#------------------------------------------------------------------------------ #$Date: 2011-09-28 14:24:46 +0000 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://cod.ibt.lt/cod/hkl/2/01/38/2013846.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013846_Fobs loop_ _publ_author_name 'Zachara, Janusz' 'Madura, Izabela' 'W\/lostowski, Marek' _publ_section_title ; Hydrogen-bonding patterns in two structural isomers of 3,6-bis(2-chlorophenyl)-1,4-dihydro-1,2,4,5-tetrazine ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o57 _journal_page_last o59 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.3382 _cell_length_b 8.6777 _cell_length_c 25.9680 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.8393 _[local]_cod_data_source_file sk1670IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2mw in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 282.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 520.78 512.12 14.07 o 4 0 0 55954.54 57529.95 330.53 o 6 0 0 9790.13 9541.97 135.11 o 8 0 0 202.41 146.20 14.06 o 10 0 0 3766.56 3966.61 72.04 o 12 0 0 614.17 610.47 29.01 o 14 0 0 1699.85 1773.47 48.56 o 2 1 0 69726.62 70648.77 293.89 o 4 1 0 637.34 634.44 16.14 o 6 1 0 19.00 5.77 9.62 o 8 1 0 132.55 118.82 13.61 o 10 1 0 1094.89 1076.21 31.53 o 12 1 0 60.70 47.79 17.75 o 14 1 0 14.89 -6.95 19.09 o 0 2 0 79904.12 84945.17 346.30 o 2 2 0 17.24 13.02 9.62 o 4 2 0 96.82 90.85 10.95 o 6 2 0 1160.82 1185.68 26.36 o 8 2 0 919.32 944.01 25.31 o 10 2 0 1335.48 1342.22 34.79 o 12 2 0 116.88 102.98 18.35 o 14 2 0 227.80 235.71 25.60 o 2 3 0 217.56 244.33 12.28 o 4 3 0 10.09 14.65 9.47 o 6 3 0 93.54 108.31 12.43 o 8 3 0 425.58 401.05 19.98 o 10 3 0 22.12 44.68 15.98 o 12 3 0 6.09 14.35 16.13 o 14 3 0 10.73 30.77 18.79 o 0 4 0 8386.16 7677.41 119.21 o 2 4 0 10574.61 9796.37 137.13 o 4 4 0 10207.79 10006.45 150.66 o 6 4 0 6655.94 6572.82 106.95 o 8 4 0 7769.57 7772.03 130.57 o 10 4 0 0.96 5.92 15.24 o 12 4 0 1402.16 1433.43 41.15 o 2 5 0 1001.53 1064.20 25.32 o 4 5 0 1385.76 1346.03 30.65 o 6 5 0 2411.12 2306.93 46.81 o 8 5 0 1125.95 1076.35 32.27 o 10 5 0 160.56 172.82 19.24 o 12 5 0 19.96 3.99 18.35 o 0 6 0 196.85 210.71 16.42 o 2 6 0 283.11 266.80 17.61 o 4 6 0 22.00 22.79 14.35 o 6 6 0 4424.33 4233.14 76.36 o 8 6 0 462.32 436.40 25.45 o 10 6 0 2.52 -2.52 17.46 o 2 7 0 125.47 145.74 17.31 o 4 7 0 1137.36 1170.94 33.46 o 6 7 0 523.50 479.04 26.79 o 8 7 0 259.48 235.42 21.46 o 10 7 0 123.37 144.41 22.05 o 0 8 0 411.97 440.54 24.56 o 2 8 0 1891.27 2091.45 44.42 o 4 8 0 747.84 826.88 30.49 o 6 8 0 56.68 99.72 18.94 o 8 8 0 777.09 753.01 34.93 o 2 9 0 5.11 -14.06 17.90 o 4 9 0 1.65 -16.57 16.57 o 6 9 0 34.25 41.72 19.68 o 0 10 0 15.33 -7.25 17.31 o 2 10 0 538.11 505.81 31.22 o 1 1 1 758.97 716.37 16.01 o 2 1 1 5222.17 5159.68 79.20 o 3 1 1 14265.99 14574.15 150.37 o 4 1 1 40.72 48.24 9.62 o 5 1 1 120.51 78.13 10.36 o 6 1 1 143.11 156.70 12.28 o 7 1 1 4231.81 4261.61 71.82 o 8 1 1 37.48 23.23 11.69 o 9 1 1 357.33 334.00 19.09 o 10 1 1 155.69 147.08 17.90 o 11 1 1 224.26 256.87 20.72 o 12 1 1 105.28 95.29 18.79 o 13 1 1 7.68 14.35 17.01 o 14 1 1 100.78 83.45 22.34 o 0 2 1 617.83 581.62 15.85 o 1 2 1 4766.41 4663.81 68.13 o 2 2 1 39591.90 39892.86 256.37 o 3 2 1 4794.33 4774.53 69.03 o 4 2 1 11361.23 11227.34 161.58 o 5 2 1 550.14 520.45 16.28 o 6 2 1 6672.66 6748.96 104.52 o 7 2 1 1724.27 1867.65 36.44 o 8 2 1 2700.95 2758.07 50.38 o 9 2 1 113.59 103.13 15.54 o 10 2 1 4575.48 4420.90 78.00 o 11 2 1 11.31 8.29 15.98 o 12 2 1 224.69 256.28 21.16 o 13 2 1 8.47 14.50 17.01 o 14 2 1 211.48 271.22 25.45 o 1 3 1 369.18 339.25 12.73 o 2 3 1 9739.24 9785.44 148.09 o 3 3 1 7604.47 7272.68 109.96 o 4 3 1 5047.59 5207.45 76.67 o 5 3 1 12.20 -0.74 9.77 o 6 3 1 748.12 726.96 20.58 o 7 3 1 1022.70 921.43 24.43 o 8 3 1 27.37 19.23 13.32 o 9 3 1 155.28 159.21 18.64 o 10 3 1 20.57 7.69 15.24 o 11 3 1 222.97 215.29 21.01 o 12 3 1 0.11 6.21 16.87 o 13 3 1 0.27 -18.20 18.20 o 14 3 1 39.25 50.01 20.12 o 0 4 1 369.56 359.94 14.21 o 1 4 1 122.48 117.93 11.39 o 2 4 1 671.21 749.35 19.10 o 3 4 1 447.49 436.91 16.28 o 4 4 1 4510.18 4554.87 72.13 o 5 4 1 143.82 148.41 14.06 o 6 4 1 202.09 227.58 16.13 o 7 4 1 505.47 519.31 22.64 o 8 4 1 301.61 304.54 21.46 o 9 4 1 1066.28 988.83 30.49 o 10 4 1 19.23 25.60 15.09 o 11 4 1 0.86 -10.95 15.24 o 12 4 1 2.87 -3.25 17.16 o 13 4 1 128.36 145.00 21.60 o 1 5 1 1274.44 1231.90 