8 3 1 15925.37 15584.29 117.18 o 9 3 1 8111.39 8955.15 102.26 o 10 3 1 150.53 24.30 65.42 o 11 3 1 552.86 440.19 44.33 o 12 3 1 893.95 826.96 72.02 o 13 3 1 1975.48 1976.74 95.79 o 14 3 1 48.44 75.23 87.76 o 15 3 1 381.59 387.60 52.47 o 16 3 1 336.31 -46.05 106.84 o 17 3 1 4018.39 3923.00 133.76 o 18 3 1 7.20 -86.16 115.39 o 19 3 1 1460.84 1311.59 113.20 o 20 3 1 1100.83 1076.52 93.41 o 21 3 1 52.25 -115.34 126.57 o 22 3 1 15.99 92.34 130.19 o 23 3 1 70.90 -126.80 139.40 o 24 3 1 160.56 -152.47 152.47 o 25 3 1 798.61 971.05 96.20 o 0 4 1 23618.83 27005.93 119.44 o 1 4 1 2183.99 2472.37 47.18 o 2 4 1 649.46 479.11 40.52 o 3 4 1 1053.28 920.25 47.54 o 4 4 1 5392.13 4248.51 65.36 o 5 4 1 10436.21 12236.12 93.41 o 6 4 1 2688.67 2326.55 63.40 o 7 4 1 4.88 86.75 28.70 o 8 4 1 1420.56 1155.19 64.89 o 9 4 1 20269.39 19375.79 139.70 o 10 4 1 2370.29 2298.51 83.37 o 11 4 1 78.22 114.38 40.29 o 12 4 1 3631.39 3491.79 99.95 o 13 4 1 668.43 864.69 70.95 o 14 4 1 3597.41 3561.07 113.14 o 15 4 1 191.61 108.44 53.24 o 16 4 1 582.74 564.50 58.59 o 17 4 1 1182.88 1332.21 118.31 o 18 4 1 4399.51 4523.86 143.80 o 19 4 1 860.29 733.49 78.32 o 20 4 1 0.95 31.02 119.97 o 21 4 1 94.78 -62.39 127.16 o 22 4 1 132.66 225.74 71.60 o 23 4 1 220.53 153.36 78.14 o 24 4 1 71.34 99.59 87.29 o 25 4 1 396.54 534.25 94.36 o 1 5 1 2677.89 3648.07 62.39 o 2 5 1 13976.71 15827.08 98.10 o 3 5 1 113.22 178.92 27.16 o 4 5 1 12884.73 13349.48 98.52 o 5 5 1 74.05 -51.34 51.34 o 6 5 1 651.55 658.80 49.79 o 7 5 1 4131.23 4619.00 79.27 o 8 5 1 0.80 117.65 32.92 o 9 5 1 1.00 -64.06 64.06 o 10 5 1 3823.81 3932.39 92.93 o 11 5 1 5551.40 5204.76 107.43 o 12 5 1 147.29 240.47 45.46 o 13 5 1 103.89 11.35 88.48 o 14 5 1 67.01 37.97 91.27 o 15 5 1 0.17 5.29 97.15 o 16 5 1 207.66 287.54 56.63 o 17 5 1 537.99 448.03 61.26 o 18 5 1 594.11 586.84 66.31 o 19 5 1 1230.94 1321.75 111.59 o 20 5 1 113.23 26.03 123.89 o 21 5 1 270.43 398.71 70.29 o 22 5 1 84.72 70.35 73.44 o 23 5 1 139.49 92.99 77.66 o 24 5 1 113.19 -7.19 154.02 o 25 5 1 211.32 91.09 165.43 o 0 6 1 34596.92 38533.10 164.12 o 1 6 1 5232.43 5670.27 75.52 o 2 6 1 17296.13 18535.94 113.55 o 3 6 1 10495.08 10146.59 93.71 o 4 6 1 1140.95 536.09 37.55 o 5 6 1 6549.70 5502.16 80.16 o 6 6 1 6297.32 5311.31 85.39 o 7 6 1 25922.06 25774.26 155.15 o 8 6 1 0.34 -67.68 67.68 o 9 6 1 21164.62 21258.24 157.11 o 10 6 1 5080.10 4739.38 104.22 o 11 6 1 11459.79 10925.78 138.45 o 12 6 1 2679.36 2790.33 105.11 o 13 6 1 958.22 776.63 75.58 o 14 6 1 12.91 -95.73 95.73 o 15 6 1 12.81 -102.32 102.32 o 16 6 1 8293.57 8721.27 159.19 o 17 6 1 36.38 -116.58 116.58 o 18 6 1 1106.07 1210.93 109.10 o 19 6 1 814.46 819.41 81.17 o 20 6 1 435.69 131.26 73.44 o 21 6 1 1019.04 1025.06 93.11 o 22 6 1 65.89 106.60 74.99 o 23 6 1 344.97 378.21 80.22 o 24 6 1 0.71 -156.34 156.34 o 1 7 1 1064.07 896.06 61.80 o 2 7 1 428.13 360.03 32.27 o 3 7 1 5489.96 5229.96 82.06 o 4 7 1 4004.07 4199.96 78.97 o 5 7 1 5416.15 5340.48 87.65 o 6 7 1 2259.08 2872.51 80.46 o 7 7 1 13739.98 14615.85 132.09 o 8 7 1 1818.40 1985.66 83.60 o 9 7 1 280.83 243.15 44.92 o 10 7 1 4645.42 4886.09 111.95 o 11 7 1 5696.34 5036.19 119.02 o 12 7 1 77.99 154.02 52.11 o 13 7 1 3661.38 3452.16 119.73 o 14 7 1 53.93 -90.02 104.05 o 15 7 1 1365.00 1644.64 115.81 o 16 7 1 2911.96 2724.08 130.49 o 17 7 1 336.79 410.89 66.49 o 18 7 1 229.31 27.57 125.14 o 19 7 1 55.11 -38.50 127.75 o 20 7 1 371.06 468.89 74.04 o 21 7 1 43.36 62.81 74.75 o 22 7 1 12.07 -57.28 141.12 o 23 7 1 279.14 226.63 89.55 o 24 7 1 132.96 136.07 163.47 o 0 8 1 467.48 721.37 59.24 o 1 8 1 5535.61 6305.83 91.98 o 2 8 1 9924.53 11018.17 109.45 o 3 8 1 432.82 290.51 35.12 o 4 8 1 8144.94 7833.77 101.97 o 5 8 1 28816.51 29426.66 171.07 o 6 8 1 157.88 49.32 73.21 o 7 8 1 29230.88 30825.18 186.16 o 8 8 1 54.41 -84.38 84.38 o 9 8 1 32976.65 34186.19 210.17 o 10 8 1 285.30 38.45 94.89 o 11 8 1 20350.09 20018.31 182.54 o 12 8 1 190.73 69.40 102.26 o 13 8 1 4913.26 4695.00 131.26 o 14 8 1 4354.18 4366.88 132.86 o 15 8 1 184.79 66.43 110.28 o 16 8 1 659.81 730.28 63.94 o 17 8 1 11.48 -60.25 120.09 o 18 8 1 1754.85 1834.97 137.32 o 19 8 1 775.14 546.31 76.59 o 20 8 1 414.01 377.74 75.23 o 21 8 1 351.53 338.16 78.85 o 22 8 1 212.37 237.21 81.11 o 23 8 1 591.72 747.15 93.05 o 24 8 1 0.13 -151.82 165.49 o 1 9 1 20824.69 23551.22 153.90 o 2 9 1 14846.77 16003.92 134.29 o 3 9 1 6556.85 6905.02 103.39 o 4 9 1 2389.54 2302.49 84.32 o 5 9 1 24473.22 25175.24 170.30 o 6 9 1 2047.93 2045.02 89.19 o 7 9 1 3200.27 2909.53 101.67 o 8 9 1 14366.55 15235.91 154.85 o 9 9 1 548.10 353.43 51.93 o 10 9 1 6302.89 6323.95 128.94 o 11 9 1 2861.03 2600.12 111.77 o 12 9 1 150.30 65.66 100.12 o 13 9 1 10844.40 10695.46 163.64 o 14 9 1 2823.52 2693.71 125.20 o 15 9 1 3431.15 3401.17 136.90 o 16 9 1 352.24 423.91 65.90 o 17 9 1 2109.18 2010.79 135.48 o 18 9 1 189.64 103.33 129.42 o 19 9 1 1353.68 1303.92 108.15 o 20 9 1 384.21 340.12 77.01 o 21 9 1 79.04 92.16 146.35 o 22 9 1 469.32 531.10 89.96 o 23 9 1 337.39 252.06 94.00 o 0 10 1 349.24 279.28 39.87 o 1 10 1 4463.45 