#------------------------------------------------------------------------------ #$Date: 2011-09-28 14:24:46 +0000 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://cod.ibt.lt/cod/hkl/2/01/38/2013836.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013836_Fobs loop_ _publ_author_name 'Muranishi, Yasunori' 'Okabe, Nobuo' _publ_section_title ; (2,2'-Bipyridine-\k^2^N,N')(1,1-cyclobutanedicarboxylato-\k^2^O,O')palladium(II), (1,1-cyclobutanedicarboxylato-\k^2^O,O')(1,10-phenanthroline-\k^2^N,N')palladium(II) monohydrate and (1,1-cyclobutanedicarboxylato-\k^2^O,O')(1,10-phenanthroline-\k^2^N,N')palladium(II) dihydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m47 _journal_page_last m50 _journal_volume 60 _journal_year 2004 _space_group_IT_number 34 _symmetry_space_group_name_Hall 'P 2 -2n' _symmetry_space_group_name_H-M 'P n n 2' _[local]_cod_data_source_file ob1156IIasup3.hkl _[local]_cod_data_source_block IIa loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 2 1 0 12225.11 633.11 12806.44 o 2 2 0 14395.67 664.18 12626.63 o 1 3 0 548.72 18.09 219.16 o 3 1 0 1580.36 68.72 1233.50 o 2 3 0 12604.40 627.70 12414.03 o 0 1 1 3209.21 176.43 3659.63 o 1 0 1 1265.94 61.88 1185.64 o 3 2 0 101.04 6.15 58.97 o 1 1 1 8872.05 465.08 9404.40 o 0 4 0 10063.14 460.55 8654.17 o 1 4 0 1553.34 79.62 1575.56 o 1 2 1 968.54 52.00 1037.97 o 2 1 1 5171.72 258.81 5140.09 o 4 0 0 3866.88 198.77 3991.19 o 3 3 0 6.04 4.71 9.47 o 4 1 0 5748.09 286.03 5666.21 o 2 4 0 185.48 14.85 308.49 o 2 2 1 7103.20 355.73 7080.50 o 0 3 1 6471.70 320.10 6327.75 o 1 3 1 28854.21 1475.18 29688.62 o 4 2 0 5715.65 293.10 5892.42 o 3 0 1 11812.20 610.77 12375.50 o 3 1 1 13621.30 683.36 13528.80 o 1 5 0 4257.73 189.00 3491.53 o 2 3 1 20386.35 1035.94 20730.21 o 3 4 0 2499.95 129.17 2579.62 o 3 2 1 19816.89 1003.33 20025.55 o 4 3 0 5379.35 273.02 5453.61 o 2 5 0 109.00 7.88 78.24 o 1 4 1 1720.06 83.71 1599.38 o 5 1 0 7504.33 375.82 7472.19 o 3 3 1 35432.57 1764.23 35031.86 o 4 1 1 41.13 3.88 26.60 o 2 4 1 15092.42 751.23 14812.16 o 5 2 0 1342.68 69.49 1357.37 o 4 4 0 2194.27 106.85 2051.61 o 3 5 0 556.76 30.99 591.53 o 0 6 0 13112.80 664.70 13205.38 o 4 2 1 911.53 49.37 964.68 o 1 6 0 18496.55 910.33 17874.05 o 0 5 1 1627.61 85.12 1685.95 o 1 5 1 4833.00 251.04 5063.46 o 5 3 0 6403.04 306.62 5937.87 o 3 4 1 20893.16 1050.07 20861.11 o 2 6 0 20553.46 979.61 18906.44 o 4 3 1 605.92 34.61 