Crystallography Open Database
| COD Home |
|---|
| Accessing COD Data |
|---|
| Add Your Data |
|---|
| Documentation |
|---|
CIF Information Card
Information card for 1100166
1100165 << 1100166 >> 1100167Preview
|
Coordinates |
1100166.cif |
Structure parameters
| Formula | - C44.75 H32 Ag O2 P2 - |
| Calculated formula | - C44.82 H32 Ag O2 P2 - |
| Title of publication | Enantioselective O- and N-Nitroso Aldol Synthesis of Tin Enolates. Isolation of Three BINAP-Silver Complexes and Their Role in Regio- and Enantioselectivity |
| Authors of publication | Norie Momiyama; Hisashi Yamamoto |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2004 |
| Journal volume | 126 |
| Pages of publication | 5360 - 5361 |
| a | 17.417 ± 0.003 Å |
| b | 21.402 ± 0.004 Å |
| c | 11.298 ± 0.002 Å |
| α | 90° |
| β | 117.15 ± 0.03° |
| γ | 90° |
| Cell volume | 3747.4 ± 1.2 Å3 |
| Cell temperature | 546 ± 2 K |
| Ambient diffraction temperature | 546 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | C 1 2/c 1 |
| Hall symmetry space group | -C 2yc |
| Residual factor for all reflections | 0.0963 |
| Residual factor for observed reflections | 0.094 |
| Weighted residual factors for the observed reflections | 0.3306 |
| Weighted residual factors for all reflections included in the refinement | 0.3336 |
| Goodness-of-fit parameter for observed reflections | 1.587 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |