#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:02:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180815 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014640.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014640_Fobs loop_ _publ_author_name 'Palusiak, Marcin' 'Janowska, Izabela' 'Zakrzewski, Janusz' 'Grabowski, S\/lawomir J.' _publ_section_title ; Charge-assisted N---H···I and C---H···I hydrogen bonding in (1R,2S)-1-(ferrocenylmethyl)-2-(methoxymethyl)pyrrolidinium iodide ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m55 _journal_page_last m57 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7770 _cell_length_b 11.5750 _cell_length_c 20.1600 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file fa1094Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' guess in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 317.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 100681.26 96385.87 3344.68 o 4 0 0 17340.79 17439.78 175.44 o 6 0 0 219.24 163.81 61.80 o 8 0 0 18.34 102.57 134.16 o 1 1 0 23994.10 25112.39 407.65 o 2 1 0 37123.75 36955.23 525.34 o 3 1 0 3398.61 3425.62 54.98 o 4 1 0 19479.76 19818.49 149.63 o 5 1 0 1995.68 2288.40 73.00 o 6 1 0 7896.01 8011.25 126.59 o 7 1 0 114.20 102.78 63.40 o 8 1 0 1839.06 1861.98 83.32 o 9 1 0 23.06 0.71 117.51 o 0 2 0 5930.59 5977.13 57.61 o 1 2 0 5505.23 5676.70 53.74 o 2 2 0 21318.83 22335.92 121.95 o 3 2 0 323.04 383.31 19.40 o 4 2 0 6.22 0.00 44.91 o 5 2 0 1174.39 1205.05 48.08 o 6 2 0 40.50 67.10 69.82 o 7 2 0 327.68 346.89 43.52 o 8 2 0 278.43 273.60 51.05 o 9 2 0 39.75 0.00 117.14 o 1 3 0 5014.64 5135.02 52.82 o 2 3 0 985.79 977.25 37.66 o 3 3 0 9.65 0.00 38.11 o 4 3 0 6511.03 6721.66 93.95 o 5 3 0 544.90 516.67 31.89 o 6 3 0 2547.12 2558.02 94.82 o 7 3 0 206.82 137.16 62.02 o 8 3 0 1212.58 1174.27 57.26 o 9 3 0 110.09 33.65 120.84 o 0 4 0 25890.81 25308.31 171.43 o 1 4 0 927.09 921.99 39.88 o 2 4 0 15531.74 14980.17 104.36 o 3 4 0 3599.02 3511.15 69.81 o 4 4 0 9323.62 9132.52 109.52 o 5 4 0 688.42 646.48 35.21 o 6 4 0 751.55 716.80 41.58 o 7 4 0 474.14 449.34 47.29 o 8 4 0 3.73 4.04 103.77 o 9 4 0 91.59 0.00 123.55 o 1 5 0 7477.53 7078.78 78.35 o 2 5 0 2160.80 1967.43 63.83 o 3 5 0 8982.71 8988.75 113.19 o 4 5 0 2248.52 2113.16 74.56 o 5 5 0 2276.24 2162.51 86.78 o 6 5 0 2182.44 2160.83 99.93 o 7 5 0 200.90 191.86 71.82 o 8 5 0 696.10 665.24 57.70 o 0 6 0 7.92 17.27 60.92 o 1 6 0 234.33 214.61 22.69 o 2 6 0 128.45 107.64 31.21 o 3 6 0 39.14 29.86 53.97 o 4 6 0 29.21 58.60 47.33 o 5 6 0 1669.48 1689.64 66.96 o 6 6 0 65.15 44.75 84.46 o 7 6 0 891.20 884.91 54.16 o 8 6 0 124.48 65.54 115.29 o 1 7 0 1.28 0.00 51.10 o 2 7 0 242.55 259.34 28.67 o 3 7 0 159.69 129.13 47.10 o 4 7 0 284.15 342.05 36.47 o 5 7 0 139.63 101.73 60.66 o 6 7 0 222.84 306.35 51.90 o 7 7 0 8.72 61.75 102.93 o 8 7 0 106.58 126.23 86.20 o 0 8 0 5274.02 5376.75 138.83 o 1 8 0 11.55 0.00 60.25 o 2 8 0 3597.74 3667.86 94.01 o 3 8 0 266.09 235.89 39.84 o 4 8 0 550.52 625.57 41.34 o 5 8 0 335.57 375.19 44.41 o 6 8 0 49.47 125.65 73.64 o 7 8 0 447.57 407.63 58.07 o 1 9 0 2377.03 2256.82 89.09 o 2 9 0 502.18 488.52 38.62 o 3 9 0 1728.95 1650.03 66.21 o 4 9 0 736.77 792.30 46.51 o 5 9 0 586.00 572.84 49.93 o 6 9 0 477.63 483.39 55.97 o 7 9 0 14.92 0.00 119.25 o 0 10 0 135.60 130.67 55.94 o 1 10 0 10.98 37.15 78.05 o 2 10 0 18.26 96.28 81.10 o 3 10 0 113.89 171.55 65.75 o 4 10 0 9.43 62.62 93.29 o 5 10 0 624.27 637.45 55.30 o 6 10 0 9.83 0.00 116.18 o 1 11 0 196.73 216.55 57.14 o 2 11 0 0.67 23.15 90.06 o 3 11 0 210.34 242.13 54.39 o 4 11 0 4.24 24.87 104.39 o 5 11 0 68.42 70.28 113.97 o 6 11 0 0.28 9.77 125.05 o 0 12 0 57.85 39.09 113.23 o 1 12 0 1.37 0.00 100.54 o 2 12 0 144.02 187.45 65.37 o 3 12 0 52.67 59.58 107.02 o 4 12 0 75.75 40.09 115.60 o 5 12 0 98.53 65.29 124.46 o 1 13 0 351.90 370.64 56.94 o 2 13 0 11.35 14.68 114.03 o 3 13 0 228.02 297.51 77.31 o 0 14 0 0.05 20.90 173.90 o 1 14 0 9.78 0.00 124.85 o 2 0 1 1316.99 1309.77 33.35 o 3 0 1 1431.93 1372.58 41.91 o 4 0 1 218.59 248.36 22.73 o 5 0 1 5220.29 4954.84 91.39 o 6 0 1 206.32 193.61 46.14 o 7 0 1 4025.58 3981.21 116.68 o 8 0 1 3.98 5.31 97.54 o 9 0 1 1171.77 1044.31 64.21 o -9 1 1 393.38 369.76 72.34 o -8 1 1 103.16 133.62 82.13 o -7 1 1 195.18 197.02 47.35 o -6 1 1 171.12 184.03 35.72 o -5 1 1 3339.51 3454.69 82.51 o -4 1 1 1507.71 1564.26 56.96 o -3 1 1 10016.07 10217.14 87.21 o -2 1 1 7782.33 8039.21 77.97 o 2 1 1 8002.08 8438.79 82.06 o 3 1 1 10040.13 10472.85 102.86 o 4 1 1 1531.85 1703.88 57.66 o 5 1 1 3287.45 3396.74 82.91 o 6 1 1 161.95 166.68 35.76 o 7 1 1 180.67 131.93 46.73 o 8 1 1 99.34 142.33 75.18 o 9 1 1 402.86 329.83 59.86 o -9 2 1 619.28 646.74 61.92 o -8 2 1 896.91 815.32 53.70 o -7 2 1 3024.01 2778.32 111.15 o -6 2 1 1369.45 1295.08 58.44 o -5 2 1 5209.40 5270.78 95.17 o -4 2 1 3123.65 3155.38 69.12 o -3 2 1 3993.36 3996.28 60.94 o -2 2 1 980.52 1007.69 34.19 o -1 2 1 646.95 630.89 24.26 o 0 2 1 3135.54 3219.51 32.72 o 1 2 1 590.07 586.36 23.67 o 2 2 1 819.22 800.53 32.86 o 3 2 1 4201.03 4226.68 62.76 o 4 2 1 3123.57 3336.35 69.87 o 5 2 1 5336.09 5643.11 96.33 o 6 2 1 1360.13 1391.05 62.58 o 7 2 1 3049.00 3075.87 