#------------------------------------------------------------------------------ #$Date: 2011-09-28 14:24:46 +0000 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://cod.ibt.lt/cod/hkl/2/20/01/2200127.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200127_Fobs loop_ _publ_author_name 'Vasuki, G.' 'Parthasarathi, V.' 'Ramamurthi, K.' 'Jaisankar, P.' 'Varghese, B.' _publ_section_title ; 3-Chloro-2-methylquinolin-4(1H)-one ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o234 _journal_page_last o235 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.240 _cell_angle_gamma 90.000 _cell_length_a 24.4932 _cell_length_b 6.3646 _cell_length_c 12.8586 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.8317 _[local]_cod_data_source_file cf6042Isup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' SHELXL INS file, from DIRDIF output for PCS1\C10 H8 N O Cl\C2c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 235.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4227.82 3802.61 9.48 o 4 0 0 29819.90 27840.18 190.26 o 6 0 0 4.62 2.23 1.74 o 8 0 0 4831.75 4440.42 21.34 o 10 0 0 667.58 695.25 9.80 o 12 0 0 7299.12 7184.15 35.84 o 14 0 0 1383.93 1239.60 17.14 o 16 0 0 0.30 2.54 2.35 o 18 0 0 50.04 33.31 3.18 o 20 0 0 271.57 293.65 8.78 o 22 0 0 177.89 188.46 6.69 o 24 0 0 437.09 507.91 13.57 o 26 0 0 108.30 116.66 5.26 o 1 1 0 12565.36 12156.32 134.20 o 3 1 0 1445.06 1135.43 7.77 o 5 1 0 55662.86 46664.95 296.15 o 7 1 0 2383.29 2157.67 14.28 o 9 1 0 3599.21 3311.56 19.91 o 11 1 0 161.44 130.76 3.96 o 13 1 0 0.46 1.23 1.83 o 15 1 0 206.12 193.78 5.88 o 17 1 0 23.56 29.72 2.79 o 19 1 0 99.96 108.90 5.08 o 21 1 0 7.46 6.67 4.53 o 23 1 0 1.06 1.34 2.94 o 25 1 0 46.70 57.43 4.47 o 0 2 0 4795.68 5275.49 26.06 o 2 2 0 12670.97 12612.56 37.41 o 4 2 0 428.40 306.08 6.05 o 6 2 0 2018.09 2062.34 15.71 o 8 2 0 149.41 86.40 2.50 o 10 2 0 18723.93 17932.82 56.62 o 12 2 0 1252.25 1125.95 15.91 o 14 2 0 182.52 151.44 4.73 o 16 2 0 75.21 70.32 4.08 o 18 2 0 35.25 28.61 3.63 o 20 2 0 284.38 271.06 8.22 o 22 2 0 973.86 1062.39 20.88 o 24 2 0 0.95 0.56 2.35 o 1 3 0 2813.26 3012.65 23.91 o 3 3 0 1240.43 1409.72 16.36 o 5 3 0 126.61 167.95 5.31 o 7 3 0 0.26 1.04 1.83 o 9 3 0 17.52 29.65 2.23 o 11 3 0 1049.49 1076.22 17.65 o 13 3 0 220.67 217.09 6.61 o 15 3 0 436.04 445.01 11.89 o 