5385.23 99.05 o 2 10 1 27.14 -16.04 74.69 o 3 10 1 65.92 17.29 73.92 o 4 10 1 1294.44 1529.19 85.74 o 5 10 1 1276.29 1214.20 88.89 o 6 10 1 417.92 312.91 48.25 o 7 10 1 14.86 11.59 87.82 o 8 10 1 1861.71 1814.70 102.92 o 9 10 1 2205.17 2405.64 105.23 o 10 10 1 1088.06 1064.82 87.82 o 11 10 1 223.87 99.53 100.90 o 12 10 1 245.71 392.24 57.34 o 13 10 1 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2 577.21 227.28 52.47 o 2 10 2 5626.13 5610.90 105.71 o 3 10 2 4001.39 4291.35 101.31 o 4 10 2 5542.18 5502.82 109.45 o 5 10 2 6653.83 7215.02 118.54 o 6 10 2 11080.29 10732.90 139.22 o 7 10 2 14635.45 13986.59 153.19 o 8 10 2 209.93 73.92 91.45 o 9 10 2 4820.72 4487.20 120.15 o 10 10 2 221.75 239.64 53.66 o 11 10 2 5658.58 5751.08 134.83 o 12 10 2 2743.44 2715.46 121.75 o 13 10 2 379.50 465.56 61.26 o 14 10 2 4335.23 4558.80 136.90 o 15 10 2 1553.17 1259.00 107.79 o 16 10 2 1032.30 928.74 72.73 o 17 10 2 426.10 479.94 69.58 o 18 10 2 4.54 -98.40 127.75 o 19 10 2 302.84 281.00 75.40 o 20 10 2 351.56 284.68 78.14 o 21 10 2 2727.15 2772.68 170.18 o 22 10 2 47.70 96.26 155.74 o 23 10 2 293.38 330.68 95.07 o 1 11 2 560.97 581.07 52.65 o 2 11 2 608.66 786.37 76.47 o 3 11 2 882.31 708.00 69.11 o 4 11 2 5200.30 5409.71 114.50 o 5 11 2 386.62 383.68 50.15 o 6 11 2 2843.22 2616.70 108.38 o 7 11 2 4740.90 5137.50 122.05 o 8 11 2 12.18 88.24 95.19 o 9 11 2 2559.67 2374.27 113.91 o 10 11 2 75.90 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9 3 84.22 149.80 45.99 o 8 9 3 11500.28 11637.22 144.04 o 9 9 3 2453.74 2244.20 105.17 o 10 9 3 4663.77 4699.39 119.73 o 11 9 3 427.96 552.67 55.38 o 12 9 3 4494.74 4051.47 125.08 o 13 9 3 450.12 467.58 59.90 o 14 9 3 1280.01 1065.59 84.56 o 15 9 3 232.78 197.99 62.63 o 16 9 3 283.37 229.90 65.60 o 17 9 3 475.21 498.42 69.52 o 18 9 3 56.58 122.35 70.53 o 19 9 3 683.41 687.20 75.58 o 20 9 3 1626.56 1489.97 134.23 o 21 9 3 178.66 -73.56 150.69 o 22 9 3 1116.93 1235.12 93.41 o 23 9 3 36.24 -164.36 164.36 o 0 10 3 146.49 366.09 52.41 o 1 10 3 3265.07 3190.88 112.60 o 2 10 3 2982.41 3465.64 103.81 o 3 10 3 10675.94 10900.28 135.36 o 4 10 3 78.36 65.96 46.76 o 5 10 3 25606.22 26387.54 189.91 o 6 10 3 1487.51 1468.46 97.63 o 7 10 3 1904.24 2215.61 100.48 o 8 10 3 158.74 -14.91 93.65 o 9 10 3 1816.21 1802.52 105.11 o 10 10 3 918.77 859.58 79.50 o 11 10 3 3089.91 3038.89 122.17 o 12 10 3 178.55 320.28 58.29 o 13 10 3 2412.97 2243.72 122.94 o 14 10 3 231.84 -9.39 114.74 o 15 10 3 671.23 667.83 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