110.99 o 8 2 1 890.90 820.18 53.80 o 9 2 1 638.85 663.37 61.78 o -9 3 1 410.95 419.83 61.85 o -8 3 1 80.32 70.40 104.64 o -7 3 1 450.84 405.69 44.81 o -6 3 1 405.72 420.89 38.35 o -5 3 1 1899.09 1846.80 82.54 o -4 3 1 1800.70 1780.59 63.16 o -3 3 1 9719.01 9662.33 91.48 o -2 3 1 1342.39 1424.93 41.27 o -1 3 1 22043.13 21657.73 159.87 o 0 3 1 4015.36 3994.44 69.60 o 1 3 1 22712.17 22410.56 108.78 o 2 3 1 1493.80 1605.97 45.68 o 3 3 1 9758.47 9826.34 91.88 o 4 3 1 1733.99 1767.17 62.22 o 5 3 1 1913.18 1830.06 75.77 o 6 3 1 395.24 428.95 38.34 o 7 3 1 432.39 423.94 44.76 o 8 3 1 77.56 46.13 103.35 o 9 3 1 407.07 325.52 68.33 o -9 4 1 652.90 645.74 65.37 o -8 4 1 18.93 13.67 104.64 o -7 4 1 2918.72 2755.70 116.85 o -6 4 1 90.84 88.49 48.50 o -5 4 1 5914.44 5715.68 107.94 o -4 4 1 542.28 536.26 28.65 o -3 4 1 5917.53 5827.85 80.56 o -2 4 1 1837.28 1816.43 48.79 o -1 4 1 696.99 695.48 27.08 o 0 4 1 2499.91 2409.12 45.35 o 1 4 1 778.04 800.27 36.59 o 2 4 1 1843.07 1912.47 50.04 o 3 4 1 6139.34 6111.33 82.09 o 4 4 1 463.69 462.38 28.26 o 5 4 1 5977.43 5872.33 108.05 o 6 4 1 96.58 64.50 59.21 o 7 4 1 2997.56 3051.99 117.88 o 8 4 1 20.06 36.08 105.79 o 9 4 1 640.08 635.54 65.03 o -8 5 1 434.62 390.36 57.23 o -7 5 1 10.00 21.29 92.64 o -6 5 1 1203.11 1161.66 52.97 o -5 5 1 1089.47 1106.17 47.25 o -4 5 1 2849.45 2831.83 80.25 o -3 5 1 8265.14 8296.20 100.19 o -2 5 1 1669.69 1625.48 54.26 o -1 5 1 13898.70 13590.35 108.85 o 0 5 1 91.40 80.53 21.36 o 1 5 1 13770.77 13822.66 147.51 o 2 5 1 1736.71 1723.26 71.80 o 3 5 1 8677.57 8925.18 102.91 o 4 5 1 2962.35 2838.26 80.41 o 5 5 1 1099.34 1076.16 47.34 o 6 5 1 1217.05 1153.85 53.25 o 7 5 1 6.88 3.96 93.45 o 8 5 1 451.21 408.65 56.95 o -8 6 1 180.61 127.13 88.32 o -7 6 1 1034.57 1012.75 54.84 o -6 6 1 348.15 405.88 43.65 o -5 6 1 1916.56 1980.45 90.91 o -4 6 1 2135.36 2053.56 80.78 o -3 6 1 2132.51 2104.53 71.74 o -2 6 1 6908.58 6614.74 144.93 o -1 6 1 435.72 456.93 23.87 o 0 6 1 12673.17 12571.56 109.10 o 1 6 1 434.77 442.15 23.89 o 2 6 1 6947.76 6801.34 93.04 o 3 6 1 2008.37 1950.25 70.68 o 4 6 1 2238.85 2218.83 81.48 o 5 6 1 2022.89 2018.73 81.88 o 6 6 1 398.40 395.34 44.31 o 7 6 1 1038.10 1033.74 54.89 o 8 6 1 186.60 226.18 73.42 o -8 7 1 136.72 134.00 92.97 o -7 7 1 255.28 202.17 67.88 o -6 7 1 532.29 538.37 47.93 o -5 7 1 501.05 498.82 42.15 o -4 7 1 1525.14 1468.71 58.67 o -3 7 1 1878.41 1906.63 77.96 o -2 7 1 3719.98 3709.21 84.41 o -1 7 1 2855.45 2820.05 74.96 o 0 7 1 2578.52 2530.29 69.97 o 1 7 1 2911.71 2946.08 75.75 o 2 7 1 3783.06 3744.53 111.11 o 3 7 1 1870.65 1822.66 77.67 o 4 7 1 