27.40 o 2 5 1 2709.75 2703.11 49.51 o 3 5 1 274.53 293.30 16.72 o 4 5 1 1858.23 1908.24 38.22 o 5 5 1 2867.65 2784.32 53.05 o 6 5 1 1426.14 1433.59 33.61 o 7 5 1 555.52 552.02 24.86 o 8 5 1 203.96 168.54 18.35 o 9 5 1 130.16 146.48 18.35 o 10 5 1 131.98 117.19 19.24 o 11 5 1 41.06 58.00 19.38 o 12 5 1 72.59 84.63 20.27 o 0 6 1 3099.47 3105.23 53.95 o 1 6 1 284.88 292.70 16.87 o 2 6 1 3477.94 3280.83 60.19 o 3 6 1 1.21 13.61 13.17 o 4 6 1 969.75 965.30 27.39 o 5 6 1 204.61 160.10 18.05 o 6 6 1 1261.77 1311.82 33.90 o 7 6 1 57.16 42.91 17.46 o 8 6 1 178.35 193.98 20.57 o 9 6 1 20.34 9.03 16.87 o 10 6 1 779.20 786.47 32.56 o 11 6 1 41.03 47.64 19.68 o 1 7 1 1620.78 1603.20 36.28 o 2 7 1 457.59 443.22 22.64 o 3 7 1 8.95 -1.78 13.61 o 4 7 1 103.40 115.85 17.61 o 5 7 1 1103.27 1167.50 33.90 o 6 7 1 982.33 1109.24 33.75 o 7 7 1 0.13 -1.33 15.83 o 8 7 1 441.71 410.50 26.93 o 9 7 1 102.66 104.16 21.31 o 10 7 1 0.24 3.55 17.61 o 0 8 1 1418.54 1440.51 38.20 o 1 8 1 1.64 -1.92 15.39 o 2 8 1 151.16 152.99 19.38 o 3 8 1 1.25 -13.61 15.39 o 4 8 1 784.43 773.17 30.49 o 5 8 1 1.94 -17.31 17.31 o 6 8 1 0.17 1.48 16.27 o 7 8 1 38.16 55.78 19.23 o 8 8 1 21.45 29.15 20.42 o 9 8 1 70.86 48.53 20.12 o 1 9 1 3.27 -10.21 18.05 o 2 9 1 1.29 11.24 17.01 o 3 9 1 0.14 18.05 16.72 o 4 9 1 64.24 32.40 19.23 o 5 9 1 8.22 9.03 19.23 o 6 9 1 12.61 -5.92 19.53 o 7 9 1 162.53 132.28 23.23 o 0 10 1 60.56 87.44 20.86 o 1 10 1 18.82 22.49 19.83 o 2 10 1 298.02 328.49 27.52 o 3 10 1 38.62 42.91 21.60 o 1 0 2 15316.00 15902.32 101.20 o 2 0 2 2557.12 2688.28 45.97 o 3 0 2 5842.71 6094.36 95.24 o 4 0 2 1380.22 1362.65 26.38 o 5 0 2 350.80 354.62 13.62 o 6 0 2 4.77 19.09 9.62 o 7 0 2 1730.81 2028.23 36.88 o 8 0 2 1622.93 1607.49 33.32 o 9 0 2 1505.50 1544.74 33.32 o 10 0 2 1342.74 1252.09 32.72 o 11 0 2 143.46 151.96 19.24 o 12 0 2 523.62 472.82 25.16 o 13 0 2 1291.94 1167.66 39.08 o 14 0 2 178.86 206.26 23.38 o 1 1 2 6677.36 6519.66 79.83 o 2 1 2 324.06 358.41 12.73 o 3 1 2 3190.80 3321.71 53.80 o 4 1 2 367.21 376.10 13.03 o 5 1 2 3159.85 3249.20 52.83 o 6 1 2 62.24 78.57 10.51 o 7 1 2 2511.47 2491.97 43.57 o 8 1 2 1.99 16.42 11.10 o 9 1 2 0.27 -10.80 12.43 o 10 1 2 31.88 21.45 15.68 o 11 1 