665.73 o 2 5 1 6500.76 327.68 6524.82 o 5 0 1 5469.25 275.97 5485.69 o 6 0 0 16.98 3.00 20.84 o 5 1 1 3416.17 171.02 3360.47 o 4 5 0 7065.76 347.70 6838.80 o 6 1 0 22372.69 1128.98 22467.96 o 5 4 0 239.67 13.90 196.63 o 3 6 0 675.26 35.97 671.94 o 5 2 1 9334.50 478.24 9619.24 o 6 2 0 957.34 44.57 777.82 o 4 4 1 10263.69 493.42 9607.21 o 3 5 1 5348.81 277.33 5586.21 o 1 6 1 97.50 9.89 138.22 o 1 7 0 565.36 28.56 483.66 o 0 0 2 8169.99 447.68 9287.74 o 5 3 1 3475.48 182.90 3684.82 o 6 3 0 6685.17 348.34 7044.12 o 1 1 2 118.58 9.55 105.98 o 2 6 1 8082.33 398.25 7842.83 o 2 7 0 374.73 21.39 365.56 o 5 5 0 3665.37 185.16 3654.15 o 4 6 0 1190.43 63.20 1231.05 o 0 2 2 4693.88 247.40 5013.22 o 2 0 2 7570.81 397.81 8082.96 o 1 2 2 1914.36 102.09 2040.96 o 4 5 1 2154.74 107.06 2061.18 o 6 1 1 846.25 38.62 638.24 o 2 1 2 755.35 42.32 820.35 o 5 4 1 12627.06 609.31 11894.32 o 6 4 0 3632.12 156.19 2785.30 o 3 6 1 4167.40 205.48 4010.36 o 3 7 0 3063.51 147.49 2819.65 o 7 1 0 5527.09 256.13 4841.73 o 6 2 1 428.94 25.69 453.67 o 2 2 2 3698.61 200.95 4116.32 o 1 3 2 15.66 2.84 13.56 o 0 7 1 10106.23 486.88 9483.84 o 7 2 0 341.72 19.03 288.58 o 1 7 1 6191.52 303.96 5953.53 o 3 1 2 333.34 20.42 342.38 o 0 8 0 1660.40 87.53 1725.08 o 6 3 1 890.27 48.34 916.31 o 2 3 2 3951.33 200.36 3964.13 o 1 8 0 14688.26 714.49 14020.11 o 5 6 0 56.82 6.26 53.96 o 3 2 2 273.26 17.71 287.77 o 2 7 1 7749.33 382.20 7519.64 o 0 4 2 17283.22 880.32 17698.60 o 5 5 1 1480.69 73.57 1380.12 o 7 3 0 570.81 38.61 795.31 o 4 6 1 3183.93 169.21 3412.46 o 4 7 0 185.62 14.07 222.63 o 6 5 0 7670.84 367.85 7121.28 o 1 4 2 2658.10 137.78 2731.09 o 2 8 0 2016.32 107.64 2147.99 o 4 0 2 3588.23 184.26 3653.69 o 3 3 2 11.68 3.35 13.03 o 4 1 2 20081.64 1018.16 20426.74 o 7 0 1 9435.20 505.53 10375.36 o 2 4 2 5892.32 299.36 5961.00 o 6 4 1 8278.23 400.34 7789.60 o 3 7 1 4265.90 202.71 3867.16 o 7 1 1 4043.01 197.20 3809.44 o 4 2 2 2358.37 125.18 2494.73 o 3 8 0 5143.28 258.81 5115.49 o 7 4 0 36.97 3.90 25.83 o 7 2 1 21226.78 1022.77 19986.28 o 8 0 0 8317.10 376.60 7049.31 o 1 5 2 11.82 3.89 2.68 o 8 1 0 12367.08 611.36 12074.17 o 1 8 1 775.33 42.51 788.47 o 3 4 2 3582.73 183.83 3644.09 o 5 6 1 3908.27 199.40 3947.29 o 5 7 0 16634.31 795.06 15452.01 o 6 6 0 354.35 21.09 340.01 o 4 3 2 8467.25 440.37 8898.98 o 7 3 1 3014.44 149.74 2894.34 o 8 2 0 982.99 54.70 1054.93 o 4 7 1 3791.52 192.37 3792.76 o 6 5 1 426.63 