1624.56 1700.68 68.78 o 5 7 1 564.38 593.77 42.53 o 6 7 1 589.40 548.86 48.15 o 7 7 1 263.93 188.05 76.20 o 8 7 1 140.29 48.05 124.00 o -7 8 1 407.94 385.30 57.94 o -6 8 1 1.18 0.00 98.37 o -5 8 1 505.57 521.81 45.57 o -4 8 1 319.93 302.35 40.39 o -3 8 1 1401.28 1433.76 73.04 o -2 8 1 1195.00 1160.74 52.76 o -1 8 1 1579.32 1543.91 72.86 o 0 8 1 3046.54 2938.08 82.56 o 1 8 1 1614.76 1570.91 73.56 o 2 8 1 1252.96 1234.37 52.51 o 3 8 1 1423.35 1341.53 58.35 o 4 8 1 374.38 375.43 40.16 o 5 8 1 438.92 451.82 45.52 o 6 8 1 2.13 19.78 97.61 o 7 8 1 408.33 407.78 57.88 o -7 9 1 31.54 0.00 119.83 o -6 9 1 482.32 449.26 55.65 o -5 9 1 169.14 102.60 73.69 o -4 9 1 820.23 762.65 46.37 o -3 9 1 478.82 496.28 41.17 o -2 9 1 893.20 855.24 40.42 o -1 9 1 319.57 368.61 36.45 o 0 9 1 7.14 28.84 68.00 o 1 9 1 310.99 350.60 36.18 o 2 9 1 858.20 850.18 40.01 o 3 9 1 466.85 506.87 41.01 o 4 9 1 767.80 783.39 46.32 o 5 9 1 159.16 155.44 53.22 o 6 9 1 492.90 438.38 62.76 o 7 9 1 32.67 91.65 118.96 o -6 10 1 172.49 151.30 69.92 o -5 10 1 71.91 71.65 104.74 o -4 10 1 288.21 264.46 52.40 o -3 10 1 104.18 134.45 77.70 o -2 10 1 1368.86 1326.49 59.60 o -1 10 1 130.91 122.00 79.86 o 0 10 1 2006.61 1975.41 78.58 o 1 10 1 123.70 100.49 59.74 o 2 10 1 1364.07 1461.93 66.92 o 3 10 1 95.00 102.07 87.63 o 4 10 1 274.82 260.70 54.04 o 5 10 1 71.78 126.21 104.29 o 6 10 1 183.41 182.55 74.60 o -6 11 1 231.10 135.64 128.56 o -5 11 1 124.22 136.20 101.95 o -4 11 1 474.98 510.52 54.48 o -3 11 1 94.57 93.91 86.93 o -2 11 1 588.19 639.13 48.96 o -1 11 1 43.14 65.64 88.76 o 0 11 1 301.95 317.49 56.49 o 1 11 1 43.86 68.36 89.27 o 2 11 1 602.76 659.87 48.51 o 3 11 1 89.63 13.17 98.14 o 4 11 1 477.44 488.14 54.42 o 5 11 1 116.19 91.11 115.54 o 6 11 1 205.56 151.49 96.22 o -5 12 1 105.28 26.60 94.62 o -4 12 1 31.24 77.58 113.70 o -3 12 1 303.20 316.59 55.15 o -2 12 1 144.98 134.86 78.83 o -1 12 1 548.69 580.08 52.38 o 0 12 1 220.90 235.15 55.41 o 1 12 1 536.18 596.65 52.51 o 2 12 1 128.94 148.63 62.16 o 3 12 1 294.43 303.69 61.45 o 4 12 1 28.55 4.20 114.40 o 5 12 1 104.69 76.70 125.68 o -3 13 1 3.93 26.47 118.60 o -2 13 1 133.47 117.28 86.61 o -1 13 1 23.64 98.24 110.59 o 0 13 1 104.20 68.12 83.88 o 1 13 1 23.77 21.41 112.03 o 2 13 1 133.31 132.80 115.23 o 3 13 1 2.33 9.78 118.61 o -1 14 1 12.64 20.43 122.89 o 0 14 1 220.43 288.34 69.34 o 1 14 1 13.18 0.00 124.30 o 1 0 2 494.96 492.05 16.94 o 2 0 2 16132.32 16786.02 99.10 o 3 0 2 384.77 411.37 18.87 o 4 0 2 11.15 53.94 37.91 o 5 0 2 2.25 0.00 54.27 o 6 0 2 79.48 92.86 44.08 o 7 0 2 26.08 0.00 82.68 o 8 0 2 233.11 224.52 63.70 