2 4.15 32.70 15.09 o 12 1 2 448.25 455.04 25.75 o 13 1 2 91.45 100.61 20.12 o 14 1 2 19.24 24.86 18.49 o 0 2 2 6901.98 6793.15 98.13 o 1 2 2 22838.26 22765.25 182.90 o 2 2 2 5648.71 5598.39 80.35 o 3 2 2 13244.87 13448.07 163.70 o 4 2 2 187.27 201.99 12.13 o 5 2 2 1086.10 1154.20 25.92 o 6 2 2 0.15 1.04 10.21 o 7 2 2 230.82 250.08 15.09 o 8 2 2 3.67 4.29 12.43 o 9 2 2 337.80 300.10 18.94 o 10 2 2 1803.12 1851.19 40.72 o 11 2 2 239.67 237.20 20.42 o 12 2 2 4.11 22.49 16.27 o 13 2 2 215.88 202.42 23.08 o 14 2 2 31.54 37.73 20.57 o 1 3 2 3904.19 3830.54 58.09 o 2 3 2 2724.54 2700.93 46.59 o 3 3 2 6837.87 6642.44 105.71 o 4 3 2 1716.13 1875.45 34.08 o 5 3 2 601.52 596.96 17.91 o 6 3 2 0.93 -1.63 9.91 o 7 3 2 1.15 9.47 11.98 o 8 3 2 2851.49 2808.70 53.79 o 9 3 2 155.76 151.22 17.02 o 10 3 2 6.42 -0.30 14.50 o 11 3 2 90.66 66.29 16.72 o 12 3 2 10.84 7.99 17.01 o 13 3 2 40.03 54.89 19.68 o 14 3 2 4.82 13.02 20.12 o 0 4 2 796.82 771.36 18.51 o 1 4 2 3220.05 3312.85 52.22 o 2 4 2 328.56 336.68 14.95 o 3 4 2 813.96 865.03 21.47 o 4 4 2 3099.90 3095.55 52.79 o 5 4 2 43.23 53.71 12.43 o 6 4 2 1026.20 1026.10 25.46 o 7 4 2 99.58 77.09 15.09 o 8 4 2 777.63 811.85 28.12 o 9 4 2 0.46 0.44 14.35 o 10 4 2 67.28 63.03 17.61 o 11 4 2 172.50 156.25 19.83 o 12 4 2 207.91 215.73 22.93 o 13 4 2 8.29 14.50 18.20 o 1 5 2 1303.73 1243.03 26.95 o 2 5 2 4.24 8.73 11.39 o 3 5 2 952.18 926.60 23.98 o 4 5 2 1.83 5.18 12.13 o 5 5 2 407.72 401.49 19.68 o 6 5 2 165.26 147.97 16.57 o 7 5 2 1377.62 1392.02 33.90 o 8 5 2 969.47 825.22 30.20 o 9 5 2 134.98 128.58 18.05 o 10 5 2 53.09 75.61 16.87 o 11 5 2 185.83 219.43 21.45 o 12 5 2 56.42 90.11 19.38 o 0 6 2 12.25 15.39 13.02 o 1 6 2 101.72 100.02 14.65 o 2 6 2 158.22 167.05 16.13 o 3 6 2 165.51 186.29 16.87 o 4 6 2 254.88 281.59 18.64 o 5 6 2 729.34 688.68 25.16 o 6 6 2 503.99 523.00 24.71 o 7 6 2 456.96 444.40 23.97 o 8 6 2 49.03 97.50 18.05 o 9 6 2 7.51 3.25 16.27 o 10 6 2 173.89 157.73 21.60 o 11 6 2 135.25 135.98 22.05 o 1 7 2 1.21 0.30 15.24 o 2 7 2 71.54 77.53 15.98 o 3 7 2 288.58 254.66 20.27 o 4 7 2 4.94 7.69 15.54 o 5 7 2 439.72 503.29 24.57 o 6 7 2 16.97 10.36 15.39 o 7 7 2 223.94 187.18 21.16 o 8 7 2 37.25 36.55 17.90 o 9 