25.92 456.34 o 2 5 2 3697.40 187.75 3701.92 o 2 8 1 4018.72 205.11 4062.04 o 1 9 0 263.60 19.78 303.61 o 5 1 2 941.31 52.11 990.06 o 4 8 0 206.55 14.79 214.56 o 7 5 0 1799.85 94.04 1829.20 o 5 2 2 697.67 38.04 683.72 o 2 9 0 1407.07 72.10 1365.34 o 8 3 0 7132.08 358.34 7095.71 o 4 4 2 2259.84 120.09 2384.69 o 3 5 2 2182.14 111.27 2156.45 o 0 6 2 15124.80 742.54 14628.79 o 3 8 1 571.40 31.90 557.30 o 7 4 1 6186.64 325.35 6581.16 o 1 6 2 11184.10 560.29 11132.72 o 5 3 2 2079.46 104.86 2006.74 o 8 1 1 917.26 49.77 925.00 o 3 9 0 1544.53 80.58 1546.25 o 5 7 1 246.77 16.39 226.74 o 2 6 2 3685.08 187.35 3688.83 o 6 6 1 3514.48 184.28 3682.20 o 6 7 0 383.80 19.17 222.83 o 8 4 0 25.85 4.10 35.15 o 8 2 1 135.63 12.99 146.50 o 0 9 1 15295.73 728.93 14129.62 o 5 8 0 34.85 4.33 36.20 o 6 0 2 353.49 20.59 293.65 o 7 6 0 255.14 17.45 268.65 o 1 9 1 4424.07 212.43 4066.19 o 4 5 2 5902.40 300.07 5959.90 o 6 1 2 21277.12 1072.44 21441.28 o 4 8 1 2867.93 149.03 2945.93 o 7 5 1 712.07 38.61 685.34 o 5 4 2 2028.04 100.26 1888.25 o 3 6 2 8820.65 431.65 8445.96 o 9 1 0 300.27 20.54 303.97 o 2 9 1 10792.26 533.34 10512.77 o 6 2 2 297.84 19.63 289.91 o 8 3 1 3999.82 188.73 3553.82 o 0 10 0 5.97 8.49 5.54 o 4 9 0 55.74 5.84 54.23 o 1 10 0 13664.97 664.77 13017.82 o 9 2 0 1066.52 55.77 1020.00 o 1 7 2 102.12 9.66 121.82 o 8 5 0 6759.24 341.37 6764.28 o 6 3 2 9756.00 496.62 9922.33 o 3 9 1 649.79 35.75 634.82 o 2 10 0 68.26 7.53 107.70 o 2 7 2 1357.47 68.47 1263.98 o 6 7 1 955.25 47.09 811.73 o 8 4 1 3999.01 210.95 4229.25 o 5 5 2 9873.84 499.66 9955.71 o 9 3 0 3529.69 168.80 3189.48 o 4 6 2 2914.57 151.62 2990.54 o 5 8 1 3326.11 160.20 3037.62 o 6 8 0 246.58 16.54 213.39 o 7 6 1 2975.25 156.04 3090.69 o 7 7 0 4774.72 247.17 4929.30 o 9 0 1 7378.87 367.87 7243.15 o 6 4 2 233.41 17.62 222.00 o 3 10 0 11853.33 562.47 10844.40 o 5 9 0 4843.89 255.20 5137.83 o 3 7 2 4743.49 243.60 4836.53 o 7 1 2 676.37 39.42 705.97 o 9 1 1 3730.46 186.37 3617.33 o 8 6 0 140.84 13.09 109.77 o 4 9 1 3989.47 201.53 3947.07 o 9 4 0 1210.76 62.01 1129.24 o 1 10 1 -30.51 16.79 110.30 o 9 2 1 7908.11 402.20 8006.65 o 7 2 2 572.59 30.42 480.39 o 8 5 1 1870.38 100.42 1966.51 o 0 8 2 63.01 6.41 63.60 o 0 1 3 340.69 22.14 368.95 o 1 8 2 6880.58 356.54 7158.62 o 1 0 3 111.90 11.79 149.47 o 5 6 2 2007.12 101.58 1925.54 o 2 10 1 5412.14 265.25 5143.65 o 1 1 3 6240.62 337.27 6901.31 o 4 10 0 169.76 14.29 155.20 o 