17 3 0 548.79 586.68 16.13 o 19 3 0 24.46 17.18 3.50 o 21 3 0 41.94 50.02 4.35 o 23 3 0 3.41 4.66 4.17 o 0 4 0 2227.81 2507.67 26.30 o 2 4 0 49.00 33.99 2.62 o 4 4 0 670.29 675.46 13.99 o 6 4 0 381.38 436.41 11.78 o 8 4 0 803.19 729.10 15.57 o 10 4 0 541.19 516.60 13.98 o 12 4 0 1079.18 1105.84 21.31 o 14 4 0 119.18 133.11 5.62 o 16 4 0 31.94 32.29 4.08 o 18 4 0 54.12 62.70 4.77 o 20 4 0 618.85 622.27 15.34 o 22 4 0 24.34 23.27 3.58 o 1 5 0 224.22 240.14 6.95 o 3 5 0 63.29 69.68 4.06 o 5 5 0 3.39 7.28 3.80 o 7 5 0 499.85 534.22 14.80 o 9 5 0 69.27 82.63 4.66 o 11 5 0 751.37 821.09 19.09 o 13 5 0 227.36 263.10 7.48 o 15 5 0 118.20 124.53 6.01 o 17 5 0 1.03 -1.06 2.01 o 19 5 0 29.05 29.44 3.76 o 0 6 0 27.39 30.99 3.42 o 2 6 0 38.99 54.08 3.77 o 4 6 0 39.49 47.52 3.88 o 6 6 0 0.32 -2.30 2.76 o 8 6 0 410.29 422.08 11.58 o 10 6 0 97.10 86.88 5.37 o 12 6 0 166.72 176.69 5.96 o 14 6 0 1.91 3.40 3.45 o 16 6 0 2.55 -2.20 2.20 o 1 7 0 13.03 13.38 3.80 o 3 7 0 411.92 416.30 11.24 o 5 7 0 6.55 10.22 4.06 o 7 7 0 59.49 57.82 4.19 o 9 7 0 76.25 78.38 4.31 o -25 1 1 15.95 23.58 3.36 o -23 1 1 19.94 24.14 3.59 o -21 1 1 0.20 1.11 2.78 o -19 1 1 462.49 455.89 11.76 o -17 1 1 1090.89 1121.66 18.45 o -15 1 1 822.80 721.16 13.42 o -13 1 1 47.53 33.24 2.07 o -11 1 1 4041.58 3882.82 23.95 o -9 1 1 6000.91 5754.93 25.27 o -7 1 1 40946.35 36026.66 289.39 o -5 1 1 48374.57 40238.27 262.15 o -3 1 1 389.53 424.71 5.02 o -1 1 1 1651.04 1639.17 10.90 o 1 1 1 2442.68 2360.41 11.20 o 3 1 1 14497.74 12696.15 145.81 o 5 1 1 14332.16 13068.42 32.23 o 7 1 1 3102.89 2622.52 17.06 o 9 1 1 1928.44 1677.78 15.22 o 11 1 1 10.11 20.34 1.85 o 13 1 1 9.48 23.02 2.09 o 15 1 1 39.80 27.19 2.94 o 17 1 1 445.57 447.18 13.01 o 19 1 1 509.44 528.91 14.73 o 21 1 1 588.86 582.04 15.46 o 23 1 1 13.22 19.37 3.66 o 25 1 1 363.73 393.36 10.67 o -26 2 1 19.56 30.14 3.73 o -24 2 1 1.97 -2.95 2.95 o -22 2 1 24.73 28.34 4.03 o -20 2 1 7.16 2.30 3.48 o -18 2 1 159.74 160.24 5.52 o -16 2 1 44.15 42.53 3.59 o -14 2 1 1670.77 1616.43 20.60 o -12 2 1 3411.31 3104.77 25.70 o -10 2 1 8548.90 8627.12 38.08 o -8 2 1 292.77 225.29 5.96 o -6 2 1 7071.01 5918.39 26.61 o -4 2 1 4685.17 4139.20 21.43 o -2 2 1 33.03 54.56 2.27 o 0 2 1 105.27 105.88 3.16 o 2 2 1 1771.37 1892.04 14.49 o 4 2 1 4.01 2.65 1.77 o 6 2 1 2813.69 2633.02 19.06 o 8 2 1 