o 9 0 2 204.75 98.44 106.39 o -9 1 2 456.07 458.60 59.89 o -8 1 2 1187.79 1092.40 55.16 o -7 1 2 1536.89 1549.23 68.55 o -6 1 2 3482.19 3375.81 99.26 o -5 1 2 2817.78 2841.69 78.97 o -4 1 2 9236.05 9385.13 142.22 o -3 1 2 2751.38 2865.01 54.00 o -2 1 2 3162.30 3249.41 56.05 o -1 1 2 17256.04 17842.83 97.97 o 1 1 2 17904.19 18543.97 181.58 o 2 1 2 3523.32 3579.68 46.52 o 3 1 2 2902.47 3120.40 54.63 o 4 1 2 8987.35 9127.61 98.29 o 5 1 2 2901.88 2918.92 79.76 o 6 1 2 3454.69 3517.08 98.38 o 7 1 2 1492.29 1549.18 68.63 o 8 1 2 1181.01 1099.09 54.87 o 9 1 2 452.25 431.30 60.02 o -9 2 2 87.60 145.29 119.42 o -8 2 2 25.87 0.00 102.05 o -7 2 2 92.85 125.71 63.80 o -6 2 2 613.08 634.38 39.00 o -5 2 2 1993.23 2186.54 76.59 o -4 2 2 9195.26 9213.44 110.33 o -3 2 2 7746.76 8200.17 81.57 o -2 2 2 15525.44 15698.40 91.00 o -1 2 2 26881.27 27244.68 128.02 o 0 2 2 71814.15 62424.77 514.49 o 1 2 2 25223.97 25463.62 112.86 o 2 2 2 15898.31 16221.41 92.19 o 3 2 2 7482.54 7793.82 79.88 o 4 2 2 9165.03 9287.05 126.21 o 5 2 2 1904.30 2016.49 75.58 o 6 2 2 623.73 595.62 39.37 o 7 2 2 100.24 67.88 87.76 o 8 2 2 28.86 79.52 100.93 o 9 2 2 87.32 118.90 120.74 o -9 3 2 285.73 285.82 61.90 o -8 3 2 778.06 776.84 55.65 o -7 3 2 1224.25 1125.38 50.73 o -6 3 2 2629.95 2561.18 95.29 o -5 3 2 4353.24 4253.86 94.78 o -4 3 2 4597.21 4668.44 81.77 o -3 3 2 6740.90 6699.55 79.57 o -2 3 2 7843.87 7991.02 73.81 o -1 3 2 10714.40 11022.23 74.94 o 0 3 2 5070.75 5292.26 80.54 o 1 3 2 11483.15 11769.96 96.57 o 2 3 2 7191.02 7250.47 85.16 o 3 3 2 6785.88 6851.93 80.62 o 4 3 2 4587.69 4515.95 81.15 o 5 3 2 4402.82 4464.48 94.07 o 6 3 2 2548.51 2461.14 94.94 o 7 3 2 1244.61 1285.39 59.27 o 8 3 2 769.17 810.47 55.51 o 9 3 2 288.96 281.25 79.44 o -9 4 2 204.40 122.17 126.00 o -8 4 2 228.39 248.49 60.12 o -7 4 2 385.33 355.60 52.10 o -6 4 2 396.66 414.28 40.22 o -5 4 2 1094.50 1044.27 49.56 o -4 4 2 193.04 210.54 27.41 o -3 4 2 942.74 893.07 38.48 o -2 4 2 2077.16 2070.10 51.64 o -1 4 2 3565.02 3658.30 54.81 o 0 4 2 4342.21 4242.80 55.73 o 1 4 2 3743.59 3774.14 54.97 o 2 4 2 2104.42 2178.45 52.06 o 3 4 2 864.03 813.11 35.42 o 4 4 2 154.91 189.81 29.90 o 5 4 2 1075.05 1021.17 42.49 o 6 4 2 395.42 382.60 40.39 o 7 4 2 376.04 324.11 46.84 o 8 4 2 216.57 188.58 75.33 o 9 4 2 208.45 145.82 90.11 o -8 5 2 270.14 204.89 85.46 o -7 5 2 547.68 518.94 49.83 o -6 5 2 723.78 714.66 43.63 o -5 5 2 773.48 815.80 38.38 o -4 5 2 1913.65 1903.92 74.10 o -3 5 2 2553.28 2697.26 69.93 o -2 5 2 1869.32 1916.88 56.66 o -1 5 2 422.27 503.22 23.05 o 0 5 2 16.18 20.18 35.94 o 1 5 2 475.22 583.79 