9 3 1 4052.62 205.52 4028.62 o 7 3 2 1450.52 76.72 1458.82 o 4 7 2 1571.68 83.82 1615.32 o 6 5 2 9954.23 513.37 10320.37 o 6 8 1 4703.15 236.37 4632.23 o 2 8 2 84.23 8.57 88.55 o 10 0 0 13791.25 680.61 13414.53 o 7 7 1 423.39 25.67 398.68 o 1 2 3 1037.91 57.23 1076.12 o 10 1 0 4202.03 205.76 3954.09 o 2 1 3 636.01 34.44 584.60 o 1 11 0 63.43 8.72 124.47 o 9 5 0 1724.40 89.39 1697.32 o 7 8 0 12.62 4.34 18.42 o 3 10 1 191.65 15.70 171.29 o 5 9 1 163.75 15.36 178.27 o 10 2 0 9002.92 445.78 8758.25 o 6 9 0 158.79 13.52 132.13 o 2 2 3 57.07 6.06 39.58 o 0 3 3 2703.72 138.45 2688.12 o 8 6 1 3019.44 153.91 2988.50 o 1 3 3 4046.40 219.66 4464.66 o 2 11 0 -6.34 10.18 0.30 o 8 7 0 3107.85 156.09 3008.73 o 3 8 2 2920.68 152.84 3016.34 o 7 4 2 286.93 19.30 254.36 o 9 4 1 4294.08 209.12 4005.81 o 3 0 3 1721.92 94.14 1846.10 o 3 1 3 6362.37 337.01 6823.81 o 8 0 2 444.53 28.72 501.28 o 10 3 0 2220.78 115.59 2235.49 o 8 1 2 7030.90 367.53 7398.29 o 2 3 3 2925.57 151.77 2982.23 o 5 10 0 840.34 43.77 744.22 o 3 2 3 5306.89 276.97 5547.63 o 5 7 2 17393.96 873.36 17394.89 o 6 6 2 132.36 11.76 136.46 o 3 11 0 5864.37 288.73 5612.11 o 4 10 1 5336.80 263.14 5110.58 o 8 2 2 382.66 23.88 361.43 o 1 4 3 1014.41 57.13 1084.91 o 9 6 0 3180.81 164.19 3213.94 o 1 9 2 100.96 9.54 117.22 o 0 11 1 7252.21 362.48 7136.66 o 10 1 1 171.56 14.96 169.72 o 4 8 2 967.78 52.31 949.30 o 1 11 1 -49.59 12.05 7.14 o 7 5 2 3463.58 179.98 3545.83 o 9 5 1 2997.92 149.57 2860.70 o 3 3 3 4023.32 211.13 4210.03 o 4 1 3 472.24 28.93 470.74 o 7 8 1 2357.63 120.41 2309.39 o 10 4 0 4677.88 235.37 4598.49 o 2 4 3 1339.38 71.94 1364.82 o 10 2 1 11.70 10.94 30.19 o 2 9 2 537.05 32.11 551.69 o 6 9 1 57.84 6.42 56.47 o 8 3 2 3582.51 191.25 3827.80 o 2 11 1 3527.29 180.57 3532.41 o 8 7 1 1877.24 94.51 1762.30 o 4 2 3 91.72 9.26 82.40 o 7 9 0 6982.08 356.17 7077.16 o 4 11 0 91.01 8.09 68.35 o 0 5 3 1905.17 105.68 2101.61 o 8 8 0 1779.54 87.25 1582.46 o 1 5 3 3039.87 164.93 3315.45 o 10 3 1 524.29 32.73 560.78 o 3 4 3 4779.71 246.52 4889.64 o 5 10 1 127.00 13.08 116.29 o 3 9 2 2674.37 140.05 2744.01 o 6 10 0 99.31 9.39 104.46 o 6 7 2 5260.56 263.56 5151.71 o 4 3 3 1936.55 98.39 1855.23 o 0 12 0 225.38 17.71 217.67 o 8 4 2 924.46 52.00 956.02 o 3 11 1 90.48 9.69 110.96 o 1 12 0 10001.02 484.79 9421.54 o 10 5 0 4963.45 241.36 4625.26 o 2 5 3 2598.11 138.61 2741.24 o 5 8 2 219.74 19.37 240.70 o 5 0 3 5736.19 300.29 