7 2 264.19 247.11 23.97 o 10 7 2 9.76 7.25 18.05 o 0 8 2 618.16 610.92 27.08 o 1 8 2 379.56 404.57 24.12 o 2 8 2 56.78 59.48 16.72 o 3 8 2 14.11 1.04 15.54 o 4 8 2 73.67 63.47 18.64 o 5 8 2 61.70 91.44 18.79 o 6 8 2 40.48 51.78 18.20 o 7 8 2 12.42 26.78 17.31 o 8 8 2 323.40 334.12 26.63 o 9 8 2 5.88 -1.33 18.94 o 1 9 2 5.54 7.25 17.16 o 2 9 2 51.26 35.95 18.49 o 3 9 2 156.96 184.66 21.90 o 4 9 2 21.60 -13.76 18.20 o 5 9 2 199.59 213.96 23.97 o 6 9 2 9.61 -9.17 18.64 o 7 9 2 1.90 0.89 19.09 o 0 10 2 62.39 60.96 20.57 o 1 10 2 44.70 15.54 18.94 o 2 10 2 204.22 205.23 23.67 o 3 10 2 0.02 28.11 19.83 o 1 1 3 118.05 115.58 9.47 o 2 1 3 382.28 401.51 13.03 o 3 1 3 928.53 908.24 20.44 o 4 1 3 9.90 10.21 9.17 o 5 1 3 94.80 88.34 10.51 o 6 1 3 766.11 805.94 19.69 o 7 1 3 345.63 371.01 16.57 o 8 1 3 376.99 397.94 18.50 o 9 1 3 95.41 82.86 14.65 o 10 1 3 554.79 552.91 23.83 o 11 1 3 115.00 124.14 18.05 o 12 1 3 6.67 4.88 16.87 o 13 1 3 18.33 10.06 17.75 o 14 1 3 158.18 148.70 23.08 o 0 2 3 2615.76 2669.46 47.09 o 1 2 3 17561.39 17444.46 164.43 o 2 2 3 1154.85 1173.10 24.30 o 3 2 3 2632.83 2711.62 44.81 o 4 2 3 915.19 996.89 22.36 o 5 2 3 782.47 870.97 20.58 o 6 2 3 2200.84 2329.54 42.68 o 7 2 3 15.84 22.19 11.24 o 8 2 3 238.29 213.08 15.83 o 9 2 3 32.30 56.96 14.50 o 10 2 3 29.21 18.64 15.68 o 11 2 3 108.23 117.78 18.35 o 12 2 3 266.43 328.79 23.23 o 13 2 3 142.57 181.40 20.71 o 14 2 3 234.23 218.69 24.71 o 1 3 3 1134.56 1141.50 23.26 o 2 3 3 2667.62 2740.81 47.03 o 3 3 3 3820.52 4030.95 65.03 o 4 3 3 529.92 596.95 17.02 o 5 3 3 1558.54 1638.53 31.55 o 6 3 3 807.77 768.29 21.17 o 7 3 3 510.85 493.72 19.54 o 8 3 3 578.89 583.27 22.35 o 9 3 3 139.61 141.75 16.87 o 10 3 3 640.99 589.92 25.46 o 11 3 3 184.78 158.18 19.24 o 12 3 3 0.34 -1.78 16.13 o 13 3 3 61.80 58.15 21.16 o 0 4 3 66.38 71.02 10.36 o 1 4 3 284.95 287.69 13.76 o 2 4 3 52.82 37.14 10.65 o 3 4 3 2595.55 2567.97 46.99 o 4 4 3 432.84 456.13 17.91 o 5 4 3 889.59 953.81 23.98 o 6 4 3 725.45 742.01 23.09 o 7 4 3 516.79 518.87 21.61 o 8 4 3 638.22 672.08 25.31 o 9 4 3 132.69 146.04 17.76 o 10 4 3 0.07 14.06 14.80 o 11 4 3 2.26 0.74 16.27 o 12 4 3 469.80 506.39 28.26 o 13 4 3 18.06 23.52 20.86 o 1 5 3 92.94 