3.23 19.37 1.80 o 10 2 1 170.16 196.10 5.74 o 12 2 1 966.70 929.44 15.62 o 14 2 1 364.50 357.86 9.46 o 16 2 1 198.75 165.47 5.60 o 18 2 1 12.73 14.82 4.83 o 20 2 1 1285.01 1320.27 23.27 o 22 2 1 130.72 135.64 6.12 o 24 2 1 79.97 86.52 4.76 o -23 3 1 13.08 25.23 3.67 o -21 3 1 83.08 84.98 5.31 o -19 3 1 92.68 81.71 4.98 o -17 3 1 2210.01 2177.36 29.89 o -15 3 1 2465.68 2411.10 29.57 o -13 3 1 6.54 7.80 3.43 o -11 3 1 1.94 0.00 0.06 o -9 3 1 449.05 387.54 9.84 o -7 3 1 1747.13 1704.12 18.51 o -5 3 1 216.17 112.00 3.39 o -3 3 1 172.09 120.42 3.51 o -1 3 1 5173.87 5577.48 33.49 o 1 3 1 781.06 941.59 13.36 o 3 3 1 869.82 919.70 13.21 o 5 3 1 1011.44 999.86 14.18 o 7 3 1 3568.96 3330.02 27.36 o 9 3 1 2097.34 2056.53 23.24 o 11 3 1 940.15 915.82 17.06 o 13 3 1 54.26 51.39 3.95 o 15 3 1 3041.80 2882.58 34.39 o 17 3 1 183.74 174.83 6.44 o 19 3 1 57.51 59.29 4.64 o 21 3 1 80.72 96.69 5.16 o 23 3 1 0.72 -2.13 2.13 o -22 4 1 346.00 349.43 9.82 o -20 4 1 47.27 33.91 4.33 o -18 4 1 368.87 424.18 12.40 o -16 4 1 216.97 231.09 7.40 o -14 4 1 302.77 318.53 9.60 o -12 4 1 183.17 189.70 6.35 o -10 4 1 150.42 145.20 5.25 o -8 4 1 56.97 56.28 3.56 o -6 4 1 1086.04 1085.06 17.73 o -4 4 1 267.34 225.86 6.55 o -2 4 1 13.63 14.34 2.33 o 0 4 1 1832.36 2075.75 31.81 o 2 4 1 2920.85 2929.55 28.43 o 4 4 1 238.73 269.16 7.99 o 6 4 1 637.61 637.71 14.24 o 8 4 1 418.77 397.44 10.47 o 10 4 1 2726.57 2778.29 32.42 o 12 4 1 105.19 112.81 5.31 o 14 4 1 139.58 145.20 5.87 o 16 4 1 0.68 -2.44 2.44 o 18 4 1 91.55 127.84 5.79 o 20 4 1 30.61 47.34 4.23 o -19 5 1 1.00 2.17 2.92 o -17 5 1 4.16 13.38 4.08 o -15 5 1 362.73 371.57 11.36 o -13 5 1 119.45 126.83 5.48 o -11 5 1 70.27 68.40 4.66 o -9 5 1 217.12 214.27 6.75 o -7 5 1 14.98 20.86 3.10 o -5 5 1 282.10 277.85 8.33 o -3 5 1 727.40 733.60 16.66 o -1 5 1 851.70 910.40 18.55 o 1 5 1 11.84 16.29 2.69 o 3 5 1 532.34 579.88 15.12 o 5 5 1 456.71 469.39 12.21 o 7 5 1 2.05 -1.47 2.63 o 9 5 1 207.72 226.64 7.13 o 11 5 1 193.94 202.44 6.75 o 13 5 1 71.22 72.59 5.24 o 15 5 1 49.50 43.54 4.06 o 17 5 1 119.70 128.86 5.24 o -16 6 1 318.23 355.69 9.90 o -14 6 1 8.55 17.93 3.04 o -12 6 1 104.02 115.00 5.36 o -10 6 1 2.68 6.08 3.41 o -8 6 1 1.10 -3.03 3.03 o -6 6 1 8.00 1.48 3.29 o -4 6 1 562.48 536.00 15.13 o -2 6 1 745.91 696.60 17.25 o 0 6 1 518.30 502.90 13.07 o 2 6 1 41.03 