6016.88 o 9 6 1 1959.41 106.39 2081.97 o 7 6 2 312.92 21.65 283.19 o 9 7 0 5063.85 255.22 4993.41 o 11 1 0 110.75 10.99 129.38 o 5 1 3 686.20 38.49 647.09 o 2 12 0 355.73 23.44 337.04 o 10 4 1 552.45 34.15 588.16 o 11 2 0 395.14 25.83 373.69 o 5 2 3 6421.78 338.76 6828.98 o 9 1 2 754.71 41.04 688.70 o 4 4 3 1953.60 104.31 2022.04 o 5 11 0 10991.17 547.93 10818.80 o 0 10 2 332.08 20.82 286.15 o 3 5 3 1950.18 101.31 1933.49 o 4 9 2 761.38 43.02 756.96 o 1 10 2 4011.64 207.02 4081.73 o 9 2 2 66.69 6.83 70.44 o 1 6 3 439.88 27.60 445.91 o 7 9 1 371.76 23.78 340.74 o 4 11 1 1107.26 60.85 1135.84 o 8 5 2 3938.17 200.69 3919.95 o 8 8 1 6219.07 316.15 6247.83 o 11 3 0 12.15 10.36 1.60 o 5 3 3 927.35 50.12 890.57 o 3 12 0 4641.37 229.87 4441.57 o 2 10 2 53.70 5.63 46.06 o 6 10 1 8270.39 420.04 8341.58 o 10 6 0 4821.77 240.90 4676.23 o 2 6 3 960.74 56.55 1076.62 o 9 3 2 823.10 46.07 814.85 o 8 9 0 -0.12 11.82 2.84 o 1 12 1 154.92 17.14 203.49 o 10 5 1 1590.24 85.87 1639.80 o 11 0 1 2411.88 125.99 2436.72 o 6 8 2 207.16 18.95 205.56 o 7 10 0 234.16 18.39 207.87 o 9 7 1 583.89 35.58 608.27 o 11 1 1 4859.28 249.85 4930.10 o 7 7 2 7336.75 366.45 7193.68 o 4 5 3 2029.55 106.95 2062.82 o 6 1 3 145.82 15.22 109.25 o 9 8 0 3067.11 154.04 2943.00 o 11 4 0 1256.64 67.42 1236.19 o 5 4 3 4278.46 221.87 4387.99 o 2 12 1 2039.35 107.89 2073.99 o 3 10 2 2950.20 152.77 2978.46 o 11 2 1 1110.78 59.75 1083.96 o 3 6 3 1341.74 71.38 1319.05 o 5 9 2 7852.69 389.37 7623.26 o 6 2 3 243.36 19.67 268.84 o 4 12 0 643.75 38.83 662.31 o 5 11 1 5.84 10.43 5.12 o 6 11 0 1.81 10.82 8.52 o 8 6 2 1296.35 69.42 1278.76 o 0 7 3 3748.15 194.62 3833.84 o 9 4 2 356.80 24.70 380.86 o 1 7 3 3155.26 166.46 3285.52 o 11 3 1 6490.72 325.26 6371.76 o 3 12 1 235.11 19.00 256.17 o 6 3 3 106.93 11.13 132.90 o 10 6 1 2135.32 114.20 2213.12 o 10 7 0 2368.83 122.54 2335.26 o 2 7 3 3732.00 191.66 3749.64 o 1 13 0 888.10 59.05 1035.35 o 11 5 0 -19.04 12.62 1.15 o 4 10 2 322.05 22.30 307.94 o 5 5 3 446.70 28.74 457.75 o 4 6 3 2777.20 142.80 2757.95 o 8 9 1 1821.37 96.90 1846.95 o 10 0 2 6134.87 310.94 6119.84 o 7 10 1 -12.12 11.61 14.17 o 10 1 2 1295.61 70.56 1314.44 o 12 0 0 7932.11 408.58 8152.46 o 1 11 2 224.88 18.98 233.45 o 9 5 2 882.04 50.23 891.88 o 2 13 0 304.25 21.26 254.27 o 5 12 0 203.32 17.09 246.22 o 12 1 0 1222.14 61.83 1066.50 o 9 8 1 1050.26 56.34 993.17 o 7 8 2 523.14 31.86 497.00 o 11 4 1 850.59 49.92 