111.42 12.58 o 2 5 3 95.90 119.26 12.87 o 3 5 3 3421.12 3501.92 60.79 o 4 5 3 51.01 53.56 13.02 o 5 5 3 1085.74 1052.89 27.54 o 6 5 3 219.32 197.84 17.76 o 7 5 3 51.46 76.05 15.98 o 8 5 3 8.22 12.58 15.24 o 9 5 3 379.41 356.48 22.49 o 10 5 3 59.62 67.17 17.61 o 11 5 3 11.01 5.47 17.46 o 12 5 3 58.01 45.13 19.53 o 0 6 3 181.38 181.56 15.98 o 1 6 3 0.73 -2.22 11.69 o 2 6 3 71.43 57.11 14.20 o 3 6 3 21.05 21.45 12.72 o 4 6 3 130.38 127.99 15.98 o 5 6 3 36.42 39.80 15.24 o 6 6 3 331.87 299.80 21.31 o 7 6 3 14.95 8.88 15.39 o 8 6 3 1.89 -4.44 14.80 o 9 6 3 170.02 173.27 21.01 o 10 6 3 266.85 263.09 22.79 o 11 6 3 0.68 14.50 17.46 o 1 7 3 65.01 77.23 15.54 o 2 7 3 29.09 22.79 14.65 o 3 7 3 76.95 81.82 16.13 o 4 7 3 47.51 59.33 16.13 o 5 7 3 368.25 341.09 23.38 o 6 7 3 51.80 37.73 17.61 o 7 7 3 1.98 -14.35 16.42 o 8 7 3 169.70 160.39 20.42 o 9 7 3 3.39 7.69 17.01 o 10 7 3 83.20 68.50 20.57 o 0 8 3 366.73 395.69 23.97 o 1 8 3 22.40 26.78 15.83 o 2 8 3 9.75 12.13 16.27 o 3 8 3 2.47 -5.77 15.68 o 4 8 3 83.00 86.85 18.49 o 5 8 3 8.31 13.17 17.46 o 6 8 3 127.02 125.32 19.68 o 7 8 3 83.83 40.39 19.09 o 8 8 3 128.49 141.45 21.31 o 9 8 3 0.16 6.66 19.23 o 1 9 3 57.57 43.20 19.23 o 2 9 3 6.73 -16.72 16.72 o 3 9 3 35.02 28.70 18.79 o 4 9 3 6.81 23.67 17.61 o 5 9 3 206.40 198.42 22.93 o 6 9 3 35.26 35.81 19.09 o 7 9 3 11.93 -19.38 20.42 o 0 10 3 2.11 5.77 18.64 o 1 10 3 0.86 9.91 19.09 o 2 10 3 59.51 64.21 21.90 o 3 10 3 246.25 286.17 26.34 o 0 0 4 18179.12 16909.48 122.17 o 1 0 4 804.28 779.50 17.79 o 2 0 4 13504.07 12969.78 128.71 o 3 0 4 1894.86 1937.27 34.71 o 4 0 4 10261.00 9923.15 142.58 o 5 0 4 366.59 392.80 14.06 o 6 0 4 442.16 390.58 15.10 o 7 0 4 3542.35 3758.18 62.44 o 8 0 4 2620.15 2562.91 47.86 o 9 0 4 48.85 47.64 13.46 o 10 0 4 1996.53 2013.13 42.95 o 11 0 4 1659.51 1724.67 39.98 o 12 0 4 1119.29 1092.42 36.12 o 13 0 4 11.26 22.93 17.75 o 14 0 4 5.44 11.10 18.49 o 1 1 4 6089.21 5978.36 86.64 o 2 1 4 2372.45 2574.56 40.54 o 3 1 4 0.44 10.21 8.73 o 4 1 4 212.13 205.55 11.10 o 5 1 4 1.30 13.61 9.32 o 6 1 4 3207.77 3482.43 56.95 o 7 1 4 0.94 0.00 10.50 o 8 1 4 722.84 715.07 22.50 o 9 1 4 227.99 254.51 18.20 o 10 1 4 59.84 72.80 16.13 o 11 1 4 136.16 