43.11 3.87 o 4 6 1 125.00 130.61 5.42 o 6 6 1 140.33 139.24 5.60 o 8 6 1 245.11 256.28 7.59 o 10 6 1 493.94 487.04 14.14 o 12 6 1 263.76 279.13 8.78 o 14 6 1 126.70 128.13 5.22 o -11 7 1 106.90 107.84 4.26 o -9 7 1 11.80 9.42 3.46 o -7 7 1 6.70 3.57 3.42 o -5 7 1 83.29 78.95 4.33 o -3 7 1 10.21 15.07 2.84 o -1 7 1 6.82 0.76 2.22 o 1 7 1 57.24 51.57 3.68 o 3 7 1 1.24 1.00 2.27 o 5 7 1 26.43 23.58 3.11 o 7 7 1 8.45 9.10 2.75 o 9 7 1 18.26 14.38 2.92 o -26 0 2 2.70 10.63 2.97 o -24 0 2 176.47 185.84 6.81 o -22 0 2 165.41 193.25 6.41 o -20 0 2 488.61 476.36 13.98 o -18 0 2 838.11 897.69 16.89 o -16 0 2 2678.28 2891.53 26.87 o -14 0 2 508.60 501.86 10.05 o -12 0 2 511.73 603.25 9.76 o -10 0 2 8076.22 8402.50 31.71 o -8 0 2 297.61 234.22 4.90 o -6 0 2 24225.38 25285.03 213.92 o -4 0 2 11.57 35.19 1.29 o -2 0 2 23876.17 25491.21 165.69 o 0 0 2 797.45 667.87 10.93 o 2 0 2 6782.25 6871.61 20.18 o 4 0 2 62.64 43.88 1.70 o 6 0 2 505.02 383.52 6.78 o 8 0 2 1172.98 1123.38 12.88 o 10 0 2 477.99 435.61 9.36 o 12 0 2 224.10 183.23 5.55 o 14 0 2 3204.63 3404.37 31.39 o 16 0 2 952.73 1069.92 19.70 o 18 0 2 58.84 80.09 4.47 o 20 0 2 46.71 51.20 4.22 o 22 0 2 44.28 42.61 3.76 o 24 0 2 98.52 94.56 4.61 o -27 1 2 6.04 7.10 4.00 o -25 1 2 83.66 78.84 4.78 o -23 1 2 0.81 5.90 3.24 o -21 1 2 0.15 0.37 1.82 o -19 1 2 94.04 89.04 4.23 o -17 1 2 9.26 13.24 3.77 o -15 1 2 2995.30 3046.50 26.17 o -13 1 2 276.07 260.82 7.24 o -11 1 2 106.47 92.21 2.95 o -9 1 2 1971.78 1861.51 14.37 o -7 1 2 14128.13 13380.77 32.61 o -5 1 2 2613.11 2129.79 11.83 o -3 1 2 622.35 609.24 6.64 o -1 1 2 2852.74 3099.77 17.12 o 1 1 2 682.37 713.27 7.18 o 3 1 2 309.47 424.97 5.81 o 5 1 2 662.17 519.81 7.30 o 7 1 2 45.39 45.93 1.91 o 9 1 2 1165.83 1178.57 14.08 o 11 1 2 12.58 26.86 2.12 o 13 1 2 32.70 31.35 2.65 o 15 1 2 165.53 162.84 5.23 o 17 1 2 453.62 448.80 13.30 o 19 1 2 6.39 4.75 3.74 o 21 1 2 36.13 44.81 4.29 o 23 1 2 94.97 110.64 5.26 o -26 2 2 12.68 13.71 3.47 o -24 2 2 1.07 0.34 1.73 o -22 2 2 28.37 36.49 4.03 o -20 2 2 299.20 295.64 9.25 o -18 2 2 152.38 172.80 5.72 o -16 2 2 3744.47 3463.68 32.42 o -14 2 2 362.05 375.28 9.93 o -12 2 2 7294.70 7241.82 38.16 o -10 2 2 2878.30 2899.11 21.39 o -8 2 2 1133.54 970.90 11.58 o -6 2 2 4098.04 3621.52 20.82 o -4 2 2 1927.54 1627.26 13.96 o -2 2 2 1981.88 2045.50 16.81 o 0 2 