899.88 o 7 0 3 7078.81 372.46 7496.30 o 6 4 3 1762.96 94.70 1808.12 o 3 7 3 1233.09 68.93 1294.34 o 7 1 3 775.19 43.95 751.65 o 6 9 2 1022.55 56.88 1031.50 o 10 2 2 3517.53 183.49 3603.19 o 4 12 1 3541.84 179.79 3480.04 o 8 10 0 412.24 27.08 396.74 o 12 2 0 6721.19 336.66 6595.53 o 2 11 2 207.49 17.40 188.29 o 6 11 1 281.38 21.49 270.59 o 8 7 2 2174.32 111.21 2095.10 o 9 9 0 4271.08 214.72 4157.06 o 7 2 3 5816.24 297.05 5857.58 o 3 13 0 5965.76 291.80 5623.81 o 7 11 0 4455.75 224.02 4345.74 o 10 3 2 765.30 45.27 800.04 o 1 8 3 191.31 17.90 193.22 o 5 10 2 348.82 24.54 322.91 o 11 6 0 8490.63 414.45 8033.66 o 5 6 3 2992.35 156.26 3045.77 o 0 13 1 6041.72 302.27 5905.11 o 10 7 1 1651.00 87.50 1638.51 o 12 3 0 231.07 20.04 258.03 o 1 13 1 94.46 9.65 120.79 o 3 11 2 1925.12 100.67 1904.86 o 11 5 1 2011.90 109.58 2123.61 o 7 3 3 514.67 31.30 482.45 o 4 7 3 1767.69 92.18 1728.56 o 6 5 3 187.77 17.51 184.90 o 10 8 0 1307.78 69.44 1249.45 o 2 8 3 1312.52 70.10 1284.11 o 9 6 2 2595.44 138.59 2709.64 o 2 13 1 4385.57 221.41 4301.51 o 5 12 1 74.57 8.02 71.19 o 12 1 1 -9.39 12.34 9.28 o 6 12 0 52.38 6.57 57.34 o 10 4 2 3123.88 163.28 3180.69 o 4 13 0 2508.29 126.78 2389.99 o 12 4 0 6360.73 322.78 6349.92 o 8 10 1 5586.62 276.86 5358.72 o 12 2 1 98.95 9.22 95.20 o 3 8 3 865.35 48.68 854.55 o 7 4 3 3357.26 181.41 3615.62 o 7 9 2 5012.80 251.57 4889.61 o 9 9 1 440.68 28.07 405.51 o 4 11 2 74.44 8.53 95.06 o 8 8 2 28.05 5.93 27.35 o 3 13 1 823.93 46.44 790.66 o 7 11 1 49.57 5.87 44.53 o 8 1 3 28.54 6.25 30.95 o 11 6 1 159.10 17.68 184.82 o 11 7 0 231.79 20.92 220.76 o 5 7 3 672.00 42.14 743.98 o 6 10 2 286.67 21.75 265.64 o 6 6 3 2922.16 157.84 3125.04 o 12 3 1 1628.04 87.46 1634.21 o 0 12 2 816.11 48.04 854.90 o 0 14 0 1436.18 77.95 1459.54 o 8 2 3 1314.65 70.43 1268.03 o 10 5 2 1059.16 57.52 1012.45 o 0 9 3 5566.54 288.50 5723.90 o 1 12 2 4026.81 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23.12 o 9 22 0 30.39 20.34 26.97 o 1 23 2 1.71 20.81 0.01 o 10 16 4 152.22 16.64 165.08 o 14 5 5 302.28 32.73 332.49 o 22 0 0 418.79 35.82 398.99 o 2 16 5 -29.82 22.21 10.17 o 15 14 3 68.13 11.54 81.74 o 10 0 6 262.43 24.31 295.89 o 21 1 2 7.66 20.44 4.09 o 22 1 0 410.87 36.73 420.84 o 10 1 6 426.40 35.95 341.56 o 17 11 3 1.58 21.85 12.41 o 16 15 2 124.64 12.73 120.80 o 1 11 6 62.41 10.42 57.67 o 9 5 6 58.19 10.10 57.89 o 18 12 2 28.75 22.62 7.57 o 11 18 3 51.97 10.54 