25.59 o 2 5 2 1823.11 1765.83 56.79 o 3 5 2 2627.75 2768.85 76.05 o 4 5 2 1875.20 1859.03 73.25 o 5 5 2 751.96 808.73 38.09 o 6 5 2 707.52 721.64 43.21 o 7 5 2 530.64 555.84 49.47 o 8 5 2 258.12 277.37 61.80 o -8 6 2 40.61 0.00 115.52 o -7 6 2 370.86 321.64 51.61 o -6 6 2 273.45 287.94 43.96 o -5 6 2 754.39 806.81 40.54 o -4 6 2 2392.82 2324.51 83.11 o -3 6 2 4142.60 4104.49 87.20 o -2 6 2 6182.31 6001.16 96.42 o -1 6 2 8222.78 8082.66 94.40 o 0 6 2 7791.00 7468.98 89.64 o 1 6 2 7942.21 7861.83 92.96 o 2 6 2 6047.31 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115.64 o 4 2 22 151.41 169.29 78.57 o -3 3 22 193.88 230.00 65.95 o -2 3 22 18.08 95.63 110.93 o -1 3 22 260.91 285.18 71.59 o 0 3 22 18.33 0.00 108.83 o 1 3 22 260.26 363.16 56.29 o 2 3 22 19.05 0.00 112.80 o 3 3 22 194.84 203.83 75.51 o -3 4 22 20.88 138.37 118.99 o -2 4 22 88.90 91.21 117.10 o -1 4 22 43.66 120.96 70.98 o 0 4 22 95.58 151.05 112.31 o 1 4 22 43.02 36.78 114.20 o 2 4 22 84.93 135.62 115.94 o 3 4 22 19.02 16.36 120.87 o -2 5 22 6.04 2.80 106.83 o -1 5 22 38.02 0.00 118.25 o 0 5 22 1.77 4.01 115.24 o 1 5 22 36.77 76.43 118.47 o 2 5 22 5.05 0.00 120.63 o -1 6 22 53.70 14.96 123.24 o 0 6 22 43.06 60.85 108.21 o 1 6 22 54.76 10.44 122.85 o 1 0 23 0.02 4.15 109.86 o 2 0 23 1.21 29.36 114.28 o 3 0 23 0.03 27.85 118.56 o -3 1 23 17.82 102.49 107.33 o -2 1 23 68.57 61.56 81.99 o -1 1 23 3.32 0.00 112.52 o 0 1 23 48.13 79.43 111.61 o 1 1 23 3.08 46.09 100.42 o 2 1 23 72.38 55.89 105.14 o 3 1 23 16.46 0.00 120.59 o -3 2 23 15.71 43.32 121.91 o -2 2 23 2.47 28.33 116.35 o -1 2 23 27.66 22.46 113.63 o 0 2 23 0.01 40.16 113.05 o 1 2 23 26.96 114.94 113.12 o 2 2 23 2.54 14.16 117.03 o 3 2 23 15.28 82.85 121.66 o -3 3 23 2.22 36.90 124.28 o -2 3 23 18.15 0.00 119.90 o -1 3 23 4.32 54.08 116.63 o 0 3 23 6.10 0.00 114.53 o 1 3 23 3.91 35.72 117.14 o 2 3 23 19.43 32.02 118.45 o 3 3 23 2.44 12.64 124.43 o -2 4 23 29.94 100.88 121.64 o -1 4 23 1.45 56.02 119.37 o 0 4 23 26.68 30.73 119.40 o 1 4 23 1.01 0.00 119.58 o 2 4 23 30.11 16.30 123.50 o -1 5 23 12.19 71.63 123.50 o 0 5 23 60.78 64.86 93.54 o 1 5 23 13.99 9.91 124.30 o 0 0 24 40.09 3.32 166.64 o 1 0 24 198.97 158.66 77.74 o 2 0 24 26.31 53.96 122.03 o -2 1 24 47.26 50.44 123.17 o -1 1 24 49.65 85.10 118.92 o 0 1 24 69.61 11.15 119.72 o 1 1 24 57.10 26.94 119.96 o 2 1 24 49.87 88.79 122.88 o -2 2 24 73.79 63.66 123.23 o -1 2 24 0.92 0.00 121.52 o 0 2 24 116.38 27.17 121.09 o 1 2 24 1.60 54.06 120.57 o 2 2 24 75.14 0.00 126.75 o -1 3 24 73.84 79.39 124.14 o 0 3 24 26.97 61.50 121.95 o 1 3 24 72.08 58.51 123.76 o