2 4199.09 4722.44 179.93 o 2 2 2 3463.69 3135.54 20.09 o 4 2 2 3329.77 2812.85 19.03 o 6 2 2 749.51 714.98 10.62 o 8 2 2 485.96 362.73 8.54 o 10 2 2 17.43 27.12 2.20 o 12 2 2 678.65 650.72 13.73 o 14 2 2 793.70 766.23 16.31 o 16 2 2 1112.86 1128.53 21.09 o 18 2 2 193.12 166.13 5.95 o 20 2 2 73.67 75.57 4.90 o 22 2 2 359.53 382.51 10.27 o -25 3 2 4.54 -0.15 1.02 o -23 3 2 13.10 11.88 3.49 o -21 3 2 211.46 167.62 6.80 o -19 3 2 512.99 514.28 13.65 o -17 3 2 3279.56 3343.34 37.04 o -15 3 2 0.51 -2.65 3.04 o -13 3 2 281.14 283.64 8.41 o -11 3 2 2081.16 1889.81 22.28 o -9 3 2 99.43 73.14 3.07 o -7 3 2 24.77 22.11 2.05 o -5 3 2 9390.11 9793.42 43.11 o -3 3 2 772.54 703.38 11.89 o -1 3 2 744.23 901.53 14.23 o 1 3 2 3032.09 2840.09 23.90 o 3 3 2 1356.20 1332.40 16.37 o 5 3 2 30.63 22.59 2.19 o 7 3 2 779.34 724.95 13.80 o 9 3 2 1293.24 1317.01 19.53 o 11 3 2 454.70 420.49 11.04 o 13 3 2 2272.90 2094.46 28.73 o 15 3 2 1680.43 1764.95 27.45 o 17 3 2 105.09 94.56 4.86 o 19 3 2 23.49 22.23 3.56 o 21 3 2 25.88 37.11 3.75 o -22 4 2 651.57 641.60 15.25 o -20 4 2 60.76 73.47 5.38 o -18 4 2 22.35 24.59 3.75 o -16 4 2 14.79 12.64 5.74 o -14 4 2 277.05 251.39 7.72 o -12 4 2 76.23 85.57 4.51 o -10 4 2 327.86 367.87 10.08 o -8 4 2 833.50 814.12 16.08 o -6 4 2 1901.26 1852.67 23.16 o -4 4 2 63.53 75.57 3.34 o -2 4 2 0.36 2.82 2.79 o 0 4 2 770.75 996.64 12.15 o 2 4 2 1471.28 1508.07 20.90 o 4 4 2 3515.68 3612.28 33.11 o 6 4 2 2621.34 2431.90 28.43 o 8 4 2 661.99 628.04 15.73 o 10 4 2 2302.10 2385.37 31.29 o 12 4 2 166.47 171.12 6.54 o 14 4 2 2.62 -3.19 3.19 o 16 4 2 250.93 246.53 7.85 o 18 4 2 66.34 80.44 4.71 o 20 4 2 0.29 -0.98 1.66 o -21 5 2 121.10 135.49 5.22 o -19 5 2 193.40 209.23 6.67 o -17 5 2 76.14 90.50 5.24 o -15 5 2 38.78 35.80 4.06 o -13 5 2 44.03 27.60 3.70 o -11 5 2 135.00 148.77 5.94 o -9 5 2 1322.00 1267.73 22.81 o -7 5 2 629.18 594.78 15.62 o -5 5 2 445.50 400.51 11.02 o -3 5 2 502.21 471.62 13.63 o -1 5 2 1.77 1.08 2.71 o 1 5 2 41.57 69.78 4.07 o 3 5 2 3272.25 3160.70 35.30 o 5 5 2 5378.62 5539.27 46.72 o 7 5 2 71.61 64.43 4.52 o 9 5 2 48.40 50.75 4.11 o 11 5 2 3.19 4.47 4.25 o 13 5 2 144.81 157.98 6.28 o 15 5 2 84.89 93.57 5.21 o 17 5 2 180.78 202.62 6.38 o -16 6 2 50.94 49.57 3.97 o -14 6 2 76.89 67.13 4.41 o -12 6 2 1.17 -0.49 1.74 o -10 6 2 40.55 50.47 4.28 o -8 6 2 14.87 