60.92 o 14 12 4 -4.98 20.70 6.45 o 2 23 2 76.03 12.49 109.30 o 6 23 1 16.36 20.41 10.45 o 7 8 6 31.33 23.32 29.12 o 10 12 5 162.98 16.70 162.15 o 17 15 1 -13.87 22.23 3.26 o 19 10 2 16.97 22.08 9.01 o 12 19 2 -20.19 20.95 29.56 o 18 14 0 21.81 18.69 0.27 o 19 6 3 190.37 20.75 208.76 o 21 2 2 128.64 13.10 115.74 o 22 2 0 374.54 35.26 350.20 o 4 19 4 241.78 26.27 203.30 o 12 20 1 15.35 21.45 12.71 o 18 9 3 41.68 9.62 18.32 o 10 2 6 382.19 35.35 368.37 o 11 21 0 -23.33 20.63 3.92 o 5 21 3 56.60 10.78 58.66 o 6 9 6 40.65 10.04 38.71 o 3 24 0 12.75 22.98 6.87 o 9 13 5 18.88 9.52 18.28 o 11 11 5 -1.89 20.36 8.58 o 3 16 5 52.25 9.97 61.60 o 2 11 6 -19.27 21.21 19.35 o 7 23 0 4.08 14.65 0.13 o 8 7 6 186.18 17.68 172.46 o 13 8 5 17.37 15.64 21.42 o 7 18 4 38.24 10.50 39.90 o 17 6 4 118.13 12.67 117.90 o 6 15 5 54.21 10.69 56.51 o 9 21 2 -12.13 24.26 42.52 o 1 24 1 -57.81 25.40 0.79 o 21 3 2 16.40 12.60 34.79 o 19 12 1 17.77 22.81 21.70 o 22 3 0 323.41 35.01 347.35 o 3 23 2 11.20 20.78 6.41 o 10 3 6 137.02 14.62 115.28 o 15 0 5 175.53 19.75 202.56 o 9 17 4 230.13 22.18 226.70 o 21 7 1 -28.84 23.60 28.81 o 16 13 3 314.93 31.74 279.81 o 5 10 6 28.25 23.71 46.31 o 15 1 5 268.03 23.28 277.26 o 8 20 3 43.26 9.43 32.44 o 14 6 5 56.24 10.10 43.55 o 20 10 1 714.53 52.16 754.77 o 2 24 1 -4.62 22.31 23.04 o 3 11 6 302.29 31.63 306.71 o 8 14 5 438.07 36.57 398.33 o 12 10 5 -1.51 20.39 2.60 o 16 9 4 20.51 9.46 30.87 o 21 8 0 128.92 12.67 131.52 o 9 22 1 335.91 31.79 282.63 o 7 22 2 0.34 20.56 4.17 o 15 18 0 379.64 32.34 266.17 o 17 14 2 129.66 13.14 117.66 o 18 0 4 49.12 10.27 67.18 o 4 24 0 75.96 12.74 104.96 o 15 2 5 190.92 20.30 185.00 o 22 1 1 22.91 10.39 28.14 o 9 6 6 127.91 12.82 132.62 o 18 1 4 528.62 41.57 540.78 o 20 8 2 -13.81 21.02 3.17 o 4 16 5 119.83 12.61 100.40 o 5 19 4 57.90 9.84 37.26 o 14 19 0 401.53 38.04 424.07 o 16 17 0 279.32 25.41 303.00 o 10 19 3 22.67 24.57 64.57 o 11 20 2 7.79 11.63 2.86 o 15 11 4 201.89 21.25 199.02 o 20 1 3 5.77 20.60 4.28 o 21 4 2 29.63 23.01 71.37 o 22 4 0 387.95 37.85 397.63 o 18 14 1 468.31 38.97 440.11 o 10 4 6 378.41 33.28 326.14 o 19 7 3 22.91 22.42 28.83 o 22 2 1 -12.87 23.44 27.38 o 18 2 4 34.93 9.42 26.70 o 11 21 1 602.33 42.52 520.36 o 3 24 1 -83.24 32.14 112.40 o 4 23 2 88.65 11.56 89.09 o 6 21 3 37.57 9.79 26.10 o 20 2 3 32.24 23.74 32.84 o 15 3 5 315.12 32.37 306.02 o 1 22 3 4.89 24.23 20.19 o 7 23 1 -31.33 23.66 1.24 o