133.91 18.79 o 12 1 4 747.01 709.81 30.04 o 13 1 4 13.75 27.22 17.46 o 14 1 4 0.21 6.81 19.23 o 0 2 4 33.43 55.34 9.77 o 1 2 4 3.84 2.37 9.17 o 2 2 4 20392.79 20106.69 192.09 o 3 2 4 9250.16 9432.10 141.05 o 4 2 4 84.34 85.97 10.95 o 5 2 4 28.97 28.26 10.21 o 6 2 4 413.98 476.55 17.02 o 7 2 4 33.65 23.53 11.10 o 8 2 4 22.69 20.42 12.87 o 9 2 4 432.94 437.60 21.01 o 10 2 4 1.70 6.81 14.65 o 11 2 4 458.94 407.99 23.68 o 12 2 4 236.57 251.69 23.67 o 13 2 4 9.76 20.27 18.79 o 14 2 4 51.19 43.50 20.57 o 1 3 4 3242.65 3190.33 50.32 o 2 3 4 2967.07 3075.37 51.34 o 3 3 4 104.59 105.06 11.10 o 4 3 4 672.50 748.90 19.10 o 5 3 4 2336.90 2583.32 45.05 o 6 3 4 128.48 172.08 13.61 o 7 3 4 1167.25 1140.33 28.28 o 8 3 4 148.00 170.16 16.42 o 9 3 4 586.86 595.54 24.27 o 10 3 4 172.94 177.11 18.94 o 11 3 4 79.54 102.09 18.05 o 12 3 4 87.21 93.07 18.49 o 13 3 4 0.86 2.37 18.94 o 0 4 4 737.70 666.64 17.91 o 1 4 4 419.12 422.85 15.39 o 2 4 4 1.26 5.18 10.36 o 3 4 4 6720.49 6811.57 106.16 o 4 4 4 6043.64 5865.05 90.92 o 5 4 4 801.12 779.08 22.06 o 6 4 4 934.85 898.87 24.72 o 7 4 4 312.83 318.01 18.65 o 8 4 4 892.80 870.80 28.57 o 9 4 4 0.13 13.02 14.50 o 10 4 4 903.71 834.94 30.05 o 11 4 4 48.72 46.46 17.02 o 12 4 4 66.56 77.09 19.38 o 13 4 4 75.02 91.88 19.83 o 1 5 4 10.76 11.98 10.50 o 2 5 4 970.19 1035.74 24.58 o 3 5 4 142.43 141.46 14.35 o 4 5 4 250.56 264.14 16.72 o 5 5 4 484.60 489.12 20.28 o 6 5 4 270.30 239.13 17.90 o 7 5 4 30.93 44.09 14.20 o 8 5 4 48.20 69.54 16.87 o 9 5 4 24.89 23.97 15.83 o 10 5 4 16.31 26.93 16.72 o 11 5 4 57.50 53.56 18.35 o 12 5 4 19.61 36.69 17.61 o 0 6 4 85.22 79.75 14.65 o 1 6 4 142.80 138.05 14.94 o 2 6 4 649.06 654.04 22.94 o 3 6 4 4.78 -3.40 13.32 o 4 6 4 857.96 806.41 25.76 o 5 6 4 542.58 504.36 23.09 o 6 6 4 351.35 391.26 22.49 o 7 6 4 0.27 22.19 15.09 o 8 6 4 0.27 1.48 15.54 o 9 6 4 118.87 103.57 19.09 o 10 6 4 87.71 89.22 21.01 o 11 6 4 19.27 -3.26 17.61 o 1 7 4 53.36 38.62 14.65 o 2 7 4 70.25 71.32 15.68 o 3 7 4 57.83 48.97 15.98 o 4 7 4 404.61 398.37 22.49 o 5 7 4 6.14 -15.54 15.54 o 6 7 4 220.90 217.66 21.31 o 7 7 4 109.43 114.52 18.20 o 8 7 4 37.61 15.98 18.20 o 9 7 4 1.20 -2.07 17.31 o 10 7 4 1.70 -9.91 17.75 o 0 8 4 1040.18 