24.33 3.35 o -6 6 2 478.05 468.56 13.87 o -4 6 2 807.25 789.09 18.36 o -2 6 2 524.34 528.61 14.73 o 0 6 2 757.00 792.01 12.49 o 2 6 2 55.06 56.57 4.14 o 4 6 2 57.21 59.88 4.27 o 6 6 2 33.41 31.63 3.96 o 8 6 2 2.16 -1.01 2.11 o 10 6 2 1.02 6.77 3.84 o 12 6 2 95.01 91.35 4.90 o 14 6 2 49.94 38.62 3.42 o -11 7 2 0.65 10.42 3.27 o -9 7 2 39.73 40.14 3.49 o -7 7 2 676.94 677.13 13.67 o -5 7 2 508.17 496.42 12.27 o -3 7 2 64.37 50.38 3.73 o -1 7 2 83.06 76.69 4.04 o 1 7 2 449.49 422.86 11.33 o 3 7 2 140.71 121.69 4.67 o 5 7 2 178.16 192.00 5.86 o 7 7 2 96.39 114.18 4.52 o -27 1 3 61.22 57.53 4.37 o -25 1 3 2.19 7.07 3.82 o -23 1 3 585.54 604.82 16.07 o -21 1 3 485.52 490.44 14.47 o -19 1 3 84.93 76.13 4.03 o -17 1 3 369.57 404.88 10.83 o -15 1 3 44.35 61.18 2.71 o -13 1 3 3164.73 2972.70 22.35 o -11 1 3 5594.07 5180.07 26.74 o -9 1 3 4362.46 3806.56 20.55 o -7 1 3 4475.48 4060.45 18.78 o -5 1 3 722.80 722.19 7.58 o -3 1 3 221.91 231.48 5.46 o -1 1 3 372.41 352.07 7.45 o 1 1 3 7933.36 7400.78 24.25 o 3 1 3 7138.27 6560.83 24.91 o 5 1 3 6935.80 6742.65 28.40 o 7 1 3 353.16 310.58 7.23 o 9 1 3 4270.30 4053.92 28.55 o 11 1 3 549.56 468.01 11.09 o 13 1 3 878.83 804.29 15.62 o 15 1 3 1456.39 1408.28 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3 3 531.20 407.46 10.61 o -9 3 3 1061.95 815.95 13.91 o -7 3 3 3338.94 3246.99 26.29 o -5 3 3 1132.29 1245.93 16.28 o -3 3 3 3041.20 3214.95 26.88 o -1 3 3 4344.86 5087.36 34.72 o 1 3 3 2362.31 2452.80 22.84 o 3 3 3 1247.27 1262.72 16.85 o 5 3 3 56.28 52.59 2.88 o 7 3 3 53.28 81.13 3.69 o 9 3 3 1822.91 1653.72 22.92 o 11 3 3 1740.28 1669.40 25.13 o 13 3 3 300.49 311.03 9.26 o 15 3 3 236.78 249.15 7.28 o 17 3 3 126.22 126.83 6.06 o 19 3 3 41.91 48.67 4.02 o -24 4 3 602.56 653.33 13.75 o -22 4 3 80.70 104.53 5.37 o -20 4 3 43.57 53.24 4.67 o -18 4 3 1.65 10.02 4.50 o -16 4 3 1027.92 1009.61 21.17 o -14 4 3 205.35 208.50 6.66 o -12 4 3 124.27 145.20 5.40 o -10 4 3 383.75 328.90 9.76 o -8 4 3 426.37 378.51 11.22 o -6 4 3 0.28 5.29 3.39 o -4 4 3 607.77 529.20 12.67 o -2 4 3 1161.69 1280.99 19.72 o 0 4 3 1129.01 1208.75 32.54 o 2 4 3 150.44 137.43 4.81 o 4 4 3 2217.77 2116.80 26.53 o 6 4 3 4.08 11.19 4.03 o 8 4 3 4031.17 4035.18 39.88 o 10 4 3 2.32 6.57 3.51 o 12 4 3 62.60 76.80 4.94 o 14 4 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