1051.70 32.71 o 1 8 4 39.63 35.36 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7 50.09 53.41 10.06 o 5 1 7 5797.72 6118.09 95.27 o 6 1 7 15.06 5.77 10.36 o 7 1 7 964.11 918.17 23.39 o 8 1 7 14.51 14.06 12.58 o 9 1 7 515.92 542.69 22.94 o 10 1 7 98.35 100.02 16.13 o 11 1 7 204.58 197.68 21.90 o 12 1 7 119.75 77.98 20.86 o 13 1 7 129.84 121.62 21.75 o 14 1 7 81.91 138.04 21.90 o 0 2 7 3725.08 3713.70 56.31 o 1 2 7 70.34 65.84 9.62 o 2 2 7 586.06 575.59 15.40 o 3 2 7 57.78 57.11 10.21 o 4 2 7 1641.88 1630.73 30.96 o 5 2 7 693.01 786.63 20.58 o 6 2 7 331.22 307.07 15.69 o 7 2 7 176.98 156.40 14.21 o 8 2 7 1254.23 1250.77 29.91 o 9 2 7 74.65 74.87 15.83 o 10 2 7 6.53 18.49 15.09 o 11 2 7 191.52 179.19 20.12 o 12 2 7 393.28 416.70 26.19 o 13 2 7 28.97 50.60 19.68 o 14 2 7 196.92 144.41 24.12 o 1 3 7 11431.24 11150.50 170.67 o 2 3 7 858.04 862.75 19.84 o 3 3 7 9620.26 9930.01 139.69 o 4 3 7 221.28 221.37 13.76 o 5 3 7 4219.64 4101.00 65.88 o 6 3 7 64.63 65.10 12.87 o 7 3 7 2998.06 3042.03 57.21 o 8 3 7 91.67 65.84 14.65 o 9 3 7 957.95 986.57 30.05 o 10 3 7 3.82 7.25 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45.77 o 8 1 13 652.75 673.70 25.90 o 9 1 13 644.95 614.93 26.94 o 10 1 13 31.61 12.13 15.98 o 11 1 13 571.68 571.83 28.71 o 12 1 13 0.00 2.22 17.31 o 13 1 13 70.71 93.21 21.75 o 0 2 13 1756.28 1753.26 32.89 o 1 2 13 198.51 213.97 13.91 o 2 2 13 89.98 59.63 11.10 o 3 2 13 299.38 295.52 16.28 o 4 2 13 1574.59 1655.02 34.36 o 5 2 13 293.72 266.07 17.31 o 6 2 13 55.79 37.58 14.35 o 7 2 13 57.34 30.48 14.94 o 8 2 13 269.53 335.75 21.31 o 9 2 13 0.07 -11.10 16.27 o 10 2 13 285.66 313.70 22.94 o 11 2 13 1.93 6.81 16.87 o 12 2 13 26.86 35.21 18.79 o 13 2 13 48.85 34.18 19.68 o 1 3 13 4645.74 4522.56 77.02 o 2 3 13 26.71 28.70 11.54 o 3 3 13 3952.86 3853.75 67.63 o 4 3 13 457.48 478.76 19.83 o 5 3 13 2165.77 2073.99 40.59 o 6 3 13 417.15 416.58 20.27 o 7 3 13 1135.82 1126.11 31.53 o 8 3 13 1138.78 1130.22 32.27 o 9 3 13 659.67 667.91 27.38 o 10 3 13 54.69 76.49 17.90 o 11 3 13 215.60 204.05 23.38 o 12 3 13 19.21 9.47 19.09 o 0 4 13 477.48 479.51 20.87 o 1 4 13 123.17 144.27 14.94 o 2 4 13 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